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CN110705012B - Oil sleeve annular pressure control method based on compression capacity of tubular column joint - Google Patents

Oil sleeve annular pressure control method based on compression capacity of tubular column joint Download PDF

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Publication number
CN110705012B
CN110705012B CN201910775446.4A CN201910775446A CN110705012B CN 110705012 B CN110705012 B CN 110705012B CN 201910775446 A CN201910775446 A CN 201910775446A CN 110705012 B CN110705012 B CN 110705012B
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compression
tcmax
joint
tubing string
pressure control
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CN110705012A (en
Inventor
王建军
杨尚谕
李方坡
陈俊
李丽锋
孙建华
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China National Petroleum Corp
CNPC Tubular Goods Research Institute
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China National Petroleum Corp
CNPC Tubular Goods Research Institute
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B17/00Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B17/00Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
    • E21B17/02Couplings; joints
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/10Geothermal energy

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Earth Drilling (AREA)

Abstract

The invention discloses an oil sleeve annular pressure control method based on the compression capacity of a tubular column joint, which comprises the following steps: 1) Calculating an annulus pressure control initial value Pos; 2) Calculating the maximum compression load Tcmax born by the tubing string; 3) Determining compression efficiency delta and compression yield strength Tc of the oil pipe airtight threaded joint according to an API RP 5C5 test, selecting a joint anti-compression safety coefficient S at the same time, and transferring to the step 4) when Tcmax/Tc is more than delta/S; when Tcmax/Tc is less than or equal to delta/S, turning to step 5); 4) Calculating a maximum allowable annular pressure value Po; 5) When the calculated equivalent sigma eq of the tubing string is lower than 90% of the yield strength of the tubing material, the annulus pressure is controlled, otherwise, the step 6) is carried out; 6) Changing the compression-resistant safety coefficient S of the joint, turning to step 3), the method can calculate the annular pressure by taking the compression-resistant capacity of the joint into consideration.

