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CN111426524A - Smoking device and use method and application thereof - Google Patents

Smoking device and use method and application thereof Download PDF

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Publication number
CN111426524A
CN111426524A CN201910022249.5A CN201910022249A CN111426524A CN 111426524 A CN111426524 A CN 111426524A CN 201910022249 A CN201910022249 A CN 201910022249A CN 111426524 A CN111426524 A CN 111426524A
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power source
auxiliary
suction
trap
main
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张怡春
侯明
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Shanghai Tobacco Group Co Ltd
Shanghai New Tobacco Products Research Institute Co Ltd
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Shanghai Tobacco Group Co Ltd
Shanghai New Tobacco Products Research Institute Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/24Suction devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/12Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion

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Abstract

本发明提供了一种吸烟装置,包括:夹持器、多通部件、主捕集器、主动力源、至少一个辅助捕集器和至少一个辅助动力源。其中,夹持器用于夹持待检测的气雾产生制品,夹持器内部设有抽吸孔道;多通部件包括第一通口、第二通口和至少一个第三通口;主捕集器一端与抽吸孔道连通,另一端与第一通口连通;主动力源用于提供主抽吸动力;辅助捕集器一端与第三通口相连通;辅助动力源用于提供辅助抽吸动力。本发明还提供了上述吸烟装置的使用方法和用途。在满足标准规定的抽吸条件下,能够实现多个通路的同时抽吸,和气溶胶中多种不同相态和多种不同类别化学成分的同时捕集,为采用相同基准样品开展分析研究提供了可能。

Figure 201910022249

The present invention provides a smoking device comprising: a holder, a multi-pass member, a main trap, a main power source, at least one auxiliary trap and at least one auxiliary power source. Wherein, the holder is used to hold the aerosol-generating product to be detected, and the holder is provided with a suction channel; the multi-pass component includes a first passage, a second passage and at least one third passage; the main trapping One end of the filter is communicated with the suction hole, and the other end is communicated with the first port; the main power source is used to provide the main suction power; one end of the auxiliary catcher is communicated with the third port; the auxiliary power source is used to provide auxiliary suction power. The present invention also provides methods and uses of the above smoking device. Under the suction conditions specified in the standard, the simultaneous suction of multiple channels and the simultaneous capture of multiple different phases and different types of chemical components in the aerosol can be realized, which provides the basis for the analysis and research using the same reference sample. possible.

Figure 201910022249

Description

一种吸烟装置及其使用方法和用途A smoking device and method of using the same

技术领域technical field

本发明涉及烟草技术领域,具体涉及一种吸烟装置及其使用方法和用途。The present invention relates to the technical field of tobacco, in particular to a smoking device and a method for using the same.

背景技术Background technique

由于烟气中化学成分众多,其中含有部分对人体有害的化学成分,因此烟气分析是卷烟、电子烟、加热不燃烧烟草制品等安全性评估和质量评价的重要测量过程。烟气分析所遵循的分析测试标准(如ISO 4387、HCI等)规定了烟支抽吸过程中每口抽吸的体积(抽吸容量)、抽吸持续时间和抽吸流量图(由抽吸时气流速度随时间变化而绘制的曲线)等抽吸参数。Since there are many chemical components in smoke, some of which are harmful to human body, smoke analysis is an important measurement process for safety evaluation and quality evaluation of cigarettes, electronic cigarettes, and heat-not-burn tobacco products. The analytical test standards followed by smoke analysis (such as ISO 4387, HCI, etc.) specify the volume of each puff (puff volume), puff duration and puff flow map (by puff) during puffing. Puffing parameters such as the curve drawn by the airflow velocity versus time).

不同的烟气化学成分需要用不同的捕集方法和所对应的装置进行捕集,而不同的捕集装置由于存在不同的物理性能(如本身存在的抽吸阻力、单位时间允许通过气流量等限制),对吸烟机动力源的调节提出了不同的补偿要求,而现有吸烟装置均采用一个抽吸引擎对应一个或多个抽吸孔道的技术方式,这就使得单次连续测试过程中无法调节抽吸引擎以适应不同烟气成分捕集的需要,实验室开展不同烟气化学成分捕集分析时就必须分多次进行抽吸,效率低下,尤其是当需要用固相吸附管捕集烟气中的气相成分时,由于固相吸附管的吸阻往往较高,且一般吸附管限制流速为100mL/min以下,而吸烟机标准规定的流速往往在17.5mL/s甚至更高,因此不能将吸附管直接串联在吸烟机抽吸捕集的气路中,采用旁路并联的方式,对于单个吸附管来说又缺乏抽吸容量等抽吸参数的精准同步控制,因此实验结果的偏差往往较大,难以实现有效的数据控制。Different chemical components of flue gas need to be captured by different capture methods and corresponding devices, and different capture devices have different physical properties (such as their own suction resistance, allowable airflow per unit time, etc.) restrictions), different compensation requirements are put forward for the adjustment of the power source of the smoking machine, and the existing smoking devices all use a technical method in which one suction engine corresponds to one or more suction holes, which makes it impossible for a single continuous test process. Adjust the suction engine to meet the needs of capturing different flue gas components. When the laboratory conducts the capture and analysis of different flue gas chemical components, it must be pumped in multiple times, which is inefficient, especially when it needs to be captured by a solid-phase adsorption tube. When there is a gas phase component in the flue gas, the suction resistance of the solid-phase adsorption tube is often high, and the general flow rate of the adsorption tube is limited to less than 100mL/min, while the flow rate specified by the smoking machine standard is often 17.5mL/s or even higher, so The adsorption tube cannot be directly connected in series in the suction and trapped air path of the smoking machine, and the bypass method is used in parallel. For a single adsorption tube, there is a lack of precise synchronous control of the suction parameters such as the suction capacity, so the deviation of the experimental results. Often large, it is difficult to achieve effective data control.

