CN1112610A - Mulberry fibre, its producing method and application - Google Patents
Mulberry fibre, its producing method and application Download PDFInfo
- Publication number
- CN1112610A CN1112610A CN 95114898 CN95114898A CN1112610A CN 1112610 A CN1112610 A CN 1112610A CN 95114898 CN95114898 CN 95114898 CN 95114898 A CN95114898 A CN 95114898A CN 1112610 A CN1112610 A CN 1112610A
- Authority
- CN
- China
- Prior art keywords
- mulberry
- fiber
- bath raio
- fibre
- minutes
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 28
- 240000000249 Morus alba Species 0.000 title claims abstract description 18
- 235000008708 Morus alba Nutrition 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 13
- 239000000126 substance Substances 0.000 claims abstract description 4
- 239000004753 textile Substances 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 3
- 238000004806 packaging method and process Methods 0.000 claims abstract description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 19
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 16
- 239000003054 catalyst Substances 0.000 claims description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 5
- 239000000460 chlorine Substances 0.000 claims description 5
- 229910052801 chlorine Inorganic materials 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 210000002615 epidermis Anatomy 0.000 claims description 4
- 238000005554 pickling Methods 0.000 claims description 4
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 2
- 240000006248 Broussonetia kazinoki Species 0.000 claims 1
- -1 bath raio 1: 12~16 Chemical compound 0.000 claims 1
- 229920000742 Cotton Polymers 0.000 abstract description 6
- 239000002253 acid Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000002932 luster Substances 0.000 abstract 1
- 238000007670 refining Methods 0.000 abstract 1
- 241000894007 species Species 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- 238000005406 washing Methods 0.000 description 10
- 238000010009 beating Methods 0.000 description 4
- 241000933832 Broussonetia Species 0.000 description 3
- 238000006298 dechlorination reaction Methods 0.000 description 3
- 238000011010 flushing procedure Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 210000003491 skin Anatomy 0.000 description 3
- 238000009960 carding Methods 0.000 description 2
- 239000003752 hydrotrope Substances 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- QUCDWLYKDRVKMI-UHFFFAOYSA-M sodium;3,4-dimethylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1C QUCDWLYKDRVKMI-UHFFFAOYSA-M 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000218231 Moraceae Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 210000001520 comb Anatomy 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 1
- 235000019801 trisodium phosphate Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention is a mulberry skin fiber and the manufacturing method. The average length of the mulberry fiber is 31.50mm. The length C and V is 33.95 percent. The fracture strength is 5.30CN/dtex. The method comprises the processes of skin-removing, chemical boiling and refining, mechanical production, rinsing, acid cleaning, softness increasing, drying, combing, packaging and so on. The products of the invention are superior to or similar with the property of cotton fiber and have the luster of silk, but the cost is only half of that of the cotton fiber. The invention expands a new domain of natural fiber, adds new species of textile fiber, and initiates a new way of utilizing mulberry skin resources.
Description
The invention relates to mulberry fibre and preparation method thereof, more particularly about from paper mulberry bark, extracting textile fiber material-mulberry fibre and preparation method thereof.
Mulberry tree belongs to Moraceae, is deciduous tree, and its branch is made up of bast and cane two parts, and bast fiber content is up to 57.5%, and 1,200 ten thousand mu in mulberry is planted by China, and resource is extremely abundant, uses but generally only make fuel or vegetables hack lever at present.
Along with the progress of society, science and technology development, the shortage of natural resources force people to seek new resources, new varieties, and increasing people has recognized the importance of paper mulberry bark, use but generally all make paper making raw material at present.
One of purpose of the present invention provides a kind of mulberry fibre that supplies textile raw material to use.
Two of purpose of the present invention provides a kind of method of extracting mulberry fibre from paper mulberry bark.
These and other objects of the present invention will further be set forth and illustrate by following detailed description.