Description

Oil sleeve annular pressure control method based on compression capacity of tubular column joint
Technical Field
The invention belongs to the technical field of oil extraction engineering, and relates to an oil sleeve annular pressure control method based on the compression capacity of a tubular column joint.
Background
In the production operation process of a gas well, an annular pressure calculation method is mainly standardized by API RP 90 marine oil and gas well annular pressure management, so that an annular pressure threshold value is obtained through calculation, but with the complexity of production working conditions of the gas well, such as frequent well switching and fracturing operations of a high-temperature high-pressure deep well, injection and production reciprocating operations of a gas storage well and the like, the load alternating times of a tubing string are increased, the annular pressure well is increased more and more, and particularly, the annular pressure A (oil jacket annular pressure) is abnormally high, so that a great safety risk is brought to production. While annulus pressure control has been performed as prescribed in API RP 90, there is still a growing trend for annulus pressure anomalies. The reason for this is mainly that various airtight threaded joints adopted in high-pressure gas wells have uneven compression resistance (compression efficiency), the compression efficiency is from 30% to 100%, the annular pressure changes (increases/decreases) simultaneously cause the axial load of the pipe string to change, and if the compression load increases, the pipe string is very easy to leak. The full-size physical test in the room also reflects that the pipe column has good sealing performance under tensile load, but is easy to leak when being stretched after being subjected to compressive load.
The current calculation of the annular pressure A is mainly determined by the minimum anti-extrusion strength of an oil pipe or the minimum anti-internal pressure strength of a production casing, and the influence of axial compression load on the sealing performance of a pipe column joint is not considered. Under the reciprocating working condition of a complex gas well, the alternating of the pulling and pressing load has a great influence on the sealing capacity of the tubular column, particularly the compression load, and the annular pressure change easily causes the increase of the compression load of the tubular column. The annulus pressure control must be performed taking into account the compression resistance of the tubular string joint.
The main problems existing in the prior art are as follows: the API RP 90 standard is used as a main calculation annulus pressure, the anti-external-extrusion and anti-internal-pressure bearing capacity of the tubular column is mainly considered, and the compression resistance of the joint is not considered.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide an oil jacket annular pressure control method based on the compression capacity of a tubular column joint, which can calculate annular pressure by considering the compression capacity of the joint.
In order to achieve the above purpose, the oil casing annulus pressure control method based on the compression capacity of the tubular column joint comprises the following steps:
1) Acquiring the extrusion resistance Pot of the oil pipe, the internal pressure resistance Pic of the production casing and the internal pressure resistance Picc of the casing of the previous layer of technology under the preset specification, and calculating an annular pressure control initial value Pos according to an API RP 90 test;
2) Calculating the maximum compression load Tcmax born by the tubing string under the annulus pressure Pos according to the gas flow Q, the temperature change T, the internal pressure Pi, the outer diameter D and the wall thickness T of the tubing under the working condition of the complex gas well and the theory of tubing string mechanics;
3) Determining compression efficiency delta and compression yield strength Tc of the oil pipe airtight threaded joint according to an API RP 5C5 test, selecting a joint anti-compression safety coefficient S at the same time, and transferring to the step 4) when Tcmax/Tc is more than delta/S; when Tcmax/Tc is less than or equal to delta/S, turning to step 5);
4) Calculating a maximum allowable annulus pressure value Po through a maximum compression load Tcmax borne by the tubing string according to a tubing string mechanics theory;
5) Checking the triaxial stress intensity of the tubing string according to the maximum allowable annulus pressure value Po or an annulus pressure control initial value Pos and the fourth intensity theory, and controlling the annulus pressure when the calculated equivalent sigma eq of the tubing string is lower than 90% of the yield intensity of the tubing material, otherwise, turning to the step 6);
6) Changing the compression-resistant safety coefficient S of the joint, and turning to the step 3).
The annulus pressure control initial value Pos in step 1) is:
Pos=Min(50%Pic,80%Picc,75%Pot) (1)。
the tubing string is subjected to a maximum compressive load Tcmax of:
Tcmax=f(D,t,Q,T,Pi,Pos) (2)
the compression safety coefficient S of the joint is 1-1.3.
And inquiring an API RP 5C3 standard to obtain the extrusion resistance strength Pot of the oil pipe, the internal pressure resistance strength Pic of the production casing and the internal pressure resistance strength Picc of the casing of the upper layer of technology under the preset specification.
The invention has the following beneficial effects:
when Tcmax/Tc is larger than delta/S, the maximum allowable annular pressure value Po is calculated by the maximum compression load Tcmax born by the tubing string; and (3) checking the triaxial stress intensity of the tubing string when Tcmax/Tc is less than or equal to delta/S, controlling the annular pressure when the calculated equivalent sigma eq of the tubing string is less than 90% of the yield strength of the tubing material, otherwise, changing the compression-resistant safety coefficient S of the joint to control the annular pressure of the oil jacket.
Drawings
FIG. 1 is a flow chart of the present invention.
Detailed Description
The invention is described in further detail below with reference to the attached drawing figures:
referring to fig. 1, the oil casing annulus pressure control method based on the compression capacity of the tubular column joint according to the invention comprises the following steps:
1) Inquiring an API RP 5C3 standard to obtain the oil pipe extrusion resistance strength Pot, the production casing internal pressure resistance strength Pic and the upper technical casing internal pressure resistance strength Picc under the preset specification, and calculating an annular pressure control initial value Pos according to an API RP 90 test;
Pos=Min(50%Pic,80%Picc,75%Pot) (1)
2) Calculating the maximum compression load Tcmax born by the tubing string under the annulus pressure Pos according to the gas flow Q, the temperature change T, the internal pressure Pi, the outer diameter D and the wall thickness T of the tubing under the working condition of the complex gas well and the theory of tubing string mechanics;
Tcmax=f(D,t,Q,T,Pi,Pos) (2)
3) Determining compression efficiency delta and compression yield strength Tc of the oil pipe airtight threaded joint according to an API RP 5C5 test, selecting a joint anti-compression safety coefficient S at the same time, and transferring to the step 4) when Tcmax/Tc is more than delta/S; when Tcmax/Tc is less than or equal to delta/S, turning to step 5), wherein under general conditions, the compression-resistant safety coefficient S of the joint has a value of 1-1.3;
4) Calculating a maximum allowable annulus pressure value Po through a maximum compression load Tcmax borne by the tubing string according to a tubing string mechanics theory;
5) Checking the triaxial stress intensity of the tubing string according to the maximum allowable annulus pressure value Po or an annulus pressure control initial value Pos and the fourth intensity theory, and controlling the annulus pressure when the calculated equivalent sigma eq of the tubing string is lower than 90% of the yield intensity of the tubing material, otherwise, turning to the step 6);
6) Changing the compression-resistant safety coefficient S of the joint, and turning to the step 3).
Example 1
From 2017, the annular pressure of the oil jacket of the western gas storage well is calculated by using the method, the compression efficiency of the P110 joint phi 114.3mm multiplied by 7.37mm is considered, the annular pressure of the oil jacket is calculated to be 22.92MPa, and the annular pressure of the oil jacket is calculated to be 43.95MPa at most according to the API RP 90 standard, so that on-site annular pressure control measures are further changed, and the sealing safety of the pipe column is ensured.
The invention is suitable for the oil collar air pressure control in various complex gas wells, and various complex gas wells are being built by great investment in China, and the construction of one well is tens of millions of yuan, even hundreds of millions of yuan. However, the existing gas well is basically produced by annular pressure, so that certain safety risks are brought, natural gas leakage accidents are easy to occur due to long-term annular pressure, and serious accidents occur once the natural gas leaks into urban living areas through stratum. By adopting the invention, the design capability of the well completion pipe column can be further improved, the leakage risk of the pipe column can be reduced to the greatest extent, and thus, accidents are avoided, so that the invention has good economic benefit and wide application prospect.