因此,如何提供一种可以同时分析多种烟气成分的吸烟装置成为本领域亟待解决的问题。Therefore, how to provide a smoking device capable of simultaneously analyzing multiple smoke components has become an urgent problem to be solved in the art.

发明内容SUMMARY OF THE INVENTION

本发明要解决的技术问题是提供可以同时分析多种烟气成分的吸烟装置。The technical problem to be solved by the present invention is to provide a smoking device that can analyze multiple smoke components at the same time.

为了解决上述问题,本发明提供了一种吸烟装置,包括:In order to solve the above problems, the present invention provides a smoking device, comprising:

夹持器,用于夹持待检测的气雾产生制品,夹持器内部设有抽吸孔道;The holder is used to hold the aerosol-generating product to be detected, and the holder is provided with a suction channel;

多通部件,包括第一通口、第二通口和至少一个第三通口;a multi-pass component, including a first pass port, a second pass port and at least one third pass port;

主捕集器,一端与抽吸孔道连通,另一端与第一通口连通;the main trap, one end is communicated with the suction channel, and the other end is communicated with the first port;

主动力源,与第二通口相连通,用于提供主抽吸动力;a main power source, communicated with the second port, and used for providing main suction power;

至少一个辅助捕集器,辅助捕集器的数量与第三通口的数量相同,辅助捕集器一端与第三通口相连通;at least one auxiliary trap, the number of the auxiliary traps is the same as that of the third port, and one end of the auxiliary trap is communicated with the third port;

至少一个辅助动力源,与辅助捕集器的另一端相连通,用于提供辅助抽吸动力。At least one auxiliary power source, communicated with the other end of the auxiliary trap, is used for providing auxiliary suction power.

进一步地,多通部件为三通管。Further, the multi-pass component is a three-way pipe.

进一步地,三通管和主动力源之间设置有第一两位三通阀,和/或辅助捕集器和辅助动力源之间设置有第二两位三通阀。Further, a first two-position three-way valve is disposed between the three-way pipe and the main power source, and/or a second two-position three-way valve is disposed between the auxiliary trap and the auxiliary power source.

进一步地,吸烟装置还包括控制系统,控制系统用于控制主动力源和辅助动力源的抽吸动作和排气动作,Further, the smoking device further includes a control system, the control system is used to control the suction action and the exhaust action of the main power source and the auxiliary power source,

控制系统控制第一两位三通阀在主动力源进行抽吸动作时,使主动力源与主捕集器之间处于连通状态,主动力源实施抽吸动作后,第一两位三通阀切换至使主动力源与主捕集器之间关断,主动力源与旁路连通,主动力源进行排气动作;The control system controls the first two-position three-way valve to keep the main power source and the main catcher in a connected state when the main power source performs the suction action. The valve is switched to shut off the main power source and the main trap, the main power source is connected to the bypass, and the main power source performs the exhaust action;

和/或控制第二两位三通阀在辅助动力源进行抽吸动作时,使辅助动力源与辅助捕集器之间处于连通状态,主动力源实施抽吸动作后,第二两位三通阀切换至使辅助动力源与辅助捕集器之间关断,辅助动力源与旁路连通,主动力源进行排气动作。And/or control the second two-position three-way valve when the auxiliary power source performs the suction action, so that the auxiliary power source and the auxiliary catcher are in a connected state. After the main power source performs the suction action, the second two-position, three-way valve The through valve is switched to shut off the auxiliary power source and the auxiliary catcher, the auxiliary power source is communicated with the bypass, and the main power source performs the exhaust action.

进一步地,三通管和辅助捕集器之间设置有截止阀。Further, a shut-off valve is arranged between the three-way pipe and the auxiliary trap.

进一步地,辅助捕集器与辅助动力源的数量相同,辅助捕集器单独的与一个辅助动力源相连通。Further, the number of auxiliary traps and auxiliary power sources is the same, and the auxiliary traps are individually communicated with one auxiliary power source.

进一步地,主捕集器为加载有玻璃纤维滤片的捕集器或不带玻璃纤维滤片的连通器。Further, the main trap is a trap loaded with a glass fiber filter or a connector without a glass fiber filter.

进一步地,辅助捕集器为热脱附管或溶液洗气瓶。Further, the auxiliary trap is a thermal desorption tube or a solution washing bottle.

