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CN111956555A - Herbal firming compound composition, facial mask and preparation method of facial mask - Google Patents

Herbal firming compound composition, facial mask and preparation method of facial mask Download PDF

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Publication number
CN111956555A
CN111956555A CN202010903856.5A CN202010903856A CN111956555A CN 111956555 A CN111956555 A CN 111956555A CN 202010903856 A CN202010903856 A CN 202010903856A CN 111956555 A CN111956555 A CN 111956555A
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Prior art keywords
extract
weight
herbal
parts
mask
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CN202010903856.5A
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Chinese (zh)
Inventor
易斌
郝姗姗
陈素梅
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Jianchang Jiangxi Gang Pharmaceutical Co ltd
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Jianchang Jiangxi Gang Pharmaceutical Co ltd
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Priority to CN202010903856.5A priority Critical patent/CN111956555A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides a herbal firming compound composition, a mask and a preparation method thereof; the herbal compact compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-0.5 parts by weight of pseudo-ginseng extract; 0.02-0.5 parts by weight of astragalus extract; 0.02-0.5 parts by weight of rose hip extract; 0.02-1 part by weight of horse chestnut extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract are compounded according to a certain proportion, and are mutually supplemented and synergized, so that the obtained herbal firming compound composition can improve skin elasticity and wrinkles, tighten skin and delay skin aging; meanwhile, the facial mask provided by the invention adopts the essence added with the herbal firming compound composition, and is matched with the specific facial mask base cloth, so that the use feeling and the efficacy are better.

Description

Herbal firming compound composition, facial mask and preparation method of facial mask
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a herbal compact compound composition, a mask and a preparation method thereof.
Background
Skin aging is a continuous, progressive physiological process determined by genetic factors and influenced by a variety of environmental factors, and is characterized in its appearance by surface roughness, wrinkle formation, skin laxity, and pigment imbalance. Skin aging is the result of the combined effects of natural aging and photoaging factors. The photoaging is mainly caused by that active oxygen free radicals are generated in the skin under the irradiation of ultraviolet rays, and the oxygen free radicals cause collagen to be crosslinked, so that the skin loses elasticity and wrinkles are generated. On the other hand, free radicals also cause damage to proteins, DNA, etc., and also have a pro-apoptotic effect, reacting with proteins to form brown spots, producing pigmentation, causing premature aging of the skin. Therefore, various anti-aging skin care products have been spotlighted in order to effectively prevent skin aging.
The raw materials with anti-aging effect can be divided into plant extracts, vitamins, biological enzymes and the like according to different sources and structures. Vitamins such as vitamin E are widely applied in anti-aging skin care products, can be absorbed by skin, and practice has also proved that the vitamin E has excellent functions, is a good antioxidant, can protect cell membranes from being invaded by pollutants in the air, can also enhance the immunologic function of human bodies, can eliminate free radicals generated in reaction in cell lipid peroxidation, prevent the lipid peroxidation damaging the cell membranes from proceeding, and slow down the deposition of uneven cytochrome with age; however, inappropriate vitamin E consumption can cause side effects such as endocrine disorders. Biological enzyme such as SOD has effects of preventing aging, resisting inflammation, and resisting radiation; however, SOD, as a biological enzyme, is easily inactivated by the influence of temperature and other chemical substances, and the inactivated SOD rather promotes the generation of radical reaction to accelerate the aging process. Is derived from anti-aging effective components of natural plants, and has the characteristics of high efficiency, safety and stability.
Along with the consumer's advocation of herbal plant products, the anti-aging research reports of herbal plant extracts are increasing in recent years. However, how to compound active ingredients from multiple herbal plants together can play a role in multiple ways from multiple target points and determine the most scientific proportion, so that the composition can generate an excellent skin tightening effect is a problem which needs to be solved urgently at present, and at present, most of research objects are facial mask essence, and the interaction between the facial mask essence and a carrier facial mask base cloth of the facial mask essence is not considered. In fact, factors such as adsorption capacity, air permeability and affinity of the mask base cloth have an important influence on the use feeling and the efficacy of the mask essence.
Disclosure of Invention
In view of the above, the invention aims to provide a herbal firming compound composition, a mask and a preparation method thereof, and the herbal firming compound composition provided by the invention can improve skin elasticity and wrinkles, tighten skin and delay skin aging; meanwhile, the facial mask provided by the invention adopts the essence added with the herbal firming compound composition, and is matched with the specific facial mask base cloth, so that the use feeling and the efficacy are better.
The invention provides a herbal compact compound composition, which comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-0.5 parts by weight of pseudo-ginseng extract;
0.02-0.5 parts by weight of astragalus extract;
0.02-0.5 parts by weight of rose hip extract;
0.02-1 part by weight of horse chestnut extract.
Preferably, the method further comprises the following steps:
0.01-0.2 parts of carnosine;
0.6-3 parts by weight of hydroxypropyl tetrahydropyrane triol.
The invention also provides a herbal firming compound mask which consists of essence and mask base cloth;
the essence is prepared from the following raw materials:
70.92-92.86 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.71-6.7 parts by weight of the compound composition;
0.22-13.77 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal compact compound composition in the technical scheme;
the mask base cloth is copper ammonia fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber or superfine fiber film cloth.
Preferably, the humectant is selected from one or more of glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea, and glyceryl polyether-26.
Preferably, the solubilizer is selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20.
Preferably, the skin conditioning agent is selected from one or more of niacinamide, ascorbyl glucoside, allantoin, althea root extract, purslane extract, atractylodes rhizome root extract, aiti bupleurum root extract, garcinia cambogia fruit extract, angelia maritima leaf/stem extract, glutamine, BPN-tesoro 1600solution, dipeptide diaminobutyrylbenzyl amide diacetate, Prolevis, dipotassium glycyrrhizinate, sodium metabisulfite, arginine, and p-hydroxyacetophenone.
