CN112097645A - High Aspect Ratio Microstructure Reflection Interferometric Microscopic Nondestructive Measurement Device - Google Patents
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Abstract
Description
技术领域technical field
本发明涉及精密光学测量工程技术领域,具体涉及一种高深宽比微结构反射式干涉显微无损测量装置,针对硅基MEMS器件沟槽结构的深度和宽度进行测量,特别适用于高深宽比的深沟槽结构。The invention relates to the technical field of precision optical measurement engineering, in particular to a high-aspect-ratio microstructure reflective interference microscopic nondestructive measurement device, which measures the depth and width of a trench structure of a silicon-based MEMS device, and is especially suitable for high aspect ratio measurement devices. Deep trench structure.
背景技术Background technique
随着微机电系统MEMS的发展,对微结构的测量要求越来越高,以硅为基础的MEMS加工工艺中,深宽比是主要指标之一,直接影响着MEMS器件的性能;现在MEMS高深宽比微结构的沟槽宽度为3~10 μm,深度为10~300 μm,深宽比一般在10~100 : 1之间,这种高深宽比微结构的发展对于驱动微机电系统技术在航空、航天、电子、生物、医疗等许多领域的应用将起到关键作用,同时在工艺中相应的测量技术和装置也不断涌现。With the development of MEMS, the measurement requirements for microstructures are getting higher and higher. In silicon-based MEMS processing technology, aspect ratio is one of the main indicators, which directly affects the performance of MEMS devices; The trench width of the aspect ratio microstructure is 3~10 μm, the depth is 10~300 μm, and the aspect ratio is generally between 10~100:1. The development of this high aspect ratio microstructure is very important for driving MEMS technology. Applications in many fields such as aviation, aerospace, electronics, biology, and medical treatment will play a key role, and corresponding measurement technologies and devices will continue to emerge in the process.
国内外现有的对高深宽比微结构器件几何测量方法大致有两种:接触式测量和非接触式测量;对于接触式测量,最常用的仪器包括扫描电子显微镜SEM和原子力显微镜,它们需要将器件从侧面剖开才能测量沟槽底部,这种破坏器件结构的方法不适用于在线检测,对提高器件性能的帮助有限;非接触式测量主要指干涉测量技术,以光波干涉原理为基础进行测量,与其他测量技术相比,干涉测量可以实现无损测量。There are roughly two types of geometric measurement methods for high aspect ratio microstructure devices at home and abroad: contact measurement and non-contact measurement; for contact measurement, the most commonly used instruments include scanning electron microscope SEM and atomic force microscope. The bottom of the trench can only be measured when the device is cut from the side. This method of destroying the device structure is not suitable for on-line inspection and has limited help in improving device performance; non-contact measurement mainly refers to interferometric measurement technology, which is based on the principle of light wave interference. , compared with other measurement techniques, interferometry can achieve non-destructive measurement.
近几年,利用光波干涉原理逐渐成熟起来的轮廓测试方法,以白光干涉仪为代表的非接触式形貌测量装置,此类装置不用接触待测样品,无需破坏器件结构,即可完成对器件的三维形貌测量。由于白光的分辨率受限于显微物镜的数值孔径NA,因此必须使用大NA物镜提高分辨率,但是,白光会被待测样品高深宽比沟槽遮挡,导致大NA探测光无法到达沟槽底部,无法满足成像要求,如图2(a)所示,例如,一个沟槽宽度为3 μm,深度为60 μm,深宽比达20 : 1,需要NA≤0.025才能照射此沟槽底部,假设波长为550 nm,此时成像分辨率超过14.4 μm,无法满足对3 μm宽度底部的成像要求。尽管有人提出将待测样品倾斜旋转,使光束照射到深槽底部,但是对待测样品的倾斜旋转过程十分繁琐,不能一次对整个底部成像,因此,使用白光干涉仪无法直接测量硅基MEMS高深宽比结构。In recent years, the contour testing method that has gradually matured using the principle of light wave interference, and the non-contact topography measuring device represented by the white light interferometer, can complete the device without touching the sample to be tested or destroying the device structure. 3D topography measurement. Since the resolution of white light is limited by the numerical aperture NA of the microscope objective, a large NA objective must be used to improve the resolution. However, the white light will be blocked by the high aspect ratio groove of the sample to be tested, so that the large NA probe light cannot reach the groove The bottom, which cannot meet the imaging requirements, as shown in Figure 2(a), for example, a trench with a width of 3 μm, a depth of 60 μm, and an aspect ratio of 20:1 requires NA≤0.025 to illuminate the bottom of this trench, Assuming that the wavelength is 550 nm, the imaging resolution exceeds 14.4 μm at this time, which cannot meet the imaging requirements for the bottom of 3 μm width. Although some people propose to tilt and rotate the sample to be tested so that the beam is irradiated to the bottom of the deep groove, the tilting and rotation process of the sample to be tested is very cumbersome, and the entire bottom cannot be imaged at one time. Therefore, it is impossible to directly measure the high depth and width of silicon-based MEMS using a white light interferometer. than the structure.
