CN111621362A - Camellia essence for cigarette bead blasting, bead blasting prepared from camellia essence and cigarette - Google Patents

Abstract

The invention relates to a camellia essence for cigarette popping beads and the prepared popping beads and cigarettes, belonging to the technical field of cigarette flavors. The essence includes camellia extract, ethyl vanillin, oak moss extract, 2-methylbutyric acid, ethyl caprylate, 2-methylbutyric acid-2-phenethyl ester, 2, 3, 5 trimethyl Pyrazine, Orange Oil Terpenes, Phenethyl Acetate, Caprolactone, Phenethyl Alcohol, Isoamyl Acetate, Gemarene D, Linalool, Acetic Acid, 2-Amyl Alcohol, Palmitic Acid, Benzyl Benzoate, Ethyl isovalerate, damascenone, isovaleric acid, acetophenone, ethyl caprate and other components. The popping beads of the invention can improve the comfort of cigarette smoking, enhance the sweetness of cigarette smoking, reduce the stinging feeling in the cigarette smoke, reduce the tingling feeling on the tongue surface, and have good coordination between the floral aroma and the cigarette aroma, and has a relatively high quality. High application value and promotion significance.

Description

A kind of camellia essence for cigarette popping beads and its prepared popping beads and cigarette

technical field

The invention belongs to the technical field of flavors for cigarettes, in particular to a camellia flavor for cigarette popping beads and the popping beads and cigarettes prepared therefrom.

Background technique

The popping bead refers to a liquid incense bead embedded in the tobacco filter tip. It wraps the liquid of different types of spices. The smoker can squeeze it during the smoking process, so that the liquid in the bead flows out of the filter rod and into the smoke, so that the The taste of cigarettes is richer and more fragrant, so that smokers can get a more comfortable experience, which is one of the important means to enhance the flavor of cigarettes.

Yunnan province flower camellia, Camellia family, plants are evergreen shrubs and small trees. Existing cigarettes often have the characteristics of poor sweetness, poor sweetness, and high smoke irritation during smoking. Although popped bead cigarettes can improve the comfort of cigarettes, their contribution to the improvement is limited, and there is no camellia to do it. The popping beads, which are the main aroma characteristic raw materials, affect the application of camellia essence for popping beads in cigarettes to a certain extent.

How to overcome the deficiencies of the prior art and utilize the camellia aroma popped beads to enrich the sense of satisfaction and sweetness during the smoking process of cigarettes is a problem to be solved in the technical field of popped beads for cigarettes.

SUMMARY OF THE INVENTION

The purpose of the present invention is to solve the deficiencies of the prior art, and provide a camellia essence for cigarette popping beads and the popping beads and cigarettes prepared therefrom.

For achieving the above object, the technical scheme adopted in the present invention is as follows:

A first aspect of the present invention provides a camellia essence for cigarette popping beads, comprising the following components in parts by weight:

Camellia extract 4.50-12.50 parts; ethyl vanillin 0.50-2.50 parts; oakmoss extract 1.15-1.35 parts; 2-methylbutyric acid 0.05-1.55 parts; ethyl caprylate 0.55-0.95 parts; 2-methyl Butyric acid-2-phenethyl ester 0.35-0.85 part; 2, 3, 5 trimethylpyrazine 0.50-1.45 part; orange oil terpene 0.45-1.35 part; phenethyl acetate 0.15-1.25 part; caprolactone 0.35-0.65 part; 0.15-0.95 part of phenethyl alcohol; 0.50-1.05 part of isoamyl acetate; 0.10-0.25 part of gemmaene D; 0.10-0.25 part of linalool; 0.15-0.45 part of acetic acid; 0.30 part; palmitic acid 0.05-0.15 part; benzyl benzoate 0.05-0.15 part; ethyl isovalerate 0.50-1.45 part; damascenone 0.35-0.65 part; isovaleric acid 0.10-0.25 part; acetophenone 0.10- 0.30 part; 0.05-0.15 part of ethyl caprate; 0.05-1.15 part of ethyl heptanoate; 0.15-0.45 part of β-caryophyllene; 0.15-0.45 part of β-myrcene; 0.80-1.35 part of eugenol; Pinene 0.10-0.50 parts; phenylacetic acid 0.10-1.05 parts.

