CN111344429B - 铁基烧结合金材料及其制造方法 - Google Patents

铁基烧结合金材料及其制造方法 Download PDF

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Publication number: CN111344429B
Authority: CN; China
Prior art keywords: iron; based sintered; sintered alloy; quenching; nitriding
Prior art date: 2017-11-10
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Active

Application number

CN201880072656.0A

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English (en)

Chinese (zh)

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CN111344429A (zh

Inventor

大守洋

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Resonac Corp

Original Assignee

Showa Denko KK

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2017-11-10

Filing date

2018-11-09

Publication date

2022-11-15

2018-11-09 Application filed by Showa Denko KK filed Critical Showa Denko KK

2018-11-09 Priority to CN202211337786.7A priority Critical patent/CN115595530A/zh

2020-06-26 Publication of CN111344429A publication Critical patent/CN111344429A/zh

2022-11-15 Application granted granted Critical

2022-11-15 Publication of CN111344429B publication Critical patent/CN111344429B/zh

Status Active legal-status Critical Current

2038-11-09 Anticipated expiration legal-status Critical

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XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims abstract description 247
239000000956 alloy Substances 0.000 title claims abstract description 151
229910052742 iron Inorganic materials 0.000 title claims abstract description 124
238000004519 manufacturing process Methods 0.000 title claims abstract description 20
238000005121 nitriding Methods 0.000 claims abstract description 100
238000010791 quenching Methods 0.000 claims abstract description 96
230000000171 quenching effect Effects 0.000 claims abstract description 96
239000000463 material Substances 0.000 claims abstract description 49
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 33
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 28
238000010438 heat treatment Methods 0.000 claims abstract description 22
229910052750 molybdenum Inorganic materials 0.000 claims abstract description 20
ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 18
239000011651 chromium Substances 0.000 claims abstract description 18
239000011733 molybdenum Substances 0.000 claims abstract description 18
229910052804 chromium Inorganic materials 0.000 claims abstract description 16
239000010949 copper Substances 0.000 claims abstract description 15
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 14
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 14
229910052759 nickel Inorganic materials 0.000 claims abstract description 14
239000012298 atmosphere Substances 0.000 claims abstract description 13
229910052802 copper Inorganic materials 0.000 claims abstract description 13
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 11
238000000034 method Methods 0.000 claims abstract description 11
WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims abstract description 5
229910045601 alloy Inorganic materials 0.000 claims description 97
239000000758 substrate Substances 0.000 claims description 32
238000005496 tempering Methods 0.000 claims description 13
238000005275 alloying Methods 0.000 claims description 12
239000011812 mixed powder Substances 0.000 claims description 10
238000001816 cooling Methods 0.000 claims description 7
230000001590 oxidative effect Effects 0.000 claims description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 72
229910052757 nitrogen Inorganic materials 0.000 abstract description 32
229910052799 carbon Inorganic materials 0.000 abstract description 27
229910000734 martensite Inorganic materials 0.000 abstract description 13
239000006104 solid solution Substances 0.000 abstract description 12
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract 1
229910052737 gold Inorganic materials 0.000 abstract 1
239000010931 gold Substances 0.000 abstract 1
239000000843 powder Substances 0.000 description 43
238000005255 carburizing Methods 0.000 description 41
239000010410 layer Substances 0.000 description 41
239000000203 mixture Substances 0.000 description 32
239000007789 gas Substances 0.000 description 29
229910000831 Steel Inorganic materials 0.000 description 24
239000010959 steel Substances 0.000 description 24
239000002994 raw material Substances 0.000 description 19
238000005245 sintering Methods 0.000 description 16
239000011572 manganese Substances 0.000 description 11
239000000047 product Substances 0.000 description 11
229910052748 manganese Inorganic materials 0.000 description 9
238000000465 moulding Methods 0.000 description 9
239000011148 porous material Substances 0.000 description 9
238000001878 scanning electron micrograph Methods 0.000 description 9
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 8
229910017112 Fe—C Inorganic materials 0.000 description 7
229910001566 austenite Inorganic materials 0.000 description 7
238000009792 diffusion process Methods 0.000 description 6
239000012535 impurity Substances 0.000 description 6
239000007769 metal material Substances 0.000 description 6
239000003921 oil Substances 0.000 description 6
229910000975 Carbon steel Inorganic materials 0.000 description 5
239000010962 carbon steel Substances 0.000 description 5
239000001257 hydrogen Substances 0.000 description 5
229910052739 hydrogen Inorganic materials 0.000 description 5
239000000314 lubricant Substances 0.000 description 5
150000004767 nitrides Chemical class 0.000 description 5
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
229910001873 dinitrogen Inorganic materials 0.000 description 4
239000007788 liquid Substances 0.000 description 4
238000005259 measurement Methods 0.000 description 4
229910001220 stainless steel Inorganic materials 0.000 description 4
230000009466 transformation Effects 0.000 description 4
230000008859 change Effects 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 3
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238000005516 engineering process Methods 0.000 description 3
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230000006872 improvement Effects 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
239000002184 metal Substances 0.000 description 3
DDTIGTPWGISMKL-UHFFFAOYSA-N molybdenum nickel Chemical compound [Ni].[Mo] DDTIGTPWGISMKL-UHFFFAOYSA-N 0.000 description 3
238000012545 processing Methods 0.000 description 3
239000000126 substance Substances 0.000 description 3
239000002344 surface layer Substances 0.000 description 3
229910000851 Alloy steel Inorganic materials 0.000 description 2
229910000640 Fe alloy Inorganic materials 0.000 description 2
229910017116 Fe—Mo Inorganic materials 0.000 description 2
229910017263 Mo—C Inorganic materials 0.000 description 2
PCEXQRKSUSSDFT-UHFFFAOYSA-N [Mn].[Mo] Chemical compound [Mn].[Mo] PCEXQRKSUSSDFT-UHFFFAOYSA-N 0.000 description 2
229910052786 argon Inorganic materials 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
VNTLIPZTSJSULJ-UHFFFAOYSA-N chromium molybdenum Chemical compound [Cr].[Mo] VNTLIPZTSJSULJ-UHFFFAOYSA-N 0.000 description 2
150000002431 hydrogen Chemical class 0.000 description 2
239000011261 inert gas Substances 0.000 description 2
150000002505 iron Chemical class 0.000 description 2
239000011159 matrix material Substances 0.000 description 2
238000012986 modification Methods 0.000 description 2
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239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
239000002245 particle Substances 0.000 description 2
239000012466 permeate Substances 0.000 description 2
238000001556 precipitation Methods 0.000 description 2
238000011084 recovery Methods 0.000 description 2
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238000005096 rolling process Methods 0.000 description 2
238000004513 sizing Methods 0.000 description 2
239000010936 titanium Substances 0.000 description 2
238000007088 Archimedes method Methods 0.000 description 1
229910000967 As alloy Inorganic materials 0.000 description 1
229910001339 C alloy Inorganic materials 0.000 description 1
UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
229910002551 Fe-Mn Inorganic materials 0.000 description 1
229910001021 Ferroalloy Inorganic materials 0.000 description 1
229910000617 Mangalloy Inorganic materials 0.000 description 1
229910017309 Mo—Mn Inorganic materials 0.000 description 1
229910017318 Mo—Ni Inorganic materials 0.000 description 1
229910018487 Ni—Cr Inorganic materials 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
229910001315 Tool steel Inorganic materials 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
230000008901 benefit Effects 0.000 description 1
230000005540 biological transmission Effects 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical class [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 1
229910002091 carbon monoxide Inorganic materials 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
OGSYQYXYGXIQFH-UHFFFAOYSA-N chromium molybdenum nickel Chemical compound [Cr].[Ni].[Mo] OGSYQYXYGXIQFH-UHFFFAOYSA-N 0.000 description 1
VNNRSPGTAMTISX-UHFFFAOYSA-N chromium nickel Chemical compound [Cr].[Ni] VNNRSPGTAMTISX-UHFFFAOYSA-N 0.000 description 1
239000003034 coal gas Substances 0.000 description 1
238000000748 compression moulding Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
229910003460 diamond Inorganic materials 0.000 description 1
239000010432 diamond Substances 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000005530 etching Methods 0.000 description 1
230000001747 exhibiting effect Effects 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000008595 infiltration Effects 0.000 description 1
238000001764 infiltration Methods 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
QMQXDJATSGGYDR-UHFFFAOYSA-N methylidyneiron Chemical compound [C].[Fe] QMQXDJATSGGYDR-UHFFFAOYSA-N 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
230000035515 penetration Effects 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
230000001737 promoting effect Effects 0.000 description 1
102200082816 rs34868397 Human genes 0.000 description 1
238000007493 shaping process Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
239000000243 solution Substances 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
238000005728 strengthening Methods 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1
229910052719 titanium Inorganic materials 0.000 description 1
LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

