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CN111890620A - Preparation device and preparation method of porous light photocatalytic material - Google Patents

Preparation device and preparation method of porous light photocatalytic material Download PDF

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Publication number
CN111890620A
CN111890620A CN202010787117.4A CN202010787117A CN111890620A CN 111890620 A CN111890620 A CN 111890620A CN 202010787117 A CN202010787117 A CN 202010787117A CN 111890620 A CN111890620 A CN 111890620A
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fixedly connected
plate
water
porous light
photocatalytic material
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曾庆理
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Jiangxi University of Technology
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Jiangxi University of Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/02Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles for articles of definite length, i.e. discrete articles
    • B29C44/04Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles for articles of definite length, i.e. discrete articles consisting of at least two parts of chemically or physically different materials, e.g. having different densities
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34Auxiliary operations
    • B29C44/3415Heating or cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34Auxiliary operations
    • B29C44/3442Mixing, kneading or conveying the foamable material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34Auxiliary operations
    • B29C44/35Component parts; Details or accessories
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34Auxiliary operations
    • B29C44/36Feeding the material to be shaped
    • B29C44/38Feeding the material to be shaped into a closed space, i.e. to make articles of definite length
    • B29C44/42Feeding the material to be shaped into a closed space, i.e. to make articles of definite length using pressure difference, e.g. by injection or by vacuum

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
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Abstract

本发明涉及一种多孔轻质光催化材料的制备装置及制备方法,该装置包括搅拌罐,在搅拌罐的底端固定连接有支撑柱,搅拌罐的一侧嵌合连接有进料管,在进料管的表面嵌合连接有测量尺,进料管的顶端两侧焊接连接有承载板,承载板的顶端焊接连接有支撑杆,支撑杆的顶端固定连接有第一顶板,第一顶板底端安装有混料机构,搅拌罐的底端嵌合连接有排料管。在本发明中,通过潜水泵可将冷却水泵入通水槽,通过通水槽对成型腔内的成型模具进行快速降温,提高冷却效果,加快了多孔轻质光催化材料的成型速度,进而提高了生产效率;此外,通过第一导管,可将冷却水导回至蓄水槽,以对冷却用水进行循环利用,降低了用水成本,节约了水资源。

Figure 202010787117

The invention relates to a preparation device and a preparation method of a porous light photocatalytic material. The device comprises a stirring tank, a support column is fixedly connected to the bottom end of the stirring tank, a feeding pipe is fitted and connected to one side of the stirring tank, and The surface of the feeding pipe is fitted and connected with a measuring ruler, the top of the feeding pipe is welded and connected with a bearing plate on both sides, the top of the bearing plate is welded and connected with a support rod, and the top of the support rod is fixedly connected with a first top plate, and the bottom of the first top plate A mixing mechanism is installed at the end, and a discharge pipe is fitted and connected to the bottom end of the mixing tank. In the present invention, the cooling water can be pumped into the water channel through the submersible pump, the molding die in the molding cavity can be rapidly cooled by the water channel, the cooling effect is improved, the molding speed of the porous light photocatalytic material is accelerated, and the production rate is improved. efficiency; in addition, through the first conduit, the cooling water can be led back to the water storage tank to recycle the cooling water, thereby reducing the cost of water and saving water resources.

Figure 202010787117

Description

多孔轻质光催化材料的制备装置及制备方法Preparation device and preparation method of porous light photocatalytic material

技术领域technical field

本发明涉及功能材料制备技术领域,特别涉及一种多孔轻质光催化材料的制备装置及制备方法。The invention relates to the technical field of functional material preparation, in particular to a preparation device and preparation method of a porous light-weight photocatalytic material.

背景技术Background technique

纳米光催化剂是污染物的克星,其作用机理简单来说就是:纳米光催化剂在特定波长的光的照射下受激生成″电子—空穴″对(一种高能粒子)。这种″电子一空穴″对和周围的水、氧气发生作用后,就具有了极强的氧化-还原能力,能将空气中甲醛、苯等污染物直接分解成无害无味的物质,以及破坏细菌的细胞壁,杀灭细菌并分解其丝网菌体,从而达到了消除空气污染的目的。Nano-photocatalysts are the nemesis of pollutants, and their mechanism of action is simply that: nano-photocatalysts are excited to generate "electron-hole" pairs (a kind of high-energy particles) under the irradiation of specific wavelengths of light. After this "electron-hole" pair interacts with the surrounding water and oxygen, it has a strong oxidation-reduction ability, which can directly decompose formaldehyde, benzene and other pollutants in the air into harmless and odorless substances, and destroy The cell wall of bacteria kills bacteria and decomposes its silk mesh, thus achieving the purpose of eliminating air pollution.

具体来说,在光照下,如果光子的能量大于半导体禁带宽度,其价带上的电子(e-)就会被激发到导带上,同时在价带上产生空穴(h+)。光生空穴有很强的氧化能力,光生电子具有很强的还原能力,它们可以迁移到半导体表面的不同位置,与表面吸附的污染物发生氧化还原反应,在空气污染及水污染治理等领域有很大的应用前景。发泡树脂是一种常用高分子材料,具有价格低廉、制备成型方便、耐腐蚀性强等优点,在各种领域广泛应用,以PU树脂为例,一般将A、B料(含发泡剂)按比例调配混合均匀,即可进入模具进行发泡固化,待固化完成脱模,即可得成型得发泡树脂材料。Specifically, under illumination, if the energy of the photon is greater than the forbidden band width of the semiconductor, the electrons (e-) in the valence band will be excited to the conduction band, and holes (h+) will be generated in the valence band at the same time. Photogenerated holes have strong oxidizing power, and photogenerated electrons have strong reducing power. They can migrate to different positions on the semiconductor surface and undergo redox reactions with pollutants adsorbed on the surface. Great application prospects. Foamed resin is a common polymer material with the advantages of low price, convenient preparation and molding, strong corrosion resistance, etc. It is widely used in various fields. Taking PU resin as an example, materials A and B (containing foaming agent) ) in proportion to mix evenly, then enter the mold for foaming and curing, and after curing is completed and demoulding, the foamed resin material can be obtained by molding.

然而,现有的多孔轻质光催化材料的制备装置,在其使用过程中,发泡成型后,通常通过自然风冷,来对成型件降温,等待降温后再进行脱模作业,使得加工效率变慢,且现有的装置不具备快速混料的功能。However, in the existing device for preparing porous light-weight photocatalytic materials, during the use process, after foaming molding, the molded part is usually cooled by natural air cooling, and then demolding operation is performed after waiting for cooling, so that the processing efficiency is improved. slow, and the existing equipment does not have the function of fast mixing.

发明内容SUMMARY OF THE INVENTION

本发明的目的在于解决现有的光催化材料制备装置,在其使用过程中,发泡成型后,通常通过自然风冷,来对成型件降温,等待降温后再进行脱模作业,使得加工效率变慢的问题。The purpose of the present invention is to solve the problem of the existing photocatalytic material preparation device. During its use, after foaming molding, the molding is usually cooled by natural air cooling, and then demolding is performed after waiting for cooling, so that the processing efficiency is improved. slow down problem.