使用近红外光可以穿透硅材料探测沟槽底部,如图2(b)所示,但对于高深宽比结构,显微物镜会聚的大数值孔径光束会被沟槽结构调制降低光束聚焦性,产生像差,严重影响了成像质量和干涉条纹,测量结果也因此产生巨大误差。Using near-infrared light to penetrate the silicon material to probe the bottom of the trench, as shown in Figure 2(b), but for high aspect ratio structures, the large numerical aperture beam focused by the microscope objective will be modulated by the trench structure and reduce the beam focus. Aberrations are generated, which seriously affect the imaging quality and interference fringes, resulting in huge errors in the measurement results.
中国专利《一种微纳深沟槽结构测量方法及装置》(CN200710053292.5),其方法是将红外光束投射到含有深沟槽结构的硅片表面,分析从深沟槽结构各分界面反射形成的干涉光得到测量反射光谱;采用等效介质理论构建该深沟槽结构等效多层薄膜堆栈光学模型的理论反射光谱,利用模拟退火算法和基于梯度的优化算法,通过理论反射光谱对该测量反射光谱进行拟合,进而提取沟槽的深度及宽度等集合特征参数。该专利所述方法需要预先对待测样品的沟槽结构进行建模并计算得到理论的反射光谱,通过与测量得到的光谱进行拟合得到沟槽深度和宽度的测量结果,其测量结果准确性受预先建立的理论模型影响,对于复杂结构或未知结构的待测样品建模难度大,难以保证测量结果的准确性。The Chinese patent "A Micro-Nano Deep Trench Structure Measurement Method and Device" (CN200710053292.5), the method is to project an infrared beam onto the surface of a silicon wafer containing a deep trench structure, and analyze the reflections from each interface of the deep trench structure. The measured reflection spectrum is obtained from the formed interference light; the theoretical reflection spectrum of the optical model of the equivalent multilayer thin film stack of the deep trench structure is constructed by using the equivalent medium theory, and the theoretical reflection spectrum is obtained by using the simulated annealing algorithm and the gradient-based optimization algorithm. Measure the reflection spectrum for fitting, and then extract the collective characteristic parameters such as the depth and width of the groove. The method described in this patent needs to model the groove structure of the sample to be tested in advance and calculate the theoretical reflection spectrum. The measurement results of the groove depth and width are obtained by fitting with the measured spectrum. The accuracy of the measurement results is affected by Due to the influence of pre-established theoretical models, it is difficult to model samples with complex structures or unknown structures, and it is difficult to ensure the accuracy of the measurement results.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种高深宽比微结构反射式干涉显微无损测量装置,用以解决现有的干涉显微无损测量方法无法对MEMS高深宽比沟槽结构的深度和宽度进行测量的问题。The purpose of the present invention is to provide a high-aspect-ratio microstructure reflection type interference microscopic nondestructive measurement device, which is used to solve the problem that the existing interference microscopic nondestructive measurement method cannot measure the depth and width of the MEMS high aspect ratio trench structure. question.
