CN111999758A - MPPC-based small-sized beta detector for particulate matter monitoring - Google Patents
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Abstract
本发明公开了一种基于MPPC的颗粒物监测用小型β闪烁探测器,其结构包括塑料闪烁体、光导、MPPC、电路板、外壳、屏蔽窗、线缆。所述闪烁体和所述MPPC之间通过所述光导用光学胶耦合在一起;所述闪烁体的侧面与所述光导的侧面均制作有反射层;所述电路板集成有温度补偿型电源电路和信号处理电路;所述外壳包括端盖、主体、后盖,所述端盖和所述主体的前端均有所述屏蔽窗。本发明采用了新型的半导体光电器件MPPC,匹配β型闪烁体和适合于MPPC的供电及信号处理电路,实现对β射线的计数探测;且利用光导在使用有效光敏面积较小的MPPC的情况下,实现较大的有效探测面积,同时保证了低本底和高探测效率,非常适合用于大气尘埃颗粒物监测、纸张测厚等领域。
The invention discloses a small β-scintillation detector for particle monitoring based on MPPC. The scintillator and the MPPC are coupled together by the optical glue used for the light guide; the side surface of the scintillator and the side surface of the light guide are both made with reflective layers; the circuit board is integrated with a temperature compensation type power supply circuit and a signal processing circuit; the casing includes an end cover, a main body, and a rear cover, and the front end of the end cover and the main body have the shielding window. The invention adopts a new type of semiconductor optoelectronic device MPPC, matches β-type scintillator and a power supply and signal processing circuit suitable for MPPC, so as to realize the counting and detection of β rays; , to achieve a large effective detection area, while ensuring low background and high detection efficiency, very suitable for atmospheric dust particle monitoring, paper thickness measurement and other fields.
Description
技术领域。technical field.
本发明涉及β射线探测技术领域,具体涉及一种基于MPPC的颗粒物监测用小型β闪烁探测器。The invention relates to the technical field of beta ray detection, in particular to a small beta scintillation detector for particle monitoring based on MPPC.
背景技术。Background technique.
随着国家对环境治理的要求越来越高,空气中的粉尘/颗粒物(PM10和PM2.5)浓度作为环境污染的组成部分,已成为各级环保部门重要的监控对象。空气颗粒物监测仪是用于环境空气中颗粒物浓度监测的、重要的仪器设备,在包括大气自动监测站、各种场所的扬尘监测、空气微站、智慧城市监测站及至家用或便携式个人颗粒物监测等广泛应用。As the country's requirements for environmental governance are getting higher and higher, the concentration of dust/particulate matter (PM10 and PM2.5) in the air, as an integral part of environmental pollution, has become an important monitoring object of environmental protection departments at all levels. Air particulate matter monitor is an important instrument for monitoring the concentration of particulate matter in ambient air, including atmospheric automatic monitoring stations, dust monitoring in various places, air micro-stations, smart city monitoring stations, and household or portable personal particulate matter monitoring, etc. widely used.
目前,空气颗粒物监测仪按原理分为四种,分别是重量法、微量振荡天平法、β射线法和光散射法,每种方法各有其优缺点。其中,采用β射线法的颗粒物监测仪,是利用β射线穿透物质后被吸收而强度衰减的原理,将环境空气用采样泵吸入采样管,使之经过滤膜后排出,空气中的颗粒物截留在滤膜上形成尘斑,然后测定β射线通过滤膜尘斑时的衰减量从而计算出颗粒物的浓度。β射线法适用范围广、测量准确、灵敏度高,是空气颗粒物浓度监测的主要方法之一,在大气监测及工地扬尘监测等各个方面发挥着越来越重要的作用。At present, air particulate matter monitors are divided into four types according to the principle, namely the gravimetric method, the micro-oscillating balance method, the β-ray method and the light scattering method. Each method has its own advantages and disadvantages. Among them, the particle monitor using the β-ray method uses the principle that the β-ray penetrates through the substance and is absorbed and attenuated in intensity. The ambient air is sucked into the sampling tube by a sampling pump, and then discharged through the filter membrane, and the particulate matter in the air is trapped. Dust specks are formed on the filter membrane, and then the attenuation of beta rays passing through the dust specks of the filter membrane is measured to calculate the concentration of particulate matter. The β-ray method has a wide range of applications, accurate measurement and high sensitivity. It is one of the main methods for monitoring the concentration of air particles, and plays an increasingly important role in various aspects such as atmospheric monitoring and construction site dust monitoring.
