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CN110951603A - A rapid detection device for water quality - Google Patents

A rapid detection device for water quality Download PDF

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Publication number
CN110951603A
CN110951603A CN201911314024.3A CN201911314024A CN110951603A CN 110951603 A CN110951603 A CN 110951603A CN 201911314024 A CN201911314024 A CN 201911314024A CN 110951603 A CN110951603 A CN 110951603A
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China
Prior art keywords
detection
light
detection unit
water quality
liquid channel
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CN201911314024.3A
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Chinese (zh)
Inventor
孙吉勇
梁凤飞
沈玮栋
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Sujing Group Automation Instrument Equipment Corp
Jiangsu Sujing Group Co Ltd
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Sujing Group Automation Instrument Equipment Corp
Jiangsu Sujing Group Co Ltd
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Priority to CN201911314024.3A priority Critical patent/CN110951603A/en
Publication of CN110951603A publication Critical patent/CN110951603A/en
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12MAPPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
    • C12M41/00Means for regulation, monitoring, measurement or control, e.g. flow regulation
    • C12M41/30Means for regulation, monitoring, measurement or control, e.g. flow regulation of concentration
    • C12M41/36Means for regulation, monitoring, measurement or control, e.g. flow regulation of concentration of biomass, e.g. colony counters or by turbidity measurements

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • Sustainable Development (AREA)
  • Biotechnology (AREA)
  • Biomedical Technology (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Analytical Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Optical Measuring Cells (AREA)

Abstract

The invention discloses a water quality rapid detection device, which comprises a flow cell, a liquid channel which is positioned in the flow cell and is used for liquid to pass through, a light source for generating light, a collimating lens for converging the light to the liquid channel and a photoelectric detector, wherein the photoelectric detector comprises a first detection unit for collecting the light penetrating through a detection light spot and generating a first electric signal, a second detection unit for collecting the light scattered by the detection light spot and generating a second electric signal and a detection circuit for analyzing the first electric signal and the second electric signal respectively and calculating the concentration and the particle size of particles in the liquid at the light spot, when water flows through the flow cell, the invention can continuously detect the concentration of real-time microorganisms, and when the number of certain microorganisms in water is suddenly increased, the number of the particles in the corresponding particle size range is also suddenly increased, therefore, can detect and early warning control the microorganism quantity in the aquatic through this practicality.