The preparation method of the camellia essence is obtained by directly mixing the above components physically until uniform.

A second aspect of the present invention provides a cigarette popping bead, wherein the content of the popping bead is the camellia essence for cigarette popping beads.

Further, it is preferred that the content of camellia essence for cigarette popping beads in the popping beads is 5-45 μL/granule.

Further, it is preferred that the diameter specification of the blasting beads is 2.0mm-4.5mm, and the crushing pressure of the blasting beads is 0.7kgf-1.7kgf.

A third aspect of the present invention provides a method for preparing the above-mentioned cigarette popping beads, comprising the following steps:

Step (1), preparation of emulsion: in parts by weight, 510-660 parts of caprylic glyceride, 1-3 parts of anhydrous calcium chloride, 0.5-1.5 parts of sodium carboxymethyl cellulose, cyclodextrin 0.05-1.00 part of essence, 2-5 parts of poloxamer and 220-260 parts of camellia essence are stirred together under the condition of 30-50 ℃ until they are evenly mixed to obtain an emulsion;

Step (2), preparation of the molding solution: in parts by weight, 90-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 parts of sorbitol, 0.1-0.3 parts of cyclodextrin and 0.1-0.5 parts of Wen-20 are stirred together under the condition of 15-45 ℃ until the mixing is uniform to obtain a molding liquid;

Step (3), setting the drop pills: the emulsion is uniformly dropped into the forming liquid, and after curing and forming, washing and air-drying are performed to obtain camellia popping beads.

Further, preferably, in step (1), the specific conditions for stirring are: stirring at a rotational speed of 40-80 r/min for 20-30 min.

Further, preferably, in step (2), the specific conditions for stirring are: stirring at a rotational speed of 40-80 r/min for 20-30 min.

Further, preferably, in step (3), the dropping speed is 5 drops/s.

Further, preferably, in step (3), the conditions for curing and forming are equilibrated at a temperature of 20° C. and a relative humidity of 60% RH for 24 hours.

The fourth aspect of the present invention provides a cigarette with popped beads prepared by the above-mentioned preparation method of popped cigarette beads, specifically: taking a popped cigarette bead and placing it in the center of the cigarette filter rod to provide a better smoking experience . For example, if the length of the filter rod is 25mm, the center of the cigarette bead is located at 12.5mm.

The beneficial effects of some of the materials used in the present invention are as follows:

1. Sodium alginate: the main raw material of the blasting bead wall material, cross-linked with calcium ions to form a film, the film has good irreversible moisture resistance;

2. Calcium chloride: increase the calcium ions required for film formation;

3. Cyclodextrin: filler, increase the concentration of solid solution;

4. Poloxamer: emulsifier, improve liquid surface activity;

5. Sorbitol: Toughening agent, with good moisturizing properties, can increase the toughness of the wall material;

6. Sodium carboxymethyl cellulose: thickener to improve liquid viscosity;

7. Tween-20: emulsifier, improve the surface tension of liquid;

8. Caprylic acid glyceride: used as essential oil to prepare emulsion.

The invention adopts the interface film-forming method to prepare the explosive beads, the principle of which is that the wall material glue and calcium ions will have a cross-linking reaction to form a tight film and realize the embedding of the core material essence. Mix and stir a certain proportion of water, essence, thickener, emulsifier and calcium ions to form an emulsion with certain fluidity, prepare a certain proportion of sodium alginate wall material glue, and drip the emulsion at a certain rate through the dripping equipment. In the sodium alginate solution, solidifying and forming, washing with water, drying and sieving to obtain explosive beads for cigarettes.

The preparation method of the camellia flower extract of the present invention is preferably obtained by supercritical carbon dioxide extraction, and the extraction conditions are: when the extraction flow rate: 22 g/min, the extraction pressure: 275 Bar, the extraction temperature: 43 ° C, and the extraction time: 1.5h; but Not limited to this method.