为实现上述目的,本发明提供如下技术方案:To achieve the above object, the present invention provides the following technical solutions:

本发明提出一种多孔轻质光催化材料的制备装置,包括搅拌罐,所述搅拌罐的底端固定连接有支撑柱,所述搅拌罐的一侧嵌合连接有进料管,在所述进料管的表面嵌合连接有测量尺,所述进料管的顶端两侧焊接连接有承载板,所述承载板的顶端焊接连接有支撑杆,所述支撑杆的顶端固定连接有第一顶板,所述第一顶板底端安装有混料机构,所述搅拌罐的底端嵌合连接有排料管,所述排料管的另一端固定连接有压力泵,所述压力泵的一侧连接有工作台,所述工作台的顶端固定连接有下模具,所述下模具的顶端开设有成型腔,所述下模具的内部开设有通水槽,所述通水槽的一侧活动套接有第一导管,所述通水槽的另一侧活动套接有第二导管,所述工作台的下端活动连接有蓄水槽,所述蓄水槽的内部一侧活动连接有潜水泵,所述潜水泵与第二导管的输入端固定连接,所述通水槽两侧分别与第一导管、第二导管之间安装有密封机构,所述工作台的顶端固定连接有四个导向杆,所述导向杆的顶端焊接连接有第二顶板,所述第二顶板的底端安装有锁模机构,所述通水槽内部安装有过滤机构。The invention provides a preparation device for porous light photocatalytic material, which comprises a stirring tank, a support column is fixedly connected to the bottom end of the stirring tank, and a feeding pipe is fitted and connected to one side of the stirring tank. The surface of the feed pipe is fitted and connected with a measuring ruler, the top of the feed pipe is welded and connected with a carrying plate on both sides, the top of the carrying plate is welded and connected with a support rod, and the top of the support rod is fixedly connected with a first The top plate, the bottom end of the first top plate is equipped with a mixing mechanism, the bottom end of the stirring tank is fitted and connected with a discharge pipe, and the other end of the discharge pipe is fixedly connected with a pressure pump. A worktable is connected to the side, a lower mold is fixedly connected to the top of the worktable, a molding cavity is opened at the top of the lower mold, a water channel is opened inside the lower mold, and one side of the water channel is movably sleeved There is a first conduit, a second conduit is movably sleeved on the other side of the water passage, a water storage tank is movably connected to the lower end of the workbench, and a submersible pump is movably connected to the inner side of the water storage tank, and the submersible The pump is fixedly connected to the input end of the second conduit, a sealing mechanism is installed between the first conduit and the second conduit on both sides of the water passage, and four guide rods are fixedly connected to the top of the workbench. The top end of the rod is welded and connected with a second top plate, the bottom end of the second top plate is provided with a clamping mechanism, and a filter mechanism is mounted inside the water channel.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述混料机构包括两个电动伸缩杆,所述电动伸缩杆与第一顶板的底端之间为固定连接,所述电动伸缩杆的底端固定连接有第一托板,所述第一托板的底端固定连接有第一转动轴,所述第一转动轴的底端转动连接有转杆,所述转杆的表面等距焊接有多个搅拌桨,所述第一托板的顶端嵌合连接有电动机,所述电动机穿过第一托板与第一转动轴固定连接。The mixing mechanism includes two electric telescopic rods, the electric telescopic rods are fixedly connected with the bottom end of the first top plate, and the bottom end of the electric telescopic rod is fixedly connected with a first support plate, and the first support plate is fixedly connected to the bottom end of the electric telescopic rod. The bottom end of the support plate is fixedly connected with a first rotating shaft, the bottom end of the first rotating shaft is rotatably connected with a rotating rod, and the surface of the rotating rod is welded with a plurality of stirring paddles at equal distances. The top end is fitted and connected with a motor, and the motor is fixedly connected to the first rotating shaft through the first support plate.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述搅拌桨通过所述转杆、所述第一转动轴与所述电动机之间构成传动结构,所述第一托板通过电动伸缩杆与第一顶板之间构成升降结构。The stirring paddle forms a transmission structure between the rotating rod, the first rotating shaft and the electric motor, and the first supporting plate forms a lifting structure between the electric telescopic rod and the first top plate.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述锁模机构包括两个液压杆,所述液压杆与第二顶板的顶端之间为固定连接,所述液压杆的底端固定连接有安装板,所述安装板的底端固定连接有上模具,所述安装板的四周分别嵌合连接有导向管,所述导向管与导向杆的表面活动套接,所述上模具的内部安装有导料管,所述导料管与所述压力泵之间为固定连接。The clamping mechanism includes two hydraulic rods, the hydraulic rods are fixedly connected with the top end of the second top plate, the bottom end of the hydraulic rod is fixedly connected with a mounting plate, and the bottom end of the mounting plate is fixedly connected with a mounting plate. In the upper mold, guide pipes are fitted and connected around the mounting plate respectively, and the guide pipes are movably sleeved with the surface of the guide rod. A material guide pipe is installed inside the upper mold, and the material guide pipe is connected with the There is a fixed connection between the pressure pumps.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述安装板通过导向管与导向杆之间构成活动结构,所述安装板通过液压杆与第二顶板之间构成升降结构。The mounting plate forms a movable structure between the guide pipe and the guide rod, and the mounting plate forms a lifting structure between the hydraulic rod and the second top plate.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述密封机构包括四个第二转动轴,所述第二转动轴与所述下模具两侧之间为固定连接,所述第二转动轴的另一侧转动连接有L型板,所述L型板的内部螺纹连接有手拧螺栓,所述手拧螺栓的一侧固定连接有压板,所述第一导管、第二导管的表面分别活动套接有密封胶圈,所述密封胶圈与所述压板之间活动连接。The sealing mechanism includes four second rotating shafts, the second rotating shafts are fixedly connected with both sides of the lower mold, and the other side of the second rotating shaft is rotatably connected with an L-shaped plate. The inner thread of the L-shaped plate is connected with a hand-tightening bolt, one side of the hand-tightening bolt is fixedly connected with a pressure plate, and the surfaces of the first conduit and the second conduit are respectively movably sleeved with a sealing rubber ring, and the sealing rubber ring Actively connected with the pressing plate.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述密封胶圈通过压板与下模具之间构成固定结构,所述压板通过所述手拧螺栓与所述L型板构成伸缩结构,所述L型板通过第二转动轴与下模具之间构成旋转结构。The sealing rubber ring forms a fixed structure between the pressing plate and the lower mold, the pressing plate forms a telescopic structure through the hand-tightening bolts and the L-shaped plate, and the L-shaped plate passes between the second rotating shaft and the lower mold. form a rotating structure.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述过滤机构包括两个滑槽,所述滑槽分别与蓄水槽的内壁两侧之间为焊接连接,所述滑槽的内部套接插设有滑块,所述滑块的另一侧固定连接有过滤网,所述过滤网的顶端焊接连接有把手。The filter mechanism includes two chutes, the chutes are respectively welded to both sides of the inner wall of the water storage tank, and a sliding block is sleeved and inserted inside the sliding trough, and the other side of the sliding block is connected by welding. A filter screen is fixedly connected, and a handle is welded and connected to the top of the filter screen.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

所述过滤网与所述蓄水槽之间为活动连接,所述过滤网通过滑块与滑槽构成滑动结构。The filter screen and the water storage tank are movably connected, and the filter screen forms a sliding structure through the slider and the chute.