实现本发明目的的技术解决方案为:一种高深宽比微结构反射式干涉显微无损测量装置,其特征在于:包括近红外短相干光源、柯勒照明系统、第一立方分光棱镜、第一光路折转系统、变形镜、第一中继镜组、第一显微物镜、待测样品、压电陶瓷PZT、第二立方分光棱镜、管镜、第一红外探测器、光瞳镜、单色滤光片、第二红外探测器、第二光路折转系统、第二平面反射镜、第二中继镜组、第二显微物镜、第三平面反射镜。The technical solution to achieve the purpose of the present invention is: a high aspect ratio microstructure reflective interference microscopic nondestructive measurement device, which is characterized in that: it includes a near-infrared short coherent light source, a Koehler illumination system, a first cubic beam splitting prism, a first Optical path refraction system, deformable mirror, first relay lens group, first microscope objective lens, sample to be tested, piezoelectric ceramic PZT, second cube beam splitter prism, tube mirror, first infrared detector, pupil mirror, single A color filter, a second infrared detector, a second optical path folding system, a second plane mirror, a second relay lens group, a second microscope objective lens, and a third plane mirror.
所述柯勒照明系统包括共光路依次设置的第一聚光镜、第二聚光镜、第一平面反射镜和第三聚光镜。The Koehler illumination system includes a first condenser mirror, a second condenser mirror, a first plane reflection mirror and a third condenser mirror which are arranged in sequence in a common optical path.
压电陶瓷PZT和第一红外探测器连接构成同步扫描采集系统;变形镜和第二红外探测器配合构成像差监测光路和主动补偿系统。The piezoelectric ceramic PZT is connected with the first infrared detector to form a synchronous scanning acquisition system; the deformation mirror and the second infrared detector cooperate to form an aberration monitoring optical path and an active compensation system.
近红外短相干光源发出的光束经过柯勒照明系统产生多视场均匀照明光后,经第一立方分光棱镜分为测试光和参考光;测试光经第一光路折转系统转折到达变形镜,经变形镜反射,依次经第一光路折转系统、第一中继镜组和第一显微物镜,照射到放置于压电陶瓷PZT上的待测样品;参考光经过第二光路折转系统转折到达第二平面反射镜,经第二平面反射镜反射,依次经第二光路折转系统、第二中继镜组和第二显微物镜,照射到第三平面反射镜上,并原路返回;待测样品被照明后,反射光原路返回到第一立方分光棱镜,经过第二立方分光棱镜,一部分光经过管镜将待测样品成像在第一红外探测器上,并与返回的参考光在第一红外探测器上发生干涉;另一部分光经过光瞳镜和单色滤光片将显微物镜的光瞳成像在第二红外探测器上,并与参考光在第二红外探测器上产生干涉,组成显微物镜出瞳像差监测光路,利用压电陶瓷PZT驱动待测样品并使用第二红外探测器采集4幅移相干涉图,计算获得光瞳像差;将显微物镜光瞳像差反馈到变形镜,再调整变形镜的形状对光瞳像差进行补偿;采用垂直扫描干涉法通过压电陶瓷PZT驱动待测样品,在第一红外探测器上同步接收待测样品不同深度表面的干涉条纹图,最后采用垂直扫描干涉算法对干涉图进行处理得到待测样品沟槽的深度和宽度测量结果。After the beam emitted by the near-infrared short coherent light source passes through the Koehler illumination system to generate uniform illumination light with multiple fields of view, it is divided into test light and reference light by the first cubic beam splitter; Reflected by the deformable mirror, the first optical path refraction system, the first relay lens group and the first microscope objective lens are in turn irradiated to the sample to be tested placed on the piezoelectric ceramic PZT; the reference light passes through the second optical path refraction system It turns to reach the second plane reflector, is reflected by the second plane reflector, passes through the second optical path refraction system, the second relay lens group and the second microscope objective lens in turn, irradiates the third plane reflector, and returns to the original path. Return; after the sample to be tested is illuminated, the reflected light returns to the first cubic beam splitter prism, and through the second cubic beam splitter prism, a part of the light passes through the tube mirror to image the sample to be tested on the first infrared detector, and is combined with the returned The reference light interferes on the first infrared detector; another part of the light passes through the pupil mirror and the monochromatic filter to image the pupil of the microscope objective on the second infrared detector, and is detected with the reference light in the second infrared detector. The optical path of exit pupil aberration monitoring of the microscope objective lens is formed. The piezoelectric ceramic PZT is used to drive the sample to be tested, and the second infrared detector is used to collect 4 phase-shifted interferograms, and the pupil aberration is calculated and obtained; The pupil aberration of the objective lens is fed back to the deformable mirror, and then the shape of the deformable mirror is adjusted to compensate for the pupil aberration; the vertical scanning interferometry method is used to drive the sample to be tested through the piezoelectric ceramic PZT, and the sample to be tested is synchronously received on the first infrared detector The interference fringe pattern of the surface of the sample at different depths, and finally the vertical scanning interference algorithm is used to process the interference pattern to obtain the measurement results of the depth and width of the groove of the sample to be tested.
