CN111939093B - Bath oil with foaming and moistening effects, and its preparation method - Google Patents
Bath oil with foaming and moistening effects, and its preparation method Download PDFInfo
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- CN111939093B CN111939093B CN202010870032.2A CN202010870032A CN111939093B CN 111939093 B CN111939093 B CN 111939093B CN 202010870032 A CN202010870032 A CN 202010870032A CN 111939093 B CN111939093 B CN 111939093B
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- 238000005187 foaming Methods 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 230000000694 effects Effects 0.000 title abstract description 8
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 19
- 238000002156 mixing Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 14
- 239000011734 sodium Substances 0.000 claims abstract description 14
- 229920006052 Chinlon® Polymers 0.000 claims abstract description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 7
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- MSCCTZZBYHQMQJ-AZAGJHQNSA-N Tocopheryl nicotinate Chemical compound C([C@@](OC1=C(C)C=2C)(C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)CC1=C(C)C=2OC(=O)C1=CC=CN=C1 MSCCTZZBYHQMQJ-AZAGJHQNSA-N 0.000 claims abstract description 7
- 150000001413 amino acids Chemical class 0.000 claims abstract description 7
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims abstract description 7
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 7
- IIRDTKBZINWQAW-UHFFFAOYSA-N hexaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCO IIRDTKBZINWQAW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940049920 malate Drugs 0.000 claims abstract description 7
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 7
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940057950 sodium laureth sulfate Drugs 0.000 claims abstract description 7
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 7
- 229950009883 tocopheryl nicotinate Drugs 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000003921 oil Substances 0.000 claims description 47
- 235000019198 oils Nutrition 0.000 claims description 47
- 238000004821 distillation Methods 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 17
- 238000000605 extraction Methods 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 230000003020 moisturizing effect Effects 0.000 claims description 14
- 238000004140 cleaning Methods 0.000 claims description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 5
- 239000010487 meadowfoam seed oil Substances 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 3
- 241001092489 Potentilla Species 0.000 claims description 2
- 230000007794 irritation Effects 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 9
- 230000001953 sensory effect Effects 0.000 abstract description 8
- 230000009286 beneficial effect Effects 0.000 abstract description 4
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 description 18
- 210000003491 skin Anatomy 0.000 description 10
- 241001531051 Potentilla chinensis Species 0.000 description 9
- 206010040880 Skin irritation Diseases 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000006260 foam Substances 0.000 description 4
- 231100000475 skin irritation Toxicity 0.000 description 4
- 230000036556 skin irritation Effects 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 3
- 238000005070 sampling Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 2
- 206010040914 Skin reaction Diseases 0.000 description 2
- 241000205578 Thalictrum Species 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 210000004209 hair Anatomy 0.000 description 2
- 230000035483 skin reaction Effects 0.000 description 2
- 231100000430 skin reaction Toxicity 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229920000298 Cellophane Polymers 0.000 description 1
- 240000000233 Melia azedarach Species 0.000 description 1
- 241000283973 Oryctolagus cuniculus Species 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 231100000022 skin irritation / corrosion Toxicity 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to bath oil with foaming property and moistening property and a preparation method thereof. The bath oil comprises the following raw materials in parts by weight: 25 to 35 parts of ethylhexyl palmitate, 22 to 25 parts of propylene glycol, 19 to 23 parts of sodium laureth sulfate, 7 to 11 parts of water, 5 to 7 parts of laureth, 3 to 5 parts of white chinlon oil, 0.4 to 0.6 part of tocopherol nicotinate, 2 to 4 parts of cocamide, 0.8 to 1.2 parts of sodium lauroyl oat amino acid, 0.8 to 1.2 parts of PEG-6 caprylic/capric glyceride, 0.8 to 1.2 parts of sodium cocoyl malate and 0.08 to 0.12 part of essence. The sensory and physical and chemical properties of the bath oil meet the national standard, and the bath oil has no irritation to skin, good moistening property and good foaming effect; the preparation method only needs simple mixing, is simple to operate, has easily-controlled process, and is beneficial to large-scale production.