在利用β射线法的颗粒物监测仪中,用来实现β射线测定的探测器部分是核心部件之一,目前所用β探测器主要为盖革计数器和基于光电倍增管(Photomultiplier Tubes,简称PMT)的β闪烁探测器。盖革计数器根据射线对气体的电离性质设计而成,工作电压约为几百伏,使用寿命相对较短,死时间长,且对高能β射线的探测效率不高,如今基本已逐渐被基于PMT的β闪烁探测器所取代。基于PMT的β闪烁探测器利用闪烁体受电离辐射时发光来进行探测,具有寿命长、响应快、探测效率高、温度特性好等优势,但所用的PMT一般需要提供上千伏的高工作电压,易受磁场的影响,体积大,功耗高,不利于便携式设备应用;且PMT的制造工艺复杂,降低成本较困难,不利于需广泛布设的监测设备应用。In the particle monitor using the β-ray method, the detector part used to realize the β-ray measurement is one of the core components. The currently used β-detectors are mainly Geiger counters and photomultiplier tubes (Photomultiplier Tubes, referred to as PMT). Beta scintillation detector. Geiger counters are designed according to the ionization properties of rays to gases. The working voltage is about a few hundred volts, the service life is relatively short, the dead time is long, and the detection efficiency of high-energy beta rays is not high. Nowadays, it has been basically based on PMT. replaced by the beta scintillation detector. PMT-based β-scintillation detectors use scintillators to emit light when they receive ionizing radiation for detection. They have the advantages of long life, fast response, high detection efficiency, and good temperature characteristics. However, the PMT used generally needs to provide a high working voltage of thousands of volts. , easily affected by the magnetic field, large size, high power consumption, not conducive to the application of portable equipment; and the complex manufacturing process of PMT, it is difficult to reduce the cost, which is not conducive to the application of monitoring equipment that needs to be widely deployed.
多像素光子计数器(Multi-Pixel Photon Counter:简称MPPC)即硅光电倍增管(Silicon photomultiplier,简称SiPM),是一种新型的光电转换器件,具有工作电压低、体积小、灵敏度高、抗磁场干扰、耐机械冲击能力强及批量化生产成本较低等优点,不仅有利于缩小探测器体积,提高探测器的稳定性及安全性,而且有利于降低成本,在高能物理实验、宇宙射线观测、核医学成像、核安全及环境监测等方面有着广泛的应用前景。Multi-Pixel Photon Counter (MPPC for short), or Silicon photomultiplier (SiPM for short), is a new type of photoelectric conversion device with low operating voltage, small size, high sensitivity, and anti-magnetic field interference. , strong mechanical shock resistance and low cost of mass production, not only help to reduce the size of the detector, improve the stability and safety of the detector, but also help to reduce costs, in high-energy physics experiments, cosmic ray observations, nuclear It has broad application prospects in medical imaging, nuclear safety and environmental monitoring.
近些年来,MPPC在各种核辐射测量领域越来越受到关注,在其中一些应用上已开始取代PMT,特别是在核医学影像设备的伽玛探测上已经获得成熟应用,在其他如环境辐射安全、核安全检查等领域也逐渐开始得到研究和使用,但在颗粒物监测方面的应用上目前却还是空白。In recent years, MPPC has attracted more and more attention in various fields of nuclear radiation measurement, and has begun to replace PMT in some of these applications, especially in the gamma detection of nuclear medicine imaging equipment, which has been maturely used in other applications such as environmental radiation. Safety, nuclear safety inspection and other fields have gradually begun to be studied and used, but the application of particle monitoring is still blank.
β射线法空气颗粒物监测仪,其检测下限、上限和检出限与滤膜尘斑的面积大小有关, 相应地要求β探测器需具有足够大的有效探测面积和足够高的探测效率。β射线法空气颗粒物监测仪通常所使用的是半衰期很长的低能量14C放射源,活度范围一般都在豁免值以下,稳定性好、安全耐用,但也由于其β射线的能量相对较弱,极容易被阻挡吸收,与塑料闪烁体相互作用后的发光也很弱,同样需β探测器具有高的探测效率。为保证较高的探测效率,一方面,探测器窗口需在满足避光的前提下尽可能减少对β射线的阻挡,一方面,塑料闪烁体的发光需尽可能没有损失的收集到光敏面上。MPPC的体积显著比PMT的小,但光敏面积也相对较小,而且其光敏面积的大小关系到器件的成本高低,在保证探测器具有较大有效探测面积的前提下,要采用相对更低成本的、有效光敏面积较小的MPPC器件,对闪烁光的有效收集十分关键。The detection limit, upper limit and detection limit of the β-ray air particulate matter monitor are related to the area of the filter dust spot. Correspondingly, the β detector is required to have a large enough effective detection area and a sufficiently high detection efficiency. The β-ray air particulate matter monitor usually uses a low-energy 14C radioactive source with a long half-life. The activity range is generally below the exempt value, with good stability, safety and durability, but also due to its relatively weak β-ray energy. , it is very easy to be blocked and absorbed, and the luminescence after interaction with the plastic scintillator is also very weak, and the β detector is also required to have high detection efficiency. In order to ensure high detection efficiency, on the one hand, the detector window should reduce the blocking of beta rays as much as possible under the premise of avoiding light. On the other hand, the luminescence of the plastic scintillator should be collected on the photosensitive surface without loss . The volume of MPPC is significantly smaller than that of PMT, but the photosensitive area is also relatively small, and the size of its photosensitive area is related to the cost of the device. On the premise of ensuring that the detector has a large effective detection area, it is necessary to use a relatively lower cost. The MPPC device with small effective photosensitive area is very important for the effective collection of scintillation light.