Compared with the prior art, the present invention has the following beneficial effects:

The invention applies the properties, taste and efficacy of camellia to the flavor of popping beads for cigarettes, and develops popping beads for cigarettes that can alleviate the uncomfortable feeling in the throat. The popping beads can improve the comfort of cigarette smoking and enhance the smoking sweetness of cigarettes. It can reduce the stinging feeling in cigarette smoke and the tingling feeling on the tongue surface.

The invention uses high-quality camellia flowers with Yunnan characteristics as raw materials, and combines with the blasting bead technology to provide a specific blasting bead essence-camellia essence. Applying it to cigarettes can create a tobacco brand with Yunnan characteristics.

The camellia essence for popping beads disclosed in the present invention can obtain the fragrance of the camellia essence through the combination of various raw materials. Since essential oil is not used as the raw material of the fragrance, the chemical composition and content of the camellia essence for popping beads disclosed in the present invention are fixed and are not subject to production. The influence of external factors such as conditions, storage environment, and manufacturer is conducive to ensuring the stability of the quality of camellia essence for popping beads.

Detailed ways

Various exemplary embodiments of the present invention will now be described in detail. It should be noted that the relative arrangement of components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the invention unless specifically stated otherwise.

The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses in any way.

Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail, but where appropriate, such techniques, methods, and apparatus should be considered part of the specification.

In all examples shown and discussed herein, any specific values should be construed as illustrative only and not limiting. Accordingly, other instances of the exemplary embodiment may have different values.

The experimental methods used in the following examples are conventional methods unless otherwise specified. The materials and reagents used can be obtained from commercial sources unless otherwise specified. The equipment used in the experiments are all available unless otherwise specified. Equipment well known to those skilled in the art.

Example 1

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 5.00 parts of camellia extract; 2.50 parts of ethyl vanillin; 1.35 parts of oak moss extract; Butyric acid 1.55 parts; ethyl octanoate 0.95 parts; 2-methylbutyric acid-2-phenylethyl ester 0.85 parts; 2, 3, 5 trimethylpyrazine 1.45 parts; orange oil terpene 1.35 parts; benzene acetate 1.25 parts of ethyl ester; 0.65 part of caprolactone; 0.55 part of phenethyl alcohol; 0.55 part of isoamyl acetate; 1.25 part of caprylactone; 0.25 part; palmitic acid 0.15 part; benzyl benzoate 0.15 part; ethyl isovalerate 1.45 part; damascenone 0.60 part isovaleric acid 0.25 part; acetophenone 0.30 part; ethyl caprate 0.15 part; ethyl heptanoate 1.05 part of ester; 0.45 part of β-caryophyllene; 0.45 part of β-myrcene; 0.45 part of phenethyl 2-furanoate; 1.35 part of eugenol;

Preparation of the emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 0.8 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and camellia 220 parts of essence were stirred together at 40° C. at a speed of 60 r/min for 25 minutes until the mixture was uniform to obtain an emulsion.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at 30°C at a rotating speed of 60r/min 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60% RH. Bead S1.

Put the camellia essence popped beads S1 into the cigarette filter rod, and then connect the cigarette samples to obtain the camellia popped beads cigarette C1.

Example 2

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 6.50 parts of camellia extract; 1.00 parts of ethyl vanillin; 1.20 parts of oak moss extract; 0.60 part of butyric acid; 0.65 part of ethyl octanoate; 0.45 part of 2-methylbutyric acid-2-phenylethyl ester; 0.75 part of 2, 3, and 5 trimethylpyrazine; 0.65 part of orange oil terpene; benzene acetate 0.35 part of ethyl ester; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of caprylactone; 0.15 part of gemene D; 0.15 part of linalool; 0.20 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; ethyl isovalerate 0.65 part; damascenone 0.45 part; isovaleric acid 0.15 part; acetophenone 0.20 part; 0.95 part of ethyl ester; 0.20 part of β-caryophyllene; 0.25 part of β-myrcene; 0.30 part of phenethyl 2-furanoate; 0.90 part of eugenol; 0.15 part of δ-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 550 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 240 parts of camellia essence are stirred together at 40-80 r/min for 20-30 minutes at 40° C. until the mixture is uniform, and an emulsion is obtained;

Preparation of molding liquid: in parts by weight, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were mixed together under the condition of 30 °C The rotating speed of 60r/min is stirred for 25min until the mixing is uniform, and the molding liquid is obtained;

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60% RH. Bead S2.