Preferably, the thickening agent is selected from one or more of carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate cross-linked polymer and hydroxyethyl cellulose.
Preferably, the chelating agent is selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA.
Preferably, the pH adjusting agent is selected from citric acid and/or sodium citrate.
The invention also provides a preparation method of the herbal compact compound mask in the technical scheme, which comprises the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal firming compound mask.
The invention provides a herbal firming compound composition, a mask and a preparation method thereof; the herbal compact compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-0.5 parts by weight of pseudo-ginseng extract; 0.02-0.5 parts by weight of astragalus extract; 0.02-0.5 parts by weight of rose hip extract; 0.02-1 part by weight of horse chestnut extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract are compounded according to a certain proportion, and are mutually supplemented and synergized, so that the obtained herbal firming compound composition can improve skin elasticity and wrinkles, tighten skin and delay skin aging; meanwhile, the facial mask provided by the invention adopts the essence added with the herbal firming compound composition, and is matched with the specific facial mask base cloth, so that the use feeling and the efficacy are better.
In addition, the preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a herbal compact compound composition, which comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-0.5 parts by weight of pseudo-ginseng extract;
0.02-0.5 parts by weight of astragalus extract;
0.02-0.5 parts by weight of rose hip extract;
0.02-1 part by weight of horse chestnut extract.
In the present invention, the herbal firming compound composition comprises a cistanche extract, a notoginseng extract, an astragalus extract, a rose hip extract and a horse chestnut extract, and preferably further comprises:
0.01-0.2 parts of carnosine;
0.6-3 parts by weight of hydroxypropyl tetrahydropyrane triol. In the invention, five traditional Chinese medicine components in the herbal medicine tightening compound composition are used in combination with carnosine and hydroxypropyl tetrahydropyrane triol, so that a synergistic effect can be further generated, and the skin tightening and anti-aging effects can be enhanced. On the basis, the herbal compact compound composition preferably comprises cistanche salsa extract, pseudo-ginseng extract, astragalus extract, rose hip extract, horse chestnut extract, carnosine and hydroxypropyl tetrahydropyrane triol.
The sources of the cistanche deserticola extract, the notoginseng extract, the astragalus extract, the rose hip extract, the horse chestnut extract, the carnosine and the hydroxypropyl tetrahydropyrane triol are not particularly limited in the present invention, and commercially available products well known to those skilled in the art can be used.
In the invention, the cistanche salsa extract is extracted by a conventional method and is available on the market. Cistanche salsa is a rare and old traditional Chinese medicine, and is preferably fleshy, thick and long, brown and moist; because the meat quality is oily, the medicinal value is high, the nourishing curative effect is strong, and the meat is generated near desert, the ginseng is called desert ginseng; the cosmetic is prepared from dried meat stem. The phenylethanoid glycosides of cistanche deserticola have anti-lipid peroxidation capability which is almost the same as the peroxidation inhibition capability of BHT (2, 6-di-tert-butyl-4-methylphenol), and is obviously higher than vitamin E; meanwhile, the phenylethanoid glycosides can absorb ultraviolet rays, reduce skin photodamage, and prevent and improve photoaging; and the literature indicates that polysaccharide substances and D-mannitol contained in the cistanche deserticola can activate superoxide dismutase and reduce the accumulation of in vivo lipofuscin, enhance the immunity of the organism and delay skin aging.
In the invention, the herbal compact compound composition comprises 0.02-1 part by weight of cistanche deserticola extract, preferably 0.02 part by weight, 0.1 part by weight, 0.4 part by weight, 0.6 part by weight, 0.8 part by weight, 1 part by weight, more preferably 0.4 part by weight.
In the invention, the pseudo-ginseng extract is extracted by a conventional method and is available on the market. Notoginseng radix (Panax notoginseng) is root of Notoginseng radix of Panax of Araliaceae, and is a unique and rare Chinese medicinal material; also named as SHANQI, JINSHI, XUESHEN, TIANQI, etc., mainly produced in Yunnan and Guangxi; the leaves, flowers and roots of pseudo-ginseng can be used as medicine; the cosmetic mainly adopts dried rhizome of Notoginseng radix. The main active component of Notoginseng radix is Notoginseng radix total saponin, mainly comprising more than 20 kinds of saponin components such as ginsenoside Rb1, Rb2, Rc, Rd, Re, Rf, Rg1, Rg2, Rh1 and notoginsenoside R1, R2, R3, R4, R6, etc.; the Notoginseng radix extract has antioxidant effect; the Notoginseng radix extract has effects of scavenging oxygen free radicals, enhancing activity of endogenous superoxide dismutase, enhancing scavenging ability of organism to oxygen free radicals, relieving chain reaction caused by oxygen free radicals, and reducing lipid peroxidation in blood, thereby delaying skin aging.
In the invention, the herbal compact compound composition comprises 0.02-0.5 part by weight of the panax notoginseng extract, preferably 0.02 part by weight, 0.1 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, and more preferably 0.1 part by weight.
In the invention, the astragalus extract is extracted by a conventional method and is available on the market. The astragalus is a perennial herb astragalus of leguminosae, has sweet taste and mild nature, enters lung and spleen channels, has the effects of tonifying qi and nourishing vitality, strengthening body resistance and eliminating evil, nourishing heart and dredging collaterals, and invigorating spleen and removing dampness, and is one of the most commonly used Chinese herbal medicines for strengthening body resistance and consolidating constitution, tonifying middle-jiao and replenishing qi; the cosmetic is prepared from dried rhizome of radix astragali. Radix astragali contains effective components such as radix astragali polysaccharide and radix astragali saponin; the radix astragali extract has strong free radical scavenging effect, and can promote collagen secretion and delay aging.