Description

Quick water quality detection device
Technical Field
The invention relates to the field of water quality monitoring, in particular to a water quality rapid detection device based on a particle counting principle.
Background
Water pollution and water quality detection are important contents for environmental management. The parameter factors of water pollution are many, and the microbial pollution is a very key index. The number of microorganisms such as cryptosporidium, giardia, escherichia coli and the like in the self-contained water is usually required to be controlled to eliminate potential harm and ensure the safety of drinking water.
Typically cryptosporidium has a size of around 5 microns and giardia has a size of around 10 microns, whereas most bacteria typically have a size between 0.5 and 5 microns and cannot be observed by the naked eye.
The existing bacteria detection is generally performed by culturing bacteria and then counting cultured colonies. This method is very time consuming and not suitable for rapid detection on site. When a sudden bacterial contamination accident occurs, the method is useless. Real-time rapid and low-cost detection schemes for bacteria have been the direction of continuous efforts of researchers.
Therefore, there is a need for a water quality monitoring device that can quickly monitor the condition of microorganisms in water.
Disclosure of Invention
The invention aims to provide a water quality detection device capable of rapidly monitoring the condition of microorganisms in water.
In order to achieve the purpose, the invention adopts the technical scheme that: the utility model provides a quality of water short-term test device, its includes the flow cell, is located be the liquid channel that supplies liquid to pass through in the flow cell, produce the light source of light, will light assembles to liquid channel's collimating lens and photoelectric detector, collimating lens assembles the light that the light source produced to liquid channel, liquid in the liquid channel is in form a detection facula under the shining of light, photoelectric detector pierces through including the collection detect the light of facula and produce the first detecting element of first signal of telecommunication, collect detect facula scattered light and produce the second detecting element of the second signal of telecommunication and analyze respectively first signal of telecommunication with the second signal of telecommunication calculates particulate matter concentration and particle size's detection circuitry in the liquid of facula department.
Preferably, the photodetector is an array detector, and the first detection unit and the second detection unit are part of pixels of the array detector.
Further preferably, the flow cell has a flat first outer wall, the first outer wall is perpendicular to the liquid channel, and the photodetector is attached and fixed to the first outer wall.
Further preferably, the first detection unit and the first detection unit are both rectangular pixels, and two pixels of the second detection unit are respectively arranged on the side edges of the two opposite sides of the first detection unit.
Further preferably, a longitudinal direction of the first detection unit and a longitudinal direction of the liquid passage are perpendicular to each other.
Further preferably, the flow cell further has a second outer wall parallel to the first outer wall, and the light passes through the collimating lens and then enters the flow cell perpendicularly to the second outer wall.
Further preferably, the light passes through the liquid channel and then enters the first detection unit.
Further preferably, part of the scattered light generated after the light is incident into the liquid channel is incident into the second detection unit.
Preferably, the first detection unit has a measurement range of 5 to 100 micrometers.
Preferably, the second detection unit has a measurement range of 0.3 to 5 micrometers.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages:
1. according to the invention, the first detection unit and the second detection unit are arranged, so that the concentration of microorganisms with larger diameters is monitored by the first detection unit, and the concentration of microorganisms with smaller diameters is monitored by the second detection unit, thereby covering the range of the sizes of microorganisms to be detected in tap water detection.
2. When water flows through the flow-through cell, the invention can continuously detect the concentration of real-time microorganisms, and when the quantity of certain microorganisms in water is increased suddenly, the quantity of particles in the corresponding particle size range is increased suddenly, so that the quantity of microorganisms in water can be detected and early-warning monitored by the utility model.
3. The invention directly and closely attaches the array detector on the surface of the flow cell, has simple structure, convenient realization and low cost.
Drawings
FIG. 1 is a schematic diagram of the principle of the present invention;
