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CN110950716A - Additive for tree infusion and preparation method thereof - Google Patents

Additive for tree infusion and preparation method thereof Download PDF

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Publication number
CN110950716A
CN110950716A CN201911353562.3A CN201911353562A CN110950716A CN 110950716 A CN110950716 A CN 110950716A CN 201911353562 A CN201911353562 A CN 201911353562A CN 110950716 A CN110950716 A CN 110950716A
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stirring
parts
acid
additive
ammonium
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彭韧
郭明哲
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The application discloses an additive for tree transfusion and a preparation method thereof, wherein the additive comprises the following substances: purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate. This application can obviously increase the activity of trees plant cell, also can obviously improve the survival rate of trees, especially stabilize earlier on the survival rate that improves trees and then rise gradually, and this application is stable and the effect is lasting long-term on effect trees survival rate.

Description

Additive for tree infusion and preparation method thereof
Technical Field
The application relates to the field of plant maintenance, in particular to an additive for tree transfusion and a preparation method thereof.
Background
In the traditional technology, it is always difficult to improve the survival rate of trees in a common growing environment, the survival rate is difficult to improve by self-driving only depending on the vitality of the trees, and the existing nutrient solution or tree infusion medicine has unstable and non-lasting effect on the survival rate of trees and has poor or no final effect. Generally, the survival rate of trees is expected to be improved by infusing the trees with water, nutrient solution or auxin, and the effect is not good even if the method is adopted.
Disclosure of Invention
The application discloses an additive for tree transfusion, which comprises the following substances: purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate. Further, the feed additive comprises the following substances in parts by weight:
900 portions of purified water, 0.015 to 0.02 portion of thiamine, 18 to 20 portions of isopropanol, 0.003 to 0.0035 portion of ammonium molybdate, 0.05 to 0.06 portion of ammonium dihydrogen phosphate, 2 to 3 portions of sodium nitrate, 0.05 to 0.06 portion of ammonium sulfate, 0.003 to 0.006 portion of potassium chloride, 0.003 to 0.006 portion of potassium carbonate, 0.005 to 0.009 portion of boric acid, 0.05 to 0.1 portion of oxalic acid, 0.005 to 0.008 portion of indoleacetic acid and 0.002 to 0.003 portion of ferroferric citrate.
Further, the feed additive comprises the following substances in parts by weight:
1080 parts of purified water, 0.016 part of thiamine, 18.5 parts of isopropanol, 0.003 part of ammonium molybdate, 0.06 part of ammonium dihydrogen phosphate, 2.5 parts of sodium nitrate, 0.05 part of ammonium sulfate, 0.005 part of potassium chloride, 0.003 part of potassium carbonate, 0.005 part of boric acid, 0.06 part of oxalic acid, 0.008 part of indoleacetic acid and 0.0025 part of ferroferric citrate.
Preferably, the following substances are also included:
chitosan, anhydrous acetic acid, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether.
Particularly preferably, the feed also comprises the following substances in parts by weight: 3 parts of deacetylated chitin, 100 parts of anhydrous acetic acid, 2 parts of chitosan oligosaccharide and 5 parts of polyethylene glycol octyl phenyl ether.
The preparation method of the additive for tree transfusion comprises the following steps:
preparing materials: preparing enough needed substances, purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate;
adding and mixing for the first time: firstly, mixing ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate and ferroferric citrate with purified water, and simply stirring to obtain a first mixed solution;
adding and mixing for the second time: adding boric acid, oxalic acid and indoleacetic acid into the primary mixed solution, simply stirring, and then adding thiamine and isopropanol to obtain a final mixed solution;
stirring: stirring the final mixed solution, regulating the stirring temperature to 30-36 ℃, and regulating the stirring speed to 2000-3000 r/min;
circularly adding and stirring: adding a proper amount of substances according to the requirement in the stirring process and regulating and controlling the adding speed;
packaging: packaging immediately after stirring the finished product to avoid volatilization or photolysis of the effective substances;
the circulation adding and stirring step is carried out as follows: firstly mixing chitosan and liquid anhydrous acetic acid to obtain auxiliary mixed liquor, and then adding the auxiliary mixed liquor, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether together into the stirring process.
