CN112033648A - Cut-off depth detection method of optical filter - Google Patents
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- 238000001514 detection method Methods 0.000 title claims abstract description 59
- 230000003287 optical effect Effects 0.000 title claims abstract description 49
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- 238000002834 transmittance Methods 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims description 29
- 239000013307 optical fiber Substances 0.000 claims description 10
- 239000012286 potassium permanganate Substances 0.000 claims description 4
- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 claims description 4
- 229940039790 sodium oxalate Drugs 0.000 claims description 4
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Abstract
Description
技术领域technical field
本发明属于物理测试中光学性质的测试技术领域,具体涉及一种滤光片的截止深度检测方法。The invention belongs to the technical field of testing optical properties in physical testing, and particularly relates to a method for detecting cut-off depth of an optical filter.
背景技术Background technique
滤光片是一种常用的光学器件,用来选取所需辐射波段,广泛用于光学设备中,如相机、摄像机等。截止深度是滤光片品质优劣的判定参数之一,滤光片的截止深度OD越大,透过率越小,噪声越小,对应的设计制造难度也更大,要求更高,价格也更贵。Optical filter is a commonly used optical device, used to select the desired radiation band, widely used in optical equipment, such as cameras, video cameras, etc. The cut-off depth is one of the parameters for judging the quality of the filter. The larger the cut-off depth OD of the filter, the lower the transmittance and the lower the noise. More expensive.
关于滤光片截止深度的检测,有如CN 103616163 A所公开的测试方法;平常的项目实验中,更常使用的是采用滨松光谱仪及其配套软件,使用时,将检测信号传递给安装了该配套软件的终端(通常是计算机),经配套软件计算处理后通过终端展示检测结果值。Regarding the detection of the cut-off depth of the optical filter, there is a test method disclosed in CN 103616163 A; in ordinary project experiments, the Hamamatsu spectrometer and its supporting software are more commonly used. The terminal (usually a computer) of the supporting software displays the test result value through the terminal after being calculated and processed by the supporting software.
但在有使用到滤光片的实验项目中,透过滤光片的特性曲线有可能因为滤光片的优劣而表现得不同,比如:某些滤光片需要在特定波长上进行吸收,却存在一定的低漏光性(透过率大);而通过目前现有的方法检测滤光片的截止深度,不便于发现滤光片因自身结构原因(如设计缺失或制造问题)造成的对某种或某些(非设计通过)特定波长所存在的吸收问题(透过率大),不便于指导设计更完善的滤光片,不便于反馈提高滤光片的品质。However, in experimental projects that use filters, the characteristic curve of the filter may be different due to the quality of the filter. For example, some filters need to absorb at specific wavelengths. However, there is a certain low light leakage (high transmittance); and the current method to detect the cut-off depth of the filter is not convenient to find the filter due to its own structural reasons (such as lack of design or manufacturing problems). The absorption problem (large transmittance) of one or some (not designed to pass) specific wavelengths is not convenient to guide the design of a more perfect filter, and it is not convenient to feedback to improve the quality of the filter.
发明内容SUMMARY OF THE INVENTION
针对现有技术的上述不足,本发明要解决的技术问题是提供一种滤光片的截止深度检测方法,避免滤光片对一些特定波长透过率检测不便的问题,取得方便找出滤光片在哪些特定波长上存在吸收问题,从而达到便于判断和反馈改进品质的效果。In view of the above-mentioned deficiencies of the prior art, the technical problem to be solved by the present invention is to provide a method for detecting the cut-off depth of an optical filter, which avoids the problem of inconvenient detection of the transmittance of some specific wavelengths by the optical filter, and makes it easy to find the filter. On which specific wavelengths the film has absorption problems, it is easy to judge and feedback to improve the quality.
