CN110754684A - Caffeine-containing fuming particle, preparation method thereof and low-temperature heating non-combustible product - Google Patents
Caffeine-containing fuming particle, preparation method thereof and low-temperature heating non-combustible product Download PDFInfo
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- CN110754684A CN110754684A CN201911055900.5A CN201911055900A CN110754684A CN 110754684 A CN110754684 A CN 110754684A CN 201911055900 A CN201911055900 A CN 201911055900A CN 110754684 A CN110754684 A CN 110754684A
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- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 title claims abstract description 80
- 239000002245 particle Substances 0.000 title claims abstract description 61
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 229960001948 caffeine Drugs 0.000 title claims abstract description 39
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 238000010438 heat treatment Methods 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 239000000779 smoke Substances 0.000 claims abstract description 19
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 12
- 239000000047 product Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 4
- 239000011248 coating agent Substances 0.000 claims description 4
- 238000000576 coating method Methods 0.000 claims description 4
- 241000411851 herbal medicine Species 0.000 claims description 4
- 238000007598 dipping method Methods 0.000 claims description 3
- 235000013599 spices Nutrition 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 2
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims description 2
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 235000013772 propylene glycol Nutrition 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 235000010356 sorbitol Nutrition 0.000 claims description 2
- 239000001069 triethyl citrate Substances 0.000 claims description 2
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims description 2
- 235000013769 triethyl citrate Nutrition 0.000 claims description 2
- 241000628997 Flos Species 0.000 claims 1
- 210000000582 semen Anatomy 0.000 claims 1
- 238000002791 soaking Methods 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 16
- 230000000391 smoking effect Effects 0.000 abstract description 13
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- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 10
- 239000007788 liquid Substances 0.000 abstract description 5
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 abstract description 3
- 206010012335 Dependence Diseases 0.000 abstract description 3
- 229960002715 nicotine Drugs 0.000 abstract description 3
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 abstract description 3
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- 244000303040 Glycyrrhiza glabra Species 0.000 description 2
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 2
- 235000020224 almond Nutrition 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
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- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 description 2
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
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- 235000006753 Platycodon grandiflorum Nutrition 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
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- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 description 1
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- 238000010586 diagram Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
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- 239000003571 electronic cigarette Substances 0.000 description 1
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- 210000004072 lung Anatomy 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- NOOLISFMXDJSKH-UHFFFAOYSA-N p-menthan-3-ol Chemical compound CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 1
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- 230000001737 promoting effect Effects 0.000 description 1
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a caffeine-containing fuming particle, which comprises the following components in parts by weight: 30-70 parts of plant raw materials, 10-40 parts of smoke agent and 0.001-1 part of caffeine-containing component. The invention also discloses a preparation method of the fuming particle and a low-temperature heating non-combustible product prepared from the fuming particle. The smoking particles adopt the formula of the components containing caffeine and natural plant raw materials, can replace tobacco containing nicotine, play a role in refreshing and relieving pressure while reducing addiction and health hazards, are convenient to carry and use in a solid particle form, and avoid the problem that the traditional atomized liquid is easy to leak and is inconvenient to carry.
Description
Technical Field
The invention relates to a low-temperature heating non-combustible product, in particular to a caffeine-containing fuming particle, a preparation method thereof and a low-temperature heating non-combustible product.
Background
The low-temperature heating non-combustible product is one of important products of novel tobacco products, and starts in the 80 th 20 th century, tobacco substances are not combusted under the condition of 200-400 ℃ through carbon heating or electric heating, and smoke is generated through low-temperature cracking. The cigarette filter avoids tar and a large amount of harmful compounds generated by high-temperature combustion of tobacco to a certain extent, reduces the influence of cigarettes on the public environment due to less flow measurement smoke, and becomes a hotspot for research and development of a plurality of tobacco manufacturing enterprises.
Structurally, the existing heating non-combustion fuming mainly comprises four independent unit sections, namely a fuming section, a hollow section, a cooling section and a filtering section from the far lip end to the near lip end. The processing and preparation method is that at present, a modified cigarette making machine is mostly adopted to prepare the smoking sections, a filter rod forming machine is used for preparing each filter tip section, and finally, a composite filter rod machine is used for designing and combining to prepare the heating non-combustible smoking product according to a quaternary composite form. The method has high requirements on the filter stick compounding machine, needs to refit a cigarette making machine, has complex compounding degree and complicated preparation procedures. The chinese patent application No. 201810932429.2, modified the above structure, proposed an integrally formed non-combustible heated smoking article, which integrally filled the respective unit segments into the hollow tube after being externally combined, and thus did not need to be prepared by compounding with a filter rod compounding machine.