In a more preferred embodiment, the rate of volatilization or photolysis loss of each species is tested prior to the cyclical addition of agitation, the threshold amount of each species is set according to a ratio, and the rate of addition of each species is controlled in real time, for each species: calculating an added integral quantity by recording the adding rate and the adding time, calculating a lost integral quantity by recording the loss rate and the loss time, and calculating the difference between the added integral quantity and the lost integral quantity; when all the substances are added in the equilibrium state, the addition of all the substances is immediately finished and packaged.
Advantageous effects
This application can obviously increase the activity of trees plant cell, also can obviously improve the survival rate of trees, especially stabilize earlier on the survival rate that improves trees and then rise gradually, and this application is stable and the effect is lasting long-term on effect trees survival rate.
Detailed Description
Example 1
An additive for tree transfusion, comprising the following substances: purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate. More specifically, the composition comprises the following substances in parts by weight: 900 portions of purified water, 0.015 to 0.02 portion of thiamine, 18 to 20 portions of isopropanol, 0.003 to 0.0035 portion of ammonium molybdate, 0.05 to 0.06 portion of ammonium dihydrogen phosphate, 2 to 3 portions of sodium nitrate, 0.05 to 0.06 portion of ammonium sulfate, 0.003 to 0.006 portion of potassium chloride, 0.003 to 0.006 portion of potassium carbonate, 0.005 to 0.009 portion of boric acid, 0.05 to 0.1 portion of oxalic acid, 0.005 to 0.008 portion of indoleacetic acid and 0.002 to 0.003 portion of ferroferric citrate.
Example 2
An additive for tree transfusion comprises the following substances in parts by weight:
1080 parts of purified water, 0.016 part of thiamine, 18.5 parts of isopropanol, 0.003 part of ammonium molybdate, 0.06 part of ammonium dihydrogen phosphate, 2.5 parts of sodium nitrate, 0.05 part of ammonium sulfate, 0.005 part of potassium chloride, 0.003 part of potassium carbonate, 0.005 part of boric acid, 0.06 part of oxalic acid, 0.008 part of indoleacetic acid and 0.0025 part of ferroferric citrate.
Example 3
The additive for tree transfusion further comprises the following substances on the basis of the embodiment: chitosan, anhydrous acetic acid, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether. More specifically, the feed additive also comprises the following substances in parts by weight: 3 parts of deacetylated chitin, 100 parts of anhydrous acetic acid, 2 parts of chitosan oligosaccharide and 5 parts of polyethylene glycol octyl phenyl ether.
In order to count the effect of the application on the tree plant cells in the specific implementation, the activity of the plant cells can be detected by using a common plasmolysis method, and the experimental principle is that a plant cell membrane has selective permeability. When the plant cell is in hypertonic solution, the intracellular fluid is exuded, the whole protoplast is shrunk, and the cell membrane is gradually separated from the cell wall to generate plasmolysis. If the cells with plasmolysis are moved into hypotonic solution or water again, the water enters the cells again, and the protoplasts gradually recover, namely, the plasmolysis is recovered. The plasmolysis experiment can detect the condition that plant cells have osmosis, and when the permselective membrane loses the function, the plasmolysis phenomenon does not occur, so the method can be used for judging the cell activity, and the experiment shows that the example 2 of the application can increase the tree plant cell activity, and the example 3 can obviously increase the tree plant cell activity.
In the specific implementation, example 3 is selected as a representative of the application and the influence of the example 3 on the survival rate of trees is counted, the survival rate of trees is counted by randomly selecting 3000 trees with poor states, averagely dividing the trees into 30 groups, each group comprises 100 trees, wherein the 1 st to 10 th groups are unprocessed groups, the 11 th to 20 th groups are common drug processing groups, the 21 st to 30 th groups are additive processing groups of the application, firstly, whether the state of each tree of each group is normal or not is recorded so as to count the survival rate (normal/abnormal, wherein the meaning of normal is possible survival), and the normal/total number is the survival rate; and survival was recorded weekly for each group for 5 weeks.
The data are recorded as follows:
Figure BDA0002334988550000031
Figure BDA0002334988550000041
Figure BDA0002334988550000051