一种高深宽比微结构反射式干涉显微无损测量方法,步骤如下:A high aspect ratio microstructure reflection type interference microscopic nondestructive measurement method, the steps are as follows:
步骤1、将待测样品放在压电陶瓷PZT上,并在第一红外探测器上得到带有像差的图像和低对比度的干涉条纹图;Step 1. Put the sample to be tested on the piezoelectric ceramic PZT, and obtain an image with aberration and a low-contrast interference fringe pattern on the first infrared detector;
步骤2、使用第二红外探测器监测显微物镜光瞳像差,利用压电陶瓷PZT驱动待测样品并使用第二红外探测器采集4幅移相干涉图,计算获得光瞳像差;
步骤3、变形镜根据监测到的光瞳像差调整形状,在第二红外探测器上观察补偿结果,补偿后在第一红外探测器上观察到清晰的图像和高对比度的干涉条纹图;Step 3. Adjust the shape of the deformable mirror according to the monitored pupil aberration, observe the compensation result on the second infrared detector, and observe a clear image and a high-contrast interference fringe pattern on the first infrared detector after compensation;
步骤4、采用垂直扫描干涉法通过压电陶瓷PZT驱动待测样品,第一红外探测器同步采集干涉条纹图,并采用垂直扫描干涉算法处理干涉图;Step 4, adopting the vertical scanning interferometry method to drive the sample to be tested through the piezoelectric ceramic PZT, the first infrared detector synchronously collects the interference fringe pattern, and using the vertical scanning interferometry algorithm to process the interferogram;
步骤5、最终得到待测样品沟槽结构的深度和宽度测量结果。
本发明与现有技术相比,其显著优点在于:Compared with the prior art, the present invention has the following significant advantages:
(1)针对硅基MEMS高深宽比沟槽结构的待测样品采用近红外短相干光源,穿透深槽到达底部,可以使用大NA显微物镜,解决了大NA光束无法探测高深宽比沟槽结构底部的问题。(1) A near-infrared short coherent light source is used for the samples of silicon-based MEMS high aspect ratio trench structure, which penetrates the deep groove to the bottom, and can use a large NA microscope objective, which solves the problem that the large NA beam cannot detect high aspect ratio trenches. Problems at the bottom of the slot structure.
(2)针对显微物镜会聚的大NA光束被待测样品沟槽结构调制降低光束聚焦性的问题,构建显微物镜出瞳像差监测光路和像差主动补偿系统,可以监测由于待测样品深沟槽结构产生的像差,并反馈到变形镜对像差进行主动补偿,提高成像质量和干涉条纹对比度,保证测量精度。(2) Aiming at the problem that the large NA beam converged by the microscope objective is modulated by the groove structure of the sample to be tested and reduces the focus of the beam, construct the optical path for the exit pupil aberration monitoring of the microscope objective and an active aberration compensation system, which can monitor the sample due to the sample to be tested. The aberration generated by the deep groove structure is fed back to the deformable mirror to actively compensate the aberration, improve the imaging quality and the contrast of interference fringes, and ensure the measurement accuracy.
附图说明Description of drawings
图1为高深宽比微结构反射式干涉显微无损测量装置示意图。Figure 1 is a schematic diagram of a high-aspect-ratio microstructure reflective interference microscopic nondestructive measurement device.
图2为汇聚光束探测待测样品沟槽底部示意图,其中图(a)为使用白光探测被侧壁遮挡图;图(b)为使用近红外光穿透侧壁探测底部,但光束聚焦性变差图;图(c)为使用变形镜补偿后光束能够汇聚到沟槽底部图。Figure 2 is a schematic diagram of the bottom of the groove of the sample to be detected by the converging beam, in which Figure (a) is a picture of using white light to detect and is blocked by the side wall; Figure (b) is using near-infrared light to penetrate the side wall to detect the bottom, but the focus of the beam changes. Aberration map; Figure (c) shows that the beam can converge to the bottom of the groove after compensation by the deformed mirror.