作为上述技术方案的进一步描述:As a further description of the above technical solution:

本发明还提出一种多孔轻质光催化材料的制备方法,应用如上所述的制备装置,包括发泡树脂的混料步骤、导模成型步骤以及冷却脱模步骤;:The present invention also proposes a method for preparing a porous light-weight photocatalytic material, using the above-mentioned preparation device, including a mixing step of the foamed resin, a guide mold forming step, and a cooling and demoulding step;

步骤一、取PU发泡树脂A料与PU发泡树脂B料各1L,取纳米光催化材料0.5~1g;Step 1, take 1L of PU foamed resin material A and 1L of PU foamed resin material B, and take 0.5-1g of nano-photocatalytic material;

步骤二、将纳米光催化材料与PU发泡树脂A料进行混合得到第一混合物,充分搅拌分散;Step 2, mixing the nano-photocatalytic material and the PU foamed resin material A to obtain the first mixture, fully stirring and dispersing;

步骤三、然后将第一混合物与PU发泡树脂B按照1∶1的体积比进行迅速混合搅拌得到第二混合物;Step 3, then the first mixture and PU foamed resin B are rapidly mixed and stirred in a volume ratio of 1:1 to obtain the second mixture;

所述导模成型的步骤为:The steps of the guide mould forming are:

步骤一、通过压力泵将混合好的第二混合物,从排料管泵出,再从导料管导入上模具;Step 1. The mixed second mixture is pumped out from the discharge pipe by the pressure pump, and then introduced into the upper mold from the guide pipe;

步骤二、通过液压杆带动着上模具向下移动,与下模具相连接,将原料导入成型腔内;Step 2: Drive the upper mold to move down through the hydraulic rod, connect with the lower mold, and introduce the raw material into the molding cavity;

步骤三、第二混合物进入到成型腔内之后,1~3min内开始发泡成型,待15~20min后发泡结束。Step 3: After the second mixture enters the molding cavity, the foaming molding starts within 1-3 minutes, and the foaming ends after 15-20 minutes.

所述冷却脱模步骤包括:The cooling and demoulding step includes:

步骤一、通过潜水泵将蓄水槽内的冷却水泵到通水槽;Step 1. Pump the cooling water pump in the water storage tank to the water channel through the submersible pump;

步骤二、通过通水槽对成型腔进行加速冷却;Step 2: Accelerate the cooling of the molding cavity through the water channel;

步骤三、冷却水再通过第一导管(14)留回蓄水槽(15),成型腔(12)内温度降低后即可脱模得到目标产物。Step 3: The cooling water is then returned to the water storage tank (15) through the first conduit (14), and the target product can be obtained by demoulding after the temperature in the molding cavity (12) is lowered.

综上所述,由于采用了上述技术方案,本发明的有益效果是:To sum up, due to the adoption of the above-mentioned technical solutions, the beneficial effects of the present invention are:

1、本发明中,通过潜水泵可将冷却水泵入通水槽,通过通水槽可以对成型腔内的成型模具进行快速降温,改变以往自然冷却的情况,提高了多孔轻质光催化材料的成型速度,加快了生产效率;此外,通过第一导管可将冷却水导回蓄水槽,对冷却用水循环利用,降低了用水成本,节约了用水资源。1. In the present invention, the cooling water can be pumped into the water channel through the submersible pump, and the molding die in the molding cavity can be rapidly cooled by the water channel, which changes the natural cooling situation in the past and improves the molding speed of the porous light photocatalytic material. , the production efficiency is accelerated; in addition, the cooling water can be led back to the water storage tank through the first conduit, the cooling water can be recycled, the water cost is reduced, and the water resources are saved.

2、本发明中,在混料机构的作用下,通过电动机带动多个搅拌桨旋转,对搅拌罐内的纳米光催化材料与发泡树脂混合搅拌,并通过电动伸缩杆带动旋转的搅拌桨升降反复移动,提高了搅拌效率,使多个原料搅拌更为均匀,提高产品的质量。2. In the present invention, under the action of the mixing mechanism, a plurality of stirring paddles are driven to rotate by the motor, the nano-photocatalytic material and the foamed resin in the stirring tank are mixed and stirred, and the rotating stirring paddles are lifted and lowered by the electric telescopic rod. The repeated movement improves the stirring efficiency, makes the stirring of multiple raw materials more uniform, and improves the quality of the product.

3、本发明中,在锁模机构的作用下,通过液压杆带动安装板,使其通过导向管在导向杆的表面升降移动,进而带动上模具与下模具之间闭合锁模;通过液压杆的推动力,使得两个模具闭合得更为紧密,防止出现缝隙,造成原料溢出的情况,防止了飞边毛刺的出现。3. In the present invention, under the action of the clamping mechanism, the mounting plate is driven by the hydraulic rod to move up and down on the surface of the guide rod through the guide tube, thereby driving the upper mold and the lower mold to close the clamping; The driving force makes the two molds close more tightly, preventing the occurrence of gaps, causing the overflow of raw materials, and preventing the appearance of flash burrs.

4、本发明中,在密封机构的作用下,通过密封胶圈可以堵住密封第一导管、第二导管与通水槽的连接处,防止冷却水从连接处溢出堆积在装置的表面;通过转动手拧螺栓带动压板伸缩移动,通过压板可将密封胶圈夹紧固定,使其密封效果更佳。4. In the present invention, under the action of the sealing mechanism, the connection between the first conduit, the second conduit and the water channel can be blocked and sealed by the sealing rubber ring, so as to prevent the cooling water from overflowing from the connection and accumulating on the surface of the device; Screw the bolts by hand to drive the pressure plate to telescopically move, and the sealing rubber ring can be clamped and fixed by the pressure plate to make the sealing effect better.

5、本发明中,在过滤机构的作用下,通过过滤网可将第一导管引入蓄水槽的冷却水进行过滤,防止冷却水内含有残渣铁屑,造成潜水泵的堵塞;并防止残渣堆积在通水槽内,造成内部的堵塞导致冷却水无法通过的情况,且通过拉动把手,可使得过滤网通过滑块在滑槽内滑动,进而便于过滤网的拆卸与安装。5. In the present invention, under the action of the filter mechanism, the cooling water introduced by the first conduit into the water storage tank can be filtered through the filter screen, so as to prevent the cooling water from containing residual iron filings and cause blockage of the submersible pump; In the water channel, the internal blockage causes the cooling water to not pass through, and by pulling the handle, the filter screen can slide in the chute through the slider, thereby facilitating the removal and installation of the filter screen.

本公开的其他特征和优点将在随后的说明书中阐述,或者,部分特征和优点可以从说明书推知或毫无疑义地确定,或者通过实施本公开的上述技术即可得知。Additional features and advantages of the present disclosure will be set forth in the description that follows, or some may be inferred or unambiguously determined from the description, or may be learned by practicing the above-described techniques of the present disclosure.

为使本发明的上述目的、特征和优点能更明显易懂,下文特举较佳实施例,并配合所附附图,作详细说明如下。In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, preferred embodiments are given below, and are described in detail as follows in conjunction with the accompanying drawings.

附图说明Description of drawings

图1为本发明提出的多孔轻质光催化材料的制备装置的整体结构示意图;Fig. 1 is the overall structure schematic diagram of the preparation device of porous light-weight photocatalytic material proposed by the present invention;

图2为本发明提出的多孔轻质光催化材料的制备装置中蓄水槽的内部结构示意图;FIG. 2 is a schematic diagram of the internal structure of a water storage tank in the preparation device of the porous light photocatalytic material proposed by the present invention;

图3为本发明提出的多孔轻质光催化材料的制备装置中下模具的内部俯视结构示意图;3 is a schematic view of the internal top-view structure of the lower mold in the preparation device of the porous light photocatalytic material proposed by the present invention;

图4为本发明提出的多孔轻质光催化材料的制备装置中混料机构的结构示意图;4 is a schematic structural diagram of a mixing mechanism in the device for preparing the porous light photocatalytic material proposed by the present invention;

图5为本发明提出的多孔轻质光催化材料的制备装置中锁模机构的结构示意图;FIG. 5 is a schematic structural diagram of the clamping mechanism in the device for preparing the porous light-weight photocatalytic material proposed by the present invention;

图6为图3中“A”部分的结构示意图;Fig. 6 is the structural representation of "A" part in Fig. 3;

图7为本发明提出的多孔轻质光催化材料的制备装置中过滤机构侧视的结构示意图。FIG. 7 is a schematic structural diagram of the side view of the filtering mechanism in the preparation device of the porous light photocatalytic material proposed by the present invention.