FIG. 2 is a schematic diagram of the detection principle of the present invention;
FIG. 3 is a surface pixel distribution diagram of an array detector;
fig. 4 is a schematic diagram of pixel connection and signal output.
In the above drawings: 1. a light source; 2. a collimating lens; 3. a flow-through cell; 401. a first detection unit; 402. a second detection unit; 5. a detection circuit.
Detailed Description
The invention will be further described with reference to examples of embodiments shown in the drawings to which:
referring to fig. 1 and 2, a rapid water quality detection device includes a flow cell 3, a liquid channel 301 located in the flow cell 3 for liquid to pass through, a light source 1 for generating light, a collimating lens 2 for converging the light to the liquid channel 301, and a photodetector, wherein the collimating lens 2 converges the light generated by the light source 1 to the liquid channel 301, and the liquid in the liquid channel 301 forms a detection light spot under the irradiation of the light. The photodetector is an array detector and has a first detecting unit 401 and a second detecting unit 402, and the first detecting unit 401 and the second detecting unit 402 are part of pixels of the array detector.
The first detecting unit 401 receives light penetrating through the detecting light spot and generates a first electric signal, the second detecting unit 402 receives light spot scattered light and generates a second electric signal, the photoelectric detector further comprises a detecting circuit 5 which respectively analyzes the first electric signal and the second electric signal and calculates the concentration and the size of particles in liquid at the light spot, and an alarm circuit (not shown) which gives an alarm when the concentration of the particles in the liquid detected by the detecting circuit 5 is stirred. The first detection unit 401, the second detection unit 402, the detection circuit 5 and the alarm circuit are all in the prior art, and those skilled in the art can purchase appropriate accessories according to the content of the embodiment to implement the method specifically.
Referring to fig. 4, the first detection unit 401 transmits a first electrical signal to the detection circuit 5 through the first port 403a, and the detection circuit 5 calculates the concentration and size of the particulate matter through a second electrical signal; the two parts of the second detection unit 402 combine the second electrical signals and transmit the combined second electrical signals to the detection circuit 5 through the second port 403b, and the detection circuit 5 calculates the concentration and size of the particulate matters through the second electrical signals. The first detection unit 401 and the second detection unit 402 share one detection circuit 5 to save the cost of the apparatus.
In the present embodiment, the measurement range of the first detection unit 401 is 5 micrometers to 100 micrometers. The second sensing unit 402 measures in the range of 0.3 microns to 5 microns. Thereby covering the range of the size of the microorganism to be detected in tap water detection. Can ensure that all microorganisms are detected by military equipment.
When rivers pass through flow-through cell 3, this embodiment can continuously detect real-time microorganism concentration, when the quantity of certain microorganism of aquatic increases suddenly, and the particulate matter quantity in its particle size range that corresponds also can increase suddenly thereupon, consequently, can detect and the early warning control the microorganism quantity in the aquatic through this practicality.
In this embodiment, referring to fig. 2 and 3, the flow cell 3 has a flat first outer wall, the first outer wall is perpendicular to the liquid channel 301, and the photodetector is attached and fixed to the first outer wall. The first detection unit 401 and the first detection unit 401 are both rectangular pixels, and two pixels of the second detection unit 402 are arranged and respectively arranged on the sides of two opposite sides of the first detection unit 401. Because this embodiment is direct with the surface of closely laminating at flow-through cell 3 of array detector, simple structure, convenient, the with low costs of realization.
Wherein the length direction of the first detection unit 401 and the length direction of the liquid channel 301 are perpendicular to each other. The flow cell 3 also has a second outer wall parallel to the first outer wall, and light rays pass through the collimating lens 2 and then enter the flow cell 3 perpendicularly to the second outer wall. To ensure that the light penetrating the liquid channel 301 falls within the range of the first detection unit 401, increasing the accuracy of detection.
The above embodiments are merely illustrative of the technical ideas and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention, and not to limit the protection scope of the present invention. All equivalent changes and modifications made according to the spirit of the present invention should be covered within the protection scope of the present invention.