图3为光瞳像差监测与主动补偿原理框图。Figure 3 is a schematic block diagram of pupil aberration monitoring and active compensation.
图4为红外探测器采集到的干涉图,其中图(a)为变形镜补偿前的干涉图;图(b)为变形镜补偿后的干涉图。Figure 4 is the interferogram collected by the infrared detector, in which Figure (a) is the interferogram before the deformation mirror compensation; Figure (b) is the interferogram after the deformation mirror compensation.
图5为高深宽比沟槽结构的测量结果图。FIG. 5 is a graph showing the measurement results of the high aspect ratio trench structure.
具体实施方式Detailed ways
为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合说明书附图对本发明的具体实施方式做详细的说明。In order to make the above objects, features and advantages of the present invention more clearly understood, the specific embodiments of the present invention will be described in detail below with reference to the accompanying drawings.
结合图1,一种高深宽比微结构反射式干涉显微无损测量装置,包括近红外短相干光源1、柯勒照明系统、第一立方分光棱镜6、第一光路折转系统7、变形镜8、第一中继镜组9、第一显微物镜10、待测样品11、压电陶瓷PZT12、第二立方分光棱镜13、管镜14、第一红外探测器15、光瞳镜16、单色滤光片17、第二红外探测器18、第二光路折转系统19、第二平面反射镜20、第二中继镜组21、第二显微物镜22、第三平面反射镜23。Referring to Figure 1, a high aspect ratio microstructure reflective interference microscopic nondestructive measurement device includes a near-infrared short coherent light source 1, a Koehler illumination system, a first cubic
所述柯勒照明系统包括共光路依次设置的第一聚光镜2、第二聚光镜3、第一平面反射镜4和第三聚光镜5。The Koehler illumination system includes a
所述压电陶瓷PZT12和第一红外探测器15连接构成同步扫描采集系统;变形镜8和第二红外探测器18配合构成像差监测光路和主动补偿系统。The piezoelectric ceramic PZT12 and the first
近红外短相干光源1发出的光束经过柯勒照明系统产生多视场均匀照明光后,经第一立方分光棱镜6分为测试光和参考光;测试光经第一光路折转系统7转折到达变形镜8,经变形镜8反射,依次经第一光路折转系统7、第一中继镜组9和第一显微物镜10,照射到放置于压电陶瓷PZT12上的待测样品11;参考光经过第二光路折转系统19转折到达第二平面反射镜20,经第二平面反射镜20反射,依次经第二光路折转系统19、第二中继镜组21和第二显微物镜22,照射到第三平面反射镜23上,并原路返回;待测样品11被照明后,反射光原路返回到第一立方分光棱镜6,经过第二立方分光棱镜13,一部分光经过管镜14将待测样品11成像在第一红外探测器15上,并与返回的参考光在第一红外探测器15上发生干涉 ;另一部分光经过光瞳镜16和单色滤光片17将显微物镜的光瞳成像在第二红外探测器18上,并与参考光在第二红外探测器18上产生干涉 ,组成显微物镜出瞳像差监测光路,利用压电陶瓷PZT12驱动待测样品11并使用第二红外探测器18采集4幅移相干涉图,计算获得光瞳像差;将显微物镜光瞳像差反馈到变形镜8,再调整变形镜8的形状对光瞳像差进行补偿;采用垂直扫描干涉法通过压电陶瓷PZT12驱动待测样品11,在第一红外探测器15上同步接收待测样品11不同深度表面的干涉条纹图,最后采用垂直扫描干涉算法对干涉图进行处理得到待测样品沟槽的深度和宽度测量结果。After the beam emitted by the near-infrared short coherent light source 1 passes through the Koehler illumination system to generate uniform illumination light with multiple fields of view, it is divided into test light and reference light by the first cube
所述近红外短相干光源1位于第一聚光镜2的前焦面上,第一聚光镜2、第二聚光镜3和第三聚光镜5依次共焦。The near-infrared short coherent light source 1 is located on the front focal plane of the
所述变形镜8位于第三聚光镜5的后焦面上,且与第一显微物镜10的光瞳关于第一中继镜组9共轭,第一中继镜组9包括两个相同并共焦的聚光镜,焦点位置放置光阑阻挡杂散光,待测样品11的待测面位于第一显微物镜10的焦面上;The deformable mirror 8 is located on the back focal plane of the
所述第一红外探测器15、第一中继镜组9的共焦面和待测样品11共轭。The first
所述第一显微物镜10的光瞳经过第一中继镜组9、变形镜8、光瞳镜16和单色滤光片17成像在第二红外探测器18上,第一显微物镜10的光瞳、变形镜8和第二红外探测器18共轭,单色滤光片17的中心波长与近红外短相干光源1的中心波长相同;利用压电陶瓷PZT12驱动待测样品11并使用第二红外探测器18采集4幅移相干涉图,计算获得光瞳像差;根据得到的光瞳像差,主动调整变形镜8进行像差补偿,使得大数值孔径光束被待测样品的沟槽结构调制后仍然能够汇聚到沟槽底部。The pupil of the
所述光路折转系统包括三片平面反射镜和一块立方分光棱镜。The optical path refraction system includes three plane reflection mirrors and a cube beam splitting prism.