为解决上述技术问题,本发明采用如下技术方案:In order to solve the above-mentioned technical problems, the present invention adopts the following technical solutions:
滤光片的截止深度检测方法,包括光源,光源出射的光束穿过待测滤光片后,由光谱强度检测设备接收并显示初测光谱强度;在待测滤光片与光谱强度检测设备之间放置高浓度的溶液,使光源出射的光束穿过待测滤光片后,透过所述高浓度的溶液,再由光谱强度检测设备接收并显示再测光谱强度;将再测光谱强度与初测光谱强度进行对比,观察是否存在光谱强度有明显差异的特定波长,如果存在光谱强度有明显差异的特定波长,则判定待测滤光片在该特定波长上的透过率存在问题。The cut-off depth detection method of the optical filter includes a light source, and after the light beam emitted from the light source passes through the optical filter to be measured, the spectral intensity detection device receives and displays the initial measured spectral intensity; A high-concentration solution is placed in between, so that the light beam emitted by the light source passes through the filter to be measured, then passes through the high-concentration solution, and is then received by the spectral intensity detection device and displays the re-measured spectral intensity; the re-measured spectral intensity and Compare the initial measured spectral intensities, and observe whether there is a specific wavelength with a significant difference in spectral intensity. If there is a specific wavelength with a significant difference in spectral intensity, it is determined that there is a problem with the transmittance of the filter to be tested at the specific wavelength.
进一步完善上述技术方案,所述高浓度的溶液的浓度大于30mg/l,溶液成分包括草酸钠、高锰酸钾、邻苯二甲酸氢钾和/或氨氮溶液。To further improve the above technical solution, the concentration of the high-concentration solution is greater than 30 mg/l, and the solution components include sodium oxalate, potassium permanganate, potassium hydrogen phthalate and/or ammonia nitrogen solution.
进一步地,所述光谱强度有明显差异为再测光谱强度相较初测光谱强度存在光谱强度有明显增长。Further, the obvious difference in the spectral intensity is that the re-measured spectral intensity has a significant increase in spectral intensity compared with the initial measured spectral intensity.
进一步地,所述待测滤光片和高浓度的溶液置于整装检测装置中,所述整装检测装置包括盒体,盒体内设有滤光片夹具用于可拆卸地夹持待测滤光片,待测滤光片被夹持固定在滤光片夹具上,盒体内设有比色皿,所述高浓度的溶液盛装于比色皿中,盒体的两相对的侧壁上分别设有入光口和出光口,入光口和出光口处分别设有平凸的准直透镜;光源出射的光束,从入光口处的准直透镜的凸面入射,准直后,穿过待测滤光片,透过比色皿与其中的高浓度溶液,然后从出光口处的准直透镜平行出射至光谱强度检测设备。Further, the filter to be tested and the high-concentration solution are placed in an integrated detection device, the integrated detection device includes a box body, and the box body is provided with a filter clamp for detachably clamping the to-be-detected. filter, the filter to be tested is clamped and fixed on the filter holder, the box is provided with a cuvette, the high-concentration solution is contained in the cuvette, and the two opposite side walls of the box are The light entrance and the light exit are respectively provided, and the light entrance and the light exit are respectively provided with a plano-convex collimating lens; the light beam emitted from the light source is incident from the convex surface of the collimating lens at the light entrance, and after collimation, passes through the lens. It passes through the filter to be tested, passes through the cuvette and the high-concentration solution in it, and then exits from the collimating lens at the light exit to the spectral intensity detection device in parallel.
进一步地,所述比色皿可拆卸地固定在盒体内;盒体的上端敞口并配设有遮光盖板;遮光盖板为整装检测装置的一部分,其作用是扣除暗噪声,避免实验结果受到暗噪声的影响。Further, the cuvette is detachably fixed in the box body; the upper end of the box body is open and is equipped with a light-shielding cover plate; the light-shielding cover plate is a part of the complete detection device, and its function is to deduct dark noise and avoid experiments. The result is affected by dark noise.
进一步地,所述光谱强度检测设备包括光谱仪,光谱仪信号连接处理数据的计算机。Further, the spectral intensity detection device includes a spectrometer, and the spectrometer is signal-connected to a computer for processing data.
进一步地,光源与整装检测装置以及整装检测装置与光谱强度检测设备之间连接有光纤,相应光束通过对应的光纤传导。Further, an optical fiber is connected between the light source and the integrated detection device and between the integrated detection device and the spectral intensity detection device, and the corresponding light beam is conducted through the corresponding optical fiber.