In terms of components, most of the existing heating non-combustible products take tobacco substances as smoking materials, and nicotine which is a main component of the existing heating non-combustible products has certain addiction and harm. For example, patent document CN 107692305a discloses a heating non-combustion tobacco sheet and a preparation method thereof, patent document CN 205611758U discloses a heating non-combustion cigarette prepared by using reconstituted tobacco, and patent document CN 103841844B discloses a multi-segment smoking article.
Caffeine is a centrally exciting drug, and can enhance the excitation process of cerebral cortex and cortex motor area with small dose, and it can refresh brain, improve metabolism, and improve the efficiency of certain behavioral activities. At present, consumers mainly take caffeine by means of oral drinks or administration, and research on caffeine taking by means of atomization is less, and patent CN 105433428A discloses caffeine-containing atomized liquid and a production method of the caffeine-containing atomized liquid, but the caffeine is added into electronic cigarette oil, but the liquid is easy to leak and is inconvenient to carry.
In addition, consumers may suffer throat discomfort such as itching, dryness or burning sensation due to the continuous intake of smoke when they smoke a low-temperature heat non-combustible article.
Disclosure of Invention
The invention aims to provide a caffeine-containing fuming particle capable of replacing tobacco and playing a role in refreshing and reducing pressure, a preparation method thereof and a low-temperature heating non-combustible product.
In order to achieve the above object, the present invention provides a caffeine-containing smoker particle comprising the following components in parts by weight: 30-70 parts of plant raw materials, 10-40 parts of smoke agent and 0.001-1 part of caffeine-containing component, wherein the caffeine-containing component is calculated by dry weight or pure substances.
Preferably, the smoker particles are composed of the following components in parts by weight: 40-60 parts of plant raw materials, 10-30 parts of a smoke agent, 0.005-0.02 part of a caffeine-containing component and 30-60 parts of essence and spice, wherein the plant raw materials are Chinese herbal medicines. Wherein the essence and perfume are optional components for regulating aroma and taste of non-combustible product heated at low temperature, and can be selected from fructus Mali Pumilae extract, cacao extract, fructus Myrtilli extract, fructus Jujubae extract, Mentholum, and cooling agent.
Preferably, the Chinese herbal medicine is one or more of radix ophiopogonis, pericarpium citri reticulatae, platycodon grandiflorum, almond, folium mori, chrysanthemum, liquorice, loquat leaves and schizonepeta. The radix ophiopogonis, the almond, the dried orange peel, the mulberry leaf, the liquorice and the loquat leaf have certain effects of moistening lung, relieving cough, promoting fluid production and quenching thirst, and are mixed and applied to a low-temperature heating non-combustible product, so that the active ingredients are released by heating, the stimulation of smoke inhalation to mucous membranes can be relieved, and the discomfort of the throat can be relieved.
Preferably, the caffeine-containing component is caffeine and/or a derivative thereof. Wherein, the caffeine derivative can adopt 8-ester group caffeine, 8-ester group caffeine is a common caffeine derivative, depending on the substituents, various components may be present, such as butyl 1, 3-dimethyl-7-propyl-2, 6-dioxo-2, 3,6, 7-tetrahydro-1H-purine-8-carboxylate, butyl 3, 7-dimethyl-1-ethyl-2, 6-dioxo-2, 3,6, 7-tetrahydro-1H-purine-8-carboxylate, isopropyl 1,3, 7-trimethyl-2, 6-dioxo-2, 3,6, 7-tetrahydro-1H-purine-8-carboxylate, and the like.
Preferably, the smoke agent is one or more of propylene glycol, glycerol, triethyl citrate, sorbitol and 1, 3-butanediol.
Preferably, the smoker particles have a particle size of: 20-40 meshes is not less than 70 wt%, 40-60 meshes is not more than 20 wt%, and 60-80 meshes is not more than 10 wt%.
The invention provides a preparation method of the fuming particles, which comprises the steps of crushing the plant raw materials into particles of 20-80 meshes, mixing the components except the plant raw materials, and adding the mixture to the particles of the plant raw materials to prepare the fuming particles; or uniformly mixing and granulating the components except the caffeine-containing component to obtain semi-finished product particles, and adding the caffeine-containing component to the surface of the semi-finished product particles to obtain the fuming particles.