β射线法的颗粒物监测应用是对低能β射线产生的弱光进行探测,相应探测器的电路的设计与阈值参数设置既要有效去除噪声、保证低的本底计数率,同时又要能对射线信号进行有效探测以进一步保证获得高的探测效率。特别是大气颗粒物监测,需要有较高的测量精度,且能适应一定范围的环境温度变化,因此要求探测器需具有良好的温度特性、以在环境温度变化的情况下也能保持输出稳定,这样才能避免要求监测仪器本身进行难度相对较大、成本相对较高的十分精确的恒温控制。通常,PMT本身具有较好的温度特性,使用PMT的闪烁计数探测器还可以根据PMT的坪特性、通过合适的参数设置使PMT工作在坪区,从而使输出闪烁计数信号不易受到温度变化的影响。MPPC器件本身的温度系数明显比PMT的高,温度特性相对较差,而且不能像PMT一样工作在坪区,因此基于MPPC来实现具有优异性能的β射线计数探测器,具有相对较大的技术难度,需根据MPPC的特性设计适配电路,通过适当的MPPC工作电压的设置,通过合适的MPPC信号引出、放大及甄别,同时保证对射线信号的有效探测和噪声信号的去除,才有可能获得低本底和高探测效率;按照MPPC温度特性进行精确的工作电压补偿也是必须的,以保证探测器具有良好的温度稳定性。The particle monitoring application of the β-ray method is to detect the weak light generated by low-energy β-rays. The circuit design and threshold parameter setting of the corresponding detector should not only effectively remove noise, ensure a low background count rate, but also be able to detect the radiation. The signal is effectively detected to further ensure a high detection efficiency. In particular, atmospheric particle monitoring requires high measurement accuracy and can adapt to a certain range of ambient temperature changes. Therefore, the detector is required to have good temperature characteristics to keep the output stable even when the ambient temperature changes. In this way Only in this way can it be avoided that the monitoring instrument itself is required to perform very precise constant temperature control, which is relatively difficult and costly. Usually, the PMT itself has good temperature characteristics. The scintillation counting detector using the PMT can also make the PMT work in the plateau area through appropriate parameter settings according to the plateau characteristics of the PMT, so that the output scintillation counting signal is not easily affected by temperature changes. . The temperature coefficient of the MPPC device itself is obviously higher than that of the PMT, and the temperature characteristics are relatively poor, and it cannot work in the plateau region like the PMT. Therefore, it is relatively difficult to implement a β-ray counting detector with excellent performance based on MPPC. , It is necessary to design an adaptation circuit according to the characteristics of MPPC, through appropriate MPPC operating voltage settings, through appropriate MPPC signal extraction, amplification and screening, while ensuring effective detection of ray signals and removal of noise signals, it is possible to obtain low Background and high detection efficiency; accurate working voltage compensation according to MPPC temperature characteristics is also necessary to ensure that the detector has good temperature stability.
发明内容。Invention content.
本发明要解决的技术问题是:针对基于PMT的β闪烁探测器的体积大、功耗高、控制成本难度大、不便用于便携设备等问题,本发明采用了体积较小、价格较低的新型MPPC光电传感器替代传统的PMT,在较大面积的闪烁体与较小光敏面积的MPPC之间设计了光导对闪烁光进行最佳的收集和传导,加上可以精确调节温度系数的温度补偿型电源电路以及适配的MPPC信号引出、放大和甄别电路的设计,在保证优异探测性能的基础上,实现了小型、低功耗、可批量显著降低成本、可适用于便携设备的β闪烁探测器。The technical problem to be solved by the present invention is: in view of the problems of the PMT-based beta scintillation detector with large volume, high power consumption, difficulty in controlling the cost, and inconvenience for use in portable devices, the present invention adopts a small size and low price scintillation detector. The new MPPC photoelectric sensor replaces the traditional PMT. A light guide is designed between the scintillator with a larger area and the MPPC with a smaller photosensitive area for optimal collection and conduction of the scintillation light, plus a temperature compensation type that can precisely adjust the temperature coefficient. The design of the power supply circuit and the adapted MPPC signal extraction, amplification and discrimination circuit, on the basis of ensuring excellent detection performance, realizes a small, low power consumption, and can significantly reduce the cost in batches, which can be applied to portable devices. .