相比现有技术,本发明具有如下有益效果:Compared with the prior art, the present invention has the following beneficial effects:
1、本发明的滤光片的截止深度检测方法,采用对比方式,可以方便快捷地找出滤光片在哪些特定波长上存在吸收问题,明确了滤光片透过率存在问题的特定波长后,可便于从设计、制造过程中更有针对性地分析并改进,从而设计制造出更完善、高品质的滤光片。1. The cut-off depth detection method of the optical filter of the present invention can easily and quickly find out which specific wavelengths the optical filter has absorption problems by using the comparison method. , which can facilitate more targeted analysis and improvement from the design and manufacturing process, so as to design and manufacture more perfect and high-quality filters.
2、本发明的滤光片的截止深度检测方法中,采用的整装检测装置设计合理,通过准直透镜实现对光源发出光束的准直,使得光束的能量损失小,光束透过滤光片的正中心,然后透过装有溶液的比色皿,整个过程使用到的器件都被集成到了一个整体结构中,可以有效地保证滤光片正中心、比色皿接收端面和准直透镜中心在同一条水平线上,使得实验的误差降至最小。2. In the cut-off depth detection method of the optical filter of the present invention, the design of the integrated detection device is reasonable, and the collimating lens is used to realize the collimation of the light beam emitted by the light source, so that the energy loss of the light beam is small, and the light beam can pass through the filter. The center of the filter, and then through the cuvette containing the solution, the devices used in the whole process are integrated into an overall structure, which can effectively ensure the center of the filter, the receiving end of the cuvette and the center of the collimating lens On the same horizontal line, the experimental error is minimized.
3、本发明的滤光片的截止深度检测方法,光束从整装检测装置出射经光纤进入光谱仪,结果可存储、可显示在移动终端上,满足现在对检测过程实时、快捷的检测要求;总的来说本方法的操作过程简单、实时、快捷,误差小,成本低,可实施性非常强,适用性高。3. In the cut-off depth detection method of the optical filter of the present invention, the light beam is emitted from the integral detection device and enters the spectrometer through the optical fiber, and the result can be stored and displayed on the mobile terminal, so as to meet the current real-time and fast detection requirements for the detection process; In conclusion, the operation process of the method is simple, real-time, fast, small in error, low in cost, very implementable, and high in applicability.
附图说明Description of drawings
图1为具体实施例的滤光片的截止深度检测方法的结构框图;Fig. 1 is the structural block diagram of the cut-off depth detection method of the optical filter of the specific embodiment;
图2为具体实施例中的整装检测装置的结构示意图;FIG. 2 is a schematic structural diagram of an integrated detection device in a specific embodiment;
图3为图2的俯视图(为便于示意,隐去遮光盖板);Fig. 3 is the top view of Fig. 2 (for the convenience of illustration, the shading cover is hidden);
图4为实施例一中的初测光谱强度示意图;4 is a schematic diagram of the initial measurement spectral intensity in Embodiment 1;
图5为实施例一中的再测光谱强度示意图;5 is a schematic diagram of the re-measured spectral intensity in Example 1;
图6为实施例二中的初测光谱强度示意图;Fig. 6 is the schematic diagram of initial measurement spectral intensity in embodiment two;
图7为实施例二中的再测光谱强度示意图;7 is a schematic diagram of the re-measurement spectral intensity in Example 2;
其中,整装检测装置1,盒体11,滤光片夹具12,比色皿13,入光口14,出光口15,遮光盖板16,待测滤光片2,溶液3。Among them, the complete detection device 1 , the
具体实施方式Detailed ways
下面结合附图对本发明的具体实施方式作进一步的详细说明。The specific embodiments of the present invention will be further described in detail below with reference to the accompanying drawings.