进一步地,夹持器为多个,吸烟装置还包括转盘,多个夹持器固定在转盘上且到转盘中轴线的距离相同,转盘可绕中轴线旋转,通过旋转转盘可以分别使每个夹持器的抽吸孔道与主捕集器相连通。Further, there are multiple grippers, the smoking device further includes a turntable, the multiple grippers are fixed on the turntable and have the same distance from the central axis of the turntable, the turntable can be rotated around the central axis, and each gripper can be made separately by rotating the turntable. The suction channel of the holder communicates with the main trap.

进一步地,气雾产生制品包括卷烟、电子烟和加热不燃烧烟草制品。Further, aerosol-generating products include cigarettes, electronic cigarettes, and heat-not-burn tobacco products.

进一步地,本发明还提供了上述任一种吸烟装置的使用方法,包括以下步骤:主动力源和辅助动力源同时进行抽吸动作和排气动作,主捕集器和辅助捕集器同时捕集烟气成分。Further, the present invention also provides a method for using any of the above-mentioned smoking devices, comprising the following steps: the main power source and the auxiliary power source simultaneously perform a suction action and an exhaust action, and the main trap and the auxiliary trap simultaneously capture Collection of smoke components.

进一步地,本发明还提供了上述任一种吸烟装置用于分析多种烟气成分的用途。Further, the present invention also provides the use of any of the above smoking devices for analyzing multiple smoke components.

为解决上述问题,本发明提供了一种多重动力源和捕集器同时对应单个抽吸孔道的装置。利用每个动力源可以独立调节的优势,保证标准抽吸条件总体不发生改变的条件下,使各捕集器具有符合自身要求的抽吸参数;在同一次抽吸过程中实现了使用多个捕集器同时捕集不同化学成分;为烟气气相成分在线定量捕集提供了可能;由于是对相同样品的不同化学成分进行同时捕集,因此提供了统一的计算和对比的基准;还能够提高检测效率,在一定程度上降低检测所需的时间、人力和物料成本。In order to solve the above problems, the present invention provides a device in which multiple power sources and traps correspond to a single suction channel at the same time. Taking advantage of the independent adjustment of each power source to ensure that the standard suction conditions do not change as a whole, each trap can have suction parameters that meet its own requirements; in the same suction process, the use of multiple The trap captures different chemical components at the same time; it provides the possibility for online quantitative capture of flue gas gas phase components; because different chemical components of the same sample are captured simultaneously, it provides a unified calculation and comparison benchmark; it can also Improve inspection efficiency and reduce the time, labor and material costs required for inspection to a certain extent.

附图说明Description of drawings

下面结合附图和具体实施方式对本发明作进一步详细地说明:Below in conjunction with the accompanying drawings and specific embodiments, the present invention will be described in further detail:

图1是本发明提供的一种吸烟装置的结构示意图;1 is a schematic structural diagram of a smoking device provided by the present invention;

图2是本发明提供的转盘的结构示意图;Fig. 2 is the structural representation of the turntable provided by the present invention;

图3是本发明提供的又一种吸烟装置的结构示意图。FIG. 3 is a schematic structural diagram of another smoking device provided by the present invention.

附图标记:Reference number:

烟支 11Cigarettes 11

夹持器 12Gripper 12

主捕集器 14Main catcher 14

多通部件 15Multi-pass assembly 15

截止阀 16Globe valve 16

辅助捕集器 17Auxiliary Trap 17

第二两位三通阀 182/2 3-way valve 18

辅助动力源 19Auxiliary Power Source 19

第一两位三通阀 201st 2/2-way valve 20

主动力源 21main power source 21

主动力源活塞 210main power source piston 210

转盘 100Turntable 100

通孔 120Through hole 120

具体实施方式Detailed ways

现在结合附图,详细介绍本发明的较佳实施方式。虽然本发明的描述将结合各个实施方式一起介绍,但这并不代表此发明的特征仅限于该几种实施方式。恰恰相反,结合实施方式作发明介绍的目的是为了覆盖基于本发明的权利要求而有可能延伸出的其它选择或改造。为了提供对本发明的深度了解,以下描述中将包含许多具体的细节。本发明也可以不使用这些细节实施。此外,为了避免混乱或模糊本发明的重点,有些具体细节将在描述中被省略。The preferred embodiments of the present invention will now be described in detail with reference to the accompanying drawings. Although the description of the present invention will be presented in conjunction with various embodiments, this does not mean that the features of this invention are limited to only these few embodiments. On the contrary, the purpose of introducing the invention in conjunction with the embodiments is to cover other options or modifications that may be extended based on the claims of the invention. The following description will contain numerous specific details in order to provide a thorough understanding of the present invention. The invention may also be practiced without these details. Furthermore, some specific details will be omitted from the description in order to avoid obscuring or obscuring the gist of the present invention.