为了实现上述目的,本发明采用以下技术方案:本发明的一种基于MPPC的颗粒物监测用小型β闪烁探测器,包括屏蔽窗、闪烁体、光导、MPPC、电路板、外壳、线缆、上圆板、第一长条板、第二长条板、下圆板、端盖、主体、后盖;所述外壳包括端盖、主体和后盖,所述主体为圆筒形,所述端盖和主体之间通过螺纹连接,所述后盖与主体之间通过螺钉连接固定;所述闪烁体、光导、MPPC、电路板安装在外壳中;所述屏蔽窗设置在所述端盖内侧和外壳主体的前端;所述闪烁体一端与屏蔽窗连接,另一端与光导的端面耦合;所述光导的另一侧端面与MPPC耦合;所述电路板包括上圆板、下圆板、第一长条板和第二长条板,上圆板、下圆板、第一长条板和第二长条板之间采用插针互相连接并固定,所述上圆板和下圆板互相平行,所述第一长条板和所述第二长条板互相平行,组成“Ⅱ”形;所述MPPC焊接在所述上圆板上;所述电路板集成了MPPC适配的电源电路和信号处理电路;所述第一长条板为电源电路,为所述MPPC提供工作电压;所述第二长条板为信号处理电路,对所述MPPC的输出信号进行放大、甄别和整形处理;所述下圆板有通孔,引出线缆,用以输入低压供电电源和输出标准TLL信号。In order to achieve the above object, the present invention adopts the following technical solutions: a small-scale beta scintillation detector for particle monitoring based on MPPC of the present invention includes a shielding window, a scintillator, a light guide, an MPPC, a circuit board, a casing, a cable, an upper circle plate, the first long plate, the second long plate, the lower circular plate, the end cover, the main body and the back cover; the shell includes an end cover, a main body and a back cover, the main body is cylindrical, the end cover It is connected with the main body by screws, and the back cover and the main body are connected and fixed by screws; the scintillator, light guide, MPPC, and circuit board are installed in the casing; the shielding window is arranged on the inner side of the end cover and the casing The front end of the main body; one end of the scintillator is connected with the shielding window, and the other end is coupled with the end face of the light guide; the other end face of the light guide is coupled with the MPPC; the circuit board includes an upper circular plate, a lower circular plate, a first long The strip and the second long strip, the upper circular plate, the lower circular plate, the first long strip and the second long strip are connected and fixed with each other by pins, and the upper circular plate and the lower circular plate are parallel to each other, The first elongated plate and the second elongated plate are parallel to each other to form a "II" shape; the MPPC is welded on the upper circular plate; the circuit board integrates the power circuit and signal adapted by the MPPC a processing circuit; the first strip board is a power supply circuit, which provides a working voltage for the MPPC; the second strip board is a signal processing circuit, which amplifies, discriminates and shapes the output signal of the MPPC; The lower circular plate has through holes and leads out cables for inputting low-voltage power supply and outputting standard TLL signals.
作为优选,所述MPPC是有效光敏面积相比闪烁体表面积小的非阵列型器件。Preferably, the MPPC is a non-array type device with an effective photosensitive area smaller than the scintillator surface area.
作为优选,所述闪烁体为塑料闪烁体薄片。Preferably, the scintillator is a plastic scintillator sheet.
作为优选,所述光导的材料为光学玻璃或光学有机玻璃中的一种。Preferably, the material of the light guide is one of optical glass or optical organic glass.
作为优选,所述光导为锥台结构,较大一端的表面与所述闪烁体表面的形状相同、面积相同,光导面积较小的端面直径与MPPC的有效面积的边长相同,用于将较大面积的闪烁体的发光收集并传导至较小面积的MPPC探测窗上。Preferably, the light guide has a truncated cone structure, the surface of the larger end has the same shape and area as the surface of the scintillator, and the diameter of the end face with the smaller light guide area is the same as the side length of the effective area of the MPPC. The luminescence of the large area scintillator is collected and conducted to the smaller area MPPC detection window.
作为优选,所述光导的高度在大于(S1-S2)/2和小于(S1-S2)之间,其中S1为光导较大端面的直径或边长、S2为光导较小端面的直径或边长;采用了幅度谱测试加计数率测试的方法,对不同高度的光导进行实测对比后所优选确定的可以实现最佳光收集与光传导的高度。Preferably, the height of the light guide is greater than (S1-S2)/2 and less than (S1-S2), wherein S1 is the diameter or side length of the larger end face of the light guide, and S2 is the diameter or side of the smaller end face of the light guide. Long; the method of amplitude spectrum test plus count rate test is adopted, and the height that can achieve the best light collection and light transmission is preferably determined after the actual measurement and comparison of light guides of different heights.
作为优选,所述光导的较大端面与所述塑料闪烁体薄片采用光学胶耦合在一起。Preferably, the larger end face of the light guide and the plastic scintillator sheet are coupled together by optical glue.
作为优选,所述光导的较小端面与所述MPPC的光敏面采用光学胶耦合在一起并固定。Preferably, the smaller end face of the light guide and the photosensitive face of the MPPC are coupled and fixed together by optical glue.
作为优选,所述闪烁体与所述光导耦合之后,其整体制作有侧面全覆盖的、具有高反射率的光反射层,尽可能的减少光损失。Preferably, after the scintillator is coupled with the light guide, a light reflective layer with full lateral coverage and high reflectivity is fabricated as a whole to reduce light loss as much as possible.