请参见图1-3,具体实施例的滤光片的截止深度检测方法,包括常规的试验过程,即使用了光源,光源出射的光束穿过待测滤光片后,由光谱强度检测设备接收并显示初测光谱强度;特殊之处在于,本实施例在检测光路上采用了一个整装检测装置1,所述整装检测装置1包括盒体11,盒体11内设有滤光片夹具12以用于可拆卸地夹持待测滤光片2,所述待测滤光片2放在盒体11内并被夹持固定在滤光片夹具12上,盒体11内还设有比色皿13,比色皿13中盛装有高浓度的溶液3,盒体11的两相对的侧壁上分别设有入光口14和出光口15,入光口14和出光口15处分别设有平凸的准直透镜,入光口14处的准直透镜的凸面朝向盒体11外侧,出光口15处的准直透镜的凸面朝向盒体11内侧,待测滤光片2的正中心、比色皿13接收端面和准直透镜的中心在同一条水平线上;光源出射的光束,从整装检测装置1的入光口14处的准直透镜的凸面入射,准直后,穿过待测滤光片2,透过比色皿13和比色皿13中具有待测滤光片敏感波长的溶液3,然后从出光口15处的准直透镜平行出射至光谱强度检测设备,光谱强度检测设备接收并显示再测光谱强度。所述比色皿13为可拆卸地固定在盒体11内,实施时,如实验过程一直使用整装检测装置1,可将比色皿13(含溶液3)取出,即可得到所述初测光谱强度。Please refer to FIGS. 1-3 . The method for detecting the cut-off depth of an optical filter according to a specific embodiment includes a conventional test process, that is, a light source is used. After the light beam emitted by the light source passes through the optical filter to be measured, it is received by a spectral intensity detection device. and display the initial measured spectral intensity; the special feature is that this embodiment adopts an integrated detection device 1 on the detection optical path. 12 is used to detachably clamp the filter to be tested 2, the filter to be tested 2 is placed in the
将再测光谱强度与初测光谱强度进行对比,观察是否存在光谱强度有明显差异的特定波长,如果存在光谱强度有明显差异的特定波长,则判定待测滤光片在该特定波长上的透过率存在问题,问题本身是待测滤光片的自身结构原因引起的,所以,也可以进一步判定待测滤光片的品质不高;又因为通过本方法明确了待测滤光片透过率存在问题的特定波长,从而便于从设计、制造过程中更有针对性地分析并改进,设计制造出更完善、高品质的滤光片。从效果来说,本方法也可以说是一种滤光片的质检方法。Compare the re-measured spectral intensity with the initial measured spectral intensity, and observe whether there is a specific wavelength with a significant difference in spectral intensity. There is a problem with the pass rate. The problem itself is caused by the structure of the filter to be tested. Therefore, it can be further determined that the quality of the filter to be tested is not high; Therefore, it is convenient to analyze and improve in a more targeted manner from the design and manufacturing process, and design and manufacture a more complete and high-quality filter. In terms of effect, this method can also be said to be a quality inspection method for optical filters.
需要说明的是,所检测出的待测滤光片透过率存在问题的特定波长,是待测滤光片的自身结构(缺陷)所确定的,与溶液没有对应关系,但在光路上应用高浓度的溶液,可以在再测光谱强度与初测光谱强度进行对比时,使特定波长上光谱强度的差异更明显。实施时,优选高浓度溶液,浓度大于30mg/l,考虑到环保和成本的问题,进一步优选溶液的浓度为30mg/l~50mg/l。It should be noted that the detected specific wavelengths that have problems with the transmittance of the filter to be tested are determined by the structure (defect) of the filter to be tested, and have no corresponding relationship with the solution, but are applied on the optical path. The solution with high concentration can make the difference of spectral intensity at a specific wavelength more obvious when the re-measured spectral intensity is compared with the initial measured spectral intensity. In implementation, a high-concentration solution is preferred, and the concentration is greater than 30 mg/l. Considering the issues of environmental protection and cost, it is further preferred that the concentration of the solution is 30 mg/l to 50 mg/l.