In the invention, the herbal compact compound composition comprises 0.02-0.5 part by weight of astragalus extract, preferably 0.02 part by weight, 0.1 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, and more preferably 0.1 part by weight.
In the invention, the rose hip extract is extracted by a conventional method and is available on the market. The rosa davurica, also called natural rosa davurica, also called rosa davurica, rosa davurica is a fruit of wild roses, is perennial deciduous shrub of rosaceous plants of the rosaceous family, and is one of higher plants in China; the cosmetic is prepared from Rosa multiflora (Rosa multiflora), and its leaves, roots, stems, fruits and flowers can be used as medicine, and its dried flowers and fruits can be mainly used. The rose hip has the highest content of vitamin C; the content of VC in the edible part of each hundred grams of fresh fruits is more than 6810 mg and up to 8300 mg by detection, the edible part of each hundred grams of fresh fruits is the head of all vegetables and fruits and is called as the crown of the fruit of the geodetic plant, namely the king of VC; the rosehips can improve the regeneration and renewal capacity of skin by promoting the activity of epidermal cells, protect the cells from being damaged by ultraviolet rays and neutralize free radicals, help to synthesize collagen, improve skin wrinkles and looseness, and enhance the elasticity of skin so as to achieve the effect of tightening the skin; can rebuild the junction between dermis and epidermis to promote collagen fiber generation; in addition, the skin care product has strong capability of scavenging free radicals, is a good antioxidant and has the effect of delaying skin aging.
In the invention, the herbal compact compound composition comprises 0.02-0.5 part by weight of rose hip extract, preferably 0.02 part by weight, 0.1 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, and more preferably 0.1 part by weight.
In the invention, the horse chestnut extract is extracted by a conventional method and is available on the market. Horse chestnut is deciduous tree of horse chestnut of Aesculaceae, and is named as semen Aesculi, pistachio nut, etc. The cosmetic mainly adopts seeds and dry leaves; the main effective component of horse chestnut is horse chestnut saponin. The horse chestnut extract has the efficacy of removing grease, is mild, has biological activity and good permeability, and can promote the decomposition of redundant fat and tighten the skin; meanwhile, the skin cream has strong eliminating effect on superoxide radicals, can activate cathepsin, enhance skin cell metabolism and delay skin aging.
In the invention, the herbal compact compound composition comprises 0.02-1 part by weight of horse chestnut extract, preferably 0.02 part by weight, 0.1 part by weight, 0.3 part by weight, 0.6 part by weight, 0.8 part by weight, 1 part by weight, more preferably 0.3 part by weight.
The five traditional Chinese medicine components of the cistanche deserticola extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract are compounded according to a certain proportion, are mutually supplemented and synergized, are used for skin tightening and aging resistance, can eliminate redundant free radicals, reduce the damage of the free radicals to cells, and improve the conditions of skin relaxation, poor elasticity and wrinkles; meanwhile, the skin-care product can activate the activity of cells of an organism, promote the synthesis of extracellular matrix and accelerate the metabolism of skin, thereby achieving the effects of skin tightening and aging resistance.
In the invention, the carnosine has wide application in anti-aging skin care products, has strong oxidation resistance, can effectively remove active oxygen free radicals, alpha-beta unsaturated aldehyde and resist saccharification, and can prolong the replication capacity of cells, thereby prolonging the service life of the cells.
In the invention, the herbal compact compound composition comprises 0.01-0.2 part by weight of carnosine, preferably 0.01 part by weight, 0.05 part by weight, 0.1 part by weight, 0.2 part by weight, and more preferably 0.05 part by weight.
In the present invention, the hydroxypropyl tetrahydropyran triol was according to research, the earliest of which was a derivative of xylose isolated by extraction from beech trees; beech contains abundant xylose, which stimulates the production of glycosaminoglycans (GAGs) and prevents the loss of water from the skin; enter the skin to promote the production and construction of proteins and polysaccharides (e.g., gelatinous protein networks and sugars that act as scaffolds and intercellular shock absorbers) in the extracellular matrix; these molecules absorb water to make the matrix in gel form, increasing the firmness of cells and skin; as skin ages, the extracellular matrix gradually loses elasticity; cells begin to deteriorate and are unable to reproduce youthful state promoting proteins, such as collagen; but also as a channel for directing the passage of repair molecules, such as proteins for cell growth.
In the invention, the herbal compact compound composition comprises 0.6-3 parts by weight of hydroxypropyl tetrahydropyrane triol, preferably 0.6 part by weight, 1 part by weight, 2 parts by weight and 3 parts by weight, and more preferably 1 part by weight.
The composition is prepared by adding carnosine and hydroxypropyl tetrahydropyrane triol to a composition consisting of five traditional Chinese medicine components of cistanche extract, pseudo-ginseng extract, astragalus extract, rose hip extract and horse chestnut extract, and can further generate a synergistic effect and enhance the effects of compactness and aging resistance of the composition.
The invention also provides a herbal firming compound mask which consists of essence and mask base cloth;
the essence is prepared from the following raw materials:
70.92-92.86 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.71-6.7 parts by weight of the compound composition;
0.22-13.77 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal compact compound composition in the technical scheme;
the mask base cloth is copper ammonia fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber or superfine fiber film cloth.
