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CN112144281A - 一种防污防水的面料及其制备方法 - Google Patents

一种防污防水的面料及其制备方法 Download PDF

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CN112144281A
CN112144281A CN202010856236.0A CN202010856236A CN112144281A CN 112144281 A CN112144281 A CN 112144281A CN 202010856236 A CN202010856236 A CN 202010856236A CN 112144281 A CN112144281 A CN 112144281A
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antifouling
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高大伟
王丽丽
王春霞
俞俭
崔红
刘丽
牛力恒
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Yancheng Institute of Technology
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Abstract

本发明公开了一种防污防水的面料及其制备方法，所述面料包括基体布料和防污防水处理剂，其中，所述防污防水处理剂由以下原料按重量份组成：水溶性丙烯酸树脂10～25份、月桂醇聚氧乙烯醚5～17份、纳米二氧化硅6～12份、蓖麻油3～8份、硬脂酸2～8份、乳化剂3～5份、偶联剂1～3份、交联剂1～3份、去离子水50～80份。本发明的防污防水的面料具有良好的纳米防水、防污功能，浸入布料的处理剂可在布料的表面形成一层极薄的润滑膜，此膜不被水浸润，也不会被水冲掉，布料经过多次水洗之后，防水、防污效果依然保持，耐水洗性能佳。