主要符号说明:Description of main symbols:

搅拌罐Mixing tank 11 第一转动轴first rotation axis 20032003 支撑柱support column 22 转杆Rod 20042004 进料管feed pipe 33 搅拌桨mixer 20052005 测量尺measuring ruler 44 电动机electric motor 20062006 承载板carrier plate 55 锁模机构Clamping mechanism 21twenty one 支撑杆support rod 66 液压杆Hydraulic rod 21012101 第一顶板first top plate 77 安装板mounting plate 21022102 排料管Discharge pipe 88 上模具upper mold 21032103 压力泵pressure pump 99 导向管guide tube 21042104 工作台workbench 1010 导料管guide tube 21052105 下模具Lower die 1111 密封机构sealing mechanism 22twenty two 成型腔Molding cavity 1212 第二转动轴second rotating shaft 22012201 通水槽Sink 1313 L型板L-shaped plate 22022202 第一导管first catheter 1414 手拧螺栓hand screw 22032203 蓄水槽cistern 1515 压板platen 22042204 潜水泵submersible pump 1616 密封胶圈Gasket 22052205 第二导管second conduit 1717 过滤机构filter mechanism 23twenty three 导向杆guide rod 1818 滑槽Chute 23012301 第二顶板second top plate 1919 滑块slider 23022302 混料机构Mixing mechanism 2020 过滤网Filter 23032303 电动伸缩杆Electric telescopic pole 20012001 把手handle 23042304 第一托板first pallet 20022002

具体实施方式Detailed ways

为了便于理解本发明,下面将参照相关附图对本发明进行更全面的描述。附图中给出了本发明的首选实施例。但是,本发明可以以许多不同的形式来实现,并不限于本文所描述的实施例。相反地,提供这些实施例的目的是使对本发明的公开内容更加透彻全面。In order to facilitate understanding of the present invention, the present invention will be described more fully hereinafter with reference to the related drawings. Preferred embodiments of the invention are shown in the accompanying drawings. However, the present invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.

除非另有定义,本文所使用的所有的技术和科学术语与属于本发明的技术领域的技术人员通常理解的含义相同。本文中在本发明的说明书中所使用的术语只是为了描述具体的实施例的目的,不是旨在于限制本发明。本文所使用的术语“及/或”包括一个或多个相关的所列项目的任意的和所有的组合。Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terms used herein in the description of the present invention are for the purpose of describing specific embodiments only, and are not intended to limit the present invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.

现有的多孔轻质光催化材料的制备装置,在其使用过程中,发泡成型后,通常通过自然风冷,来对成型件降温,等待降温后再进行脱模作业,使得加工效率变慢,且现有的装置不具备快速混料的功能。In the existing preparation device of porous light photocatalytic material, during its use, after foaming molding, the molded part is usually cooled by natural air cooling, and then demoulding operation is performed after cooling down, so that the processing efficiency is slowed down , and the existing device does not have the function of rapid mixing.

为了解决这一技术问题,本发明提出一种多孔轻质光催化材料的制备装置,请参阅图1至图7,本发明提出的多孔轻质光催化材料的制备装置,包括搅拌罐1,搅拌罐1的底端固定连接有支撑柱2,搅拌罐1的一侧嵌合连接有进料管3,进料管3的表面嵌合连接有测量尺4。In order to solve this technical problem, the present invention proposes a preparation device for porous light photocatalytic material, please refer to FIG. 1 to FIG. 7 , the preparation device for porous light photocatalytic material proposed by the present A support column 2 is fixedly connected to the bottom end of the tank 1 , a feed pipe 3 is fitted and connected to one side of the stirring tank 1 , and a measuring ruler 4 is fitted and connected to the surface of the feed pipe 3 .

进料管3的顶端两侧焊接连接有承载板5,承载板5的顶端焊接连接有支撑杆6,支撑杆6的顶端固定连接有第一顶板7,第一顶板7底端安装有混料机构20。搅拌罐1的底端嵌合连接有排料管8,排料管8的另一端固定连接有压力泵9,压力泵9的一侧连接有工作台10。Both sides of the top of the feeding pipe 3 are welded and connected with a bearing plate 5, the top of the bearing plate 5 is welded and connected with a support rod 6, the top of the support rod 6 is fixedly connected with a first top plate 7, and the bottom end of the first top plate 7 is installed with a mixing material. Agency 20. A discharge pipe 8 is fitted and connected to the bottom end of the stirring tank 1 , a pressure pump 9 is fixedly connected to the other end of the discharge pipe 8 , and a workbench 10 is connected to one side of the pressure pump 9 .

工作台10的顶端固定连接有下模具11,下模具11的顶端开设有成型腔12。在下模具11的内部开设有通水槽13,通水槽13的一侧活动套接有第一导管14。在通水槽13的另一侧活动套接有第二导管17,工作台10的下端活动连接有蓄水槽15,在蓄水槽15的内部一侧活动连接有潜水泵16。A lower mold 11 is fixedly connected to the top of the worktable 10 , and a molding cavity 12 is opened at the top of the lower mold 11 . A water passage 13 is opened inside the lower mold 11 , and a first conduit 14 is movably sleeved on one side of the water passage 13 . A second conduit 17 is movably sleeved on the other side of the water passage 13 , a water storage tank 15 is movably connected to the lower end of the worktable 10 , and a submersible pump 16 is movably connected to the inner side of the water storage tank 15 .

其中,潜水泵16与第二导管17的输入端固定连接,通水槽13两侧分别与第一导管14、第二导管17之间安装有密封机构22。此外,工作台10的顶端固定连接有四个导向杆18,导向杆18的顶端焊接连接有第二顶板19,第二顶板19的底端安装有锁模机构21。The submersible pump 16 is fixedly connected to the input end of the second conduit 17 , and a sealing mechanism 22 is installed between the two sides of the water passage 13 and the first conduit 14 and the second conduit 17 respectively. In addition, four guide rods 18 are fixedly connected to the top of the worktable 10 , the top of the guide rods 18 are welded to the second top plate 19 , and the bottom end of the second top plate 19 is installed with a clamping mechanism 21 .

与此同时,在通水槽13内部安装有过滤机构23,进料管3与搅拌罐1之间安装有控制阀,可以打开使得进料管3内的原料进入搅拌罐1。通过表面预设的测量尺4,可以测量进料管3内原料的量。此外,潜水泵16以及压力泵9通过连接线接有外接电源,压力泵9将搅拌罐1内混合好的原料以从排料管8泵出,再从导料管2105导入上模具2103,潜水泵16将蓄水槽15内的冷却水泵到通水槽13内,通过通水槽13对成型腔12快速散热。At the same time, a filter mechanism 23 is installed inside the water channel 13 , and a control valve is installed between the feeding pipe 3 and the stirring tank 1 , which can be opened to allow the raw materials in the feeding pipe 3 to enter the stirring tank 1 . The amount of raw material in the feeding pipe 3 can be measured by the measuring ruler 4 preset on the surface. In addition, the submersible pump 16 and the pressure pump 9 are connected with an external power supply through the connecting line, and the pressure pump 9 pumps the mixed raw materials in the mixing tank 1 from the discharge pipe 8, and then introduces the upper mold 2103 from the material guide pipe 2105, submersible The pump 16 pumps the cooling water in the water storage tank 15 to the water passage 13 , and rapidly dissipates heat to the molding cavity 12 through the water passage 13 .