In the present invention, the essence includes a solvent, a humectant, a solubilizer, a complex composition, a skin conditioner, a thickener, a chelating agent, a fragrance, a preservative, and a pH adjuster, and preferably consists of a solvent, a humectant, a solubilizer, a complex composition, a skin conditioner, a thickener, a chelating agent, a fragrance, a preservative, and a pH adjuster.
In the present invention, the solvent includes one or more of water, butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, and 1, 2-propanediol, and more preferably one or more of water, butanediol, and 1, 2-pentanediol. The source of the solvent is not particularly limited in the present invention, and commercially available products of the above-mentioned butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, and 1, 2-propanediol, which are well known to those skilled in the art, may be used; the water may be deionized water as is well known to those skilled in the art. In the invention, the solvent is used to ensure that other components can be dissolved, dispersed and uniformly mixed.
In the present invention, the humectant is preferably selected from one or more of glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea, and glyceryl polyether-26. The source of the moisturizer is not particularly limited in the present invention, and commercially available products of the above glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea and glyceryl polyether-26, which are well known to those skilled in the art, may be used.
In the present invention, the solubilizer is preferably selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20, and more preferably PEG-40 hydrogenated castor oil.
In the invention, the compound composition is the herbal compact compound composition in the technical scheme. In the invention, the essence comprises 0.71-6.7 parts by weight of the compound composition, preferably 0.71 part by weight, 2.05 parts by weight, 3 parts by weight, 5 parts by weight, 6.7 parts by weight, and more preferably 2.05 parts by weight.
In the present invention, the skin conditioning agent is preferably selected from niacinamide, ascorbyl glucoside, allantoin, Althea officinalis root extract, purslane extract, Atractylodes macrocephala root extract, Altai bupleurum root extract, Garcinia cambogia fruit extract, angelica maritima leaf/stem extract, glutamine, BPN-tetro 1600 solubilization (palmitoyl tetrapeptide-7/palmitoyl pentapeptide-4/acetyl hexapeptide-8/water/polysorbate-20/1, 2-hexanediol/glycerin/carbomer), dipeptide diaminobutyryl benzylamide diacetate, Prolevis (water/hydrolyzed vegetable protein/phenoxyethanol/sodium benzoate/potassium sorbate/ethylhexylglycerin), dipotassium glycyrrhizinate, sodium metabisulfite, arginine and p-hydroxyacetophenone. The source of the skin conditioning agent is not particularly limited in the present invention, and the above-mentioned niacinamide, ascorbyl glucoside, allantoin, althea root extract, purslane extract, atractylodes macrocephala root extract, alveolus alata root extract, garcinia cambogia extract, angelicae bigelia leaf/stem extract, glutamine, BPN-tesoro 1600 solubilization (palmitoyl tetrapeptide-7/palmitoyl pentapeptide-4/acetyl hexapeptide-8/water/polysorbate-20/1, 2-hexanediol/glycerin/carbomer), dipeptide diaminobutyryl benzylamide diacetate, Prolevis (water/hydrolyzed vegetable protein/phenoxyethanol/sodium benzoate/potassium sorbate/ethylhexylglycerin), glycyrrhizic acid dipotassium salt, glycyrrhizic acid, and the like, well known to those skilled in the art, can be used, Sodium metabisulfite, arginine and p-hydroxyacetophenone.
In the present invention, the thickener is preferably selected from one or more of carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer, hydroxyethyl cellulose, more preferably one or more of polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer, and hydroxyethyl cellulose. The source of the thickener in the present invention is not particularly limited, and commercially available carbomers, polyacrylic acid, xanthan gum, acrylates/C10-30 alkanol acrylate crosspolymer, hydroxyethyl cellulose, as described above, which are well known to those skilled in the art, may be used.
In the present invention, the chelating agent is preferably selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA, more preferably disodium EDTA. The source of the chelating agent is not particularly limited in the present invention, and commercially available products of disodium EDTA, trisodium EDTA, and tetrasodium EDTA, which are well known to those skilled in the art, may be used.
In the present invention, the fragrance is preferably a perfume; the present invention is not particularly limited in its kind and origin.
In the present invention, the preservative is preferably selected from one or more of phenoxyethanol, potassium sorbate and sodium benzoate, more preferably phenoxyethanol. The source of the preservative is not particularly limited in the present invention, and commercially available products of phenoxyethanol, potassium sorbate and sodium benzoate as described above, which are well known to those skilled in the art, may be used.
In the present invention, the pH adjusting agent is preferably selected from citric acid and/or sodium citrate, more preferably citric acid and sodium citrate. The source of the pH adjuster is not particularly limited in the present invention, and commercially available products of the above citric acid and sodium citrate, which are well known to those skilled in the art, may be used.
In the invention, the mask base cloth is cuprammonium fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber or superfine fiber membrane cloth, preferably superfine fiber membrane cloth. The source of the mask base cloth is not particularly limited, and the mask base cloth can be commercially available from the above-mentioned cuprammonium fibers, hydrogel, pure cotton fibers, biological fibers, viscose fibers, wormwood fibers, bamboo charcoal fibers and ultrafine fiber mask cloth, which are well known to those skilled in the art.
The copper ammonia fiber is a regenerated cellulose fiber, which is prepared by dissolving natural cellulose raw materials such as cotton linters and the like in a concentrated ammonia solution of copper hydroxide or alkaline copper salt to prepare spinning solution, decomposing copper ammonia cellulose molecular chemicals in a coagulating bath to regenerate cellulose, and post-processing the generated hydrated cellulose to obtain the copper ammonia fiber, wherein the dry strength of the copper ammonia fiber is close to that of viscose fiber, but the wet strength is higher than that of the viscose fiber, the wear resistance is also better than that of the viscose fiber, and the copper ammonia fiber has the characteristics of fine and soft fiber, proper gloss, good hygroscopicity and performance similar to silk.