Put the camellia essence popping beads S2 into the cigarette filter rod, and then connect the cigarette samples to obtain the camellia popping beads cigarette C2.

Example 3

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 8.50 parts of camellia extract; 1.50 parts of ethyl vanillin; 1.25 parts of oak moss extract; 1.05 parts of butyric acid; 0.75 parts of ethyl octanoate; 0.65 parts of 2-methylbutyric acid-2-phenylethyl ester; 1.15 parts of 2, 3, 5 trimethylpyrazine; 1.05 parts of orange oil terpenes; benzene acetate 1.05 part of ethyl ester; 0.50 part of caprolactone; 0.75 part of phenethyl alcohol; 0.90 part of isoamyl acetate; 1.05 part of caprylactone; 0.20 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; ethyl isovalerate 1.05 part; damascenone 0.55 part; isovaleric acid 0.15 part; acetophenone 0.20 part; 0.05-0.95 part of ethyl ester; 0.35 part of β-caryophyllene; 0.35 part of β-myrcene; 0.40 part of phenylethyl 2-furanoate; 1.20 part of eugenol;

Preparation of emulsion: in parts by weight, 600 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3 parts of poloxamer and camellia 245 parts of the essence were stirred together at 40° C. at a rotating speed of 60 r/min for 25 minutes until the mixture was uniform, and an emulsion was obtained.

Preparation of molding liquid: in parts by weight, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were mixed together under the condition of 30 °C The rotating speed of 60r/min is stirred for 25min until the mixing is uniform, and the molding liquid is obtained;

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60% RH. Bead S3.

Put the camellia essence popping beads S3 into the cigarette filter rod, and then get the camellia popping beads cigarette C3 after receiving the cigarette samples.

Example 4

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 12 parts of camellia extract; 2.25 parts of ethyl vanillin; 1.25 parts of oak moss extract; 1.45 parts of butyric acid; 0.90 parts of ethyl octanoate; 0.80 parts of 2-methylbutyric acid-2-phenylethyl ester; 1.40 parts of 2, 3, 5 trimethylpyrazine; 1.30 parts of orange oil terpenes; benzene acetate 1.20 part of ethyl ester; 0.60 part of caprolactone; 0.90 part of phenethyl alcohol; 1.00 part of isoamyl acetate; 1.25 part of caprylactone; 0.25 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; ethyl isovalerate 1.40 part; damascenone 0.60 part; isovaleric acid 0.20 part; acetophenone 0.25 part; 1.10 parts of ethyl ester; 0.40 part of β-caryophyllene; 0.40 part of β-myrcene; 0.40 part of phenylethyl 2-furanoate; 1.30 part of eugenol; 0.45 part of δ-juniperene; 1.00 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 610 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3 parts of poloxamer and camellia flower 255 parts of essence were stirred together at 40° C. at a speed of 60 r/min for 25 minutes until the mixture was uniform to obtain an emulsion.

Preparation of molding liquid: in parts by weight, 95 parts of deionized water, 2 parts of sodium alginate, 0.8 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were mixed together under the condition of 30 °C The rotating speed of 60r/min is stirred for 25min until the mixing is uniform, and the molding liquid is obtained;

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60% RH. Bead S4.

The camellia flavor popped beads S4 were placed in the cigarette filter rod, and the camellia popped beads cigarette C4 was obtained after receiving the cigarette samples.

Example 5

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 4.50 parts of camellia extract; 0.50 parts of ethyl vanillin; 1.15 parts of oak moss extract; 0.05 part of butyric acid; 0.55 part of ethyl octanoate; 0.35 part of 2-methylbutyric acid-2-phenylethyl ester; 0.50 part of 2, 3, 5 trimethylpyrazine; 0.45 part of orange oil terpene; benzene acetate 0.15 part of ethyl ester; 0.35 part of caprolactone; 0.15 part of phenethyl alcohol; 0.50 part of isoamyl acetate; 0.10 part of gemmaene D; 0.10 part of linalool; 0.15 part of acetic acid; 0.10 part of 2-pentanol; 0.05 part of benzyl benzoate; 0.50 part of ethyl isovalerate; 0.35 part of damascone; 0.10 part of isovaleric acid; 0.10 part of acetophenone; 0.05 part of ethyl caprate; 0.05 part of ethyl heptanoate; - Caryophyllene 0.15 part; β-myrcene 0.15 part; Eugenol 0.80 part; δ-juniperene 0.10 part; phenylacetic acid 0.10 part.