作为优选,所述光导的材料、几何形状与尺寸规格,所述闪烁体和所述光导的耦合及侧面全包覆的高反射率的光反射层,共同最大程度地保证了光的收集效率,从而保证了对低能β射线所产生的微弱闪烁光的探测效率。Preferably, the material, geometry and size of the light guide, the coupling between the scintillator and the light guide, and the high-reflectivity light reflective layer fully covered on the side, together ensure the light collection efficiency to the greatest extent. Thus, the detection efficiency of weak scintillation light generated by low-energy beta rays is ensured.
作为优选,所述电路板包括上圆板、下圆板、第一长条板和第二长条板,各分板之间采用插针互相连接并固定,所述上圆板和所述下圆板互相平行,所述第一长条板和所述第二长条板互相平行,组成“Ⅱ”形,是按照细长圆筒形的外壳结构所设计。Preferably, the circuit board includes an upper circular board, a lower circular board, a first long strip board and a second long strip board, and pins are used to connect and fix each sub-board to each other, and the upper circular board and the lower circular board are The circular plates are parallel to each other, and the first elongated plate and the second elongated plate are parallel to each other, forming a "II" shape, which is designed according to the slender cylindrical shell structure.
作为优选,所述电路板集成了MPPC适配的电源电路和信号处理电路;所述MPPC焊接在所述上圆板上;所述第一长条板为电源电路,为所述MPPC提供工作电压;所述第二长条板为信号处理电路,对所述MPPC的输出信号进行放大、甄别和整形处理,针对所用MPPC的特性所设定的信号放大电路和甄别阈值的参数设置,兼顾平衡了低本底计数率和高探测效率、同时还保证了探测器的抗干扰性能;所述下圆板引出线缆/连接器,用以输入低压供电电源和输出标准TLL信号。Preferably, the circuit board integrates an MPPC-adapted power supply circuit and a signal processing circuit; the MPPC is welded on the upper circular plate; the first elongated board is a power supply circuit, which provides the MPPC with a working voltage The second elongated board is a signal processing circuit, and the output signal of the MPPC is amplified, discriminated and shaped, and the signal amplification circuit and the parameter setting of the discrimination threshold are set for the characteristics of the MPPC used, taking into account the balance of the The low background count rate and high detection efficiency also ensure the anti-interference performance of the detector; the lower circular plate leads out the cable/connector for inputting the low-voltage power supply and outputting the standard TLL signal.
作为优选,所述电源电路是温度补偿型电路,设计为能够精细调节温度系数和输出电压,可根据环境温度为所述MPPC提供合适的工作电压,在一定的温度变化范围内,使MPPC的输出增益稳定、探测器的输出计数率稳定。Preferably, the power supply circuit is a temperature compensation type circuit, designed to be able to finely adjust the temperature coefficient and the output voltage, and to provide the MPPC with a suitable working voltage according to the ambient temperature, so that the output of the MPPC can be adjusted within a certain temperature variation range. The gain is stable and the output count rate of the detector is stable.
作为优选,所述外壳包括端盖、主体和后盖,由铝合金材料制成;所述主体为圆筒形,所述端盖和中筒之间通过螺纹连接,所述后盖与中筒之间通过螺钉连接固定。Preferably, the shell includes an end cover, a main body and a back cover, which are made of aluminum alloy material; the main body is cylindrical, the end cover and the middle cylinder are connected by threads, and the back cover and the middle cylinder are connected by thread. Fixed by screw connection.
作为优选,所述屏蔽窗为双面镀铝聚酯薄膜,所述双面镀铝聚酯薄膜屏蔽窗共为两层,分别设置在所述端盖内侧和所述主体的前端,采用密封胶进行粘接固定,在尽可能减小对β射线的阻挡的前提下、同时实现了对探测器前端的避光与密封。Preferably, the shielding window is made of double-sided aluminized polyester film, and the double-sided aluminized polyester film shielding window has two layers, which are respectively arranged on the inner side of the end cover and the front end of the main body, and a sealant is used. By bonding and fixing, under the premise of reducing the blocking of beta rays as much as possible, the front end of the detector is protected from light and sealed at the same time.
作为优选,所述闪烁体、所述光导、所述MPPC和所述电路板装在所述外壳中。Preferably, the scintillator, the light guide, the MPPC and the circuit board are housed in the housing.
作为优选,所述闪烁体的前端表面贴近所述主体前端的所述屏蔽窗,所述屏蔽窗同时起到了光反射的作用,将从所述闪烁体前端面出射的光子反射回去、经由所述光导收集至所述MPPC,减少了所述闪烁体前端面的光损失,进一步保证了探测器的探测效率。Preferably, the front end surface of the scintillator is close to the shielding window at the front end of the main body, and the shielding window also plays the role of light reflection, and the photons emitted from the front end surface of the scintillator are reflected back and passed through the The light guide is collected to the MPPC, which reduces the light loss on the front face of the scintillator and further ensures the detection efficiency of the detector.
作为优选,所述下圆板与所述外壳之间采用黑胶进行固定,同时实现探测器后端的避光和密封。Preferably, black glue is used for fixing between the lower circular plate and the casing, and at the same time, the rear end of the detector is protected from light and sealed.