Description
Technical Field
The invention belongs to the field of daily chemicals, and particularly relates to bath oil with foaming property and moisturizing property and a preparation method thereof.
Background
The bath oil is a product integrating cleaning and skin care, and the common use method comprises the steps of firstly wetting the skin of the whole body by water, directly wiping and rubbing the skin by the bath oil, and then washing the skin clean; or squeezing appropriate amount of bath oil on wet bath ball, kneading to obtain foam, rubbing whole body, and washing.
The existing bath oil has the disadvantages of difficult avoidance of damage to skin, poor moisturizing effect and poor foaming effect.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides bath oil with foaming property and moistening property and a preparation method thereof. The sensory and physical and chemical properties of the bath oil meet the national standard, and the bath oil has no irritation to skin, good moistening property and good foaming effect; the preparation method only needs simple mixing, is simple to operate, has easily-controlled process, and is beneficial to large-scale production.
The invention provides bath oil with foaming property and moistening property, which comprises the following raw materials in parts by weight: 25 to 35 parts of ethylhexyl palmitate, 22 to 25 parts of propylene glycol, 19 to 23 parts of sodium laureth sulfate, 7 to 11 parts of water, 5 to 7 parts of laureth, 3 to 5 parts of white chinlon oil, 0.4 to 0.6 part of tocopherol nicotinate, 2 to 4 parts of cocamide, 0.8 to 1.2 parts of sodium lauroyl oat amino acid, 0.8 to 1.2 parts of PEG-6 caprylic/capric glyceride, 0.8 to 1.2 parts of sodium cocoyl malate and 0.08 to 0.12 part of essence.
Preferably, the bath oil with foaming property and moisturizing property comprises the following raw materials in parts by weight: 30 parts of ethylhexyl palmitate, 23.4 parts of propylene glycol, 21 parts of sodium laureth sulfate, 9 parts of water, 6 parts of laureth-30, 4 parts of white chinlon oil, 0.5 part of tocopherol nicotinate, 3 parts of cocamide, 1 part of sodium lauroyl oat amino acid, 1 part of PEG-6 caprylic/capric glyceride, 1 part of sodium cocoyl malate and 0.1 part of essence.
Preferably, the preparation method of the meadowfoam seed oil comprises the following steps:
(1) Taking the white pond flower and the white pond flower seeds, cleaning, mixing with water, distilling and extracting to obtain a primary extracting solution and primary distillation residues;
(2) Mixing the primary distillation residues obtained in the step (1) with ethanol, and performing secondary distillation extraction to obtain a secondary extracting solution and secondary distillation residues;
(3) Mixing the primary extract and the secondary extract to obtain a mixed solution; and (4) centrifuging the combined solution, and taking an oil phase to obtain the white chinaberry seed oil.
Preferably, in the step (1), the weight ratio of the white pond flowers to the white pond flower seeds is 1:2-3.
Preferably, in the step (1), the weight ratio of the total amount of the white pond flowers and the white pond flower seeds to the water is 1:3-5.
Preferably, in the step (1), the temperature of the distillation extraction is 85-93 ℃, and the time of the distillation extraction is 2-4 h.
Preferably, in the step (2), the weight ratio of the primary distillation residues to the ethanol is 1:1-3.
Preferably, in the step (2), the temperature of the secondary distillation extraction is 65-70 ℃, and the time of the secondary distillation extraction is 4-6 h.
Preferably, in the step (3), the rotation speed of the centrifugal separation is 8000-10000 r/min.
Based on the same technical conception, the invention also provides a preparation method of the bath oil with foamability and moisturizing property, which comprises the following steps: mixing the raw materials, and stirring.
The invention has the beneficial effects that:
1. the bath oil with foamability and moistening property provided by the invention has the advantages that various effective components are reasonably combined, and the sensory and physical and chemical properties of the bath oil meet the national standards through verification, and the bath oil has no irritation to skin, and has good moistening property and foaming effect.