如图1所示,本发明提供了一种吸烟装置,包括:夹持器12、多通部件15、主捕集器14、主动力源21、至少一个辅助捕集器17和至少一个辅助动力源19。其中,夹持器12用于夹持待检测的气雾产生制品,夹持器12内部设有抽吸孔道;多通部件15包括第一通口、第二通口和至少一个第三通口;主捕集器14一端与抽吸孔道连通,另一端与第一通口连通;主动力源21与第二通口相连通,用于提供主抽吸动力;至少一个辅助捕集器17,辅助捕集器17的数量与第三通口的数量相同,辅助捕集器17一端与第三通口相连通;至少一个辅助动力源19与辅助捕集器17的另一端相连通,用于提供辅助抽吸动力。As shown in FIG. 1, the present invention provides a smoking device comprising: a holder 12, a multi-pass member 15, a main catcher 14, a main power source 21, at least one auxiliary catcher 17 and at least one auxiliary power Source 19. Wherein, the holder 12 is used to hold the aerosol-generating product to be detected, and the holder 12 is provided with a suction hole; the multi-pass component 15 includes a first passage, a second passage and at least one third passage One end of the main trap 14 is communicated with the suction hole, and the other end is communicated with the first port; the main power source 21 is communicated with the second port for providing the main suction power; at least one auxiliary trap 17, The number of auxiliary traps 17 is the same as that of the third port, and one end of the auxiliary trap 17 is communicated with the third port; at least one auxiliary power source 19 is communicated with the other end of the auxiliary trap 17 for Provides auxiliary suction power.

进一步地,主捕集器14由前盖和后盖两部分组成,合并时构成密闭空间,“密闭空间”指的是在抽吸过程中,主捕集器14前、后端分别与抽吸孔道和多通部件15气密连接。气雾产生制品所释放的气溶胶不会向空间外溢漏,同时防止向空间内渗入气体或液体。Further, the main trap 14 is composed of two parts, a front cover and a rear cover, which form a closed space when combined. The orifice and the multi-pass member 15 are connected in a gas-tight manner. The aerosol released by the aerosol-generating article does not leak out of the space, and at the same time prevents gas or liquid from penetrating into the space.

进一步地,主捕集器14为加载有玻璃纤维滤片的捕集器或不带玻璃纤维滤片的连通器。Further, the main trap 14 is a trap loaded with a glass fiber filter or a connector without a glass fiber filter.

优选的是,主捕集器14为加载有玻璃纤维滤片的捕集器,密闭空间内固定放置一张玻璃纤维滤片,由此,保证气溶胶经过滤片时,其中的粒相成分被全部过滤在滤片上,且不被稀释和污染,所述辅助捕集器17捕集的是烟气气相成分。当主捕集器14是不带玻璃纤维滤片的连通器时,辅助捕集器17捕集的是全烟气成分。Preferably, the main trap 14 is a trap loaded with a glass fiber filter, and a glass fiber filter is fixedly placed in the closed space, thereby ensuring that when the aerosol passes through the filter, the particulate components in it are removed All filtered on the filter without dilution and pollution, the auxiliary trap 17 traps the gas phase components of the flue gas. When the primary trap 14 is a connector without a glass fiber filter, the secondary trap 17 traps all flue gas components.

进一步地,本发明中的气雾产生制品不但包括传统的烟支11,还包括新型烟草制品例如电子烟和加热不燃烧烟草制品。以下以烟支11为例结合附图进行描述。Further, the aerosol-generating products in the present invention include not only traditional cigarettes 11, but also novel tobacco products such as electronic cigarettes and heat-not-burn tobacco products. The following description will be given by taking the cigarette 11 as an example in conjunction with the accompanying drawings.

进一步地,如图1所示多通部件15为三通管,此时辅助捕集器17只有一个,单独与一个辅助动力源19连通。Further, as shown in FIG. 1 , the multi-pass component 15 is a three-way pipe, and at this time, there is only one auxiliary trap 17 , which is communicated with an auxiliary power source 19 alone.

进一步地,三通管和主动力源21之间设置有第一两位三通阀20,辅助捕集器17和辅助动力源19之间设置有第二两位三通阀18。当主动力源21按测试标准规定的抽吸容量、抽吸持续时间、抽吸间隔时间等参数,提供抽吸动力来抽吸烟支11的过程中。第一两位三通阀20在抽吸持续时间内使主动力源21与主捕集器14之间处于连通状态,完成一定抽吸容量和抽吸持续时间的抽吸动作后(即向图1所示的Z方向移动主动力源活塞210),第一两位三通阀20切换至使主动力源21与主捕集器14之间关断,主动力源21与旁路连通,在抽吸间隔时间内,主动力源活塞210向Z’移动,将抽吸来的烟气从旁路排出,进行排气动作。待抽吸间隔时间结束,第一两位三通阀20切换至主动力源21与主捕集器14连通,开始下一个抽吸动作。同样地,第二两位三通阀18和辅助动力源19之间也根据辅助捕集器17需要的测试标准配合实现抽吸动作和排气动作。Further, a first two-position three-way valve 20 is disposed between the three-way pipe and the main power source 21 , and a second two-position three-way valve 18 is disposed between the auxiliary trap 17 and the auxiliary power source 19 . When the main power source 21 provides the suction power to smoke the cigarette 11 according to the parameters such as the suction volume, the suction duration, and the suction interval time specified in the test standard. The first two-position three-way valve 20 keeps the main power source 21 and the main trap 14 in a connected state during the suction duration, and after the suction action of a certain suction capacity and suction duration is completed (ie, the direction shown in Fig. 1 moves the main power source piston 210 in the Z direction), the first two-position three-way valve 20 is switched to shut off the main power source 21 and the main catcher 14, and the main power source 21 is connected to the bypass. During the suction interval, the main power source piston 210 moves to Z' to discharge the suctioned flue gas from the bypass to perform the exhaust operation. After the suction interval is over, the first two-position three-way valve 20 is switched to the main power source 21 to communicate with the main trap 14, and the next suction action is started. Similarly, the suction action and the exhaust action are also cooperated between the second two-position three-way valve 18 and the auxiliary power source 19 according to the test standard required by the auxiliary trap 17 .