作为优选,所述电路板的地与所述外壳之间为电气导通,进一步保证了探测器的优异的抗干扰性能。Preferably, there is electrical conduction between the ground of the circuit board and the casing, which further ensures the excellent anti-interference performance of the detector.
作为优选,在其中一个实施例中,所述MPPC为有效面积3mm×3mm的器件。Preferably, in one of the embodiments, the MPPC is a device with an effective area of 3 mm×3 mm.
作为优选,在其中一个实施例中,所述MPPC为有效面积4mm×4mm的器件。Preferably, in one embodiment, the MPPC is a device with an effective area of 4 mm×4 mm.
作为优选,在其中一个实施例中,所述MPPC为有效面积6mm×6mm的器件。Preferably, in one embodiment, the MPPC is a device with an effective area of 6 mm×6 mm.
作为优选,在其中一个实施例中,所述反射层是特氟龙包裹加外覆铝箔制成。Preferably, in one of the embodiments, the reflective layer is made of Teflon wrapping and overlying aluminum foil.
作为优选, 在其中一个实施例中,所述反射层是二氧化钛反光涂层。Preferably, in one of the embodiments, the reflective layer is a titanium dioxide reflective coating.
作为优选,在其中一个实施例中,所述反射层是纳米反光涂层。Preferably, in one of the embodiments, the reflective layer is a nano-reflective coating.
本发明的有益效果为:1.采用了新型的半导体光电器件MPPC代替传统的PMT,匹配塑料闪烁体和发明者自行设计的适配MPPC的供电及信号处理电路,实现了适于颗粒物监测用的低能β射线闪烁计数探测器;2.经试验验证优选的光导形状和规格设计,使探测器在使用有效光敏面积较小的MPPC的情况下,实现了较大的有效探测面积和高探测效率,有利于低成本控制;3.MPPC适配的供电及信号放大、甄别参数的设置,同时保证了探测器的低本底、高探测效率和良好的温度特性,输出计数率稳定、不易受温度影响;4.在实现优异探测性能的基础上,探测器集成度高、结构紧凑、外形小巧,可将探测到的β射线转换为标准TTL信号输出,功耗小、安全性高,使用方便,可适用于便携设备;5.探测器还具有避光性好、密封性好、不易受磁场影响、抗电磁干扰能力强等优点。The beneficial effects of the present invention are as follows: 1. A new type of semiconductor optoelectronic device MPPC is adopted to replace the traditional PMT, and the plastic scintillator is matched with the power supply and signal processing circuit adapted to the MPPC designed by the inventor, so as to realize a device suitable for particle monitoring. Low-energy beta-ray scintillation counting detector; 2. The optimal light guide shape and specification design have been verified by experiments, so that the detector can achieve a large effective detection area and high detection efficiency under the condition of using MPPC with a small effective photosensitive area, Conducive to low-cost control; 3. MPPC-adapted power supply and signal amplification, setting of screening parameters, while ensuring the detector's low background, high detection efficiency and good temperature characteristics, stable output count rate, not easily affected by temperature ;4. On the basis of achieving excellent detection performance, the detector has high integration, compact structure and small appearance, and can convert the detected beta rays into standard TTL signal output, with low power consumption, high safety, convenient use, and It is suitable for portable equipment; 5. The detector also has the advantages of good light protection, good sealing, not easily affected by magnetic fields, and strong anti-electromagnetic interference ability.
附图说明。Description of drawings.
图1为本发明的工作原理示意图。FIG. 1 is a schematic diagram of the working principle of the present invention.
图2为本发明的结构示意图。FIG. 2 is a schematic structural diagram of the present invention.
图上:屏蔽窗1、闪烁体2、光导3、MPPC4、电路板5、外壳6、线缆7、 上圆板51、第一长条板52、第二长条板53、下圆板54、端盖61、主体62、后盖63。Above: Shielding window 1, scintillator 2, light guide 3, MPPC4, circuit board 5, housing 6, cable 7, upper
具体实施方式。Detailed ways.
下面结合附图与具体实施方式对本发明作进一步说明,但所举实施例不作为对本发明的限定。The present invention will be further described below with reference to the accompanying drawings and specific embodiments, but the examples are not intended to limit the present invention.
参阅附图1本实施例中的颗粒物监测用小型β闪烁探测器工作原理示意,β射线通过探测器屏蔽窗,通过闪烁体的发光收集到MPPC光敏面上有效收集闪烁光,根据MPPC的特性设计适配电路,通过适当的MPPC工作电压的设置,通过合适的MPPC信号引出、放大及甄别,同时保证对射线信号的有效探测和噪声信号的去除,才有可能获得低本底和高探测效率;按照MPPC温度特性进行精确的工作电压补偿也是必须的,以保证探测器具有良好的温度稳定性,后端由电路板引出线缆,用于低压电源输入与TTL信号输出。Referring to Figure 1, the working principle of a small beta scintillation detector for particle monitoring in this embodiment is shown. The adaptation circuit can obtain low background and high detection efficiency only by setting the appropriate MPPC working voltage, through the appropriate MPPC signal extraction, amplification and screening, and at the same time ensuring the effective detection of the ray signal and the removal of the noise signal; It is also necessary to perform accurate working voltage compensation according to the temperature characteristics of MPPC to ensure that the detector has good temperature stability. The back end is drawn from the circuit board for low-voltage power input and TTL signal output.