Claims (10)

1.一种水质快速检测装置,其包括流通池、位于所述流通池内是供液体通过的液体通道、产生光线的光源、将所述光线汇聚至液体通道的准直透镜和光电探测器,所述准直透镜将光源产生的光线汇聚至液体通道,所述液体通道内的液体在所述光线的照射下形成一个检测光斑,其特征在于:所述光电探测器包括收集穿透所述检测光斑的光线并产生第一电信号的第一检测单元、收集所述检测光斑散射光线并产生第二电信号的第二检测单元和分别分析所述第一电信号与所述第二电信号并计算出所述光斑处液体内颗粒物浓度和颗粒大小的检测电路。1. A rapid detection device for water quality, comprising a flow cell, a liquid channel for liquid to pass through in the flow cell, a light source for generating light, a collimating lens and a photodetector for converging the light into the liquid channel, so The collimating lens gathers the light generated by the light source into the liquid channel, and the liquid in the liquid channel forms a detection spot under the illumination of the light, and it is characterized in that: the photodetector includes a collection of light that penetrates the detection spot. a first detection unit that collects the light scattered by the detection spot and generates a first electrical signal, a second detection unit that collects the scattered light from the detection spot and generates a second electrical signal, and analyzes the first electrical signal and the second electrical signal respectively and calculates A detection circuit for particle concentration and particle size in the liquid at the light spot is output. 2.根据权利要求1所述的一种水质快速检测装置,其特征在于:所述光电探测器为阵列探测器,所述第一检测单元和所述第二检测单元均为所述阵列探测器的部分像元。2 . The device for rapid water quality detection according to claim 1 , wherein the photodetector is an array detector, and both the first detection unit and the second detection unit are the array detector. 3 . part of the pixels. 3.根据权利要求2所述的一种水质快速检测装置,其特征在于:所述流通池具有一个平整的第一外壁,所述第一外壁与所述液体通道相互垂直,所述光电探测器贴合固定在所述第一外壁上。3 . The device for rapid water quality detection according to claim 2 , wherein the flow cell has a flat first outer wall, the first outer wall and the liquid channel are perpendicular to each other, and the photodetector It is fitted and fixed on the first outer wall. 4.根据权利要求3所述的一种水质快速检测装置,其特征在于:所述第一检测单元和所述第一检测单元均为矩形的像元,所述第二检测单元的像元设置有两个,分别设置在所述第一检测单元相对的两边的侧边。4 . The device for rapid detection of water quality according to claim 3 , wherein the first detection unit and the first detection unit are both rectangular pixels, and the pixel of the second detection unit is set to There are two, which are respectively arranged on the sides of the two opposite sides of the first detection unit. 5.根据权利要求4所述的一种水质快速检测装置,其特征在于:所述第一检测单元的长度方向与所述液体通道的长度方向相互垂直。5 . The device for rapid water quality detection according to claim 4 , wherein the length direction of the first detection unit and the length direction of the liquid channel are perpendicular to each other. 6 . 6.根据权利要求5所述的一种水质快速检测装置,其特征在于:所述流通池还具有平行所述第一外壁的第二外壁,所述光线通过所述准直透镜后垂直所述第二外壁射入所述流通池。6 . The device for rapid detection of water quality according to claim 5 , wherein the flow cell further has a second outer wall parallel to the first outer wall, and the light passes through the collimating lens and is perpendicular to the The second outer wall projects into the flow cell. 7.根据权利要求6所述的一种水质快速检测装置,其特征在于:所述光线通过所述液体通道后射入所述第一检测单元。7 . The device for rapid detection of water quality according to claim 6 , wherein the light enters the first detection unit after passing through the liquid channel. 8 . 8.根据权利要求6所述的一种水质快速检测装置,其特征在于:所述光线射入所述液体通道后产生的散射光中的部分射入所述第二检测单元。8 . The device for rapid detection of water quality according to claim 6 , wherein part of the scattered light generated after the light enters the liquid channel enters the second detection unit. 9 . 9.根据权利要求1所述的一种水质快速检测装置,其特征在于:所述第一检测单元的测量范围为5微米至100微米。9 . The device for rapid detection of water quality according to claim 1 , wherein the measurement range of the first detection unit is 5 microns to 100 microns. 10 . 10.根据权利要求1所述的一种水质快速检测装置,其特征在于:所述第二检测单元的测量范围为0.3微米至5微米。10 . The device for rapid detection of water quality according to claim 1 , wherein the measurement range of the second detection unit is 0.3 microns to 5 microns. 11 .
CN201911314024.3A 2019-12-19 2019-12-19 A rapid detection device for water quality Pending CN110951603A (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006135902A2 (en) * 2005-06-13 2006-12-21 Jmar Research, Inc. Systems and methods for a multiple angle light scattering (mals) instrument having two-dimensional dectector array
US20070194244A1 (en) * 2005-09-19 2007-08-23 Jmar Technologies, Inc. Systems and methods for detecting normal levels of bacteria in water using a multiple angle light scattering (MALS) instrument
CN102353621A (en) * 2011-06-28 2012-02-15 上海理工大学 Measuring device and method of light scattering particles
CN103454203A (en) * 2013-09-09 2013-12-18 中国科学院合肥物质科学研究院 Real-time online measurement system and method of particle size and chemical components of atmospheric particulate
CN105588789A (en) * 2016-03-18 2016-05-18 清华大学深圳研究生院 Detection method for particle size distribution of insulator surface dirt
CN106198327A (en) * 2016-09-21 2016-12-07 江苏苏净集团有限公司 A kind of liquid particles detection device
FR3041433A1 (en) * 2015-09-21 2017-03-24 Microfactory PORTABLE OPTICAL DEVICE FOR DETECTION OF FLUORESCENCE.
CN211570646U (en) * 2019-12-19 2020-09-25 江苏苏净集团有限公司 Quick water quality detection device

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006135902A2 (en) * 2005-06-13 2006-12-21 Jmar Research, Inc. Systems and methods for a multiple angle light scattering (mals) instrument having two-dimensional dectector array
US20070194244A1 (en) * 2005-09-19 2007-08-23 Jmar Technologies, Inc. Systems and methods for detecting normal levels of bacteria in water using a multiple angle light scattering (MALS) instrument
CN102353621A (en) * 2011-06-28 2012-02-15 上海理工大学 Measuring device and method of light scattering particles
CN103454203A (en) * 2013-09-09 2013-12-18 中国科学院合肥物质科学研究院 Real-time online measurement system and method of particle size and chemical components of atmospheric particulate
FR3041433A1 (en) * 2015-09-21 2017-03-24 Microfactory PORTABLE OPTICAL DEVICE FOR DETECTION OF FLUORESCENCE.
CN105588789A (en) * 2016-03-18 2016-05-18 清华大学深圳研究生院 Detection method for particle size distribution of insulator surface dirt
CN106198327A (en) * 2016-09-21 2016-12-07 江苏苏净集团有限公司 A kind of liquid particles detection device
CN211570646U (en) * 2019-12-19 2020-09-25 江苏苏净集团有限公司 Quick water quality detection device

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