进一步地,旁路上可以连接有收集装置,将收集到的烟气进一步进行其他分析。Further, a collection device can be connected to the bypass to further analyze the collected flue gas.

进一步地,第一两位三通阀20和第二两位三通阀18可以是由其物理结构直接实现的上述连通状态切换的功能,也可以是吸烟装置还包括控制系统,控制系统在控制主动力源21和辅助动力源19的抽吸动作和排气动作的同时,控制两位三通阀的连通状态切换。控制系统可以根据测试需要的抽吸容量、抽吸持续时间、抽吸间隔时间等参数分别控制主动力源21和辅助动力源19。Further, the first two-position three-way valve 20 and the second two-position three-way valve 18 can be directly realized by their physical structure of the above-mentioned communication state switching function, or the smoking device also includes a control system, and the control system is in the control system. At the same time as the suction operation and the exhaust operation of the main power source 21 and the auxiliary power source 19, the switching of the communication state of the two-position three-way valve is controlled. The control system can respectively control the main power source 21 and the auxiliary power source 19 according to parameters such as suction volume, suction duration, and suction interval time required for the test.

进一步地,三通管和辅助捕集器17之间设置有截止阀16,截止阀16可以是人工控制开闭,也可以是控制系统控制截止阀16开闭。关闭截止阀16时,控制系统仅控制主动力源21的抽吸动作和排气动作,可以实现常规烟气分析中的基础功能;打开截止阀16时,控制系统分别同时控制主动力源21和辅助动力源19的抽吸动作和排气动作,即可同时实现烟气中的粒相成分分析和烟气气相成分分析。Further, a shut-off valve 16 is provided between the three-way pipe and the auxiliary trap 17 , and the shut-off valve 16 may be manually controlled to open and close, or the shut-off valve 16 may be controlled to be opened and closed by a control system. When the shut-off valve 16 is closed, the control system only controls the suction and exhaust actions of the main power source 21, which can realize basic functions in conventional flue gas analysis; when the shut-off valve 16 is opened, the control system controls the main power source 21 and The suction action and the exhaust action of the auxiliary power source 19 can simultaneously realize the analysis of the particle phase composition in the flue gas and the analysis of the gas phase composition of the flue gas.

具体来说,本发明提供的吸烟装置抽吸烟支11并捕集其所释放的气溶胶之前,通过电脑控制系统关闭截止阀16,按烟气分析相关标准方法的要求,通过主动力源21提供抽吸动力,测定整个装置的气密性、抽吸容量、抽吸曲线的参数是否符合标准的要求,然后,将烟支11插装在夹持器12中,启动吸烟程序,在通过电脑控制系统始终保持截止阀16关闭的状态下,按标准规定的抽吸容量、抽吸持续时间、抽吸间隔时间等参数,由主动力源21单独提供抽吸动力抽吸烟支11,并由主捕集器14来捕集烟支11所释放气溶胶中的粒相成分。实现常规烟气分析中吸烟所必备的基础功能。Specifically, before the smoking device provided by the present invention smokes the cigarettes 11 and captures the aerosols released by them, the shut-off valve 16 is closed by the computer control system, and the main power source 21 provides the smoking device according to the requirements of the relevant standard methods of smoke analysis. The suction power is used to determine whether the air tightness, suction capacity, and suction curve parameters of the entire device meet the standard requirements. Then, insert the cigarette 11 into the holder 12, start the smoking program, and control it through the computer The system keeps the shut-off valve 16 closed all the time, according to the parameters such as the suction volume, the suction duration and the suction interval time specified by the standard, the main power source 21 alone provides the suction power to smoke the cigarette 11, and the main capture The collector 14 is used to capture the particulate components in the aerosol released by the cigarettes 11 . Realize the basic functions necessary for smoking in conventional smoke analysis.