Description

一种防污防水的面料及其制备方法
技术领域
本发明属于纺织面料技术领域，具体涉及一种防污防水的面料及其制备方法。
背景技术
纺织面料按织造方法分，有纬编针织面料和经编针织面料两类。纬编针织面料常以低弹涤纶丝或异型涤纶丝、锦纶丝、棉纱、毛纱等为原料，采用平针组织，变化平针组织，罗纹平针组织，双罗纹平针组织、提花组织，毛圈组织等，在各种纬编机上编织而成。随着人们生活水平的提高，纺织面料在一定程度上需要防污防水功能，因此防污防水处理剂应用量加大，传统油溶性防污防水处理剂中含有大量有机溶剂，如苯及苯类衍生物，且处理剂的稳定性也比较差，容易挥发造成环境污染，损害使用者的身体健康。
发明内容
针对现有技术的不足，本发明提供一种防污防水的面料及其制备方法，具有良好的纳米防水、防污功能，布料经过多次水洗之后，防水、防污效果依然保持，耐水洗性能佳。
本发明是通过以下技术方案实现的：
一种防污防水的面料，包括基体布料和防污防水处理剂，其中，所述防污防水处理剂由以下原料按重量份组成：水溶性丙烯酸树脂10～25份、月桂醇聚氧乙烯醚5～17份、纳米二氧化硅6～12份、蓖麻油3～8份、硬脂酸2～8份、乳化剂3～5份、偶联剂1～3份、交联剂1～3份、去离子水50～80份。
优选地，所述基体布料包括经纱和纬纱，所述经纱采用秸秆纤维与氨纶纤维混合纺织，秸秆纤维与氨纶纤维的质量比为(6～7):(3～4)，所述纬纱采用苎麻纤维与氨纶纤维混合纺织，苎麻纤维与氨纶纤维的质量比为(6～7):(3～4)。
优选地，所述乳化剂为N-十二烷基二甲胺或季铵盐。
优选地，所述偶联剂为N-β-(氨乙基)-γ-氨丙基三甲氧基硅烷或γ-缩水甘油醚氧丙基三甲氧基硅烷。
优选地，所述交联剂为丙烯酸羟乙酯或丙烯酸羟丙酯。
一种防污防水的面料的制备方法，包括以下步骤：
步骤1)将经纱和纬纱通过纺织制成基体布料；
步骤2)按重量份向反应釜中加入水溶性丙烯酸树脂、月桂醇聚氧乙烯醚、纳米二氧化硅、蓖麻油、硬脂酸及40～50％的去离子水，常温下600～900r/min搅拌20～30min；升温至50～65℃，加入乳化剂、偶联剂、交联剂和剩余的去离子水，1000～1200r/min下搅拌15～20min，再冷却至室温，制得防污防水处理剂；
步骤3)将步骤1)制得的基体布料浸入步骤2)制得的防污防水处理剂中，3～5h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，60～80℃预烘，120～150℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
本发明的有益效果如下：
本发明的防污防水的面料具有良好的纳米防水、防污功能，浸入布料的处理剂可在布料的表面形成一层极薄的润滑膜，此膜不被水浸润，也不会被水冲掉，布料经过多次水洗之后，防水、防污效果依然保持，耐水洗性能佳。
附图说明
图1为实施例1制得的面料的扫描电镜图。
具体实施方式
下面结合附图与具体实施例对本发明做进一步详细说明。
实施例1
一种防污防水的面料的制备方法，具体步骤如下：
(1)将质量比为6:4的秸秆纤维与氨纶纤维制成纤维生条(经纱)，将质量比为6:4的苎麻纤维与氨纶纤维制成纤维生条(纬纱)，将两种纤维生条在混条机上并合，制成熟条，将熟条在粗纱机上进行牵伸和加捻，再经过细纱机、络筒机、并线机、捻线机后制成混纺纱，最后采用剑杆织机引纬织造的方法制得基体布料。
(2)按重量份向反应釜中加入10份水溶性丙烯酸树脂、5份月桂醇聚氧乙烯醚、6份纳米二氧化硅、3份蓖麻油、2份硬脂酸及25份去离子水，常温下600r/min搅拌20min；升温至50℃，加入3份N-十二烷基二甲胺乳化剂、1份N-β-(氨乙基)-γ-氨丙基三甲氧基硅烷偶联剂、1份丙烯酸羟乙酯交联剂和25份去离子水，1000r/min下搅拌15min，再冷却至室温，制得防污防水处理剂。
(3)将(1)制得的基体布料浸入(2)制得的防污防水处理剂中，3h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，60℃预烘，120℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
通过对所得面料性能进行测试，其SEM图如图1所示，图1中标尺为30μm，从图1中可以看出，防污防水处理剂颗粒已明显附着于面料纤维上。面料手感光滑，面料表面防水能力强，面料经20次水洗后防水等级为90分，防污等级为5级。
实施例2
一种防污防水的面料的制备方法，具体步骤如下：
(1)将质量比为7:3的秸秆纤维与氨纶纤维制成纤维生条(经纱)，将质量比为7:3的苎麻纤维与氨纶纤维制成纤维生条(纬纱)，将两种纤维生条在混条机上并合，制成熟条，将熟条在粗纱机上进行牵伸和加捻，再经过细纱机、络筒机、并线机、捻线机后制成混纺纱，最后采用剑杆织机引纬织造的方法制得基体布料。
(2)按重量份向反应釜中加入25份水溶性丙烯酸树脂、17份月桂醇聚氧乙烯醚、12份纳米二氧化硅、8份蓖麻油、8份硬脂酸及32份去离子水，常温下900r/min搅拌30min；升温至65℃，加入5份季铵盐乳化剂、3份γ-缩水甘油醚氧丙基三甲氧基硅烷偶联剂、3份丙烯酸羟丙酯交联剂和48份去离子水，1200r/min下搅拌20min，再冷却至室温，制得防污防水处理剂。
(3)将(1)制得的基体布料浸入(2)制得的防污防水处理剂中，5h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，80℃预烘，150℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
通过对所得面料性能进行测试，面料光滑，面料表面防水能力强，面料经20次水洗后防水等级为90分，防污等级为5级。
实施例3
一种防污防水的面料的制备方法，具体步骤如下：
(1)将质量比为6:4的秸秆纤维与氨纶纤维制成纤维生条(经纱)，将质量比为6:4的苎麻纤维与氨纶纤维制成纤维生条(纬纱)，将两种纤维生条在混条机上并合，制成熟条，将熟条在粗纱机上进行牵伸和加捻，再经过细纱机、络筒机、并线机、捻线机后制成混纺纱，最后采用剑杆织机引纬织造的方法制得基体布料。
(2)按重量份向反应釜中加入15份水溶性丙烯酸树脂、7份月桂醇聚氧乙烯醚、8份纳米二氧化硅、6份蓖麻油、5份硬脂酸及30份去离子水，常温下800r/min搅拌20min；升温至60℃，加入4份N-十二烷基二甲胺乳化剂、2份N-β-(氨乙基)-γ-氨丙基三甲氧基硅烷偶联剂、2份丙烯酸羟乙酯交联剂和34份去离子水，1100r/min下搅拌15min，再冷却至室温，制得防污防水处理剂。
(3)将(1)制得的基体布料浸入(2)制得的防污防水处理剂中，4h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，70℃预烘，140℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
通过对所得面料性能进行测试，面料光滑，面料表面防水能力强，面料经20次水洗后防水等级为90分，防污等级为5级。
实施例4
一种防污防水的面料的制备方法，具体步骤如下：
(1)将质量比为7:3的秸秆纤维与氨纶纤维制成纤维生条(经纱)，将质量比为7:3的苎麻纤维与氨纶纤维制成纤维生条(纬纱)，将两种纤维生条在混条机上并合，制成熟条，将熟条在粗纱机上进行牵伸和加捻，再经过细纱机、络筒机、并线机、捻线机后制成混纺纱，最后采用剑杆织机引纬织造的方法制得基体布料。
(2)按重量份向反应釜中加入18份水溶性丙烯酸树脂、10份月桂醇聚氧乙烯醚、11份纳米二氧化硅、7份蓖麻油、3份硬脂酸及32份去离子水，常温下700r/min搅拌30min；升温至55℃，加入5份季铵盐乳化剂、2份γ-缩水甘油醚氧丙基三甲氧基硅烷偶联剂、3份丙烯酸羟丙酯交联剂和38份去离子水，1200r/min下搅拌20min，再冷却至室温，制得防污防水处理剂。
(3)将(1)制得的基体布料浸入(2)制得的防污防水处理剂中，5h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，60℃预烘，130℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
通过对所得面料性能进行测试，面料光滑，面料表面防水能力强，面料经20次水洗后防水等级为90分，防污等级为5级。