Claims (1)

1. The oil casing annulus pressure control method based on the compression capacity of the tubular column joint is characterized by comprising the following steps of:
1) Acquiring the extrusion resistance Pot of the oil pipe, the internal pressure resistance Pic of the production casing and the internal pressure resistance Picc of the casing of the previous layer of technology under the preset specification, and calculating an annular pressure control initial value Pos according to an API RP 90 test;
2) Calculating the maximum compression load Tcmax born by the tubing string under the annulus pressure Pos according to the gas flow Q, the temperature change T, the internal pressure Pi, the outer diameter D and the wall thickness T of the tubing under the working condition of the complex gas well and the theory of tubing string mechanics;
3) Determining compression efficiency delta and compression yield strength Tc of the oil pipe airtight threaded joint according to an API RP 5C5 test, selecting a joint anti-compression safety coefficient S at the same time, and transferring to the step 4) when Tcmax/Tc is more than delta/S; when Tcmax/Tc is less than or equal to delta/S, turning to step 5);
4) Calculating a maximum allowable annulus pressure value Po through a maximum compression load Tcmax borne by the tubing string according to a tubing string mechanics theory;
5) Checking the triaxial stress intensity of the tubing string according to the maximum allowable annulus pressure value Po or an annulus pressure control initial value Pos and the fourth intensity theory, and controlling the annulus pressure when the calculated equivalent sigma eq of the tubing string is lower than 90% of the yield intensity of the tubing material, otherwise, turning to the step 6);
6) Changing the compression-resistant safety coefficient S of the joint, and turning to the step 3);
the annulus pressure control initial value Pos in step 1) is:
Pos=Min(50%Pic,80%Picc,75%Pot) (1)
the tubing string is subjected to a maximum compressive load Tcmax of:
Tcmax=f(D,t,Q,T,Pi,Pos) (2)
the value of the compression-resistant safety coefficient S of the joint is 1-1.3;
and inquiring an API RP 5C3 standard to obtain the extrusion resistance strength Pot of the oil pipe, the internal pressure resistance strength Pic of the production casing and the internal pressure resistance strength Picc of the casing of the upper layer of technology under the preset specification.
CN201910775446.4A 2019-08-21 2019-08-21 Oil sleeve annular pressure control method based on compression capacity of tubular column joint Active CN110705012B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111287724B (en) * 2020-04-01 2022-02-01 中国石油天然气集团有限公司 Acidification operation safety control method for preventing packer from failing

Citations (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3964544A (en) * 1975-06-20 1976-06-22 Halliburton Company Pressure operated isolation valve for use in a well testing and treating apparatus, and its method of operation
US4105075A (en) * 1977-07-21 1978-08-08 Baker International Corporation Test valve having automatic bypass for formation pressure
US4125165A (en) * 1977-07-21 1978-11-14 Baker International Corporation Annulus pressure controlled test valve with locking annulus pressure operated pressure trapping means
US5518073A (en) * 1994-05-05 1996-05-21 Halliburton Company Mechanical lockout for pressure responsive downhole tool
CN1225976A (en) * 1998-02-10 1999-08-18 丰田自动车株式会社 Hydraulic pump control device and method
CN101172317A (en) * 2007-11-30 2008-05-07 重庆大学 Device and method for controlling flash in oil storage cylinder of friction welding motorcycle shock absorber
CN102061152A (en) * 2009-11-11 2011-05-18 中国石油天然气股份有限公司 High-strength controllable gel breaking chemical temporary plugging liquid rubber plug
CN102539241A (en) * 2011-11-18 2012-07-04 国营第六一六厂 Strength and sealing performance test method for diesel engine high pressure oil pipe
CN102733772A (en) * 2012-07-12 2012-10-17 刘庆梅 Christmas tree of tubing head for borehole operation without killing well
CN103235605A (en) * 2013-04-19 2013-08-07 南京工业大学 Working condition simulation load loading control system and method for numerical control turntable test bed
CN103344495A (en) * 2013-07-22 2013-10-09 长江水利委员会长江科学院 Test device for servo control of deep rock mass deformation by using rigid bearing plate center hole method, and method for device
CN103821464A (en) * 2013-11-12 2014-05-28 山东科瑞石油装备有限公司 Tubing string vertical vehicular full-automatic smart hydraulic workover rig
CN104373053A (en) * 2014-11-28 2015-02-25 中国石油天然气集团公司 Underground natural gas storage injection-production pipe column designing method
CN104594834A (en) * 2014-12-01 2015-05-06 中国石油大学(华东) Method for monitoring drilling overflow condition of deepwater oil-based drilling fluid
CN104632172A (en) * 2013-11-15 2015-05-20 中国石油天然气股份有限公司 Method for controlling annulus pressure of gas field horizontal well immovable pipe column hydraulic sand blasting fracturing
WO2017121112A1 (en) * 2016-01-14 2017-07-20 中国石油集团川庆钻探工程有限公司长庆井下技术作业公司 Method for evaluating performance of multistage hydraulic jet fracturing string
CN107191164A (en) * 2017-05-23 2017-09-22 中海石油(中国)有限公司 The analogue experiment installation and method of shock loading suffered by a kind of perforation tubular column
CN107269239A (en) * 2017-08-04 2017-10-20 西南石油大学 A kind of devices and methods therefor of stable oil jacket annular pressure
CN108915669A (en) * 2018-08-15 2018-11-30 南智(重庆)能源技术有限公司 Gas storage gas injection tube column vibrating fatigue life-span prediction method
CN109404741A (en) * 2018-11-16 2019-03-01 中国石油天然气股份有限公司 Gas storage reservoir injection and production well annular pressure treatment method