又例如,本发明提供的吸烟装置抽吸烟支11并捕集其所释放的气溶胶之前,通过电脑控制系统打开截止阀16,并使之始终处于打开的状态,接入辅助捕集器17,通过主动力源21和辅助动力源19共同提供抽吸动力,测定整个装置的气密性。按标准测定和调节抽吸容量时。首先,使辅助动力源19进行抽吸,以测定并调节辅助动力源19所提供的抽吸容量,当设定抽吸持续时间为2s时,优选的抽吸容量为1mL-3mL,为提高烟气气相成分的富集量,更为优选的抽吸容量为3mL,当设定持续抽吸时间为3s时,优选的抽吸容量为1mL-5mL,相同理由,更为优选的抽吸容量为5mL;然后,使主动力源21和辅助动力源19共同进行抽吸,调节主动力源21的抽吸容量,使总的抽吸容量达到烟气分析测试标准方法所规定的容量要求。后续抽吸烟支11并捕集气溶胶成分的过程中,主动力源21和辅助动力源19同步工作,直至完成全部抽吸捕集的过程。For another example, before the smoking device provided by the present invention smokes the cigarettes 11 and captures the aerosols released by them, the shut-off valve 16 is opened through the computer control system, and is always in an open state, and the auxiliary trap 17 is connected to, The main power source 21 and the auxiliary power source 19 jointly provide the suction power, and the air tightness of the whole device is measured. When measuring and adjusting the suction volume according to the standard. First, the auxiliary power source 19 is sucked to measure and adjust the suction capacity provided by the auxiliary power source 19. When the suction duration is set to 2s, the preferred suction capacity is 1mL-3mL. For the enrichment volume of gas-phase components, the more preferred suction capacity is 3mL. When the continuous suction time is set to 3s, the preferred suction capacity is 1mL-5mL. For the same reason, the more preferred suction capacity is 5mL; then, the main power source 21 and the auxiliary power source 19 are pumped together, and the suction capacity of the main power source 21 is adjusted so that the total suction capacity meets the capacity requirements specified in the standard method for flue gas analysis and testing. During the subsequent process of smoking the cigarette 11 and capturing the aerosol components, the main power source 21 and the auxiliary power source 19 work synchronously until the entire process of smoking and capturing is completed.

进一步地,辅助捕集器17与辅助动力源19的数量可以相同也可以不同,多个辅助捕集器17可以以并联或串联的方式与辅助动力源19连通。优选地,辅助捕集器17与辅助动力源19的数量相同,辅助捕集器17单独的与一个辅助动力源19相连通。Further, the number of the auxiliary traps 17 and the auxiliary power source 19 may be the same or different, and a plurality of the auxiliary traps 17 may be connected to the auxiliary power source 19 in parallel or in series. Preferably, the number of the auxiliary catchers 17 and the auxiliary power sources 19 are the same, and the auxiliary catchers 17 are individually communicated with one auxiliary power source 19 .

进一步地,辅助捕集器17为热脱附管或溶液洗气瓶。热脱附管和溶液洗气瓶可以是单独存在,也可以是多个串联,其中热脱附管的种类可以根据需要选择,每个溶液洗气瓶中捕集溶液的种类和体积也可以按需调节。Further, the auxiliary trap 17 is a thermal desorption tube or a solution washing bottle. The thermal desorption tube and the solution washing bottle can exist alone or in series. The type of thermal desorption tube can be selected according to the needs. The type and volume of the trapping solution in each solution washing bottle can also be selected according to the requirements. Adjustment is required.

进一步地,如图2和图3所示,夹持器12为多个,吸烟装置还包括转盘100,转盘100固定在吸烟装置上,多个夹持器12固定在转盘100上且到转盘100中轴线的距离相同,转盘100可绕其中轴线旋转,通过旋转转盘100可以分别使每个夹持器12的抽吸孔道与主捕集器14气密连通。Further, as shown in FIG. 2 and FIG. 3 , there are multiple grippers 12 , the smoking device further includes a turntable 100 , the turntable 100 is fixed on the smoking device, and a plurality of grippers 12 are fixed on the turntable 100 and reach the turntable 100 . The distance from the central axis is the same, and the turntable 100 can rotate around the central axis. By rotating the turntable 100, the suction channel of each holder 12 can be airtightly communicated with the main trap 14 respectively.

进一步地,如图2所示,圆盘上沿圆周方向均布有多个供夹持器12安装的通孔120。Further, as shown in FIG. 2 , a plurality of through holes 120 for installing the holder 12 are evenly distributed on the disc along the circumferential direction.

进一步地,夹持器12的数量没有特殊限制,可以根据使用的需要设定相应数量的夹持器12,优选夹持器12的数量为2-10个。Further, the number of the grippers 12 is not particularly limited, and a corresponding number of grippers 12 can be set according to the needs of use, and preferably the number of grippers 12 is 2-10.

进一步地,当设置有转盘100时,可以同时在转盘100上插装多种品牌和规格的烟支11。在根据前述的抽吸方法完整抽吸完一个烟支11后,旋转到下一个烟支11。依次逐支对单个夹持器12夹持的烟支11进行全部气溶胶或者逐口气溶胶的捕集。Further, when the turntable 100 is provided, cigarettes 11 of various brands and specifications can be inserted on the turntable 100 at the same time. After one cigarette 11 is completely smoked according to the aforementioned smoking method, it is rotated to the next cigarette 11 . The cigarettes 11 held by a single holder 12 are sequentially collected for all aerosols or aerosols one by one.