参阅附图1和附图2,本实施例中的颗粒物监测用小型β闪烁探测器包括:屏蔽窗1、闪烁体2、光导3、MPPC4、电路板5、外壳6和线缆7。MPPC4焊接在电路板5上,闪烁体2和MPPC4分别与光导3的两个端面耦合,闪烁体2、光导3、MPPC4、电路板5安装在外壳6中,外壳6前端固定有屏蔽窗1,后端由电路板引出线缆7,用于低压电源输入与TTL信号输出。Referring to FIG. 1 and FIG. 2 , the small beta scintillation detector for particle monitoring in this embodiment includes: a shielding window 1 , a scintillator 2 , a light guide 3 , an MPPC 4 , a circuit board 5 , a casing 6 and a cable 7 . The MPPC4 is welded on the circuit board 5, the scintillator 2 and the MPPC4 are respectively coupled to the two end faces of the light guide 3, the scintillator 2, the light guide 3, the MPPC4 and the circuit board 5 are installed in the casing 6, and the front end of the casing 6 is fixed with a shielding window 1, The rear end is led out by a cable 7 from the circuit board, which is used for low-voltage power input and TTL signal output.
本实施例中,闪烁体2为塑料闪烁体薄片,规格为φ14mm×0.5mm,可实现φ12mm的有效探测面积,0.5mm的厚度对于所探测的14C放射源的较低能β射线有足够的阻挡作用,可以保证探测效率。In this embodiment, the scintillator 2 is a plastic scintillator sheet with a specification of φ14mm×0.5mm, which can achieve an effective detection area of φ12mm, and the thickness of 0.5mm can sufficiently block the lower energy beta rays of the detected 14C radiation source function to ensure the detection efficiency.
本实施例中,MPPC4为一个由日本滨松光子学株式会社开发的非阵列型产品,有效光敏面积为3mm*3mm。In this embodiment, MPPC4 is a non-array type product developed by Hamamatsu Photonics Co., Ltd. of Japan, and the effective photosensitive area is 3mm*3mm.
本实施例中,光导3为光学有机玻璃材料、圆台结构;光导3面积较大的端面直径与闪烁体2的表面直径相同,采用光学硅胶与闪烁体2耦合在一起;光导3面积较小的端面直径与MPPC4的有效面积的边长相同,采用光学硅胶与MPPC4的光敏面耦合在一起;光导3和闪烁体2的整体侧面制作了全覆盖的、有一定厚度的光反射层,具有良好的光反射作用;光导3的高度在5.5mm~11mm之间,经由实验对比优选的、可实现最佳的光收集与光传导的高度;这样的几何结构使到达侧面的光,大部分可以通过反射较快的被收集到MPPC4的光敏面上,尽可能的减少光损失。由此可以在采用成本相对较低的、有效光敏面积较小的MPPC4的情况下,实现较大的探测面积及高的探测效率。In this embodiment, the light guide 3 is made of optical plexiglass material and has a circular truncated structure; the diameter of the end face of the light guide 3 with a larger area is the same as the diameter of the surface of the scintillator 2, and optical silica gel is used to couple with the scintillator 2; The diameter of the end face is the same as the side length of the effective area of MPPC4. Optical silica gel is used to couple with the photosensitive surface of MPPC4. Light reflection; the height of the light guide 3 is between 5.5mm and 11mm, and the height of the optimal light collection and light transmission can be achieved through experimental comparison; such a geometric structure makes most of the light reaching the side can be reflected by Faster is collected on the photosensitive surface of MPPC4, reducing light loss as much as possible. In this way, a larger detection area and high detection efficiency can be achieved under the condition of using the MPPC4 with relatively low cost and small effective photosensitive area.
在本实施例中,光反射层采用了一定厚度的、反射率可达95%及以上的纳米反光涂层,减少闪烁体2和光导3侧面的光透过损失。In this embodiment, the light reflective layer adopts a nano-reflective coating with a certain thickness and a reflectivity of 95% and above, so as to reduce the loss of light transmission on the sides of the scintillator 2 and the light guide 3 .
本实施例中,光导3和MPPC4之间的耦合,使用了固定胶进行加固,以防止因受力而发生脱耦。In this embodiment, the coupling between the light guide 3 and the MPPC 4 is reinforced with a fixing glue to prevent decoupling due to force.