Preparation of emulsion: in parts by weight, 510 parts of caprylic acid glyceride, 1 part of anhydrous calcium chloride, 0.5 part of sodium carboxymethyl cellulose, 0.05 part of cyclodextrin, 2 parts of poloxamer and 220 parts of camellia essence were mixed together under the condition of 30°C and stirred at a speed of 40r/min for 20min until the mixture was uniform to obtain an emulsion;

Preparation of molding liquid: in parts by weight, 90 parts of deionized water, 1 part of sodium alginate, 0.5 part of sorbitol, 0.1 part of cyclodextrin and 0.1 part of Tween-20 were mixed together under the condition of 15°C to The rotating speed of 40r/min is stirred for 20min until the mixing is uniform, and the molding liquid is obtained;

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 ° C and the relative humidity is 60% RH. Bead S11.

The camellia flavor popped beads S11 were put into the cigarette filter rod, and the camellia popped beads cigarette C11 was obtained after receiving the cigarette samples.

Example 6

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 12.50 parts of camellia extract; 2.50 parts of ethyl vanillin; 1.35 parts of oak moss extract; Butyric acid 1.55 parts; ethyl octanoate 0.95 parts; 2-methylbutyric acid-2-phenylethyl ester 0.85 parts; 2, 3, 5 trimethylpyrazine 1.45 parts; orange oil terpene 1.35 parts; benzene acetate 1.25 parts of ethyl ester; 0.65 part of caprolactone; 0.95 part of phenethyl alcohol; 1.05 part of isoamyl acetate; 0.25 part of gemmaene D; 0.25 part of linalool; 0.45 part of acetic acid; 0.15 part of benzyl benzoate; 1.45 part of ethyl isovalerate; 0.65 part of damascone; 0.25 part of isovaleric acid; 0.30 part of acetophenone; 0.15 part of ethyl decanoate; - Caryophyllene 0.45 parts; β-myrcene 0.45 parts; Eugenol 1.35 parts; δ-juniperene 0.50 parts; phenylacetic acid 1.05 parts.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 3 parts of anhydrous calcium chloride, 1.5 parts of sodium carboxymethyl cellulose, 1.00 parts of cyclodextrin, 5 parts of poloxamer and 260 parts of camellia essence were stirred together at a speed of 80 r/min for 30 min under the condition of 50 ° C until the mixture was uniform to obtain an emulsion;

Preparation of the molding solution: in parts by weight, 100 parts of deionized water, 3 parts of sodium alginate, 1.0 part of sorbitol, 0.3 part of cyclodextrin and 0.5 part of Tween-20 were mixed together under the condition of 45 ° C to The rotating speed of 80r/min is stirred for 30min until the mixing is uniform, and the molding liquid is obtained;

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 ° C and the relative humidity is 60% RH. Bead S12.

The camellia flavor popped beads S12 were put into the cigarette filter rod, and the camellia popped beads cigarette C12 was obtained after receiving the cigarette samples.

Comparative Example 1

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 1.00 part of ethyl vanillin; 1.20 part of oak moss extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl octanoate; 0.45 part of 2-methylbutyric acid-2-phenylethyl ester; 0.75 part of 2, 3, 5 trimethylpyrazine; 0.65 part of orange oil terpene; 0.35 part of phenethyl acetate; Lactone 0.45 part; Phenethyl alcohol 0.35 part; Isoamyl acetate 0.70 part; Caprylactone 0.80 part; Gemene D 0.15 part; Linalool 0.15 part; Acetic acid 0.30 part; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl caprate; 0.95 part of ethyl heptanoate; - Caryophyllene 0.20 part; β-myrcene 0.25 part; 2-furanoic acid phenethyl ester 0.30 part; eugenol 0.90 part; delta-juniperene 0.15 part; phenylacetic acid 0.30 part.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of camellia essence were mixed together under the condition of 40° C. at a rotating speed of 60 r/min for 25 minutes until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60%RH. S5.