还可以是利用抽吸方法标准所规定的对每支烟支11连续抽吸2口间的间隔时间,每抽完一支烟的一口后,通过转盘100转动切换到下一个抽吸孔道与主捕集器14连通,抽吸下一支烟的一口,依次轮换,直至全部烟支11的全部抽吸口数的抽吸捕集完成。利用转盘100的转动,在完成一支烟抽吸的时间内,实际可完成多支烟的抽吸和气溶胶捕集过程,在提高工作效率的同时,增加了主捕集器14和辅助捕集器17的气溶胶富集量,更加有利于对所捕集的气溶胶中化学成分的后续准确测定。It is also possible to use the interval time between two consecutive puffs of each cigarette 11 specified by the smoking method standard, and after each puff of a cigarette, the turntable 100 is rotated to switch to the next puff channel and the main puff. The traps 14 are connected, and one puff of the next cigarette is sucked in turn, until all the puffs of all the cigarettes 11 are sucked and captured. Using the rotation of the turntable 100, the process of smoking multiple cigarettes and capturing aerosols can actually be completed within the time of completing the smoking of one cigarette. While improving the work efficiency, a main trap 14 and an auxiliary trap are added. The aerosol enrichment amount of the device 17 is more conducive to the subsequent accurate determination of the chemical components in the captured aerosol.

进一步地,还可以是在转盘100每转一圈后,也就是转盘100上每个插装的烟支11完成一口抽吸后,在下一圈的第一口抽吸开始之前,及时调换一个新的主捕集器14或/和辅助捕集器17。通过在多支烟支11相同口抽吸完成后调换捕集器,可以在标准规定的抽吸条件下,在每个捕集器上富集多支烟支11相同口数所释放的气溶胶,进而通过提高单个捕集器上气溶胶富集量而满足后续化学成分准确测定的基础上,可以获得烟支11在连续抽吸过程中,逐口气溶胶以及其中化学成分释放量的变化规律,为降低烟气中有害成分的研究提供帮助。Further, after each turn of the turntable 100, that is, after each inserted cigarette 11 on the turntable 100 completes one puff of puff, before the first puff of puff in the next circle starts, a new one can be exchanged in time. main trap 14 or/and auxiliary trap 17. By replacing the traps after the same puffs of multiple cigarettes 11 are puffed, the aerosols released by the same puffs of the multiple cigarettes 11 can be enriched on each trap under the smoking conditions specified in the standard. Furthermore, on the basis of increasing the aerosol enrichment amount on a single trap to meet the accurate determination of subsequent chemical components, the variation law of the aerosol and the release amount of chemical components in the cigarette 11 in the continuous smoking process can be obtained, as follows: Research to reduce harmful constituents in smoke provides assistance.

进一步地,本发明还提供了上述任一种吸烟装置的使用方法,包括以下步骤:Further, the present invention also provides a method for using any of the above-mentioned smoking devices, comprising the following steps:

主动力源21和辅助动力源19同时进行抽吸动作和排气动作,主捕集器14和辅助捕集器17同时捕集烟气成分,即可同时实现烟气中的粒相成分分析和烟气气相成分分析。The main power source 21 and the auxiliary power source 19 perform the suction action and the exhaust action at the same time, and the main trap 14 and the auxiliary trap 17 capture the flue gas components at the same time, which can simultaneously realize the analysis and analysis of the particle phase components in the flue gas. Gas-phase composition analysis of flue gas.

进一步地,主捕集器14用于捕集烟气中的粒相成分,辅助捕集器17用于捕集烟气中的气相成分。Further, the main trap 14 is used to capture the particulate components in the flue gas, and the auxiliary trap 17 is used to trap the gas phase components in the flue gas.

进一步地,本发明还提供了上述任一种吸烟装置用于分析多种烟气成分的用途。Further, the present invention also provides the use of any of the above smoking devices for analyzing multiple smoke components.

综上所述,本发明提供了一种多重动力源和捕集器同时对应单个抽吸孔道的方法和装置。利用每个动力源可以独立调节的优势,保证标准抽吸条件总体不发生改变的条件下,使各捕集器具有符合自身要求的抽吸参数;在同一次抽吸过程中实现了使用多个捕集器同时捕集不同化学成分;为烟气气相成分在线定量捕集提供了可能;由于是对相同样品的不同化学成分进行同时捕集,因此提供了统一的计算和对比的基准;还能够提高检测效率,在一定程度上降低检测所需的时间、人力和物料成本。在满足标准规定的抽吸条件下,能够实现多个通路的同时抽吸,和气溶胶中多种不同相态和多种不同类别化学成分的同时捕集方法和装置,为采用相同基准样品开展分析研究提供了可能。To sum up, the present invention provides a method and device in which multiple power sources and traps simultaneously correspond to a single suction channel. Taking advantage of the independent adjustment of each power source to ensure that the standard suction conditions do not change as a whole, each trap can have suction parameters that meet its own requirements; in the same suction process, the use of multiple The trap captures different chemical components at the same time; it provides the possibility for online quantitative capture of flue gas gas phase components; because different chemical components of the same sample are captured simultaneously, it provides a unified calculation and comparison benchmark; it can also Improve inspection efficiency and reduce the time, labor and material costs required for inspection to a certain extent. Under the suction conditions specified in the standard, simultaneous suction of multiple channels, and simultaneous capture of multiple different phases and different types of chemical components in aerosols can be achieved, so as to use the same reference sample for analysis Research offers the possibility.