In the present invention, method of the present invention comprises to be removed that epidermis, chemical boiling-off, machinery are produced, rinsing, pickling, increases gentle, dry, combing, packaging and other steps, and the prepared mulberry fibre that goes out has following feature at least:
Average length 31.50mm
Length C, V 33.95%
The following fiber 7.95% of 16mm
Public of line density 2.86dtex(3500)
Fracture strength 5.30CN/dtex
Ultimate strength 15.15CN
Powerful C, V 10.35CN
Than resistance Ω 1.20 * 10
8
As can be seen from the table, product of the present invention has the performance that is better than or is similar to cotton fiber, and gloss with natural silk, but price only is cotton fiber half, the present invention has increased new varieties again for natural fabric family, for saving cotton resource, utilize Ramulus Mori to start a new way.
Further, in the method for the invention, remove epidermis and can adopt Mechanical Method, promptly crumple and add wind epidermis is removed with the machine of allowancing for bark.Can also use microbial method, promptly in water with the raw material submergence, meet bacterial classification such as T with 44 ℃ water temperatures
66(biological institute of Chinese Academy of Sciences product) took out fully washing after 2 hours.The chemistry boiling-off can utilize NaOH, and bath raio 1: 12～16 is preferably 1: 14, concentration sodium hydroxide 7～12g/L adds catalyst JF2g/L, fully dissolving, 100 ℃ of normal pressures in 1.5～2 hours processing times, utilize the dual impulse force of machinery and water under high pressure to clean then.Rinsing can be used clorox, and concentration is available chlorine content 0.5～0.8g/L, and bath raio 1: 10～20 is preferably 15, and normal temperature was handled 15～20 minutes down.
Pickling in the present invention can be used sulfuric acid; bath raio 1: 15～25, better is 1: 20, and concentration is 0.3g/L; 10～20 minutes time; better be 15 minutes, fully be washed to neutrality, increases gentle step and can use the HS softener; consumption be 2.5%(and fiber than); bath raio is 1: 8, and temperature is 70～90 ℃, 1.5～3 hours time; then with centrifuge dewatering to moisture content below 53～55%; then drying makes product moisture content 8-11%, and dry back is cloudy supports, the cloudy phase spray HS softener of supporting; content is 2～2.5%(and fiber ratio); humidity is 15～18%, 5～8 days time, combs into filament with numb cotton carding machine then.
In the present invention, all parts, amount are unit of weight, and used equipment comprises beating to be washed machine, centrifuge, carding machine etc. and all can buy from market, and all industrial chemicals all can be bought from Heze, Shandong spark technology research institute.
Below further specify the present invention by specific embodiment, but embodiment only be used for the explanation, can not limit the scope of the invention.
Example 1
With the mulberry skin 100Kg behind the machine barking, normal temperature immersion 1.5 hours, the flush away hydrotrope is stand-by then.Put into the water of 1400Kg in 1: 14 ratio of bath raio, 9Kg NaOH, 2.8KgJF catalyst, stirred evenly the Ramulus Mori boiling-off of putting into after the dissolving after the washing 1.5 hours, utilizing garden dish or straight line to beat the machine of washing and high pressure warm water then beats and washed flushing 4 circles about 6 minutes, the product of beating after washing is taken out the water in 1: 15 ratio of bath raio adding 1500Kg, the 30Kg clorox, normal temperature was handled 15 minutes, floated afterwash, and then added sulfuric acid; bath raio 1: 20; 2000 kilograms in water, sulfuric acid consumption are 0.3g/L, handled 15 minutes to remove chlorine remaining in the fiber; To put into the soft treatment pot behind the fiber dewatering after the dechlorination, add the water of 800Kg, the softener HS of 2.5Kg under 70 ℃ of temperature, handles and finished soft step in 1.5 hours; Pull out then and put into centrifuge dewatering to moisture below 53%, send into hothouse and be dried to moisturely 8%, take out and carry Zhiyin to support the chamber to spray the HS softener simultaneously and reach 2%, humidity can be carried out combing in 15%, 5 day, combed into filament and can pack and dispatch from the factory.
