CN111393963A - Environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish - Google Patents
Environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish Download PDFInfo
- Publication number
- CN111393963A CN111393963A CN202010206102.4A CN202010206102A CN111393963A CN 111393963 A CN111393963 A CN 111393963A CN 202010206102 A CN202010206102 A CN 202010206102A CN 111393963 A CN111393963 A CN 111393963A
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- parts
- photocuring
- saving
- woodenware
- environment
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- 238000000016 photochemical curing Methods 0.000 title claims abstract description 17
- 238000005507 spraying Methods 0.000 title claims abstract description 10
- 239000000178 monomer Substances 0.000 claims abstract description 15
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 11
- 229920000728 polyester Polymers 0.000 claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004841 bisphenol A epoxy resin Substances 0.000 claims abstract description 9
- 239000006229 carbon black Substances 0.000 claims abstract description 9
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002270 dispersing agent Substances 0.000 claims abstract description 9
- 238000009736 wetting Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000006185 dispersion Substances 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- 238000005498 polishing Methods 0.000 claims description 7
- 230000007613 environmental effect Effects 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 2
- 239000003973 paint Substances 0.000 description 14
- 238000000576 coating method Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 238000001723 curing Methods 0.000 description 3
- 239000004814 polyurethane Substances 0.000 description 3
- 238000004134 energy conservation Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 244000137852 Petrea volubilis Species 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 230000004992 fission Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/06—Unsaturated polyesters having carbon-to-carbon unsaturation
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/002—Priming paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Macromonomer-Based Addition Polymer (AREA)
Abstract
The invention discloses an environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish, which comprises the following raw materials, by weight, 3-8 parts of L ED photoinitiator, 26-71 parts of monomer, 5-20 parts of bisphenol A epoxy resin oligomer, 15-60 parts of polyester acrylate oligomer, 2-7 parts of wetting dispersant, 0.2-2.5 parts of white carbon black and 5-25 parts of talcum powder.
Description
Technical Field
The invention relates to an environment-friendly energy-saving L ED photocureable woodenware spraying primer easy to polish, and belongs to the technical field of paint preparation.
Background
At present, ultraviolet-cured UV (ultraviolet) coatings are the main woodware coatings on the market, and water-based coatings taking water as a solvent are replacing PU (polyurethane) coatings.
In the use process of the UV coating, the high-pressure mercury lamp can generate ozone, the environment is polluted, the energy consumption is too high, and the polishing performance of the primer is generally poor. The water-based paint has long drying period, and because of the existence of water solubility, the paint film is hydrolyzed again all the time, thereby generating hidden trouble, so the water-based paint is rarely used in the current woodware market. The PU paint has been banned by national requirements because of environmental protection problems, but no mature product is effectively substituted at present.
Disclosure of Invention
Aiming at the problems, the invention aims to provide a preparation method of L ED photocuring woodware spray primer which is environment-friendly, energy-saving and easy to polish.
In order to achieve the purpose, the invention provides the following technical scheme that the environment-friendly energy-saving easy-to-polish L ED photocuring woodenware spray primer comprises the following raw materials, by weight, 3-8 parts of L ED photoinitiator, 26-71 parts of monomer, 5-20 parts of bisphenol A epoxy resin oligomer, 15-60 parts of polyester acrylate oligomer, 2-7 parts of wetting dispersant, 0.2-2.5 parts of white carbon black and 5-25 parts of talcum powder.
Further preferably, the environment-friendly energy-saving easy-polishing L ED photocuring woodenware spray primer comprises the following raw materials, by weight, 5 parts of L ED photoinitiator, 50 parts of monomer, 15 parts of bisphenol A epoxy resin oligomer, 35 parts of polyester acrylate oligomer, 5 parts of wetting dispersant, 2 parts of white carbon black and 15 parts of talcum powder.
Preferably, the L ED photoinitiator is a 395 nm wavelength photoinitiator.
Preferably, the monomer is any one or more of TPGDA, DPGDA or NPGDA.
Preferably, the viscosity of the polyester acrylate oligomer is 50 to 500CPS/25 ℃.
A preparation method of L ED photocuring woodenware spray primer with the advantages of environmental protection, energy saving and easy polishing comprises the following steps of firstly, adding L ED photoinitiator into a part of monomers according to the weight part of raw materials of the spray primer, dispersing and stirring for 15 minutes to obtain mixed liquid for later use;
step two, pouring all the residual monomers into a pulling cylinder;
putting the bisphenol A epoxy resin oligomer into a drawing cylinder, and starting to disperse at the speed of 800 revolutions per minute;
pouring the polyester acrylate oligomer into a drawing cylinder for dispersion;
pouring the wetting dispersant into a pulling cylinder for dispersion;
step six, pouring the white carbon black into a drawn cylinder for dispersion;
step seven, adding talcum powder into a pulling cylinder, adjusting the rotating speed to 1200 revolutions per minute, and dispersing for 15 minutes;
pouring the mixed solution obtained in the first step into a drawn cylinder, and dispersing at a low speed for 8-10 minutes at a rotating speed of 500 revolutions per minute;
and step nine, filtering and subpackaging.