Put the flavor S5 explosive beads into the cigarette filter rod, and then get the explosive beads cigarette C5 after receiving the cigarette samples.

Comparative Example 2

A camellia flower essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 6.50 parts of camellia extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl octanoate; 0.45 part of 2-phenylethyl butyrate; 0.75 part of 2, 3, 5 trimethylpyrazine; 0.65 part of orange oil terpene; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol 0.70 part of isoamyl acetate; 0.80 part of capryllactone; 0.15 part of gemmaene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-pentanol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; Ethyl isovalerate 0.65 parts; damascenone 0.45 parts; isovaleric acid 0.15 parts; acetophenone 0.20 parts; ethyl caprate 0.10 parts; ethyl heptanoate 0.95 parts; 0.25 part of alkene; 0.30 part of phenethyl 2-furancarboxylate; 0.90 part of eugenol; 0.15 part of delta-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of camellia essence were mixed together under the condition of 40° C. at a rotating speed of 60 r/min for 25 minutes until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60% RH. Bead S6.

The camellia essence S6 popped beads were put into the cigarette filter rod, and the camellia popped beads cigarette C6 was obtained after receiving the cigarette samples.

Comparative Example 3

A flavor for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 6.50 parts of rose flower extract; 0.60 part of 2-methylbutyric acid; 0.65 part of ethyl caprylate; 0.45 part of 2-phenylethyl butyrate; 0.75 part of 2, 3, 5 trimethylpyrazine; 0.65 part of orange oil terpene; 0.35 part of phenethyl acetate; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol 0.70 part of isoamyl acetate; 0.80 part of caprolactone; 0.15 part of gemmaene D; 0.15 part of linalool; 0.30 part of acetic acid; 0.20 part of 2-pentanol; 0.10 part of palmitic acid; 0.10 part of benzyl benzoate; 0.65 part of ethyl isovalerate; 0.45 part of damascenone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl caprate; 0.95 part of ethyl heptanoate; 0.20 part of beta-caryophyllene; 0.25 part of alkene; 0.30 part of phenethyl 2-furancarboxylate; 0.90 part of eugenol; 0.15 part of delta-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of essence were stirred together at 40° C. for 25 minutes at a rotational speed of 60 r/min until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60%RH. S7.

Put the S7 popping beads into the cigarette filter rod, and then get the camellia popping beads cigarette C7 after receiving the cigarette samples.

Comparative Example 4

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 6.50 parts of camellia extract; 1.25 parts of levomenthol; 2-methylbutyric acid-2-phenethyl ester 0.45 part; 2, 3, 5 trimethylpyrazine 0.75 part; orange oil terpene 0.65 part; phenethyl acetate 0.35 part; caprolactone 0.45 part; phenethyl alcohol 0.35 part; isoamyl acetate 0.70 part; Lactone 0.80 part; gemene D 0.15 part; linalool 0.15 part; acetic acid 0.30 part; 2-pentanol 0.20 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; 0.45 part of horse ketone; 0.15 part of isovaleric acid; 0.20 part of acetophenone; 0.10 part of ethyl decanoate; 0.95 part of ethyl heptanoate; 0.20 part of β-caryophyllene; 0.25 part of β-myrcene; 0.30 part of ethyl ester; 0.90 part of eugenol; 0.15 part of delta-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of camellia essence were mixed together under the condition of 40° C. at a rotating speed of 60 r/min for 25 minutes until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60%RH. S8.

Put the S8 popping beads into the cigarette filter rod, and then get the camellia popping beads cigarette C8 after receiving the cigarette samples.