Example 2
With the mulberry skin 100Kg behind the machine barking, normal temperature immersion 2 hours, the flush away hydrotrope is stand-by then.Put into the water of 1400Kg in 1: 14 ratio of bath raio, 7Kg NaOH, the 2KgJF catalyst, 0.28C catalyst, stirred evenly the Ramulus Mori boiling-off of putting into after the dissolving after the washing 2 hours, utilizing garden dish or straight line to beat the machine of washing and high pressure warm water then beats and washed flushing 4 circles about 6 minutes, the product of beating after washing is taken out the water in 1: 15 ratio of bath raio adding 1500Kg, the 20Kg clorox, normal temperature was handled 20 minutes, float afterwash, and then add sulfuric acid, bath raio 1: 20,2000 kilograms in water, the sulfuric acid consumption is 0.3g/L, handles 15 minutes to remove chlorine remaining in the fiber; To put into the soft treatment pot behind the fiber dewatering after the dechlorination, add the water of 800Kg, the softener HS of 2.5Kg under 75 ℃ of temperature, handles and finished soft step in 3 hours; Pull out then and put into centrifuge dewatering to moisture below 55%, send into hothouse and be dried to moisturely 12%, take out and carry Zhiyin to support the chamber to spray the HS softener simultaneously and reach 2.5%, humidity can be carried out combing in 18%, 5～7 days, combed into filament and can pack and dispatch from the factory.
Example 3
With mulberry skin 100Kg, immerse in the inoculation liquid, in 0.3% trisodium phosphate solution, temperature is 42 ℃, adds t bacteria by 15% of product volume
66, 40 ℃ of mixing insulations, 6 hours time, be warming up to 55 ℃ then, to soak and finish fermentation after 1 hour, effluent discharge waits usefulness.Put into the water of 1400Kg in 1: 14 ratio of bath raio, 6Kg NaOH, 1.5KgJF catalyst, stirred evenly the Ramulus Mori boiling-off of putting into after the dissolving after the washing 1.5～2 hours, utilizing garden dish or straight line to beat the machine of washing and high pressure warm water then beats and washed flushing 4 circles about 6 minutes, the product of beating after washing is taken out the water in 1: 15 ratio of bath raio adding 1500Kg, 15Kg time
Acid sodium, normal temperature was handled 18 minutes, floated afterwash, and then added sulfuric acid, bath raio 1: 20,2000 kilograms in water, sulfuric acid consumption are 0.3g/L, handle 15 minutes to remove chlorine remaining in the fiber; To put into the soft treatment pot behind the fiber dewatering after the dechlorination, add the water of 800Kg, the softener HS of 2.5Kg under 80 ℃ of temperature, handles and finished soft step in 3 hours; Pull out then and put into centrifuge dewatering to moisture below 54%, send into hothouse and be dried to moisturely 10%, take out and carry Zhiyin to support the chamber to spray the HS softener simultaneously and reach 2.3%, humidity can be carried out combing in 17%, 7 day, combed into filament and can pack and dispatch from the factory.
Claims (8)
1, a kind of mulberry fibre is characterized in that average length is 31.50mm, and length C, V are 33.95%, and fracture strength is 5.30CN/dtex, and ultimate strength is 15.15CN.
2, a kind of preparation method of mulberry fibre is characterized in that comprising and removes that epidermis, chemical boiling-off, machinery are produced, rinsing, pickling, increases gentle, dry, combing, packaging and other steps.
3, method as claimed in claim 2 is characterized in that chemical boiling-off can utilize NaOH, bath raio 1: 12～16, and naoh concentration is 7～12g/L, adds catalyst JF2g/L, fully dissolving, 1.5～2 hours processing times.
4, method as claimed in claim 2 is characterized in that rinsing can utilize clorox, and concentration is available chlorine content 0.5～0.8g/L, bath raio 1: 10～20, and normal temperature was handled 15～30 minutes.
5, method as claimed in claim 2 is characterized in that pickling can use sulfuric acid, and bath raio 1: 15～25, concentration are 0.3g/L, and the time is 10～20 minutes, fully is washed to neutrality then.
6, method as claimed in claim 2 is characterized in that increasing softening and can use the HS softener, and consumption is 2.5%(and fibre weight ratio), bath raio is 1: 8, temperature is 70～90 ℃, 1.5～3 hours time.