the general statistical remarks show that the survival rate of the trees in the 1 st to 10 th groups of untreated groups is relatively reduced in the survival rate recorded at the last time and the survival rate recorded at the first time, the survival rate of the trees in the 11 th to 20 th groups of common medicine treatment groups is relatively reduced basically in the survival rate recorded at the last time and the survival rate recorded at the first time, only one group of the trees is unchanged in the survival rate (the 17 th group), the survival rate of the trees in the 21 st to 30 th groups of the additive treatment groups is relatively increased obviously in the survival rate recorded at the last time and the survival rate recorded at the first time, and the change of each group can be known to have regularity through careful analysis:
the 5 survival records of groups 1-10 fall within the interval 72-81%, 69-73%, 65-69%, 60-65%, 53-59%, respectively;
the 5 survival records of groups 11-20 fall within the interval of 72-81%, 72-76%, 72-76%, 70-76%, 65-70%, respectively;
the 5 survival records of groups 21-30 fall within the interval 72-81%, 72-81%, 80-86%, 86-90%, 91-97%, respectively;
the data show that survival rate recording intervals of all groups recorded for the first time are 72-81%, 5 survival rate recording intervals of 1-10 groups are reduced successively, which shows that the survival rate is difficult to improve by self-driving only depending on the vitality of the trees, and 5 survival rate recording intervals of 11-20 groups are reduced firstly, then stabilized and then reduced, which also shows that the traditional medicine has unstable and non-lasting effect on the survival rate of trees and poor or no effect on the final effect; the 5 survival rate recording intervals of the 21 st to 30 th groups are stable firstly and then gradually increased, which also indicates that the application has stable effect on the survival rate of trees and has lasting and long-acting effect.
In specific implementation, the application also discloses a preparation method of the additive for tree infusion, which comprises the following steps: preparing materials: preparing enough needed substances, purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate;
adding and mixing for the first time: firstly, mixing ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate and ferroferric citrate with purified water, and simply stirring to obtain a first mixed solution;
adding and mixing for the second time: adding boric acid, oxalic acid and indoleacetic acid into the primary mixed solution, simply stirring, and then adding thiamine and isopropanol to obtain a final mixed solution;
stirring: stirring the final mixed solution, regulating the stirring temperature to 30-36 ℃, and regulating the stirring speed to 2000-3000 r/min;
circularly adding and stirring: adding a proper amount of substances according to the requirement in the stirring process and regulating and controlling the adding speed;
packaging: packaging immediately after stirring the finished product to avoid volatilization or photolysis of the effective substances;
more specifically, the following operations are carried out in the step of circularly adding and stirring: firstly mixing chitosan and liquid anhydrous acetic acid to obtain auxiliary mixed liquor, and then adding the auxiliary mixed liquor, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether together into the stirring process. In this embodiment, chitosan and liquid anhydrous acetic acid are first mixed in order to complete the combination of chitosan and acetic acid to better perform the function of chitosan. More specifically, the volatilization or photolysis loss rate of each substance is tested before the stirring is cyclically added, the addition threshold of each substance is set according to the proportion, and the addition rate of each substance is controlled in real time, and for each substance: the integral amount of addition is calculated by recording the rate of addition and the time of addition (this integral amount is essentially the amount of addition, since in practice the efficiency of addition may vary and cannot be directly calculated by the product of efficiency and time, and since a better practice is to stir while adding, so it cannot be weighed once and is most accurately preferred by calculation by means of integration), the integral amount of loss is calculated by recording the rate of loss and the time of loss (likewise in practice the rate of loss is not constant and therefore needs to be calculated by integration), the integral amount of addition and the integral amount of loss are differentiated (i.e. the actual amount of addition), the rate of addition is adjusted to be equal to the rate of loss and addition is continued when this difference is equal to the threshold value of addition during the addition, and this state is defined as the equilibrium state of addition of the substance (in practice the addition of the substance is completed, subsequent addition of the substance is not required, the substance only needs to be added in equilibrium, i.e. the amount is kept constant and equal to the threshold value, and other substances need to be added); when all the substances are added in the equilibrium state, the addition of all the substances is immediately finished and packaged. Through the microcontrol, the mass proportion of each substance can be effectively ensured to be scientific and accurate, and a foundation is provided for the application to play a role.