进一步需要说明的是,在定性的判定待测滤光片在特定波长上的透过率存在问题后,其判据中的特定波长的光谱强度在前后对比中有“明显差异”的界定或定量问题,这个差异量,实际就是一个质检的标准量,可以结合购方或订货方关于对滤光片的品质要求而定,甚至也可以使本方法成为一种检测标准后,再执行标准的差异量赋值以及定溶液成分、溶液浓度定值,总的来说,不允许的差异量越小,则对滤光片的品质要求越高。It should be further noted that, after qualitatively judging that there is a problem with the transmittance of the filter to be tested at a specific wavelength, there is a definition or quantification of “significant difference” in the spectral intensity of the specific wavelength in the criterion before and after the comparison. The problem is that this difference is actually a standard quantity for quality inspection, which can be determined in combination with the quality requirements of the purchaser or the orderer for the filter, and even after this method can be made a testing standard, the standard inspection can be carried out. The assignment of the difference amount and the determination of the composition and concentration of the solution, in general, the smaller the amount of difference that is not allowed, the higher the quality requirements for the filter.
当然,作为本领域的常识,在光路上增加了溶液,对光强有一定的吸收,所以光强值(光谱强度)会衰减,包括中心波长,再测光谱强度与初测光谱强度对比,中心波长必然是有明显衰减的,也即在对比时存在明显差异,这是滤光片的本身制造特性决定的,并不是并发明要找的有明显差异的“特定波长”,在光强应该衰减的常识下,本发明指的光谱强度有明显差异应为光谱强度有明显增长,来确定“特定波长”。进一步的,还可以取值为:如果存在光谱强度有明显增长的特定波长,且前后增长差异量不小于50cd,则判定待测滤光片在该特定波长上的透过率存在问题。Of course, as common knowledge in the field, adding a solution to the light path has a certain absorption of light intensity, so the light intensity value (spectral intensity) will be attenuated, including the center wavelength. The wavelength must be significantly attenuated, that is, there is a significant difference in comparison. This is determined by the manufacturing characteristics of the filter itself, and it is not the "specific wavelength" that has obvious differences to be found. The light intensity should be attenuated. Under the common sense, the present invention refers to the obvious difference of the spectral intensity should be the obvious increase of the spectral intensity to determine the "specific wavelength". Further, it can also be taken as: if there is a specific wavelength with a significant increase in spectral intensity, and the difference between the front and back increases is not less than 50cd, it is determined that there is a problem with the transmittance of the filter to be tested at the specific wavelength.
其中,溶液成分可以是:草酸钠、高锰酸钾、邻苯二甲酸氢钾和/或氨氮溶液。Wherein, the solution components can be: sodium oxalate, potassium permanganate, potassium hydrogen phthalate and/or ammonia nitrogen solution.
其中,盒体的上端采用敞口形式,这样,方便待测滤光片的卸装、更换,方便比色皿以及溶液的取放,当然,盒体的上端敞口也要配设遮光盖板,在实验过程中对上端敞口进行覆盖,保障实验过程的实施和实验的准确性。Among them, the upper end of the box body adopts an open form, which is convenient for the removal and replacement of the filter to be tested, and the taking and placing of the cuvette and the solution. Of course, the upper end of the box body is open. Cover the upper end exposure during the experiment to ensure the implementation of the experiment process and the accuracy of the experiment.
其中,所述光谱强度检测设备为光谱仪,光谱仪信号连接处理数据的计算机,计算机还可以信号连接存储单元以及移动终端,光谱仪接收的信号数据经过计算机处理之后可显示光谱强度,计算机可以将数据上传到云端(一种可选的存储单元)进行存储、可以传输到移动终端(手机、笔记本电脑等)上进行显示以便共享。Wherein, the spectral intensity detection device is a spectrometer, the spectrometer signal is connected to the computer that processes the data, the computer can also be connected to the storage unit and the mobile terminal by signal, the signal data received by the spectrometer can display the spectral intensity after being processed by the computer, and the computer can upload the data to It is stored in the cloud (an optional storage unit), and can be transmitted to a mobile terminal (mobile phone, laptop, etc.) for display for sharing.
其中,光源与整装检测装置以及整装检测装置与光谱强度检测设备之间连接有光纤,光源出射的光束通过光纤射入整装检测装置,从整装检测装置出射的光束又通过光纤传导进入光谱仪。The optical fiber is connected between the light source and the integrated detection device and the integrated detection device and the spectral intensity detection device. The light beam emitted by the light source enters the integrated detection device through the optical fiber, and the light beam emitted from the integrated detection device is transmitted through the optical fiber into the integrated detection device. spectrometer.