2. The preparation method of the bath oil with foamability and moisturizing property only needs simple mixing, has simple operation and easily controlled process, and is beneficial to large-scale production.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It should be apparent that the described embodiments are only some embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
Example 1
This example provides a method for preparing a bath oil having foaming and moisturizing properties, comprising the steps of:
(I) The method for preparing the white Potentilla seed oil comprises the following steps:
(1) Cleaning 1kg of white Potentilla chinensis and 2kg of seeds of the white Potentilla chinensis, mixing with 9kg of water, and distilling at 85 deg.C for 2 hr to obtain primary extractive solution and primary distilled residue;
(2) Mixing the primary distillation residue obtained in the step (1) with ethanol according to the weight ratio of 1:1, and carrying out secondary distillation extraction for 4 hours at the temperature of 65 ℃ to obtain a secondary extraction solution and secondary distillation residue;
(3) Mixing the primary extract and the secondary extract to obtain a mixed solution; and (4) carrying out centrifugal separation on the combined solution at 8000r/min, and taking an oil phase to obtain the white chinlon oil.
(II) preparing the bath oil with foaming property and moistening property, the method comprises the following steps:
250g of ethylhexyl palmitate, 220g of propylene glycol, 190g of sodium laureth sulfate, 70g of water, 50g of laureth-30, 30g of white chinlon oil, 4g of tocopherol nicotinate, 20g of coconut oil amide, 8g of sodium lauroyl oat amino acid, 8g of PEG-6 caprylic/capric glyceride, 8g of sodium cocoyl malate and 0.8g of essence are mixed and stirred, and after the system is uniform, the bath oil with foamability and moisturizing property is obtained by sequentially discharging, standing, inspecting, filling, packaging, code spraying, sampling and warehousing.
Example 2
This example provides a method for preparing a bath oil having foaming and moisturizing properties, comprising the steps of:
(I) The method for preparing the meadowrue root oil comprises the following steps:
(1) Cleaning 1kg of white Potentilla chinensis and 3kg of white Potentilla chinensis seeds, mixing with 20kg of water, and distilling at 93 deg.C for 4 hr to obtain primary extractive solution and primary distillation residue;
(2) Mixing the primary distillation residue obtained in the step (1) with ethanol according to the weight ratio of 1:3, and carrying out secondary distillation extraction for 6 hours at the temperature of 70 ℃ to obtain a secondary extraction solution and secondary distillation residue;
(3) Mixing the primary extract and the secondary extract to obtain a mixed solution; centrifuging the combined solution at 10000r/min, and collecting oil phase to obtain white Potentilla chinensis seed oil.
(II) preparing the bath oil with foaming property and moistening property, the method comprises the following steps:
350g of ethylhexyl palmitate, 250g of propylene glycol, 230g of sodium laureth sulfate, 110g of water, 70g of laureth-30, 50g of white Potentilla chinensis seed oil, 6g of tocopherol nicotinate, 40g of cocamide, 12g of sodium lauroyl oat amino acid, 12g of PEG-6 caprylic/capric glyceride, 12g of sodium cocoyl malate and 1.2g of essence are mixed and stirred, and after the system is uniform, the bath oil with foamability and moisturizing property is obtained by sequentially discharging, standing, inspecting, filling, packaging, code spraying, sampling and warehousing.
Example 3
This example provides a method for preparing a bath oil having foaming and moisturizing properties, comprising the steps of:
(I) The method for preparing the meadowrue root oil comprises the following steps:
(1) Cleaning 1kg of white Potentilla chinensis and 2.5kg of seeds of the white Potentilla chinensis, mixing with 14kg of water, and distilling at 89 deg.C for 3 hr to obtain primary extractive solution and primary distilled residue;
(2) Mixing the primary distillation residue obtained in the step (1) with ethanol according to the weight ratio of 1:2, and performing secondary distillation extraction for 5 hours at 68 ℃ to obtain a secondary extraction solution and secondary distillation residue;
(3) Mixing the primary extract and the secondary extract to obtain a mixed solution; centrifuging the combined solution at 9000r/min, and collecting oil phase to obtain white Potentilla chinensis seed oil.
