Catalytic cracking slurry oil static adsorber
Technical Field
The invention belongs to the field of filtering equipment, and relates to a catalytic cracking slurry oil electrostatic adsorber.
Background
The electrostatic separation method is a novel liquid-solid separation technology developed in recent years, is suitable for a liquid-solid system with small solid particle diameter, relatively low particle concentration and relatively large liquid phase resistivity, and has the following basic principle: when a liquid stream containing particles flows through a bed of packing under the action of an electric field, the particles are polarized in the high-voltage electric field and adsorb on the packing, so that the liquid stream is purified.
Disclosure of Invention
In view of the problems in the prior art, the invention discloses a catalytic cracking slurry oil electrostatic absorber which adopts the technical scheme that the catalytic cracking slurry oil electrostatic absorber comprises a temperature-control vertical tower, a cathode cylinder is fixedly arranged in the inner cavity of the temperature-control vertical tower through a cathode cylinder fixing piece, the cathode cylinder fixing piece is fixedly connected to the side wall of the temperature-control vertical tower, the upper part of the cathode cylinder is electrically and fixedly connected with an insulated electrode, the insulated electrode extends out of the temperature-control vertical tower and is subjected to insulation treatment between the temperature-control vertical tower and the cathode cylinder, a central rod is fixedly arranged at the central shaft position of the temperature-control vertical tower, flange connecting parts are arranged on the upper end surface and the lower end surface of the temperature-control vertical tower, an upper cover plate is fixedly connected to the flange connecting part at the upper end of the temperature-control vertical tower, a glass ball replacing inlet is arranged, the device comprises a temperature control vertical tower, a cathode barrel, a purification product outlet, a backwashing nitrogen outlet, a glass ball outlet fixing part, a filling port, a backwashing waste liquid outlet and glass balls, wherein the purification product outlet and the backwashing nitrogen outlet are fixedly arranged on the side wall of the upper end of the temperature control vertical tower, the glass ball outlet fixing part is fixedly connected to the flange connecting part of the lower end of the temperature control vertical tower, the filling port and the backwashing waste liquid outlet are fixedly arranged on the side wall of the lower end.
As a preferred embodiment of the present invention, the temperature-controlled vertical tower and the central rod are electrically connected to a high-voltage positive electrode and grounded.
As a preferred scheme of the invention, the glass ball outlet fixing member comprises a sealing plate which is pressed on an opening at the lower end of the temperature-controlled vertical tower, the lower part of the sealing plate is fixedly connected with a fixing plate through a connecting bolt, the connecting bolt is in threaded fit with the sealing plate and the fixing plate, and the fixing plate is fixedly connected to a flange connecting part at the lower end of the temperature-controlled vertical tower through the fixing bolt.
As a preferable scheme of the present invention, the cathode tube fixing member is made of ceramic, the insulated electrode is electrically connected to the high voltage negative electrode, and the insulating material is a ceramic insulating sleeve.
As a preferred scheme of the invention, the glass balls filled in the tower are specially-made glass balls with the diameter of 1-8 mm.
The invention has the beneficial effects that: according to the invention, the central rod of the anode, the temperature-control vertical tower shell and the cathode cylinder are matched to form an annular polarized electric field, the polarized electric field is filled with glass balls, the high-voltage direct-current electric field can polarize the glass balls to generate countless small electric fields, so that catalyst particles in a substance to be treated can be effectively adsorbed and adsorbed on the cylinder wall and the surface of the glass balls, the catalyst has a better filtering effect, the adsorber can be cleaned through back washing operation, the selected nitrogen pulse type flushing mode can be used for efficiently cleaning the glass balls, so that the glass balls are recovered to an efficient adsorption state, the operation is simple, and the reuse can be realized.
Drawings
FIG. 1 is a cross-sectional view of the overall construction of the present invention;
FIG. 2 is a schematic cross-sectional top view of the present invention;
in the figure: 1-temperature control vertical tower, 2-cathode cylinder, 3-center rod, 4-filling port, 5-glass ball outlet fixing piece, 501-sealing plate, 502-fixing plate, 503-fixing bolt, 504-connecting bolt, 6-backwashing waste liquid outlet, 7-cathode cylinder fixing piece, 8-insulating electrode, 9-purified product outlet, 10-upper cover plate, 11-glass ball replacement inlet sealing cover plate and 12-backwashing nitrogen outlet.