本发明提供的滤光片的截止深度检测方法,采用对比方式,可以方便快捷地找出滤光片在哪些特定波长上存在吸收问题,明确了滤光片透过率存在问题的特定波长,可便于从设计、制造过程中更有针对性地分析并改进,从而设计制造出更完善、高品质的滤光片。本发明采用的整装检测装置设计合理,通过准直透镜实现对光源发出光束的准直,使得光束的能量损失小,光束透过滤光片的正中心,然后透过装有溶液的比色皿,整个过程使用到的器件都被集成到了一个整体结构中,可以有效地保证滤光片正中心、比色皿接收端面和准直透镜中心在同一条水平线上,使得实验的误差降至最小;光束从整装检测装置出射经光纤进入光谱仪,结果可显示在移动终端上,满足现在对检测过程实时、快捷的检测要求。The method for detecting the cut-off depth of the optical filter provided by the present invention adopts the comparison method, which can conveniently and quickly find out which specific wavelengths the optical filter has absorption problems, and clarifies the specific wavelengths that have problems in the transmittance of the optical filter. It is convenient for more targeted analysis and improvement from the design and manufacturing process, so as to design and manufacture more perfect and high-quality filters. The integrated detection device adopted in the present invention has a reasonable design. The collimating lens is used to realize the collimation of the light beam emitted by the light source, so that the energy loss of the light beam is small. The devices used in the whole process are integrated into an overall structure, which can effectively ensure that the center of the filter, the receiving end face of the cuvette and the center of the collimating lens are on the same horizontal line, so that the experimental error is minimized ; The light beam is emitted from the whole-installed detection device and enters the spectrometer through the optical fiber, and the result can be displayed on the mobile terminal, which meets the current real-time and fast detection requirements for the detection process.
本发明提供的滤光片的截止深度检测方法,操作过程简单、实时、快捷,误差小,成本低。The method for detecting the cut-off depth of the optical filter provided by the invention has the advantages of simple, real-time and fast operation process, small error and low cost.
实施例一Example 1
光源:紫外可见LED光源,可以出射出一部分波段的近紫外光束和可见光光束。Light source: UV-visible LED light source, which can emit near-ultraviolet beams and visible light beams in a part of the band.
光纤:抗紫外石英光纤、其中的光源波长范围为200nm-760nm,数值孔径NA=0.26。Optical fiber: UV-resistant silica fiber, the wavelength range of the light source is 200nm-760nm, and the numerical aperture is NA=0.26.
准直透镜:光纤准直镜,由紫外熔融石英制成。Collimating Lens: Fiber-optic collimating lens, made of UV fused silica.
滤光片夹具:可调式滤光片夹具,夹持范围10-20mm可调。Filter holder: Adjustable filter holder, the clamping range is adjustable from 10-20mm.
待测滤光片:待测214nm(中心波长)滤光片A。Filter to be tested: Filter A of 214nm (center wavelength) to be tested.
比色皿:抗紫外比色皿。Cuvette: UV resistant cuvettes.
溶液成分:溶剂为水,溶质为草酸钠和高锰酸钾(含量比不限);溶液浓度:30mg/l。Solution composition: solvent is water, solute is sodium oxalate and potassium permanganate (content ratio is not limited); solution concentration: 30mg/l.
先取出比色皿(含溶液),检测获得初测光谱强度,光谱强度示意图可见图4。First take out the cuvette (containing the solution), and detect to obtain the initial measured spectral intensity. The schematic diagram of the spectral intensity can be seen in Figure 4.
放入比色皿(含溶液),检测获得再测光谱强度,光谱强度示意图可见图5。Put it into the cuvette (containing the solution), and detect and obtain the spectral intensity again. The schematic diagram of the spectral intensity can be seen in Figure 5.