混料机构20包括两个电动伸缩杆2001,电动伸缩杆2001与第一顶板7的底端之间为固定连接。电动伸缩杆2001的底端固定连接有第一托板2002,第一托板2002的底端固定连接有第一转动轴2003。第一转动轴2003的底端转动连接有转杆2004,在转杆2004的表面等距焊接有多个搅拌桨2005。第一托板2002的顶端嵌合连接有电动机2006,电动机2006穿过第一托板2002与第一转动轴2003固定连接。电动机2006通过连接线接有外接电源,可带动搅拌桨2005对搅拌罐1内的发泡树脂与纳米光催化材料进行混合搅拌。The mixing mechanism 20 includes two electric telescopic rods 2001 , and the electric telescopic rods 2001 are fixedly connected with the bottom end of the first top plate 7 . A first supporting plate 2002 is fixedly connected to the bottom end of the electric telescopic rod 2001 , and a first rotating shaft 2003 is fixedly connected to the bottom end of the first supporting plate 2002 . A rotating rod 2004 is rotatably connected to the bottom end of the first rotating shaft 2003 , and a plurality of stirring paddles 2005 are welded equidistantly on the surface of the rotating rod 2004 . A motor 2006 is fitted and connected to the top of the first supporting plate 2002 , and the motor 2006 is fixedly connected to the first rotating shaft 2003 through the first supporting plate 2002 . The motor 2006 is connected to an external power source through a connecting wire, and can drive the stirring paddle 2005 to mix and stir the foamed resin and the nano-photocatalytic material in the stirring tank 1 .

在本实施例中,搅拌桨2005通过转杆2004、第一转动轴2003与电动机2006之间构成传动结构,第一托板2002通过电动伸缩杆2001与第一顶板7之间构成升降结构,电动伸缩杆2001可以带动着转动的搅拌桨2005升降往复移动。In this embodiment, the stirring paddle 2005 forms a transmission structure through the rotating rod 2004, the first rotating shaft 2003 and the motor 2006, the first support plate 2002 forms a lifting structure through the electric telescopic rod 2001 and the first top plate 7, and the electric The telescopic rod 2001 can drive the rotating stirring paddle 2005 to lift and reciprocate.

锁模机构21包括两个液压杆2101,液压杆2101与第二顶板19的顶端之间为固定连接。液压杆2101的底端固定连接有安装板2102,安装板2102的底端固定连接有上模具2103。安装板2102的四周分别嵌合连接有导向管2104,导向管2104与导向杆18的表面活动套接。在上模具2103的内部安装有导料管2105,导料管2105与压力泵9之间为固定连接。液压杆2101推动着安装板2102,可使得上模具2103向下移动,与下模具11重合。The clamping mechanism 21 includes two hydraulic rods 2101 , and the hydraulic rods 2101 are fixedly connected with the top end of the second top plate 19 . A mounting plate 2102 is fixedly connected to the bottom end of the hydraulic rod 2101 , and an upper mold 2103 is fixedly connected to the bottom end of the mounting plate 2102 . Guide tubes 2104 are fitted and connected around the mounting plate 2102 respectively, and the guide tubes 2104 are movably sleeved with the surface of the guide rod 18 . A material guide pipe 2105 is installed inside the upper mold 2103 , and the material guide pipe 2105 and the pressure pump 9 are fixedly connected. The hydraulic rod 2101 pushes the mounting plate 2102 , which can make the upper mold 2103 move downward and overlap with the lower mold 11 .

在本实施例中,安装板2102通过导向管2104与导向杆18之间构成活动结构,安装板2102通过液压杆2101与第二顶板19之间构成升降结构。可以理解的,通过液压杆2101,可使得两个模具紧密贴合。In this embodiment, the mounting plate 2102 forms a movable structure between the guide tube 2104 and the guide rod 18 , and the mounting plate 2102 forms a lifting structure between the hydraulic rod 2101 and the second top plate 19 . It can be understood that the hydraulic rod 2101 can make the two molds closely fit.

密封机构22包括四个第二转动轴2201,第二转动轴2201分别与下模具11两侧之间为固定连接。第二转动轴2201的另一侧转动连接有L型板2202,L型板2202的内部螺纹连接有手拧螺栓2203。此外,手拧螺栓2203的一侧固定连接有压板2204,第一导管14、第二导管17的表面分别活动套接有密封胶圈2205。在本实施例中,密封胶圈2205与压板2204之间活动连接,密封胶圈2205可以堵住密封第一导管14、第二导管17与通水槽13的连接处。The sealing mechanism 22 includes four second rotating shafts 2201 , and the second rotating shafts 2201 are fixedly connected to two sides of the lower mold 11 respectively. The other side of the second rotating shaft 2201 is rotatably connected with an L-shaped plate 2202 , and the interior of the L-shaped plate 2202 is threadedly connected with a hand-tightening bolt 2203 . In addition, a pressing plate 2204 is fixedly connected to one side of the hand-tightening bolt 2203, and a sealing rubber ring 2205 is movably sleeved on the surfaces of the first conduit 14 and the second conduit 17 respectively. In this embodiment, the sealing rubber ring 2205 and the pressing plate 2204 are movably connected, and the sealing rubber ring 2205 can block and seal the connection between the first conduit 14 , the second conduit 17 and the water passage 13 .

密封胶圈2205通过压板2204与下模具11之间构成固定结构,压板2204通过手拧螺栓2203与L型板2202构成伸缩结构。在本实施例中,L型板2202通过第二转动轴2201与下模具11之间构成旋转结构。通过转动手拧螺栓2203,手拧螺栓2203在L型板2202内伸缩移动,使得压板2204将密封胶圈2205夹紧固定。The sealing rubber ring 2205 forms a fixed structure between the pressing plate 2204 and the lower mold 11 , and the pressing plate 2204 forms a telescopic structure through the hand-tightening bolts 2203 and the L-shaped plate 2202 . In this embodiment, the L-shaped plate 2202 forms a rotating structure between the second rotating shaft 2201 and the lower mold 11 . By rotating the hand screw 2203, the hand screw 2203 telescopically moves in the L-shaped plate 2202, so that the pressing plate 2204 clamps and fixes the sealing rubber ring 2205.

过滤机构23包括两个滑槽2301,滑槽2301分别与蓄水槽15的内壁两侧之间为焊接连接。滑槽2301的内部套接插设有滑块2302,滑块2302的另一侧固定连接有过滤网2303。此外,在过滤网2303的顶端焊接连接有把手2304。可以理解的,过滤网2303可将第一导管14引入蓄水槽15的冷却水进行过滤。The filtering mechanism 23 includes two chutes 2301 , and the chutes 2301 are respectively connected with two sides of the inner wall of the water storage tank 15 by welding. A sliding block 2302 is sleeved and inserted inside the chute 2301 , and a filter screen 2303 is fixedly connected to the other side of the sliding block 2302 . In addition, a handle 2304 is welded and connected to the top end of the filter screen 2303 . It can be understood that the filter screen 2303 can filter the cooling water introduced into the water storage tank 15 by the first conduit 14 .

过滤网2303与蓄水槽15之间为活动连接,过滤网2303通过滑块2302与滑槽2301构成滑动结构。在实际应用中,通过拉动把手2304,可便于过滤网2303的安装与拆卸。The filter screen 2303 and the water storage tank 15 are movably connected, and the filter screen 2303 forms a sliding structure through the slider 2302 and the chute 2301 . In practical applications, by pulling the handle 2304, the installation and removal of the filter screen 2303 can be facilitated.