Comparative Example 5

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 3.00 parts of camellia extract; 0.25 part of ethyl vanillin; 1.00 part of oak moss extract; 0.60 part of butyric acid; 0.65 part of ethyl octanoate; 0.45 part of 2-methylbutyric acid-2-phenylethyl ester; 0.75 part of 2, 3, and 5 trimethylpyrazine; 0.65 part of orange oil terpene; benzene acetate 0.35 part of ethyl ester; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of caprylactone; 0.15 part of gemene D; 0.15 part of linalool; 0.20 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; ethyl isovalerate 0.65 part; damascenone 0.45 part; isovaleric acid 0.15 part; acetophenone 0.20 part; 0.95 part of ethyl ester; 0.20 part of β-caryophyllene; 0.25 part of β-myrcene; 0.30 part of phenethyl 2-furanoate; 0.90 part of eugenol; 0.15 part of δ-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of camellia essence were mixed together under the condition of 40° C. at a rotating speed of 60 r/min for 25 minutes until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60%RH. S9.

Put the S9 popping beads into the cigarette filter rod, and then get the camellia popping beads cigarette C9 after receiving the cigarette samples.

Comparative Example 6

A camellia essence for cigarette popping beads, comprising the following components in parts by weight: in parts by weight, 15.00 parts of camellia extract; 3.00 parts of ethyl vanillin; 1.50 parts of oak moss extract; 0.60 part of butyric acid; 0.65 part of ethyl octanoate; 0.45 part of 2-methylbutyric acid-2-phenylethyl ester; 0.75 part of 2, 3, and 5 trimethylpyrazine; 0.65 part of orange oil terpene; benzene acetate 0.35 part of ethyl ester; 0.45 part of caprolactone; 0.35 part of phenethyl alcohol; 0.70 part of isoamyl acetate; 0.80 part of caprylactone; 0.15 part of gemene D; 0.15 part of linalool; 0.20 part; palmitic acid 0.10 part; benzyl benzoate 0.10 part; ethyl isovalerate 0.65 part; damascenone 0.45 part; isovaleric acid 0.15 part; acetophenone 0.20 part; 0.95 part of ethyl ester; 0.20 part of β-caryophyllene; 0.25 part of β-myrcene; 0.30 part of phenethyl 2-furanoate; 0.90 part of eugenol; 0.15 part of δ-juniperene; 0.30 part of phenylacetic acid.

Preparation of emulsion: in parts by weight, 660 parts of caprylic acid glyceride, 2 parts of anhydrous calcium chloride, 1.0 part of sodium carboxymethyl cellulose, 0.5 part of cyclodextrin, 3.5 parts of poloxamer and 210 parts of camellia essence were stirred together at 40° C. at a speed of 60 r/min for 25 minutes until the mixture was uniform.

Preparation of molding liquid: 95 parts of deionized water, 2 parts of sodium alginate, 0.7 part of sorbitol, 0.2 part of cyclodextrin and 0.3 part of Tween-20 were stirred together at a speed of 60 r/min under the condition of 30 °C 25min until the mixture is uniform to obtain a molding liquid.

Dropping pill setting: The emulsion is uniformly dripped into the molding liquid at a dripping rate of 5 drops/s through the dripping equipment, and the temperature is 20 °C and the relative humidity is 60%RH. S10.

Put the S10 popping beads into the cigarette filter rod, and then get the camellia popping beads cigarette C10 after receiving the cigarette samples.

For the cigarettes C1-C12 with camellia flavor burst beads, and the cigarettes with blank (flavor beads without flavor), the samples were smoked according to the evaluation method of Chinese cigarettes. The results are shown in Table 1.

Table 1

It can be seen from the above smoking evaluation results: Compared with blank cigarettes, C5-C10 has a slight decrease in sensory quality, and various indicators are basically the same or decreased. Sex, fineness decline and other issues. The quality of C1-C4, C11, and C12 is stable, which not only solves the problems of the C5-C10 camellia-flavor popped pearl cigarettes that do not meet the protection scope of the present invention, such as the reduction of hair permeability and fineness, but also further improves the aroma quality of the cigarettes. , the aroma volume is further increased, the sweetness and penetrability of the smoke caused by the camellia fragrance are further increased, the aftertaste is more comfortable, and the sweetness is increased. At the same time, the significance of camellia popping beads and the preference of smokers have also been greatly improved, and the sensory quality score has increased by more than 2 points, which has important practical value

The foregoing has shown and described the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above-mentioned embodiments, and the descriptions in the above-mentioned embodiments and the description are only to illustrate the principle of the present invention. Without departing from the spirit and scope of the present invention, the present invention will have Various changes and modifications fall within the scope of the claimed invention. The claimed scope of the present invention is defined by the appended claims and their equivalents.