(II) preparing the bath oil with foaming property and moistening property, the method comprises the following steps:
300g of ethylhexyl palmitate, 234g of propylene glycol, 210g of sodium laureth sulfate, 90g of water, 60g of laureth-30, 40g of white chinlon oil, 5g of tocopherol nicotinate, 30g of coconut oil amide, 10g of sodium lauroyl oat amino acid, 10g of PEG-6 caprylic/capric glyceride, 10g of sodium cocoyl malate and 1g of essence are mixed and stirred, and after the system is uniform, the bath oil with foaming property and moisturizing property is obtained by sequentially discharging, standing, inspecting, filling, packaging, code spraying, sampling and warehousing.
Comparative example
The comparative example differs from example 3 in that it does not contain meadowfoam seed oil and the other components and amounts are the same.
In order to verify various performances of the bath oil with foamability and moisturizing property, the test is carried out by referring to GB/T34857-2017 bathing agent, the sensory and physicochemical test standards are shown in Table 1, and the sensory and physicochemical test results are shown in Table 2.
The appearance detection method comprises the following steps: not less than 200mL of sample was taken and placed in a dry, clean, colorless, stoppered glass jar for observation under non-direct light conditions.
The odor detection method comprises the following steps: taking a proper amount of sample and identifying by smell sense.
Stability: measuring two parts of a sample with the volume not less than 100mL, respectively placing the two parts in a 250mL colorless wide-mouth glass bottle with a plug, placing one part in a heat preservation box with the temperature of 38-42 ℃ for 24 hours, taking out the sample, returning the sample to the room temperature, and then comparing the sample with the sample before the test for analysis; and the other part is placed in a refrigerator at (-7 to-3) DEG C for 24 hours, taken out and restored to the room temperature, and then is compared with the sample before the test for analysis.
Total effective substances: the measurement was carried out according to method A defined in chapter 7 of GB/T13173-2008.
pH: the method is carried out according to the method specified in technical Specification for cosmetic safety (2015 edition).
Formaldehyde: the method is carried out according to the method specified in technical Specification for cosmetic safety (2015 edition).
TABLE 1 sensory and physicochemical test standards
TABLE 2 sensory and physicochemical test results
To verify the irritation of the bath oil, a skin irritation/corrosion test was performed by:
(1) Shearing off hairs on two sides of the spine of the white rabbit about 24 hours before the test, wherein the epidermis cannot be damaged, and the hair removing range is about 3cm multiplied by 3cm respectively on the left side and the right side;
(2) About 0.5mL (g) of the test substance (bath oil) was applied directly to the skin, covered with two layers of gauze (2.5 cm. Times.2.5 cm) and a layer of cellophane or the like, and fixed with a non-irritating adhesive tape and bandage. The other side of the skin served as a control. Adopting a closed test, wherein the application time is 2h, and removing residual test substances by using warm water or a non-irritant solvent after the test is finished;
(3) Skin reactions at the smeared sites were observed for 1, 24, 48 and 72h after removal of the test substances, skin reaction scores were made according to table 3, comprehensive evaluation was made with the average value of the scores of the test animals, and skin irritation intensity was judged according to table 4 based on the highest average value of the scores at each observation time point of 24, 48 and 72 h.
TABLE 3 skin irritation response score
Table 4 skin irritation intensity grading
The test results are shown in table 5.
TABLE 5 test results
| Group of | Example 1 | Example 2 | Example 3 | Comparative example |
| Results | Has no irritation | Has no irritation | Has no irritation | Middle irritation |
10 volunteers were selected to try out the bath oil of the invention and compared with similar products on the market to test the foaming effect, and the scores were averaged. The evaluation criteria for the foaming effect are shown in Table 6, and the evaluation results are shown in Table 7.