将再测光谱强度与初测光谱强度进行对比,可以观察到,透过高浓度的溶液后,在特定波长有吸收,可以观察到该光谱有明显的吸收峰。设光谱强度前后增长差异量达到50cd的波长即判断为有明显差异的特定波长,那么,待测滤光片A在496~518nm的特定波长上的透过率存在问题,有待改进完善。Comparing the re-measured spectral intensity with the initial measured spectral intensity, it can be observed that there is absorption at a specific wavelength after passing through a high-concentration solution, and an obvious absorption peak can be observed in the spectrum. Assuming that the wavelength at which the difference in spectral intensity increases by 50 cd before and after is judged to be a specific wavelength with a significant difference, then the transmittance of the filter A to be tested at a specific wavelength of 496-518 nm has problems and needs to be improved.
实施例二
设备和各器件同实施例一。The equipment and components are the same as those in the first embodiment.
待测滤光片:待测546nm(中心波长)滤光片B。Filter to be tested: Filter B of 546nm (center wavelength) to be tested.
先取出比色皿(含溶液),检测获得初测光谱强度,光谱强度示意图可见图6。First take out the cuvette (containing the solution), and detect to obtain the initial measured spectral intensity. The schematic diagram of the spectral intensity can be seen in Figure 6.
放入比色皿(含溶液),检测获得再测光谱强度,光谱强度示意图可见图7。Put it into the cuvette (containing the solution), and detect and obtain the spectral intensity again. The schematic diagram of the spectral intensity can be seen in Figure 7.
将再测光谱强度与初测光谱强度进行对比,设光谱强度前后差异量增长达到50cd的波长即判断为有明显差异的特定波长,经观察对比(可以是计算机通过软件对比),待测滤光片B在各波长上的透过率不存在问题,品质良好。The re-measured spectral intensity is compared with the initial measured spectral intensity, and the wavelength at which the difference before and after the spectral intensity increases to 50cd is judged as a specific wavelength with obvious difference. There was no problem in the transmittance of the sheet B at each wavelength, and the quality was good.
实施例三
设备和各器件同实施例一。The equipment and components are the same as those in the first embodiment.
溶液浓度:50mg/l。Solution concentration: 50mg/l.
先取出比色皿(含溶液),检测获得初测光谱强度。First take out the cuvette (containing the solution), and detect to obtain the initial measured spectral intensity.
放入比色皿(含溶液),检测获得再测光谱强度。Put it into the cuvette (containing the solution), and detect to obtain the re-measured spectral intensity.
将再测光谱强度与初测光谱强度进行对比,可以观察到该光谱有更明显一些的吸收峰(图示差异不显著,未再图示,可借鉴图5)。还是设光谱强度前后增长差异量达到50cd的波长即判断为有明显差异的特定波长,那么,待测滤光片A依旧在496~518nm的特定波长上的透过率存在问题。Comparing the re-measured spectral intensity with the initial measured spectral intensity, it can be observed that the spectrum has more obvious absorption peaks (the difference in the figure is not significant, and it is not shown again, you can refer to Figure 5). It is also assumed that the wavelength with the difference in the increase of spectral intensity before and after reaching 50 cd is determined as a specific wavelength with a significant difference. Then, the transmittance of the filter A to be tested at the specific wavelength of 496-518 nm still has problems.
现有的实验方法中,可以用不同的光谱仪和软件得到本发明判断的佐证,比如上海复享光谱仪和配套软件。In the existing experimental methods, different spectrometers and software can be used to obtain evidence for the judgment of the present invention, such as Shanghai Fuxiang spectrometer and supporting software.
最后说明的是,以上实施例仅用以说明本发明的技术方案而非限制,尽管参照较佳实施例对本发明进行了详细说明,本领域的普通技术人员应当理解,可以对本发明的技术方案进行修改或者等同替换,而不脱离本发明技术方案的宗旨和范围,其均应涵盖在本发明的权利要求范围当中。Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention and not to limit them. Although the present invention has been described in detail with reference to the preferred embodiments, those of ordinary skill in the art should understand that the technical solutions of the present invention can be Modifications or equivalent substitutions without departing from the spirit and scope of the technical solutions of the present invention should be included in the scope of the claims of the present invention.
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