本发明还提出一种多孔轻质光催化材料的制备方法,包括有发泡树脂的混料、导模成型和冷却脱模,其中,发泡树脂的混料的步骤为:The present invention also proposes a method for preparing a porous light-weight photocatalytic material, which includes the mixing of foamed resin, guide molding and cooling and demoulding, wherein the steps of mixing the foamed resin are:

步骤一、取PU发泡树脂A料与PU发泡树脂B料各1L,取纳米光催化材料0.5~1g;Step 1, take 1L of PU foamed resin material A and 1L of PU foamed resin material B, and take 0.5-1g of nano-photocatalytic material;

步骤二、将纳米光催化材料与PU发泡树脂A料进行混合得到第一混合物,充分搅拌分散;Step 2, mixing the nano-photocatalytic material and the PU foamed resin material A to obtain the first mixture, fully stirring and dispersing;

步骤三、然后将第一混合物与PU发泡树脂B按照1∶1的体积比进行迅速混合搅拌得到第二混合物;Step 3, then the first mixture and PU foamed resin B are rapidly mixed and stirred in a volume ratio of 1:1 to obtain the second mixture;

导模成型的步骤为:The steps of guide molding are:

步骤一、通过压力泵9将混合好的第二混合物,从排料管8泵出,再从导料管2105导入上模具2103;Step 1. The mixed second mixture is pumped out from the discharge pipe 8 through the pressure pump 9, and then introduced into the upper mold 2103 from the material guide pipe 2105;

步骤二、通过液压杆2101带动着上模具2103向下移动,与下模具11相连接,将原料导入成型腔12内;Step 2, the upper mold 2103 is driven downward by the hydraulic rod 2101, connected with the lower mold 11, and the raw material is introduced into the molding cavity 12;

步骤三、第二混合物进入到成型腔12内之后,1~3min内开始发泡成型,待15~20min后发泡结束;Step 3: After the second mixture enters the molding cavity 12, foaming starts within 1 to 3 minutes, and the foaming ends after 15 to 20 minutes;

冷却脱模的步骤为:The steps of cooling and demoulding are:

步骤一、通过潜水泵16将蓄水槽15内的冷却水泵到通水槽13;Step 1. Pump the cooling water in the water storage tank 15 to the water passage tank 13 through the submersible pump 16;

步骤二、通过通水槽13对成型腔12进行加速冷却;Step 2: Accelerate the cooling of the molding cavity 12 through the water channel 13;

步骤三、冷却水再通过第一导管14留回蓄水槽15,成型腔12内温度降低后即可脱模得到目标产物。Step 3: The cooling water is then returned to the water storage tank 15 through the first conduit 14, and the target product can be obtained by demoulding after the temperature in the molding cavity 12 is lowered.

工作原理:working principle:

使用时,首先取PU发泡树脂A料与PU发泡树脂B料各1L,纳米光催化材料(纳米TiO2)0.5~1g,将PU发泡树脂A料与纳米光催化材料放入进料管3,通过进料管3表面嵌合的测量尺4,观察放入原料的计量,通过进料管3将原料导入搅拌罐1内;When in use, firstly take 1L each of PU foamed resin material A and PU foamed resin material B, and 0.5-1 g of nano-photocatalytic material (nano TiO 2 ), and put PU foamed resin material A and nano-photocatalytic material into the feed. Pipe 3, through the measuring ruler 4 fitted on the surface of the feeding pipe 3, observe the metering of the raw material, and introduce the raw material into the stirring tank 1 through the feeding pipe 3;

接通电动机2006的外接电源,电动机2006带动着转杆2004转动,转杆2004带动着表面的搅拌桨2005转动;搅拌桨2005对搅拌罐1内的发泡树脂与纳米光催化材料进行混合搅拌,第一混合物与PU发泡树脂B按照1:1的体积比进行迅速混合搅拌得到第二混合物;The external power supply of the motor 2006 is turned on, the motor 2006 drives the rotating rod 2004 to rotate, and the rotating rod 2004 drives the stirring paddle 2005 on the surface to rotate; the stirring paddle 2005 mixes the foamed resin and the nano-photocatalytic material in the stirring tank 1, The first mixture and the PU foamed resin B are rapidly mixed and stirred in a volume ratio of 1:1 to obtain the second mixture;

接通压力泵9的外接电源,通过压力泵9将搅拌罐1内混合好的第二混合物,从排料管8泵出;再从导料管2105导入上模具2103,通过液压杆2101推动着安装板2102,安装板2102四周的导向管2104在导向杆18的表面向下移动;安装板2102带动着上模具2103向下移动,上模具2103与下模具11相连接,将上模具2103内的原料导入成型腔12内;The external power supply of the pressure pump 9 is turned on, and the second mixture mixed in the mixing tank 1 is pumped out from the discharge pipe 8 through the pressure pump 9; Mounting plate 2102, the guide tube 2104 around the mounting plate 2102 moves downward on the surface of the guide rod 18; the mounting plate 2102 drives the upper mold 2103 to move downward, the upper The raw material is introduced into the molding cavity 12;

导入成型腔12内之后约1~3min内开始发泡成型,期间伴随少量发热,待15~20min后发泡结束;接通潜水泵16的外接电源,通过潜水泵16将蓄水槽15内的冷却水泵到第二导管17内,通过第二导管17将冷却水导入通水槽13内;通过通水槽13对成型腔12快速散热,冷却水再通过第一导管14导回蓄水槽15,形成水循环利用;After being introduced into the molding cavity 12, foaming begins within about 1 to 3 minutes, accompanied by a small amount of heat during the period, and the foaming is completed after 15 to 20 minutes; The water is pumped into the second conduit 17, and the cooling water is introduced into the water passage 13 through the second conduit 17; the molding cavity 12 is rapidly dissipated through the water passage 13, and the cooling water is led back to the water storage tank 15 through the first conduit 14 to form a water cycle. ;

通过蓄水槽15内安装的过滤网2303,将第一导管14引入蓄水槽15的冷却水进行过滤,再送到潜水泵16旁;手动拉动把手2304,把手2304带动过滤网2303使其两侧的滑块2302在滑槽2301内滑动,过滤网2303从蓄水槽15内抽出,从而拆卸过滤网2303,反之便可进行安装;Through the filter screen 2303 installed in the water storage tank 15, the cooling water introduced by the first conduit 14 into the water storage tank 15 is filtered, and then sent to the side of the submersible pump 16; manually pull the handle 2304, and the handle 2304 drives the filter screen 2303 to make it slide on both sides. The block 2302 slides in the chute 2301, and the filter screen 2303 is pulled out from the water storage tank 15, so that the filter screen 2303 can be disassembled, and vice versa can be installed;

通过密封胶圈2205,可堵住密封第一导管14、第二导管17与通水槽13的连接处;手动转动L型板2202,L型板2202通过第二转动轴2201转动,带动着压板2204移动至密封胶圈2205表面,再转动手拧螺栓2203,手拧螺栓2203在L型板2202内伸缩移动,带动着压板2204伸缩移动,通过压板2204将密封胶圈2205夹紧固定。Through the sealing rubber ring 2205, the connection between the first conduit 14, the second conduit 17 and the water passage 13 can be blocked; manually rotate the L-shaped plate 2202, and the L-shaped plate 2202 rotates through the second rotating shaft 2201 to drive the pressing plate 2204. Move to the surface of the sealing rubber ring 2205, and then turn the hand-tightening bolt 2203, the hand-tightening bolt 2203 telescopically moves in the L-shaped plate 2202, and drives the pressing plate 2204 to telescopically move, and the sealing rubber ring 2205 is clamped and fixed by the pressing plate 2204.