TABLE 6 Scoring standards
| Scoring criteria | Corresponding score/score |
| No obvious foam after use | 1～3 |
| Has less foam after use | 4～7 |
| After use, the foam is full | 8～10 |
TABLE 7 scoring results
| Group of | Example 1 | Example 2 | Example 3 | The same kind of products sold in the market |
| Score/score | 9 | 9 | 10 | 6 |
In conclusion, the bath oil with foamability and moisturizing property of the invention has the sensory and physical and chemical properties meeting the national standard; and after animal experiments, the bath oil obtained in the examples 1 to 3 has no skin irritation; the bath oil obtained by the comparative example has moderate irritation, which shows that the meadowfoam seed oil can well moisten skin and reduce irritation; and compared with similar products, the foaming performance is good.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (2)
1. The bath oil with foaming property and moistening property is characterized by comprising the following raw materials in parts by weight: 30 parts of ethylhexyl palmitate, 23.4 parts of propylene glycol, 21 parts of sodium laureth sulfate, 9 parts of water, 306 parts of laureth, 4 parts of white chinlon oil, 0.5 part of tocopherol nicotinate, 3 parts of cocoamide, 1 part of sodium lauroyl oat amino acid, 1 part of PEG-6 caprylic/capric glyceride, 1 part of sodium cocoyl malate and 0.1 part of essence;
the preparation method of the meadowfoam seed oil comprises the following steps:
(1) Taking the white pond flower and the white pond flower seeds, cleaning, mixing with water, distilling and extracting to obtain a primary extracting solution and primary distillation residues; wherein the weight ratio of the white pond flowers to the white pond flower seeds is 1:2-3; the weight ratio of the total amount of the white pond flowers and the white pond flower seeds to the water is 1:3-5; the temperature of the distillation extraction is 85-93 ℃, and the time of the distillation extraction is 2-4 h;
(2) Mixing the primary distillation residues obtained in the step (1) with ethanol, and performing secondary distillation extraction to obtain a secondary extracting solution and secondary distillation residues; wherein the weight ratio of the primary distillation residues to the ethanol is 1:1-3; the temperature of the secondary distillation extraction is 65-70 ℃, and the time of the secondary distillation extraction is 4-6 h;
(3) Mixing the primary extract and the secondary extract to obtain a mixed solution; centrifuging the combined solution, and collecting oil phase to obtain white Potentilla seed oil; wherein the rotating speed of the centrifugal separation is 8000-10000 r/min.
2. The method for preparing a bath oil having foamability and moisturizing property of claim 1, wherein the raw materials are mixed and then sufficiently stirred uniformly.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4924223B1 (en) * | 1969-02-17 | 1974-06-21 | ||
| CN103271860A (en) * | 2013-06-18 | 2013-09-04 | 菏泽尧舜牡丹生物科技有限公司 | Skin care oil containing peony oil and preparation method thereof |
| CN110897937A (en) * | 2019-12-20 | 2020-03-24 | 广州蜜妆生物科技有限公司 | Bubble bath oil and preparation method thereof |
| CN111265437A (en) * | 2020-04-10 | 2020-06-12 | 中山爱护日用品有限公司 | Multi-effect repair oil for infants and children and preparation method thereof |
-
2020
- 2020-08-26 CN CN202010870032.2A patent/CN111939093B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4924223B1 (en) * | 1969-02-17 | 1974-06-21 | ||
| CN103271860A (en) * | 2013-06-18 | 2013-09-04 | 菏泽尧舜牡丹生物科技有限公司 | Skin care oil containing peony oil and preparation method thereof |
| CN110897937A (en) * | 2019-12-20 | 2020-03-24 | 广州蜜妆生物科技有限公司 | Bubble bath oil and preparation method thereof |
| CN111265437A (en) * | 2020-04-10 | 2020-06-12 | 中山爱护日用品有限公司 | Multi-effect repair oil for infants and children and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 婴童沐浴产品温和表面活性剂的研究;钱洁等;《《中国洗涤用品工业》个人与家居清洁护理》;20191231(第12期);第48-53段 * |
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