Detailed Description
Example 1
As shown in figures 1 and 2, the catalytic cracking slurry oil electrostatic adsorber adopts the technical scheme that the adsorber comprises a temperature-controlled vertical tower 1, a cathode cylinder 2 is fixedly installed in an inner cavity of the temperature-controlled vertical tower 1 through a cathode cylinder fixing piece 7, the cathode cylinder fixing piece 7 is fixedly connected to the side wall of the temperature-controlled vertical tower 1, an insulated electrode 8 is electrically and fixedly connected to the upper portion of the cathode cylinder 2, the insulated electrode 8 extends out of the temperature-controlled vertical tower 1 and is subjected to insulation treatment between the temperature-controlled vertical tower 1 and the cathode cylinder, a central rod 3 is fixedly installed at the central axis position of the temperature-controlled vertical tower 1, flange connection parts are arranged on the upper end face and the lower end face of the temperature-controlled vertical tower 1, an upper cover plate 10 is fixedly connected to the flange connection part at the upper end of the temperature-controlled vertical tower 1, a glass ball replacement inlet is formed in the, the central rod 3 is fixedly connected to the upper cover plate 10, a purified product outlet 9 and a back-washing nitrogen outlet 12 are fixedly arranged on the side wall of the upper end of the temperature control vertical tower 1, a glass ball outlet fixing part 5 is fixedly connected to the flange connecting part of the lower end of the temperature control vertical tower 1, a filling port 4 and a back-washing waste liquid outlet 6 are fixedly arranged on the side wall of the lower end of the temperature control vertical tower 1, and glass balls are filled in the inner cavity of the temperature control vertical tower 1 and the inner cavity of the cathode barrel 2.
The temperature control vertical tower 1 and the central rod 3 are electrically connected with a high-voltage anode and grounded.
Glass ball export mounting 5 is in including the gland the board 501 is sealed to the open-ended of 1 lower extreme of accuse temperature vertical tower, seal the board 501 lower part and pass through connecting bolt 504 fixedly connected with fixed plate 502, connecting bolt 504 with seal the board 501 and screw-thread fit between the fixed plate 502, fixed plate 502 passes through fixing bolt 503 fixed connection and is in on the flange joint position of accuse temperature vertical tower 1 lower extreme.
The cathode cylinder fixing piece 7 is made of ceramic, the insulated electrode 8 is electrically connected with the high-voltage cathode, and the insulating material of the insulated electrode is a ceramic insulating sleeve.
The glass balls filled in the tower are specially-made glass balls with the diameter of 1 mm.
Example 2
As shown in figures 1 and 2, the catalytic cracking slurry oil electrostatic adsorber adopts the technical scheme that the adsorber comprises a temperature-controlled vertical tower 1, a cathode cylinder 2 is fixedly installed in an inner cavity of the temperature-controlled vertical tower 1 through a cathode cylinder fixing piece 7, the cathode cylinder fixing piece 7 is fixedly connected to the side wall of the temperature-controlled vertical tower 1, an insulated electrode 8 is electrically and fixedly connected to the upper portion of the cathode cylinder 2, the insulated electrode 8 extends out of the temperature-controlled vertical tower 1 and is subjected to insulation treatment between the temperature-controlled vertical tower 1 and the cathode cylinder, a central rod 3 is fixedly installed at the central axis position of the temperature-controlled vertical tower 1, flange connection parts are arranged on the upper end face and the lower end face of the temperature-controlled vertical tower 1, an upper cover plate 10 is fixedly connected to the flange connection part at the upper end of the temperature-controlled vertical tower 1, a glass ball replacement inlet is formed in the, the central rod 3 is fixedly connected to the upper cover plate 10, a purified product outlet 9 and a back-washing nitrogen outlet 12 are fixedly arranged on the side wall of the upper end of the temperature control vertical tower 1, a glass ball outlet fixing part 5 is fixedly connected to the flange connecting part of the lower end of the temperature control vertical tower 1, a filling port 4 and a back-washing waste liquid outlet 6 are fixedly arranged on the side wall of the lower end of the temperature control vertical tower 1, and glass balls are filled in the inner cavity of the temperature control vertical tower 1 and the inner cavity of the cathode barrel 2.
The temperature control vertical tower 1 and the central rod 3 are electrically connected with a high-voltage anode and grounded.
Glass ball export mounting 5 is in including the gland the board 501 is sealed to the open-ended of 1 lower extreme of accuse temperature vertical tower, seal the board 501 lower part and pass through connecting bolt 504 fixedly connected with fixed plate 502, connecting bolt 504 with seal the board 501 and screw-thread fit between the fixed plate 502, fixed plate 502 passes through fixing bolt 503 fixed connection and is in on the flange joint position of accuse temperature vertical tower 1 lower extreme.
The cathode cylinder fixing piece 7 is made of ceramic, the insulated electrode 8 is electrically connected with the high-voltage cathode, and the insulating material of the insulated electrode is a ceramic insulating sleeve.