In the invention, the hydrogel takes hydrophilic gel as a mask matrix, and is rich in a large amount of nutrients and moisture required by the skin; when the hydrogel facial mask is attached to the skin, the nutritional ingredients contained in the facial mask gradually permeate into the skin, and the facial mask has no stimulation to the skin.
In the invention, the pure cotton fiber is made of 100 percent pure natural cellulose, and the spunlace nonwoven fabric structure is prepared by a cross lapping method, so that the spunlace nonwoven fabric structure has the characteristics of difficult deformation after water absorption, strong longitudinal and transverse tension, white and soft property, good skin-attaching property and the like; the pure cotton cloth film is thickened and encrypted, has strong water absorption capacity, can absorb high-concentration nutrient substances and can effectively prevent the evaporation and the loss of nutrient components.
In the invention, the biological fiber is microbial cellulose generated by natural fermentation of acetobacter xylinum, has excellent water retention capacity, good biocompatibility and no stimulation; the biological fiber has the function similar to that of skin, has the fiber diameter of 50-80 nm, can penetrate into skin gully repair cells and tightly hold the skin cells to generate an upward pulling effect.
In the invention, the viscose fiber is cellulose fiber produced by using cotton or other natural fibers as raw materials, has the moisture content meeting the physiological requirement of human skin, and has the characteristics of smoothness, coolness, ventilation, static resistance and the like.
In the invention, the wormwood fiber takes tencel fiber as a carrier, and is complexed with natural wormwood extraction factors, so that the wormwood fiber has strong moisture absorption performance and good skin adhesion.
In the invention, the bamboo charcoal fiber is prepared by taking moso bamboo as a raw material, adopting a new calcining process and a new technology of pure oxygen high temperature and nitrogen blocking delay to enable micropores of the natural bamboo charcoal to be more refined and honeycombed, and then carrying out melt spinning with a polyester modified slice with a honeycomb micropore structure trend; the unique fiber structure enables the bamboo charcoal fiber mask to have good moisture absorption, air permeability and bacteriostatic effects.
In the invention, the superfine fiber membrane cloth is famous for extremely soft fit and fine touch feeling; the material has the antibacterial and bacteriostatic effects, and is safer and more sanitary; the human skin-like texture has unique smooth and fine touch feeling; the diameter of the single fiber is only 4 mu m, 100 percent of superfine fiber and the fineness of the hair 1/100 can absorb more essence than other membrane cloths; the special fiber structure is similar to human collagen, brings the skin feeling as fine as emulsion, can perfectly attach to the skin by reasonable cutting, is extremely soft, has outstanding adsorbability and water release property, and can deeply nourish the skin.
The facial mask provided by the invention adopts the essence added with the herbal firming compound composition, and through skin tests, the firming and anti-aging effects are good; the use feeling and the efficacy are better by matching with the specific mask base cloth. In a preferred embodiment of the invention, the mask base cloth is superfine fiber mask cloth, the mask cloth is soft in texture and strong in air permeability, can be perfectly attached to the skin, covers the whole face, is excellent in liquid receiving performance and osmotic pressure, and can effectively delay skin aging, keep the skin tender and elastic and eliminate and reduce skin wrinkles by combining the mask essence.
The invention also provides a preparation method of the herbal compact compound mask in the technical scheme, which comprises the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal firming compound mask.
The invention firstly mixes solvent, humectant, solubilizer, skin conditioner, thickener, chelating agent, aromatic and pH regulator evenly in a vacuum emulsification tank. In the present invention, the solvent, the humectant, the solubilizer, the skin conditioner, the thickener, the chelating agent, the fragrance, and the pH adjuster are the same as those described in the above technical solution, and are not described herein again.
The invention carries out the mixing process according to the solubility between the specific components of the humectant, the solubilizer, the skin conditioner, the thickener, the chelating agent, the aromatic and the pH regulator and different solvents; preferably specifically
a1) Putting water, glycerol, sodium hyaluronate, hydrolyzed sodium hyaluronate, hydroxyethyl urea, trehalose, glyceryl polyether-26, allantoin, p-hydroxyacetophenone, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, xanthan gum, polyacrylic acid, hydroxyethyl cellulose, EDTA disodium, EDTA trisodium and EDTA tetrasodium into a vacuum emulsification tank, dissolving at 80-85 ℃, uniformly stirring, and cooling to 43-47 ℃ to obtain phase A;
a2) completely dissolving arginine, citric acid and sodium citrate with a part of water in a separate dissolving tank to obtain a phase B;
a3) completely dissolving butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, 1, 2-propanediol, essence, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20 in a single dissolving tank to obtain a phase C;
a4) adding the phase B and the phase C into a vacuum emulsification tank (phase A) in sequence, and uniformly dispersing.
Then, adding the compound composition and the preservative to disperse uniformly; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain the essence. In the present invention, the compound composition and the preservative are the same as those described in the above technical scheme, and are not described herein again.
After the essence is obtained, the obtained essence and mask base cloth are filled together to obtain the herbal firming compound mask. In the invention, the mask base cloth is the same as that in the technical scheme, and is not described again.
The preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
The invention provides a herbal firming compound composition, a mask and a preparation method thereof; the herbal compact compound composition comprises the following components: 0.02-1 part by weight of cistanche extract; 0.02-0.5 parts by weight of pseudo-ginseng extract; 0.02-0.5 parts by weight of astragalus extract; 0.02-0.5 parts by weight of rose hip extract; 0.02-1 part by weight of horse chestnut extract. Compared with the prior art, the five traditional Chinese medicine components of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract are compounded according to a certain proportion, and are mutually supplemented and synergized, so that the obtained herbal firming compound composition can improve skin elasticity and wrinkles, tighten skin and delay skin aging; meanwhile, the facial mask provided by the invention adopts the essence added with the herbal firming compound composition, and is matched with the specific facial mask base cloth, so that the use feeling and the efficacy are better.
In addition, the preparation method provided by the invention has the advantages of simple process, mild conditions, easiness in operation control, suitability for large-scale production and wide application prospect.
To further illustrate the present invention, the following examples are provided for illustration. The starting materials used in the following examples of the present invention are all commercially available products.
Example 1: the herbal compact compound composition
(1) Formulations 1 to 8
Table 1 formula of herbal compact compound composition in example 1
Figure BDA0002660696500000131
(2) Comparative examples 1 to 6
Comparative example 1: compared with the formula 3, the composition only contains carnosine and hydroxypropyl tetrahydropyrane triol, and the rest is unchanged;
comparative example 2: compared with the formula 3, the traditional Chinese medicine composition does not contain cistanche salsa extract, and the rest is unchanged;
comparative example 3: compared with the formula 3, the traditional Chinese medicine composition does not contain the pseudo-ginseng extract, and the rest is unchanged;
comparative example 4: compared with the formula 3, the traditional Chinese medicine composition does not contain astragalus extract, and the rest is unchanged;
comparative example 5: compared with the formula 3, the rose hip cream does not contain rose hip extract, and the rest is unchanged;
comparative example 6: compared with formula 3, the composition does not contain horse chestnut extract, and the rest is unchanged.
Test example:
the free radical scavenging capacity, the skin elasticity and the wrinkle improvement effect of the herbal compact compound composition provided by the embodiment 1 of the invention are tested and compared with the compositions of comparative examples 1-6:
firstly, preparing the toning lotion to be tested, wherein the specific preparation method is as follows (if the formula does not contain a certain component according to 100 parts by weight, the component is not added in the preparation process):
putting a proper amount of water, 0.2 part by weight of xanthan gum and 0.02 part by weight of disodium EDTA into a vacuum emulsification tank, dissolving at 80-85 ℃ (preferably 82 ℃), uniformly stirring, and cooling to 43-47 ℃ (preferably 45 ℃); then adding the cistanche deserticola extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract, the horse chestnut extract, the carnosine, the hydroxypropyl tetrahydropyrane triol and 0.5 weight part of ethylhexyl glycerin/phenoxyethanol preservative into a vacuum emulsification tank in sequence, and dispersing uniformly; cooling to 32-35 deg.C (preferably 33 deg.C), defoaming, filtering, and discharging to obtain the final product.
And then (1) testing the free radical scavenging capacity of the formula 1-8 and the comparative examples 1-6:
carrying out free radical scavenging test on the toning lotion prepared from each composition, and calculating the inhibition rate of the toning lotion; the specific detection method is as follows: the toning lotion is prepared into sample solutions with the concentration of 1 percent by mass and volume ratio by using dimethyl sulfoxide, then 2mL of the sample solutions and 2mL of diphenyl picrophenylhydrazine (DPPH) solutions with the concentration of 100 mu mol/L are added into the same test tube with a plug, the test tube is shaken up and kept stand for 30 minutes at room temperature, and the absorbance of the samples is measured at the wavelength of 510nm by taking a solvent as a blank. The specific test results are shown in Table 2.
The inhibition ratio (k%) is calculated as follows:
k%=[1-(Ai-Aj)/Ac]×100%;
wherein Ai is the absorbance of 2mL of DPPH solution +2mL of sample solution;
aj is the absorbance of 2mL of sample solution +2mL of dimethyl sulfoxide;
ac was absorbance of 2mL DPPH solution +2mL dimethylsulfoxide.
TABLE 2 ability data to clear DPPH
Formulation 1 Formulation 2 Formulation 3 Formulation 4 Formulation 5 Formulation 6 Formulation 7 Formulation 8
Inhibition rate 91.6% 93.2% 95.9% 94.8% 93.7% 92.5% 95.7% 92.4%
TABLE 2
Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4 Comparative example 5 Comparative example 6
Inhibition rate 60.7% 77.3% 77.9% 78.7% 80.4% 79.3%
(2) The skin elasticity and wrinkle improvement effects of formulas 1 to 8 and comparative examples 1 to 6 were tested:
test subjects: 420 healthy volunteers aged 30-55 years.
And (3) inclusion standard: poor skin elasticity and skin aging phenomena such as wrinkles appear; no other cosmetic was used throughout the test period.
The test method comprises the following steps: the test volunteers were randomly divided into 14 groups of 30 cases by parallel control, and each lotion was used. After the test volunteers clean the face in the morning and in the evening, 1-1.5 mL of lotion is respectively applied to the face, the skin elasticity is tested by using a skin elasticity tester Cutomer MPA580 (CK company, Germany) after the test volunteers use the face for 0 day and use the face for 4 weeks, a high-definition and standardized image is shot for the face of the volunteers by using a face imaging tester VISIA XZ-25 (Canfield company, USA), thin lines of skin strips are read, and 3 groups of data are averaged for each test. And calculates the rate of change of elasticity and the rate of wrinkle improvement of the skin.
Skin elasticity change rate (x) (elasticity after 4 weeks use-elasticity before use (day 0)/elasticity before use (day 0);
the skin wrinkle improvement rate (y) is (number of fine lines before use (day 0) -number of fine lines after 4 weeks of use)/number of fine lines before use (day 0).