Claims (6)

1.一种防污防水的面料，其特征在于，包括基体布料和防污防水处理剂，其中，所述防污防水处理剂由以下原料按重量份组成：水溶性丙烯酸树脂10～25份、月桂醇聚氧乙烯醚5～17份、纳米二氧化硅6～12份、蓖麻油3～8份、硬脂酸2～8份、乳化剂3～5份、偶联剂1～3份、交联剂1～3份、去离子水50～80份。
2.根据权利要求1所述的一种防污防水的面料，其特征在于，所述基体布料包括经纱和纬纱，所述经纱采用秸秆纤维与氨纶纤维混合纺织，秸秆纤维与氨纶纤维的质量比为(6～7):(3～4)，所述纬纱采用苎麻纤维与氨纶纤维混合纺织，苎麻纤维与氨纶纤维的质量比为(6～7):(3～4)。
3.根据权利要求1所述的一种防污防水的面料，其特征在于，所述乳化剂为N-十二烷基二甲胺或季铵盐。
4.根据权利要求1所述的一种防污防水的面料，其特征在于，所述偶联剂为N-β-(氨乙基)-γ-氨丙基三甲氧基硅烷或γ-缩水甘油醚氧丙基三甲氧基硅烷。
5.根据权利要求1所述的一种防污防水的面料，其特征在于，所述交联剂为丙烯酸羟乙酯或丙烯酸羟丙酯。
6.权利要求1所述的一种防污防水的面料的制备方法，其特征在于，包括以下步骤：
步骤1)将经纱和纬纱通过纺织制成基体布料；
步骤2)按重量份向反应釜中加入水溶性丙烯酸树脂、月桂醇聚氧乙烯醚、纳米二氧化硅、蓖麻油、硬脂酸及40～50％的去离子水，常温下600～900r/min搅拌20～30min；升温至50～65℃，加入乳化剂、偶联剂、交联剂和剩余的去离子水，1000～1200r/min下搅拌15～20min，再冷却至室温，制得防污防水处理剂；
步骤3)将步骤1)制得的基体布料浸入步骤2)制得的防污防水处理剂中，3～5h后取出，在常温下浸轧处理剂，然后将面料放入预烘焙烘机中，60～80℃预烘，120～150℃焙烘，再经水洗、烘干后，即得所述防污防水的面料。
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