Claims (8)

1. An additive for tree transfusion, which is characterized by comprising the following substances: purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate.
2. The additive for tree transfusion as claimed in claim 1, which comprises the following components in parts by weight:
900 portions of purified water, 0.015 to 0.02 portion of thiamine, 18 to 20 portions of isopropanol, 0.003 to 0.0035 portion of ammonium molybdate, 0.05 to 0.06 portion of ammonium dihydrogen phosphate, 2 to 3 portions of sodium nitrate, 0.05 to 0.06 portion of ammonium sulfate, 0.003 to 0.006 portion of potassium chloride, 0.003 to 0.006 portion of potassium carbonate, 0.005 to 0.009 portion of boric acid, 0.05 to 0.1 portion of oxalic acid, 0.005 to 0.008 portion of indoleacetic acid and 0.002 to 0.003 portion of ferroferric citrate.
3. The additive for tree infusion as claimed in claim 1 or 2, which comprises the following components in parts by weight:
1080 parts of purified water, 0.016 part of thiamine, 18.5 parts of isopropanol, 0.003 part of ammonium molybdate, 0.06 part of ammonium dihydrogen phosphate, 2.5 parts of sodium nitrate, 0.05 part of ammonium sulfate, 0.005 part of potassium chloride, 0.003 part of potassium carbonate, 0.005 part of boric acid, 0.06 part of oxalic acid, 0.008 part of indoleacetic acid and 0.0025 part of ferroferric citrate.
4. The additive for infusion of trees according to claim 1 or 2, further comprising:
chitosan, anhydrous acetic acid, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether.
5. The additive for infusion of trees according to claim 2 or 3, characterized by further comprising the following substances in parts by weight: 3 parts of deacetylated chitin, 100 parts of anhydrous acetic acid, 2 parts of chitosan oligosaccharide and 5 parts of polyethylene glycol octyl phenyl ether.
6. The method for preparing the additive for tree transfusion as claimed in any one of claims 1 to 3, comprising the steps of:
preparing materials: preparing enough needed substances, purified water, thiamine, isopropanol, ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate, boric acid, oxalic acid, indoleacetic acid and ferroferric citrate;
adding and mixing for the first time: firstly, mixing ammonium molybdate, ammonium dihydrogen phosphate, sodium nitrate, ammonium sulfate, potassium chloride, potassium carbonate and ferroferric citrate with purified water, and simply stirring to obtain a first mixed solution;
adding and mixing for the second time: adding boric acid, oxalic acid and indoleacetic acid into the primary mixed solution, simply stirring, and then adding thiamine and isopropanol to obtain a final mixed solution;
stirring: stirring the final mixed solution, regulating the stirring temperature to 30-36 ℃, and regulating the stirring speed to 2000-3000 r/min;
circularly adding and stirring: adding a proper amount of substances according to the requirement in the stirring process and regulating and controlling the adding speed;
packaging: and the finished product is immediately packaged after being stirred so as to avoid volatilization or photolysis of effective substances.
7. The method for preparing the additive for tree transfusion as set forth in claim 4, comprising the steps of claim 6, and wherein the step of cyclically adding and stirring as set forth in claim 6 comprises the steps of: firstly mixing chitosan and liquid anhydrous acetic acid to obtain auxiliary mixed liquor, and then adding the auxiliary mixed liquor, chitosan oligosaccharide and polyethylene glycol octyl phenyl ether together into the stirring process.
8. The method of claim 6, wherein the loss rate of each substance due to volatilization or photolysis is measured before the stirring is cyclically added, the threshold value of the addition amount of each substance is set according to the ratio, and the addition rate of each substance is controlled in real time, and for each substance: calculating an added integral quantity by recording the adding rate and the adding time, calculating a lost integral quantity by recording the loss rate and the loss time, and calculating the difference between the added integral quantity and the lost integral quantity; when all the substances are added in the equilibrium state, the addition of all the substances is immediately finished and packaged.
CN201911353562.3A 2019-12-25 2019-12-25 Additive for tree infusion and preparation method thereof Pending CN110950716A (en)

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CN113133459A (en) * 2021-04-20 2021-07-20 河南省莱恩坪安园林植保有限公司 Special growth regulator for plant infusion

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CN113133459A (en) * 2021-04-20 2021-07-20 河南省莱恩坪安园林植保有限公司 Special growth regulator for plant infusion

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Application publication date: 20200403