The test results are shown in Table 3.
TABLE 3 data on skin elasticity and wrinkle improvement
Figure BDA0002660696500000151
As can be seen from tables 2 and 3, the effects of the formula 6 and the formula 8 are superior to those of the comparative examples 2 to 6, which shows that the cistanche extract, the panax notoginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract can be synergized, reduce the damage of free radicals to cells, and improve the conditions of skin relaxation, poor elasticity and wrinkles; meanwhile, the composition can activate the activity of organism cells, promote the synthesis of extracellular matrix and accelerate the metabolism of skin, thereby achieving the effects of tightening and resisting aging. Formulas 6 and 8 are superior to formula 1, which shows that the adding proportion of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract is 4: 1: 1: 1: 3, the effect is better; formula 6 is superior to formula 8, which shows that the effect is better when the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract are 1 part by weight; formulas 2 and 5 are superior to formulas 1, 6 and 8, which shows that the tightening and anti-aging effects of the invention can be enhanced by further adding carnosine or hydroxypropyl tetrahydropyrane triol to the cistanche extract, the notoginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract, formulas 3, 4 and 7 are superior to formulas 2 and 5, which shows that the tightening and anti-aging effects of the invention can be enhanced by further adding carnosine and hydroxypropyl tetrahydropyrane triol to the cistanche extract, the notoginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract, formulas 3, 4 and 7 are superior to formulas 2, 5 and 6 and comparative examples 1 to 6, which shows that the cistanche extract, the notoginseng extract, the astragalus extract, the rose hip extract, the horse chestnut extract, the carnosine and the hydroxypropyl tetrahydropyrane triol must be synergistically used, the effect is better; formulas 3 and 7 are superior to formula 4, which shows that the adding proportion of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract, the horse chestnut extract, the carnosine and the hydroxypropyl tetrahydropyrane triol is 4: 1: 1: 1: 3: 0.5: when 10, the effect is better; formula 3 is superior to formula 7, and shows that the best effect is achieved when the addition amount of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract, the horse chestnut extract, the carnosine and the hydroxypropyl tetrahydropyrane triol is 2.05 parts by weight; as can be seen from tables 2 and 3, the compositions of the present invention, when combined reasonably, can effectively inhibit the generation of free radicals and improve skin elasticity and wrinkles, and have significant effects.
Example 2: the herbal firming compound mask provided by the invention
(1) 1-5 mask
Table 4 formula of herbal firming compound mask in example 2
Figure BDA0002660696500000161
Figure BDA0002660696500000171
Figure BDA0002660696500000181
(2) Comparative examples 7 to 13
Comparative example 7, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 1, the remainder being unchanged;
comparative example 8, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 2, the remainder being unchanged;
comparative example 9, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 3, the remainder being unchanged;
comparative example 10, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 4, the remainder being unchanged;
comparative example 11, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 5, the remainder being unchanged;
comparative example 12, compared to mask 3, the tightening compound composition of formula 3 was replaced with the composition of comparative example 6, the remainder being unchanged;
comparative example 13, compared to mask 3, the tightening compound composition of formula 3 was replaced with the tightening compound composition of formula 6, the remainder being unchanged.
The preparation method of the facial mask is as follows (when a certain component is not contained in the formula, the component is not added in the preparation process):
(1) putting water, glycerol, sodium hyaluronate, hydrolyzed sodium hyaluronate, hydroxyethyl urea, trehalose, glyceryl polyether-26, allantoin, p-hydroxyacetophenone, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, xanthan gum, polyacrylic acid, hydroxyethyl cellulose, EDTA disodium, EDTA trisodium and EDTA tetrasodium into a vacuum emulsification tank, dissolving at 82 ℃, uniformly stirring, and cooling to 45 ℃ to obtain phase A;
(2) completely dissolving arginine, citric acid and sodium citrate with a part of water in a separate dissolving tank to obtain a phase B;
(3) completely dissolving butanediol, 1, 2-hexanediol, 1, 2-pentanediol, 1, 3-propanediol, 1, 2-propanediol, essence, PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20 in a single dissolving tank to obtain a phase C;
(4) sequentially adding the phase B and the phase C into a vacuum emulsification tank (phase A), and uniformly dispersing;
(5) sequentially adding Cistanchis herba extract, Notoginseng radix extract, radix astragali extract, fructus Rosae Davuricae extract, horse chestnut extract, carnosine, hydroxypropyl tetrahydropyrane triol, nicotinamide, ascorbic acid glucoside, radix Althaeae Roseae extract, herba Portulacae extract, Atractylodis rhizoma root extract, radix Altaicae extract, Garcinia Cambogia fruit extract, Angelica Bischofskii leaf/stem extract, glutamine, BPN-tesoro 1600solution, dipeptide diaminobutyrylbenzyl amide diacetate, Prolevis, dipotassium glycyrrhizinate, sodium pyrosulfite, phenoxyethanol, sodium benzoate, and potassium sorbate into a vacuum emulsification tank, and uniformly dispersing;
(6) cooling to 33 ℃, defoaming, filtering and discharging;
(7) after being inspected to be qualified, the mask base cloth and the mask base cloth are filled into finished products, and the finished products are packaged and put in storage.