Claims (10)

1. a camellia essence for cigarette popping beads, is characterized in that, comprises the following components according to parts by weight: Camellia extract 4.50-12.50 parts; ethyl vanillin 0.50-2.50 parts; oakmoss extract 1.15-1.35 parts; 2-methylbutyric acid 0.05-1.55 parts; ethyl caprylate 0.55-0.95 parts; 2-methyl Butyric acid-2-phenethyl ester 0.35-0.85 part; 2, 3, 5 trimethylpyrazine 0.50-1.45 part; orange oil terpene 0.45-1.35 part; phenethyl acetate 0.15-1.25 part; caprolactone 0.35-0.65 part; 0.15-0.95 part of phenethyl alcohol; 0.50-1.05 part of isoamyl acetate; 0.10-0.25 part of gemmaene D; 0.10-0.25 part of linalool; 0.15-0.45 part of acetic acid; 0.30 part; palmitic acid 0.05-0.15 part; benzyl benzoate 0.05-0.15 part; ethyl isovalerate 0.50-1.45 part; damascenone 0.35-0.65 part; isovaleric acid 0.10-0.25 part; acetophenone 0.10- 0.30 part; 0.05-0.15 part of ethyl caprate; 0.05-1.15 part of ethyl heptanoate; 0.15-0.45 part of β-caryophyllene; 0.15-0.45 part of β-myrcene; 0.80-1.35 part of eugenol; Pinene 0.10-0.50 parts; phenylacetic acid 0.10-1.05 parts. 2. A cigarette quick-fried pearl, characterized in that, the quick-fried pearl content is the camellia essence for cigarette quick-fried pearl of claim 1. 3. cigarette popping beads according to claim 2, is characterized in that, the content of camellia essence for cigarette popping beads in the popping beads is 5-45 μL/granule. 4. cigarette bursting beads according to claim 2, is characterized in that, described bursting beads diameter specification is 2.0mm-4.5mm, and the crushing pressure of bursting beads is 0.7kgf-1.7kgf. 5. the preparation method of the described cigarette popping beads of any one of claims 2～4, is characterized in that, comprises the steps: Step (1), preparation of emulsion: in parts by weight, 510-660 parts of caprylic acid glyceride, 1-3 parts of anhydrous calcium chloride, 0.5-1.5 parts of sodium carboxymethyl cellulose, cyclodextrin 0.05-1.00 part of essence, 2-5 parts of poloxamer and 220-260 parts of camellia essence are stirred together under the condition of 30-50 ℃ until they are evenly mixed to obtain an emulsion; Step (2), preparation of the molding solution: in parts by weight, 90-100 parts of deionized water, 1-3 parts of sodium alginate, 0.5-1.0 parts of sorbitol, 0.1-0.3 parts of cyclodextrin and 0.1-0.5 parts of Wen-20 are stirred together under the condition of 15-45 ℃ until the mixing is uniform to obtain a molding liquid; Step (3), setting the drop pills: the emulsion is uniformly dropped into the forming liquid, and after curing and forming, washing and air-drying are performed to obtain camellia popping beads. 6 . The preparation method of cigarette popping beads according to claim 5 , wherein, in step (1), the specific conditions for stirring are: stirring at a rotational speed of 40-80 r/min for 20-30 min. 7 . 7 . The preparation method of cigarette popping beads according to claim 5 , wherein, in step (2), the specific conditions for stirring are: stirring at a rotational speed of 40-80 r/min for 20-30 min. 8 . 8 . The preparation method of cigarette popping beads according to claim 5 , wherein, in step (3), the dripping speed is 5 drops/s. 9 . 9 . The preparation method of cigarette popping beads according to claim 5 , wherein, in step (3), the conditions for curing and molding are equilibrated for 24 hours at a temperature of 20° C. and a relative humidity of 60% RH. 10 . 10. A cigarette containing the cigarette popping beads obtained by the preparation method of any one of claims 5 to 9, wherein the cigarette popping beads are taken at the central position of the cigarette filter rod.