Preferably, the mixture of components other than the plant material is added to the surface of the plant material particles in any one of spraying, dipping or coating; the caffeine-containing component is added to the surface of the semi-finished product particles in any of spraying, dipping or coating.
Meanwhile, the invention also provides a low-temperature heating non-combustible product which comprises a hollow tubular shell, wherein the hollow tubular shell is filled with the smoke particles.
Preferably, the low-temperature heating non-combustible product adopts an integrated structure, and each independent unit section in the hollow tubular shell is externally combined and then integrally filled into the hollow tubular shell. Compared with the existing sectional butt joint structure, the integrated structure does not need to be prepared by compounding the filter rod compounding machine and refitting cigarette making machine equipment, simplifies the preparation process, reduces the turnover link, reduces the preparation cost and simultaneously endows combination and selection of more functional units.
Compared with the prior art, the invention has the beneficial effects that: 1) the smoking particles adopt a formula containing caffeine components and natural plant raw materials, can replace tobacco containing nicotine, and play a role in refreshing and decompressing while reducing addiction and health hazards; 2) the fuming particles are applied in a solid particle form, so that the fuming particles are convenient to carry and use, and the problem that the traditional atomized liquid is easy to leak and is inconvenient to carry is solved; 3) the low-temperature heating non-combustible product enables smoke particles to generate smoke through low-temperature cracking at the temperature of 200-400 ℃, combustion does not occur, and compared with the traditional cigarette, tar and a large amount of harmful compounds generated by high-temperature combustion of tobacco are avoided, and the influence on the public environment is reduced by flow measurement smoke.
Drawings
Fig. 1 is a schematic structural diagram of a low-temperature heating non-combustible product designed according to an embodiment of the invention.
Wherein: 1-filtering unit, 2-gel cooling fragrance-carrying unit, 3-hollow special particle unit, 4-blocking unit, 5-cavity unit, 6-hollow supporting unit and 7-fuming unit
Detailed Description
The invention is described in further detail below with reference to the figures and the specific embodiments.
Examples 1 to 5
The fuming particles provided by each embodiment 8 of the invention are composed of the following components in parts by weight: 30-70 parts of plant raw materials, 10-40 parts of smoke agents, 0.001-1 part of caffeine-containing components and 30-60 parts of essence and spices, wherein the components are calculated by dry weight or pure substances. The specific components and the proportion are shown in tables 1-3, wherein the unit is g in each table, and the caffeine-containing components in tables 1 and 3 are converted into the weight of caffeine.
Table 1 general formula of smoker particles in each example
Table 2 formula of plant materials in each example
TABLE 3 formulation of the smoke agent, caffeine-containing component and other ingredients of each example
Example 6
The embodiment provides a preparation method of the fuming particle in any one of embodiments 1 to 3, which comprises the following steps: the method comprises the steps of crushing all plant raw materials into particles of 20-80 meshes, uniformly mixing caffeine-containing components, a smoking agent and essence perfume, and spraying the mixture on the surfaces of the particles to prepare the smoking particles. The particle size distribution of the prepared fuming particles is as follows: 20-40 meshes is not less than 70 wt%, 40-60 meshes is not more than 20 wt%, and 60-80 meshes is not more than 10 wt%.
Example 7
This example provides a method of making the smoker particles of example 4 or 5, comprising the steps of: the preparation method comprises pulverizing the above plant materials into fine powder, mixing with smoke agent and essence (no essence in example 5), making into semi-finished granule by swing granulation, boiling granulation, spray drying granulation, and crushing granulation, and spraying caffeine-containing component onto the surface of the semi-finished granule to obtain smoke-forming granule. The particle size distribution of the prepared fuming particles is as follows: 20-40 meshes is not less than 70 wt%, 40-60 meshes is not more than 20 wt%, and 60-80 meshes is not more than 10 wt%.