And (3) efficacy verification:
performing efficacy verification on the facial masks 1-5 and the facial masks of comparative examples 7-13; the specific verification method comprises the following steps:
360 volunteers with 30-55 years old and healthy bodies are selected, wherein 180 male volunteers and 180 female volunteers are randomly divided into 12 groups of 30 volunteers. And (3) inclusion standard: poor skin elasticity and skin aging phenomena such as wrinkles appear; no other cosmetic was used throughout the test period. The using method comprises the following steps: after the face is cleaned in the morning and evening every day, the facial mask is applied for 5-15 min (preferably 8min), and the face mask is continuously used for 2 months. Different items are respectively scored according to skin changes, the different items comprise wrinkle changes, skin elasticity, tightening effects and skin overall conditions, each item is fully divided into 100 points, and the higher the score value is, the better the effect is. And counting the scoring results, and then calculating the mean value to obtain the final scoring result.
Evaluation of feeling of use: the volunteers evaluated the feeling of use after 7 days of continuous use. People who feel more than 80% feel very soft, close to the face, and breathable, and are rated as "+++", 60% -80% are rated as "+++", and below 60% are rated as "+".
The results are shown in Table 5.
Table 5 efficacy test results of the mask
Figure BDA0002660696500000191
Figure BDA0002660696500000201
As can be seen from table 5, (1) efficacy: after the facial mask 1-5 and the comparative example 13 are used, the wrinkle change, the skin elasticity, the tightening effect and the overall skin condition are all superior to those of the comparative examples 7-12; further, a comparative example 13 is superior to comparative examples 8-12, which shows that the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract provided by the invention can well achieve the effect of tightening the skin by combining; the tightening effect of the facial mask 1-5 is superior to that of the comparative example 13, and shows that on the basis of the cistanche extract, the pseudo-ginseng extract, the astragalus extract, the rose hip extract and the horse chestnut extract, carnosine and hydroxypropyl tetrahydropyrane triol are further added, so that the synergistic effect can be achieved, the effect of tightening the skin of the composition is further improved, and the tightening effect of the facial mask 1-5 is superior to that of the comparative examples 7-13. Compared with the facial masks 1-2 and the facial masks 4-5, the facial mask 3 has the advantages that the firming effect is improved along with the increase of the adding amount of the firming composition, but when the adding amount of the firming composition in the facial mask is 2.05 parts by weight, the firming effect is optimal when the superfine fibers are used as facial mask base cloth, and the effect of the facial mask base cloth of the superfine fibers on the firming composition provided by the invention is promoted. (2) The use feeling is as follows: compared with the facial masks 1-2 and 4-5, the facial mask 3 has the best use feeling when the material of the facial mask base cloth is made of superfine fibers.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (10)

1. The herbal compact compound composition comprises the following components:
0.02-1 part by weight of cistanche extract;
0.02-0.5 parts by weight of pseudo-ginseng extract;
0.02-0.5 parts by weight of astragalus extract;
0.02-0.5 parts by weight of rose hip extract;
0.02-1 part by weight of horse chestnut extract.
2. The herbal compact compound composition of claim 1, further comprising:
0.01-0.2 parts of carnosine;
0.6-3 parts by weight of hydroxypropyl tetrahydropyrane triol.
3. A herbal firming compound facial mask comprises essence and facial mask base cloth;
the essence is prepared from the following raw materials:
70.92-92.86 parts by weight of a solvent;
0-11.75 parts by weight of a humectant;
0-1 part by weight of a solubilizer;
0.71-6.7 parts by weight of the compound composition;
0.22-13.77 parts by weight of a skin conditioner;
0.1-0.8 parts of thickening agent;
0.02-0.1 part by weight of a chelating agent;
0-0.05 parts by weight of an aromatic;
0.1-0.6 parts by weight of a preservative;
0-0.3 part of pH regulator;
the compound composition is the herbal compact compound composition as defined in any one of claims 1-2;
the mask base cloth is copper ammonia fiber, hydrogel, pure cotton fiber, biological fiber, viscose fiber, wormwood fiber, bamboo charcoal fiber or superfine fiber film cloth.
4. The herbal firming compound mask as claimed in claim 3, wherein the moisturizer is one or more selected from the group consisting of glycerin, sodium hyaluronate, trehalose, hydrolyzed sodium hyaluronate, hydroxyethyl urea and glyceryl polyether-26.
5. The herbal firming compound mask as claimed in claim 3, wherein the solubilizer is selected from one or more of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether and Tween-20.
6. The herbal firming compound mask as claimed in claim 3, wherein the skin conditioning agent is selected from one or more of niacinamide, ascorbyl glucoside, allantoin, althea root extract, purslane extract, atractylodes macrocephala root extract, bupleurum root extract, garcinia cambogia extract, angelicae bigelovii leaf/stem extract, glutamine, BPN-tesoro 1600solution, dipeptide diaminobutyryl benzylamide diacetate, proles, dipotassium glycyrrhizinate, sodium metabisulfite, arginine and p-hydroxyacetophenone.
7. The herbal firming compound mask as claimed in claim 3, wherein the thickener is one or more selected from carbomer, polyacrylic acid, xanthan gum, acrylate/C10-30 alkanol acrylate crosspolymer, and hydroxyethyl cellulose.
8. The herbal firming compound mask as claimed in claim 3, wherein the chelating agent is selected from disodium EDTA, trisodium EDTA or tetrasodium EDTA.
9. The herbal firming compound mask as claimed in claim 3, wherein the pH regulator is selected from citric acid and/or sodium citrate.
10. A preparation method of the herbal compact compound mask as claimed in any one of claims 3 to 9, comprising the following steps:
a) uniformly mixing a solvent, a humectant, a solubilizer, a skin conditioner, a thickening agent, a chelating agent, an aromatic and a pH regulator in a vacuum emulsification tank; then adding the compound composition and the preservative to be uniformly dispersed; then cooling to 32-35 ℃, defoaming, filtering and discharging to obtain essence;
b) filling the essence obtained in the step a) and mask base cloth together to obtain the herbal firming compound mask.
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