进一步地,光束经过第一光路折转系统7后方向与原方向垂直,正面照射变形镜8并反射,再经过第一光路折转系统7中的立方分光棱镜反射,光束方向转为与原方向一致。Further, the direction of the light beam after passing through the first optical path refraction system 7 is perpendicular to the original direction, the front side illuminates the deformable mirror 8 and reflects, and then is reflected by the cube beam splitter prism in the first optical path refraction system 7, and the beam direction is turned to the original direction. Consistent.
进一步地,光束经过第二光路折转系统19后方向与原方向垂直,正面照射第二平面反射镜20并反射,再经过第二光路折转系统19中的立方分光棱镜反射,光束方向转为与原方向一致。Further, after the light beam passes through the second optical
结合图2,所述白光被待测样品11沟槽结构遮挡如图2(a)所示,近红外光穿透待测样品11但被沟槽结构调制降低聚焦性如图2(b)所示 ,使用变形镜8补偿像差后近红外大数值孔径光束能够汇聚到沟槽底部如图2(c)所示。Referring to Fig. 2, the white light is blocked by the groove structure of the sample to be tested 11, as shown in Fig. 2(a), the near-infrared light penetrates the sample to be tested 11 but is modulated by the groove structure to reduce focusing as shown in Fig. 2(b) As shown in Figure 2(c), the near-infrared large numerical aperture beam can converge to the bottom of the groove after using the deformable mirror 8 to compensate the aberration.
结合图3、图4和图5,一种高深宽比微结构反射式干涉显微无损测量方法,步骤如下:With reference to Fig. 3, Fig. 4 and Fig. 5, a reflection interference microscopic nondestructive measurement method of high aspect ratio microstructure, the steps are as follows:
步骤1、将待测样品11放在压电陶瓷PZT12上,并在第一红外探测器15上得到带有像差的图像和低对比度的干涉条纹图,如图4(a)所示;Step 1. Put the sample 11 to be tested on the piezoelectric ceramic PZT12, and obtain an image with aberration and a low-contrast interference fringe pattern on the first
步骤2、使用第二红外探测器18监测显微物镜光瞳像差,利用压电陶瓷PZT12驱动待测样品11并使用第二红外探测器18采集4幅移相干涉图,计算获得光瞳像差;
步骤3、变形镜8根据监测到的光瞳像差调整形状,在第二红外探测器18上观察补偿结果,补偿后在第一红外探测器15上观察到清晰的图像和高对比度的干涉条纹图,如图4(b)所示;Step 3. The deformable mirror 8 adjusts the shape according to the detected pupil aberration, observes the compensation result on the second
步骤4、采用垂直扫描干涉法通过压电陶瓷PZT12驱动待测样品11,第一红外探测器15同步采集干涉条纹图,并采用垂直扫描干涉算法处理干涉图;Step 4, using the vertical scanning interferometry method to drive the sample to be tested 11 through the piezoelectric ceramic PZT12, the first
步骤5、最终得到待测样品11沟槽结构的深度和宽度测量结果,如图5所示。Step 5: Finally, the depth and width measurement results of the trench structure of the sample to be tested 11 are obtained, as shown in FIG. 5 .
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