Example 8
As shown in fig. 1, the low-temperature heating non-combustible product designed in this embodiment is a hollow tubular casing made of plant fiber paper, and the following unit sections are arranged in sequence from the distal lip end to the proximal lip end: the device comprises a smoking unit 7, a hollow supporting unit 6, a cavity unit 5, a blocking unit 4, a hollow special particle unit 3, a gel cooling fragrance-carrying unit 2 and a filtering unit 1. Wherein the fuming unit 7 is filled with the fuming particles provided in the embodiments 1-5. The assembly mode of each independent unit section and the shell adopts an integrated structure disclosed in Chinese patent application with application number 201810932429.2, namely, the independent unit sections are externally combined and then integrally filled into the hollow tubular shell.
Example 9
The low-temperature heating non-combustible product designed in the embodiment adopts a conventional structure as described in the background art, and is provided with a smoking section, a hollow section, a cooling section and a filtering section from the far lip end to the near lip end respectively. Wherein, the smoking section is filled with the smoking particles provided by embodiments 1-5.
Claims (10)
1. A caffeine-containing smoker particle, comprising: comprises the following components in parts by weight: 30-70 parts of plant raw materials, 10-40 parts of smoke agent and 0.001-1 part of caffeine-containing component.
2. The smoker particle according to claim 1, wherein: the composition comprises the following components in parts by weight: 40-60 parts of plant raw materials, 10-30 parts of a smoke agent, 0.005-0.02 part of a caffeine-containing component and 30-60 parts of essence and spice, wherein the plant raw materials are Chinese herbal medicines.
3. The smoker particle according to claim 2, wherein: the Chinese herbal medicine is one or more of radix Ophiopogonis, pericarpium Citri Tangerinae, radix Platycodi, semen Armeniacae amarum, folium Mori, flos Chrysanthemi, Glycyrrhrizae radix, folium Eriobotryae, and herba Schizonepetae.
4. The smoker particle according to any one of claims 1 to 3, wherein: the caffeine-containing component is caffeine and/or a derivative thereof.
5. The smoker particle according to any one of claims 1 to 3, wherein: the smoke agent is one or more of propylene glycol, glycerol, triethyl citrate, sorbitol and 1, 3-butanediol.
6. The smoker particle according to any one of claims 1 to 3, wherein: the particle size of the fuming particle is as follows: 20-40 meshes is not less than 70 wt%, 40-60 meshes is not more than 20 wt%, and 60-80 meshes is not more than 10 wt%.
7. A method of making the smoker particles according to any one of claims 1 to 6, wherein: the method comprises the steps of firstly, crushing plant raw materials into particles of 20-80 meshes, mixing all components except the plant raw materials, and adding the mixture to the plant raw material particles to prepare the smoke-forming particles; or uniformly mixing and granulating the components except the caffeine-containing component to obtain semi-finished product particles, and adding the caffeine-containing component to the surface of the semi-finished product particles to obtain the fuming particles.
8. The method of claim 7, wherein: the mixture of each component except the plant raw material and the smoke agent is added to the surface of the plant raw material particles in any one mode of spraying, soaking or coating; the caffeine-containing component is added to the surface of the semi-finished product particles in any of spraying, dipping or coating.
9. A low-temperature heating non-combustible product comprises a hollow tubular shell, and is characterized in that: the hollow tubular shell is filled with the fuming particles as set forth in any one of claims 1 to 6.
10. A low-temperature-heating non-combustible article according to claim 9, characterized in that: the low-temperature heating non-combustible product adopts an integrated structure, and each independent unit section in the hollow tubular shell is integrally filled into the hollow tubular shell after being externally combined.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911055900.5A CN110754684A (en) | 2019-10-31 | 2019-10-31 | Caffeine-containing fuming particle, preparation method thereof and low-temperature heating non-combustible product |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911055900.5A CN110754684A (en) | 2019-10-31 | 2019-10-31 | Caffeine-containing fuming particle, preparation method thereof and low-temperature heating non-combustible product |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112401292A (en) * | 2020-11-19 | 2021-02-26 | 云南纯旭生物科技有限公司 | Atomized smoking material for heating non-combustible product |
| CN113208146A (en) * | 2021-04-02 | 2021-08-06 | 汉觅科技(福建)有限公司 | Atomized smoking material for heating non-combustible product and preparation method thereof |
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| CN102217788A (en) * | 2010-04-17 | 2011-10-19 | 徐兵 | Method and cigarette (fog) for smoking cessation in gradual active ingredients substitution manner |
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| CN113208146A (en) * | 2021-04-02 | 2021-08-06 | 汉觅科技(福建)有限公司 | Atomized smoking material for heating non-combustible product and preparation method thereof |
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