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- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
- C—CHEMISTRY; METALLURGY
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- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D2211/00—Microstructure comprising significant phases
- C21D2211/008—Martensite
- C—CHEMISTRY; METALLURGY
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- C22C—ALLOYS
- C22C33/00—Making ferrous alloys
- C22C33/02—Making ferrous alloys by powder metallurgy
- C22C33/0257—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements
- C22C33/0264—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements the maximum content of each alloying element not exceeding 5%

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CN201880072656.0A 2017-11-10 2018-11-09 铁基烧结合金材料及其制造方法 Active CN111344429B (zh)

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TWI726451B (zh) *	2019-10-21	2021-05-01	晟銘電子科技股份有限公司	具有滲氮層的成型體的製備方法及其成型體
CN112475304B (zh) *	2020-12-09	2021-09-28	福州大学	一种基于放电等离子烧结的12Cr不锈钢表面强化方法
JP2022126017A (ja) *	2021-02-18	2022-08-30	株式会社日立製作所	摺動部材並びにその製造方法及び製造装置
KR102586490B1 (ko) *	2021-08-13	2023-10-06	현대자동차주식회사	아우터링 및 아우터링을 제조하는 방법

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US20230211413A1 (en)	2023-07-06
US20200331068A1 (en)	2020-10-22
JP7167428B2 (ja)	2022-11-09
CN115595530A (zh)	2023-01-13
CN111344429A (zh)	2020-06-26
WO2019093480A1 (ja)	2019-05-16
JP2019085634A (ja)	2019-06-06

Publication	Publication Date	Title
CN111344429B (zh)	2022-11-15	铁基烧结合金材料及其制造方法
JP5671526B2 (ja)	2015-02-18	高強度低合金焼結鋼
RU2699882C2 (ru)	2019-09-11	Предварительно легированный порошок на основе железа, порошковая смесь на основе железа, содержащая предварительно легированный порошок на основе железа, и способ изготовления прессованных и спеченных деталей из порошковой смеси на основе железа
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