Compared with the prior art, the invention has the following beneficial effects: the spraying primer initiates the polymerization or fission of oligomer by light with a wavelength of 395 nm to realize rapid curing and form a dry paint film. The spraying primer replaces the existing UV primer, solves the problems of difficult polishing and high energy consumption, replaces the waterborne wood primer to solve the problem of rib bursting, replaces the traditional solvent-containing paint, and solves the problem of environmental protection.
Detailed Description
The technical solutions of the present invention will be described clearly and completely in the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
a preparation method of L ED photocuring woodware spray primer with the advantages of environmental protection, energy conservation and easy polishing comprises the following steps:
step one, adding 5 parts of L ED photoinitiator into 10 parts of monomer, and dispersing and stirring for 15 minutes for later use;
step two, pouring 32 parts of monomers into a drawn cylinder;
step three, putting 5 parts of bisphenol A epoxy resin oligomer into a drawing cylinder, and starting to disperse at the speed of 800 revolutions per minute;
step four, pouring 28 parts of polyester acrylate oligomer with the viscosity of 50-500(CPS/25 ℃) into a drawn cylinder for dispersion;
pouring 3 parts of wetting dispersant into a drawing cylinder for dispersion;
step six, adding 2 parts of white carbon black for dispersion;
step seven, adding 15 parts of talcum powder into a pulling cylinder, adjusting the rotating speed to 1200 revolutions per minute, and dispersing for 15 minutes;
pouring the mixed solution obtained in the first step into a drawn cylinder, and dispersing at a low speed for 8-10 minutes at a rotating speed of 500 revolutions per minute;
and ninthly, filtering and subpackaging to obtain the gray-white opaque L ED photocuring spraying primer.
Example 2
A preparation method of L ED photocuring woodware spray primer with the advantages of environmental protection, energy conservation and easy polishing comprises the following steps:
step one, adding 5 parts of L ED photoinitiator into 15 parts of monomer, and dispersing and stirring for fifteen minutes for later use;
step two, pouring 25 parts of monomers into a drawn cylinder;
step three, putting 5 parts of bisphenol A epoxy resin oligomer into a drawing cylinder, and starting to disperse at the speed of 800 revolutions per minute;
step four, pouring 20 parts of polyester acrylate oligomer with the viscosity of 50-500(CPS/25 ℃) into a drawing cylinder for dispersion;
pouring 3 parts of wetting dispersant into a drawing cylinder for dispersion;
step six, adding 2 parts of white carbon black for dispersion;
step seven, adding 25 parts of talcum powder into a pulling cylinder, adjusting the rotating speed to 1200 revolutions per minute, and dispersing for 15 minutes;
pouring the mixed solution obtained in the first step into a drawn cylinder, and dispersing at a low speed for 8-10 minutes at a rotating speed of 500 revolutions per minute;
and ninthly, filtering and subpackaging to obtain the gray-white opaque L ED photocuring spraying primer.
The wood ware is coated with the UV paint in the comparative examples 1 and 2Spraying on the surface of the device, wherein the first application amount is 100 g/square meter, the second application amount is 200 g/square meter, curing is carried out by using a curing lamp with the wavelength of 395 nm, and the irradiation energy is 300mj/cm2The following table shows the two paint film drying times for the examples and comparative examples.
TABLE 1
| Experimental group | Drying time of 100 grams per square meter paint film | 200 g/square meter paint film drying time |
| Example 1 | 3 seconds | 6.2 seconds |
| Example 2 | 2.8 seconds | 6 seconds |
| Comparative example | 15 seconds | 32 seconds |
The embodiment shows that the primer can be quickly cured to form a dry paint film, the paint films of the embodiment 1 and the embodiment 2 are polished by 400-mesh sand paper, the paint films can be effectively and quickly polished, and no VOC is discharged in the film forming process.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. An environment-friendly energy-saving L ED photocuring woodenware spray primer easy to polish is characterized by comprising the following raw materials, by weight, 3-8 parts of L ED photoinitiator, 26-71 parts of monomer, 5-20 parts of bisphenol A epoxy resin oligomer, 15-60 parts of polyester acrylate oligomer, 2-7 parts of wetting dispersant, 0.2-2.5 parts of white carbon black and 5-25 parts of talcum powder.
2. The environment-friendly energy-saving L ED photocuring woodenware spray primer easy to polish according to claim 1, which is characterized by comprising the following raw materials, by weight, 5 parts of L ED photoinitiator, 50 parts of monomer, 15 parts of bisphenol A epoxy resin oligomer, 35 parts of polyester acrylate oligomer, 5 parts of wetting dispersant, 2 parts of white carbon black and 15 parts of talcum powder.
3. The environment-friendly energy-saving L ED photocuring woodenware spray primer easy to polish according to claim 1, characterized in that the L ED photoinitiator is a 395 nm wavelength photoinitiator.