综上所述,本发明提供的上述实施例仅例示性说明本发明的原理及其功效,而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下,对上述实施例进行修饰或改变。因此,举凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变,仍应由本发明的权利要求所涵盖。To sum up, the above-mentioned embodiments provided by the present invention merely illustrate the principles and effects of the present invention, but are not intended to limit the present invention. Anyone skilled in the art can modify or change the above embodiments without departing from the spirit and scope of the present invention. Therefore, all equivalent modifications or changes made by those with ordinary knowledge in the technical field without departing from the spirit and technical idea disclosed in the present invention should still be covered by the claims of the present invention.

Claims (12)

1. A smoking device, comprising:
the holder is used for holding an aerosol-generating product to be detected, and a suction duct is arranged inside the holder;
a multi-pass component comprising a first pass, a second pass, and at least one third pass;
one end of the main catcher is communicated with the suction duct, and the other end of the main catcher is communicated with the first through hole;
a primary power source in communication with the second port for providing primary suction power;
the number of the auxiliary traps is the same as that of the third ports, and one end of each auxiliary trap is communicated with the third ports;
and the at least one auxiliary power source is communicated with the other end of the auxiliary catcher and is used for providing auxiliary suction power.
2. A smoking device according to claim 1, wherein the manifold is a tee.
3. A smoking device according to claim 2, wherein a first two-position three-way valve is provided between the tee and the primary power source and/or a second two-position three-way valve is provided between the auxiliary trap and the auxiliary power source.
4. A smoking device according to claim 3, further comprising a control system for controlling the suction and exhaust actions of the primary and secondary power sources,
the control system controls the first two-position three-way valve to enable the main power source and the main trap to be in a communicated state when the main power source performs suction, after the main power source performs suction, the first two-position three-way valve is switched to enable the main power source and the main trap to be shut off, the main power source is communicated with the bypass, and the main power source performs exhaust;
and/or controlling the second two-position three-way valve to enable the auxiliary power source and the auxiliary trap to be in a communicated state when the auxiliary power source performs a pumping action, switching the second two-position three-way valve to enable the auxiliary power source and the auxiliary trap to be closed after the main power source performs the pumping action, enabling the auxiliary power source to be communicated with the bypass, and enabling the main power source to perform an exhaust action.
5. A smoking device according to claim 4, wherein a shut-off valve is provided between the tee and the auxiliary trap.
6. A smoking device according to claim 5, wherein the auxiliary traps are in the same number as the auxiliary power sources, the auxiliary traps being individually in communication with one auxiliary power source.
7. The smoking device of any one of claims 1 to 6, wherein the primary trap is a glass fibre filter loaded trap or a communicator without a glass fibre filter.
8. A smoking device according to any one of claims 1 to 6, wherein the auxiliary trap is a heat desorption tube or a solution scrubber bottle.
9. A smoking device according to any one of claims 1-6, wherein the holder is provided in a plurality, the smoking device further comprising a turntable, the plurality of holders being fixed to the turntable at the same distance from a central axis of the turntable, the turntable being rotatable about the central axis, and the suction duct of each holder being adapted to communicate with the main trap by rotating the turntable.
10. A smoking device according to any of claims 1-6, wherein the aerosol-generating article comprises a cigarette, an e-cigarette, or a heat-not-burn tobacco article.
11. A method of using a smoking device according to any one of claims 1 to 10, comprising the steps of: the main power source and the auxiliary power source simultaneously perform suction action and exhaust action, and the main catcher and the auxiliary catcher simultaneously catch smoke components.
12. Use of a smoking device according to any one of claims 1 to 10 for the analysis of a plurality of smoke constituents.
CN201910022249.5A 2019-01-10 2019-01-10 Smoking device and use method and application thereof Pending CN111426524A (en)

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CN105954474A (en) * 2016-07-06 2016-09-21 中国烟草总公司郑州烟草研究院 Rotary smoking method capable of fixing cigarette
CN107144450A (en) * 2017-06-30 2017-09-08 国家烟草质量监督检验中心 A kind of cigarette holder and its application suitable for rotating disc type smoking machine provided with adsorbent chamber
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CN112304803A (en) * 2020-11-13 2021-02-02 上海烟草集团有限责任公司 A kind of cigarette dynamic drawing resistance detection instrument and method
CN112304803B (en) * 2020-11-13 2023-02-28 上海烟草集团有限责任公司 Cigarette dynamic suction resistance detection instrument and method
CN112557270A (en) * 2020-12-11 2021-03-26 中国烟草总公司郑州烟草研究院 Device for synchronously detecting smoke discharge amount of multiple cigarettes
CN112557270B (en) * 2020-12-11 2024-06-07 中国烟草总公司郑州烟草研究院 Device for synchronously detecting smoke discharge amount of multiple cigarettes
CN113188858A (en) * 2021-05-07 2021-07-30 中国烟草总公司郑州烟草研究院 Detachable flue gas segmentation collection system
CN113188858B (en) * 2021-05-07 2023-08-04 中国烟草总公司郑州烟草研究院 Detachable flue gas segmentation collection system

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