The glass balls filled in the tower are specially-made glass balls with the diameter of 6 mm.
Example 3
As shown in figures 1 and 2, the catalytic cracking slurry oil electrostatic adsorber adopts the technical scheme that the adsorber comprises a temperature-controlled vertical tower 1, a cathode cylinder 2 is fixedly installed in an inner cavity of the temperature-controlled vertical tower 1 through a cathode cylinder fixing piece 7, the cathode cylinder fixing piece 7 is fixedly connected to the side wall of the temperature-controlled vertical tower 1, an insulated electrode 8 is electrically and fixedly connected to the upper portion of the cathode cylinder 2, the insulated electrode 8 extends out of the temperature-controlled vertical tower 1 and is subjected to insulation treatment between the temperature-controlled vertical tower 1 and the cathode cylinder, a central rod 3 is fixedly installed at the central axis position of the temperature-controlled vertical tower 1, flange connection parts are arranged on the upper end face and the lower end face of the temperature-controlled vertical tower 1, an upper cover plate 10 is fixedly connected to the flange connection part at the upper end of the temperature-controlled vertical tower 1, a glass ball replacement inlet is formed in the, the central rod 3 is fixedly connected to the upper cover plate 10, a purified product outlet 9 and a back-washing nitrogen outlet 12 are fixedly arranged on the side wall of the upper end of the temperature control vertical tower 1, a glass ball outlet fixing part 5 is fixedly connected to the flange connecting part of the lower end of the temperature control vertical tower 1, a filling port 4 and a back-washing waste liquid outlet 6 are fixedly arranged on the side wall of the lower end of the temperature control vertical tower 1, and glass balls are filled in the inner cavity of the temperature control vertical tower 1 and the inner cavity of the cathode barrel 2.
The temperature control vertical tower 1 and the central rod 3 are electrically connected with a high-voltage anode and grounded.
Glass ball export mounting 5 is in including the gland the board 501 is sealed to the open-ended of 1 lower extreme of accuse temperature vertical tower, seal the board 501 lower part and pass through connecting bolt 504 fixedly connected with fixed plate 502, connecting bolt 504 with seal the board 501 and screw-thread fit between the fixed plate 502, fixed plate 502 passes through fixing bolt 503 fixed connection and is in on the flange joint position of accuse temperature vertical tower 1 lower extreme.
The cathode cylinder fixing piece 7 is made of ceramic, the insulated electrode 8 is electrically connected with the high-voltage cathode, and the insulating material of the insulated electrode is a ceramic insulating sleeve.
The glass balls filled in the tower are specially-made glass balls with the diameter of 4 mm.
The working principle of the invention is as follows: the glass ball replacing inlet sealing cover plate 11 is opened to fill the glass balls into the whole adsorber, after the adsorber is electrified, the temperature control vertical tower 1 and the central rod 3 are used as the anode, the cathode cylinder 2 is used as the cathode, a polarized electric field is formed in the inner cavity of the whole temperature control vertical tower 1, raw materials to be filtered are injected into the inner cavity of the temperature control vertical tower 1 through the filling port 4, catalysts in the raw materials are adsorbed to the cylinder wall and the surfaces of the glass balls under the action of the electric field, and the filtered raw materials are discharged through the purification product outlet 9. When the device needs to be backwashed, a high-voltage power supply is disconnected, a purification product outlet 9 and a backwash waste liquid outlet 6 are closed, the filtered raw material product is used as a backwashing raw material, the inner cavity of the whole temperature control vertical tower 1 is immersed, nitrogen is injected into the backwashing vertical tower through a filling port 4, the used nitrogen pressure difference is 0.5-1.1MPa, the filling mode of the nitrogen is a pulse mode, a strand of nitrogen is sprayed every ten seconds, the backwashing raw material is disturbed by the nitrogen, catalyst particles can fall off from glass balls, the nitrogen is discharged from a backwash nitrogen outlet 12, the filling port 4 is closed after the backwashing is completed, the waste liquid is discharged after the backwash waste liquid outlet 6 is opened, the glass balls can be recovered to a high-efficiency adsorption state, and the adsorption and filtration work can be continued. When the glass balls in the temperature-controlled vertical tower 1 need to be taken out, the sealing plate 501 can be opened by rotating the connecting bolt 504, and the glass balls can be discharged from the opening at the lower end of the temperature-controlled vertical tower 1.
Components and circuit connections not described in detail herein are prior art.
Although the present invention has been described in detail with reference to the specific embodiments, the present invention is not limited to the above embodiments, and various changes and modifications without inventive changes may be made within the knowledge of those skilled in the art without departing from the spirit of the present invention.