4. The environment-friendly energy-saving L ED photocuring woodenware spray primer easy to polish according to claim 1, wherein the monomer is any one or more of TPGDA, DPGDA or NPGDA.
5. The environment-friendly energy-saving L ED photocuring woodenware spray primer easy to polish according to claim 1, characterized in that the viscosity of the polyester acrylate oligomer is 50-500CPS/25 ℃.
6. A preparation method of L ED photocuring woodware spraying primer with the advantages of environmental protection, energy saving and easy polishing is characterized by comprising the following specific steps of firstly, adding L ED photoinitiator into a part of monomers according to the weight part of raw materials of the spraying primer, dispersing and stirring for 15 minutes to obtain mixed liquid for later use;
step two, pouring all the residual monomers into a pulling cylinder;
putting the bisphenol A epoxy resin oligomer into a drawing cylinder, and starting to disperse at the speed of 800 revolutions per minute;
pouring the polyester acrylate oligomer into a drawing cylinder for dispersion;
pouring the wetting dispersant into a pulling cylinder for dispersion;
step six, pouring the white carbon black into a drawn cylinder for dispersion;
step seven, adding talcum powder into a pulling cylinder, adjusting the rotating speed to 1200 revolutions per minute, and dispersing for 15 minutes;
pouring the mixed solution obtained in the first step into a drawn cylinder, and dispersing at a low speed for 8-10 minutes at a rotating speed of 500 revolutions per minute;
and step nine, filtering and subpackaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010206102.4A CN111393963A (en) | 2020-03-23 | 2020-03-23 | Environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010206102.4A CN111393963A (en) | 2020-03-23 | 2020-03-23 | Environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111393963A true CN111393963A (en) | 2020-07-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010206102.4A Pending CN111393963A (en) | 2020-03-23 | 2020-03-23 | Environment-friendly energy-saving L ED photocuring woodenware spraying primer easy to polish |
Country Status (1)
| Country | Link |
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| CN (1) | CN111393963A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116284589A (en) * | 2023-04-11 | 2023-06-23 | 上饶市聚微星科技有限公司 | Photosensitive resin composition for additive manufacturing modified by black talc and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0718365A2 (en) * | 1994-12-24 | 1996-06-26 | Herberts Gesellschaft mit beschränkter Haftung | Binder composition, coatings therewith and their use |
| CN1526772A (en) * | 2003-03-03 | 2004-09-08 | 珠海东诚化工有限公司 | Visible light cured woodenware paint |
| EP1616923A1 (en) * | 2004-07-13 | 2006-01-18 | Tarkett SAS | Rubber-polyolefin surface covering |
| US8268737B1 (en) * | 2005-10-04 | 2012-09-18 | Building Materials Investment Corporation | Facer and construction materials made therewith |
| CN103396689A (en) * | 2013-08-01 | 2013-11-20 | 苏州市明大高分子科技材料有限公司 | LED-UV light source curable coating and preparation method |
| CN106867393A (en) * | 2017-02-10 | 2017-06-20 | 湖南容佳新材料技术有限公司 | A kind of easy sanding priming paint of LED UV woodenware large arch dams and preparation method thereof |
| CN108753119A (en) * | 2018-06-21 | 2018-11-06 | 恒昌涂料（惠阳）有限公司 | A kind of high covering LED solidification based white primer and preparation method thereof |
-
2020
- 2020-03-23 CN CN202010206102.4A patent/CN111393963A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0718365A2 (en) * | 1994-12-24 | 1996-06-26 | Herberts Gesellschaft mit beschränkter Haftung | Binder composition, coatings therewith and their use |
| CN1526772A (en) * | 2003-03-03 | 2004-09-08 | 珠海东诚化工有限公司 | Visible light cured woodenware paint |
| EP1616923A1 (en) * | 2004-07-13 | 2006-01-18 | Tarkett SAS | Rubber-polyolefin surface covering |
| US8268737B1 (en) * | 2005-10-04 | 2012-09-18 | Building Materials Investment Corporation | Facer and construction materials made therewith |
| CN103396689A (en) * | 2013-08-01 | 2013-11-20 | 苏州市明大高分子科技材料有限公司 | LED-UV light source curable coating and preparation method |
| CN106867393A (en) * | 2017-02-10 | 2017-06-20 | 湖南容佳新材料技术有限公司 | A kind of easy sanding priming paint of LED UV woodenware large arch dams and preparation method thereof |
| CN108753119A (en) * | 2018-06-21 | 2018-11-06 | 恒昌涂料（惠阳）有限公司 | A kind of high covering LED solidification based white primer and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116284589A (en) * | 2023-04-11 | 2023-06-23 | 上饶市聚微星科技有限公司 | Photosensitive resin composition for additive manufacturing modified by black talc and preparation method thereof |
| CN116284589B (en) * | 2023-04-11 | 2024-02-20 | 上饶市聚微星科技有限公司 | Photosensitive resin composition for additive manufacturing modified by black talc and preparation method thereof |
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Application publication date: 20200710 |