最后应说明的是:以上所述实施例,仅为本发明的具体实施方式,用以说明本发明的技术方案,而非对其限制,本发明的保护范围并不局限于此,尽管参照前述实施例对本发明进行了详细的说明,本领域的普通技术人员应当理解:任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,其依然可以对前述实施例所记载的技术方案进行修改或可轻易想到变化,或者对其中部分技术特征进行等同替换;而这些修改、变化或者替换,并不使相应技术方案的本质脱离本发明实施例技术方案的精神和范围,都应涵盖在本发明的保护范围之内。因此,本发明的保护范围应以所述权利要求的保护范围为准。Finally, it should be noted that the above-mentioned embodiments are only specific implementations of the present invention, and are used to illustrate the technical solutions of the present invention, but not to limit them. The protection scope of the present invention is not limited thereto, although referring to the foregoing The embodiment has been described in detail the present invention, those of ordinary skill in the art should understand: any person skilled in the art who is familiar with the technical field within the technical scope disclosed by the present invention can still modify the technical solutions described in the foregoing embodiments. Or can easily think of changes, or equivalently replace some of the technical features; and these modifications, changes or replacements do not make the essence of the corresponding technical solutions deviate from the spirit and scope of the technical solutions of the embodiments of the present invention, and should be covered in the present invention. within the scope of protection. Therefore, the protection scope of the present invention should be based on the protection scope of the claims.

Claims (10)