7, method as claimed in claim 2, it is characterized in that increasing product after gentle with centrifuge dewatering to moisture content below 53～55%, then drying makes product moisture content 8～11%, dry back is cloudy supports, the cloudy phase spray HS softener of supporting, content is 2～2.5%(and fibre weight ratio), humidity is 15～18%, 5～8 days time.
8, mulberry fibre as claimed in claim 1 is characterized in that this kind mulberry fibre is to extract, and can be made for the usefulness of textile fabric from paper mulberry bark.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95114898 CN1112610A (en) | 1995-04-28 | 1995-04-28 | Mulberry fibre, its producing method and application |
| CN 95117638 CN1048763C (en) | 1995-04-28 | 1995-11-08 | Mulberry bark fibre and preparing process and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95114898 CN1112610A (en) | 1995-04-28 | 1995-04-28 | Mulberry fibre, its producing method and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1112610A true CN1112610A (en) | 1995-11-29 |
Family
ID=5080376
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 95114898 Pending CN1112610A (en) | 1995-04-28 | 1995-04-28 | Mulberry fibre, its producing method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1112610A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100415954C (en) * | 2005-04-19 | 2008-09-03 | 天维纺织科技(深圳)有限公司 | Cotton stalk bark fiber and processing method therefor |
| CN100415955C (en) * | 2005-04-19 | 2008-09-03 | 天维纺织科技(深圳)有限公司 | Tree bast fiber and processing method therefor |
| CN101831740A (en) * | 2010-05-21 | 2010-09-15 | 盐城纺织职业技术学院 | Mulberry fiber and viscose-based chitin fiber blended yarn and processing technique thereof |
| CN101634049B (en) * | 2009-08-28 | 2012-04-18 | 广西绢麻纺织科学研究所 | Method for quickly separating bast surface layer of mulberry twig |
| CN104032380A (en) * | 2014-06-30 | 2014-09-10 | 滁州惠智科技服务有限公司 | Preparation method of mulberry bark fibers |
| CN105386133A (en) * | 2014-06-30 | 2016-03-09 | 耿云花 | Preparation method of cotton stalk bark fiber |
| CN107419341A (en) * | 2017-07-06 | 2017-12-01 | 温美群 | A kind of mulberry tree barking method |
| CN112030236A (en) * | 2020-08-30 | 2020-12-04 | 塔里木大学 | A kind of method for preparing Xinjiang catalpa fruit fiber |
-
1995
- 1995-04-28 CN CN 95114898 patent/CN1112610A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100415954C (en) * | 2005-04-19 | 2008-09-03 | 天维纺织科技(深圳)有限公司 | Cotton stalk bark fiber and processing method therefor |
| CN100415955C (en) * | 2005-04-19 | 2008-09-03 | 天维纺织科技(深圳)有限公司 | Tree bast fiber and processing method therefor |
| CN101634049B (en) * | 2009-08-28 | 2012-04-18 | 广西绢麻纺织科学研究所 | Method for quickly separating bast surface layer of mulberry twig |
| CN101831740A (en) * | 2010-05-21 | 2010-09-15 | 盐城纺织职业技术学院 | Mulberry fiber and viscose-based chitin fiber blended yarn and processing technique thereof |
| CN104032380A (en) * | 2014-06-30 | 2014-09-10 | 滁州惠智科技服务有限公司 | Preparation method of mulberry bark fibers |
| CN105154997A (en) * | 2014-06-30 | 2015-12-16 | 耿云花 | Preparing method for mulberry fibers |
| CN105386133A (en) * | 2014-06-30 | 2016-03-09 | 耿云花 | Preparation method of cotton stalk bark fiber |
| CN104032380B (en) * | 2014-06-30 | 2016-10-26 | 宁夏康诚机电产品设计有限公司 | A kind of preparation method of mulberry fibre |
| CN107419341A (en) * | 2017-07-06 | 2017-12-01 | 温美群 | A kind of mulberry tree barking method |
| CN112030236A (en) * | 2020-08-30 | 2020-12-04 | 塔里木大学 | A kind of method for preparing Xinjiang catalpa fruit fiber |
| CN112030236B (en) * | 2020-08-30 | 2023-01-24 | 塔里木大学 | Method for preparing Xinjiang catalpa fruit fiber |
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