本实施例中,电路板5包括上圆板51、第一长条板52、第二长条板53和下圆板54,各分板之间采用插针互相连接并固定,其中上圆板和下圆板互相平行、第一长条板和第二长条板互相平行,组成“Ⅱ”形,适合装入细长圆筒形的外壳结构中并固定、同时也适合根据不同功能进行电路划分。MPPC4焊接在上圆板51上;第一长条板52设置的是具有温度补偿功能的电源电路,其温度系数和输出电压设计为可以精细地进行调节,从而可以根据MPPC4附近的温度传感器的实时反馈温度及MPPC4的温度系数为MPPC4提供合适的工作电压,保证了在-10℃至﹢45℃的温度范围内,使MPPC4的输出增益保持稳定,进而使探测器的输出计数率保持稳定;第二长条板53为信号处理电路,是根据所用MPPC的特性引出脉冲信号,然后进行放大、甄别、并整形为标准的TTL电平信号,放大及甄别电路的参数设置是由实测优选设定的,使探测器在低的本底计数率和高的探测器效率之间兼顾平衡;下圆板54为输入输出电路板,引出线缆7至外壳6之外,为电路板5提供低压电源输入并输出TTL信号。In this embodiment, the circuit board 5 includes an upper
本实施例中,外壳6由端盖61、主体62和后盖63组成,整体为圆筒形,材质均为铝合金。端盖61和主体62的前端分别用密封胶固定有一层屏蔽窗1;屏蔽窗1为双面镀铝聚酯薄膜,两层屏蔽窗的设计在满足完全避光的前提下,又尽可能不影响到低能β射线的通过;端盖61和主体62通过螺纹连接固定并良好电气导通,后盖63与主体62通过螺钉连接固定并良好电气导通;后盖63上有通孔,用于线缆7穿出。In this embodiment, the housing 6 is composed of an end cover 61 , a
本实施例中,闪烁体2、光导3、MPPC4、电路板5安装在外壳6中;闪烁体2的前端表面贴近主体前端的镀铝箔膜屏蔽窗1,此结构使屏蔽窗1在满足避光作用的同时也起到了光反射的作用,减少了闪烁发光从闪烁体2前端面的损失,从而为探测器获得高的探测效率提供了进一步保障;下圆板54与主体62之间采用黑胶进行固定,同时实现对探测器后端的避光和密封,使得探测器应用于颗粒物监测仪设备中时不必对设备避光提出过高的要求、也尽可能避免了在气路中由于漏气所导致的测量精度问题。In this embodiment, the scintillator 2, the light guide 3, the MPPC 4 and the circuit board 5 are installed in the casing 6; the front end surface of the scintillator 2 is close to the aluminum foil film shielding window 1 at the front end of the main body, and this structure makes the shielding window 1 meet the requirements of avoiding light At the same time, it also plays the role of light reflection, reducing the loss of scintillation light from the front end of the scintillator 2, thereby providing a further guarantee for the detector to obtain high detection efficiency; black glue is used between the lower circular plate 54 and the
本实施例中,电路板5的地通过下圆板54引出地线与后盖63连接,实现电气连通,形成良好的屏蔽,进一步保障探测器的优异的抗干扰能力。In this embodiment, the ground of the circuit board 5 is connected to the
综上,本方案中的小型β闪烁探测器通过采用新型的半导体光电传感器MPPC4、利用圆台形光导3、匹配薄片形塑料闪烁体2,加上适配于MPPC的供电及信号处理电路设计及电路参数设置、合理紧凑的结构与外壳设计,在使用有效光敏面积较小的、相对低成本的MPPC4的情况下,实现了较大的有效探测面积及高探测效率,将探测到的β射线转换为标准的TTL信号,同时具有小巧的外形(φ20mm*75mm)、低的功耗(0.2W),十分便于使用并适用于便携设备,还具有温度特性好、避光性好、密封性好、不易受磁场影响、抗电磁干扰能力强的特点,非常适合应用于大气尘埃颗粒物监测、各种场合的扬尘监测、纸张测厚等领域。To sum up, the small beta scintillation detector in this scheme adopts a new type of semiconductor photoelectric sensor MPPC4, a circular truncated light guide 3, a matching sheet-shaped plastic scintillator 2, and the power supply and signal processing circuit design and circuit suitable for MPPC. Parameter setting, reasonable and compact structure and housing design, in the case of using MPPC4 with a small effective photosensitive area and relatively low cost, a large effective detection area and high detection efficiency are realized, and the detected β rays are converted into Standard TTL signal, with compact shape (φ20mm*75mm), low power consumption (0.2W), very easy to use and suitable for portable equipment, also has good temperature characteristics, good light protection, good sealing, not easy to use Affected by magnetic fields, it has the characteristics of strong anti-electromagnetic interference ability, which is very suitable for the monitoring of atmospheric dust particles, dust monitoring in various occasions, paper thickness measurement and other fields.
上述描述仅为充分说明本发明而所举的较佳实施例,描述中的特征在其他实施例中仍然满足或部分满足;凡是在本发明的精神和原则之下进行的任何局部修改或等同替换,都将视为在本发明的保护范围之内。The above description is only a preferred embodiment for fully illustrating the present invention, and the features in the description are still satisfied or partially satisfied in other embodiments; any partial modification or equivalent replacement made under the spirit and principle of the present invention , all will be regarded as being within the protection scope of the present invention.
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