1.一种多孔轻质光催化材料的制备装置,包括搅拌罐(1),其特征在于,所述搅拌罐(1)的底端固定连接有支撑柱(2),在所述搅拌罐(1)的一侧嵌合连接有进料管(3),在所述进料管(3)的表面嵌合连接有测量尺(4),所述进料管(3)的顶端两侧焊接连接有承载板(5),所述承载板(5)的顶端焊接连接有支撑杆(6),所述支撑杆(6)的顶端固定连接有第一顶板(7),所述第一顶板(7)的底端安装有混料机构(20),所述搅拌罐(1)的底端嵌合连接有排料管(8),所述排料管(8)的另一端固定连接有压力泵(9),所述压力泵(9)的一侧连接有工作台(10);1. A preparation device for a porous light photocatalytic material, comprising a stirring tank (1), characterized in that the bottom end of the stirring tank (1) is fixedly connected with a support column (2), and a support column (2) is fixedly connected to the bottom end of the stirring tank (1). One side of 1) is fitted and connected with a feeding pipe (3), a measuring ruler (4) is fitted and connected on the surface of the feeding pipe (3), and both sides of the top of the feeding pipe (3) are welded A bearing plate (5) is connected, the top of the bearing plate (5) is welded with a support rod (6), and the top of the support rod (6) is fixedly connected with a first top plate (7), the first top plate A mixing mechanism (20) is installed at the bottom end of (7), a discharge pipe (8) is fitted and connected to the bottom end of the stirring tank (1), and the other end of the discharge pipe (8) is fixedly connected with a a pressure pump (9), a workbench (10) is connected to one side of the pressure pump (9); 所述工作台(10)的顶端固定连接有下模具(11),所述下模具(11)的顶端开设有成型腔(12),所述下模具(11)的内部开设有通水槽(13),所述通水槽(13)的一侧活动套接有第一导管(14),所述通水槽(13)的另一侧活动套接有第二导管(17),所述工作台(10)的下端活动连接有蓄水槽(15),所述蓄水槽(15)的内部一侧活动连接有潜水泵(16),所述潜水泵(16)与所述第二导管(17)的输入端固定连接,所述通水槽(13)的两侧分别与所述第一导管(14)、所述第二导管(17)之间安装有密封机构(22),所述工作台(10)的顶端固定连接有四个导向杆(18),所述导向杆(18)的顶端焊接连接有第二顶板(19),所述第二顶板(19)的底端安装有锁模机构(21),所述通水槽(13)内部安装有过滤机构(23)。A lower mold (11) is fixedly connected to the top of the worktable (10), a molding cavity (12) is opened at the top of the lower mold (11), and a water channel (13) is opened inside the lower mold (11). ), a first conduit (14) is movably sleeved on one side of the water passage (13), and a second conduit (17) is movably sleeved on the other side of the water passage (13). 10) A water storage tank (15) is movably connected to the lower end of the water storage tank (15), and a submersible pump (16) is movably connected to the inner side of the water storage tank (15). The input end is fixedly connected, and a sealing mechanism (22) is installed between the two sides of the water passage (13) and the first conduit (14) and the second conduit (17) respectively, and the workbench (10) ) are fixedly connected with four guide rods (18) at the top of the guide rods (18), the top of the guide rods (18) are welded and connected with a second top plate (19), and the bottom end of the second top plate (19) is installed with a clamping mechanism ( 21), a filter mechanism (23) is installed inside the water channel (13). 2.根据权利要求1所述的多孔轻质光催化材料的制备装置,其特征在于,所述混料机构(20)包括两个电动伸缩杆(2001),所述电动伸缩杆(2001)与所述第一顶板(7)的底端之间为固定连接,所述电动伸缩杆(2001)的底端固定连接有第一托板(2002),所述第一托板(2002)的底端固定连接有第一转动轴(2003),所述第一转动轴(2003)的底端转动连接有转杆(2004),所述转杆(2004)的表面等距焊接有多个搅拌桨(2005),所述第一托板(2002)的顶端嵌合连接有电动机(2006),所述电动机(2006)穿过所述第一托板(2002)与所述第一转动轴(2003)固定连接。2 . The device for preparing porous light-weight photocatalytic material according to claim 1 , wherein the mixing mechanism ( 20 ) comprises two electric telescopic rods ( 2001 ), the electric telescopic rods ( 2001 ) and the The bottom ends of the first top plates (7) are fixedly connected, the bottom ends of the electric telescopic rods (2001) are fixedly connected with a first support plate (2002), and the bottom of the first support plate (2002) is fixedly connected. The end is fixedly connected with a first rotating shaft (2003), the bottom end of the first rotating shaft (2003) is rotatably connected with a rotating rod (2004), and the surface of the rotating rod (2004) is equidistantly welded with a plurality of stirring paddles (2005), a motor (2006) is fitted and connected to the top of the first support plate (2002), and the motor (2006) passes through the first support plate (2002) and the first rotating shaft (2003). ) fixed connection. 3.根据权利要求2所述的多孔轻质光催化材料的制备装置,其特征在于,所述搅拌桨(2005)通过所述转杆(2004)、所述第一转动轴(2003)与所述电动机(2006)之间构成传动结构,所述第一托板(2002)通过所述电动伸缩杆(2001)与所述第一顶板(7)之间构成升降结构。3. The device for preparing porous light photocatalytic material according to claim 2, wherein the stirring paddle (2005) passes through the rotating rod (2004), the first rotating shaft (2003) and the A transmission structure is formed between the electric motors (2006), and a lifting structure is formed between the first support plate (2002) through the electric telescopic rod (2001) and the first top plate (7). 4.根据权利要求1所述的多孔轻质光催化材料的制备装置,其特征在于,所述锁模机构(21)包括两个液压杆(2101),所述液压杆(2101)与所述第二顶板(19)的顶端之间为固定连接,所述液压杆(2101)的底端固定连接有安装板(2102),所述安装板(2102)的底端固定连接有上模具(2103),所述安装板(2102)的四周分别嵌合连接有导向管(2104),所述导向管(2104)与所述导向杆(18)的表面活动套接,所述上模具(2103)的内部安装有导料管(2105),所述导料管(2105)与所述压力泵(9)之间为固定连接。4. The device for preparing porous light-weight photocatalytic material according to claim 1, characterized in that, the clamping mechanism (21) comprises two hydraulic rods (2101), the hydraulic rods (2101) and the The top ends of the second top plate (19) are fixedly connected, the bottom end of the hydraulic rod (2101) is fixedly connected with a mounting plate (2102), and the bottom end of the mounting plate (2102) is fixedly connected with the upper mold (2103). ), a guide tube (2104) is fitted and connected around the mounting plate (2102), the guide tube (2104) is movably sleeved with the surface of the guide rod (18), and the upper die (2103) A material guide pipe (2105) is installed inside the pipe, and the material guide pipe (2105) and the pressure pump (9) are fixedly connected. 5.根据权利要求4所述的多孔轻质光催化材料的制备装置,其特征在于,所述安装板(2102)通过所述导向管(2104)与所述导向杆(18)之间构成活动结构,所述安装板(2102)通过所述液压杆(2101)与所述第二顶板(19)之间构成升降结构。5. The device for preparing porous light-weight photocatalytic material according to claim 4, characterized in that, the mounting plate (2102) constitutes a movement between the guide tube (2104) and the guide rod (18) structure, the mounting plate (2102) constitutes a lifting structure through between the hydraulic rod (2101) and the second top plate (19). 6.根据权利要求1所述的多孔轻质光催化材料的制备装置,其特征在于,所述密封机构(22)包括四个第二转动轴(2201),所述第二转动轴(2201)与所述下模具(11)的两侧之间为固定连接,所述第二转动轴(2201)的另一侧转动连接有L型板(2202),所述L型板(2202)的内部螺纹连接有手拧螺栓(2203),所述手拧螺栓(2203)的一侧固定连接有压板(2204),所述第一导管(14)、所述第二导管(17)的表面分别活动套接有密封胶圈(2205),所述密封胶圈(2205)与压板(2204)之间为活动连接。6. The device for preparing porous light-weight photocatalytic materials according to claim 1, wherein the sealing mechanism (22) comprises four second rotating shafts (2201), and the second rotating shafts (2201) It is fixedly connected with both sides of the lower mold (11), and the other side of the second rotating shaft (2201) is rotatably connected with an L-shaped plate (2202), and the interior of the L-shaped plate (2202) A hand-tightening bolt (2203) is threadedly connected, a pressure plate (2204) is fixedly connected to one side of the hand-tightening bolt (2203), and the surfaces of the first conduit (14) and the second conduit (17) are respectively movable A sealing rubber ring (2205) is sleeved, and the sealing rubber ring (2205) and the pressing plate (2204) are movably connected. 7.根据权利要求6所述的多孔轻质光催化材料的制备装置,其特征在于,所述密封胶圈(2205)通过所述压板(2204)与所述下模具(11)之间构成固定结构,所述压板(2204)通过所述手拧螺栓(2203)与所述L型板(2202)构成伸缩结构,所述L型板(2202)通过所述第二转动轴(2201)与所述下模具(11)之间构成旋转结构。7. The device for preparing porous light-weight photocatalytic material according to claim 6, wherein the sealing rubber ring (2205) is fixed between the pressing plate (2204) and the lower mold (11) structure, the pressing plate (2204) forms a telescopic structure with the L-shaped plate (2202) through the hand-tightening bolt (2203), and the L-shaped plate (2202) is connected to the A rotating structure is formed between the lower molds (11). 8.根据权利要求1所述的多孔轻质光催化材料的制备装置,其特征在于,所述过滤机构(23)包括两个滑槽(2301),所述滑槽(2301)与所述蓄水槽(15)的内壁两侧之间为焊接连接,所述滑槽(2301)的内部套接插设有滑块(2302),所述滑块(2302)的另一侧固定连接有过滤网(2303),所述过滤网(2303)的顶端焊接连接有把手(2304)。8. The device for preparing porous light-weight photocatalytic material according to claim 1, characterized in that, the filtering mechanism (23) comprises two chutes (2301), the chutes (2301) and the accumulator The two sides of the inner wall of the water tank (15) are welded and connected, the sliding groove (2301) is internally sleeved and inserted with a sliding block (2302), and the other side of the sliding block (2302) is fixedly connected with a filter screen (2303), a handle (2304) is welded and connected to the top of the filter screen (2303). 9.根据权利要求8所述的多孔轻质光催化材料的制备装置,其特征在于,所述过滤网(2303)与所述蓄水槽(15)之间为活动连接,所述过滤网(2303)通过所述滑块(2302)与所述滑槽(2301)之间构成滑动结构。9. The device for preparing porous light-weight photocatalytic materials according to claim 8, wherein the filter screen (2303) and the water storage tank (15) are movably connected, and the filter screen (2303) ) constitute a sliding structure between the slider (2302) and the chute (2301). 10.一种多孔轻质光催化材料的制备方法,其特征在于,应用如上述权利要求1至9任意一项所述的制备装置,包括发泡树脂的混料步骤、导模成型步骤以及冷却脱模步骤;10. A method for preparing a porous light-weight photocatalytic material, characterized in that, applying the preparation device according to any one of the above claims 1 to 9, comprising a mixing step of foamed resin, a guide molding step and cooling demoulding step; 其中,所述发泡树脂的混料步包括:Wherein, the mixing step of described foamed resin comprises: 步骤一、取PU发泡树脂A料与PU发泡树脂B料各1L,取纳米光催化材料0.5~1g;Step 1, take 1L of PU foamed resin material A and 1L of PU foamed resin material B, and take 0.5-1g of nano-photocatalytic material; 步骤二、将纳米光催化材料与PU发泡树脂A料进行混合得到第一混合物,充分搅拌分散;Step 2, mixing the nano-photocatalytic material and the PU foamed resin material A to obtain the first mixture, fully stirring and dispersing; 步骤三、然后将第一混合物与PU发泡树脂B按照1∶1的体积比进行迅速混合搅拌得到第二混合物;Step 3, then the first mixture and PU foamed resin B are rapidly mixed and stirred in a volume ratio of 1:1 to obtain the second mixture; 所述导模成型步骤包括:The guide molding step includes: 步骤一、通过压力泵(9)将混合好的第二混合物,从排料管(8)泵出,再从导料管(2105)导入上模具(2103);Step 1. The mixed second mixture is pumped out from the discharge pipe (8) through the pressure pump (9), and then introduced into the upper mold (2103) from the material guide pipe (2105); 步骤二、通过液压杆(2101)带动着上模具(2103)向下移动,与下模具(11)相连接,将原料导入成型腔(12)内;In step 2, the upper mold (2103) is driven downward by the hydraulic rod (2101) to be connected with the lower mold (11), and the raw material is introduced into the molding cavity (12); 步骤三、第二混合物进入到成型腔(12)内之后,1~3min内开始发泡成型,待15~20min后发泡结束;Step 3: After the second mixture enters the molding cavity (12), foaming starts within 1 to 3 minutes, and the foaming ends after 15 to 20 minutes; 所述冷却脱模步骤包括:The cooling and demoulding step includes: 步骤一、通过潜水泵(16)将蓄水槽(15)内的冷却水泵到通水槽(13);Step 1, pump the cooling water pump in the water storage tank (15) to the water channel (13) through the submersible pump (16); 步骤二、通过通水槽(13)对成型腔(12)进行加速冷却;Step 2: Accelerate cooling of the molding cavity (12) through the water channel (13); 步骤三、冷却水再通过第一导管(14)留回蓄水槽(15),成型腔(12)内温度降低后即可脱模得到目标产物。Step 3: The cooling water is then returned to the water storage tank (15) through the first conduit (14), and the target product can be obtained by demoulding after the temperature in the molding cavity (12) is lowered.
CN202010787117.4A 2020-08-07 2020-08-07 Preparation device and preparation method of porous light photocatalytic material Pending CN111890620A (en)

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