Patent Citations (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3964544A (en) * 1975-06-20 1976-06-22 Halliburton Company Pressure operated isolation valve for use in a well testing and treating apparatus, and its method of operation
US4105075A (en) * 1977-07-21 1978-08-08 Baker International Corporation Test valve having automatic bypass for formation pressure
US4125165A (en) * 1977-07-21 1978-11-14 Baker International Corporation Annulus pressure controlled test valve with locking annulus pressure operated pressure trapping means
US5518073A (en) * 1994-05-05 1996-05-21 Halliburton Company Mechanical lockout for pressure responsive downhole tool
CN1225976A (en) * 1998-02-10 1999-08-18 丰田自动车株式会社 Hydraulic pump control device and method
CN101172317A (en) * 2007-11-30 2008-05-07 重庆大学 Device and method for controlling flash in oil storage cylinder of friction welding motorcycle shock absorber
CN102061152A (en) * 2009-11-11 2011-05-18 中国石油天然气股份有限公司 High-strength controllable gel breaking chemical temporary plugging liquid rubber plug
CN102539241A (en) * 2011-11-18 2012-07-04 国营第六一六厂 Strength and sealing performance test method for diesel engine high pressure oil pipe
CN102733772A (en) * 2012-07-12 2012-10-17 刘庆梅 Christmas tree of tubing head for borehole operation without killing well
CN103235605A (en) * 2013-04-19 2013-08-07 南京工业大学 Working condition simulation load loading control system and method for numerical control turntable test bed
CN103344495A (en) * 2013-07-22 2013-10-09 长江水利委员会长江科学院 Test device for servo control of deep rock mass deformation by using rigid bearing plate center hole method, and method for device
CN103821464A (en) * 2013-11-12 2014-05-28 山东科瑞石油装备有限公司 Tubing string vertical vehicular full-automatic smart hydraulic workover rig
CN104632172A (en) * 2013-11-15 2015-05-20 中国石油天然气股份有限公司 Method for controlling annulus pressure of gas field horizontal well immovable pipe column hydraulic sand blasting fracturing
CN104373053A (en) * 2014-11-28 2015-02-25 中国石油天然气集团公司 Underground natural gas storage injection-production pipe column designing method
CN104594834A (en) * 2014-12-01 2015-05-06 中国石油大学(华东) Method for monitoring drilling overflow condition of deepwater oil-based drilling fluid
WO2017121112A1 (en) * 2016-01-14 2017-07-20 中国石油集团川庆钻探工程有限公司长庆井下技术作业公司 Method for evaluating performance of multistage hydraulic jet fracturing string
CN107191164A (en) * 2017-05-23 2017-09-22 中海石油(中国)有限公司 The analogue experiment installation and method of shock loading suffered by a kind of perforation tubular column
CN107269239A (en) * 2017-08-04 2017-10-20 西南石油大学 A kind of devices and methods therefor of stable oil jacket annular pressure
CN108915669A (en) * 2018-08-15 2018-11-30 南智(重庆)能源技术有限公司 Gas storage gas injection tube column vibrating fatigue life-span prediction method
CN109404741A (en) * 2018-11-16 2019-03-01 中国石油天然气股份有限公司 Gas storage reservoir injection and production well annular pressure treatment method

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