CN110682721A - Method for making cinnabar inlaid picture - Google Patents
Method for making cinnabar inlaid picture Download PDFInfo
- Publication number
- CN110682721A CN110682721A CN201910859628.XA CN201910859628A CN110682721A CN 110682721 A CN110682721 A CN 110682721A CN 201910859628 A CN201910859628 A CN 201910859628A CN 110682721 A CN110682721 A CN 110682721A
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- parts
- cinnabar
- pattern
- adhesive
- making
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
- B44C5/04—Ornamental plaques, e.g. decorative panels, decorative veneers
- B44C5/043—Ornamental plaques, e.g. decorative panels, decorative veneers containing wooden elements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44D—PAINTING OR ARTISTIC DRAWING, NOT OTHERWISE PROVIDED FOR; PRESERVING PAINTINGS; SURFACE TREATMENT TO OBTAIN SPECIAL ARTISTIC SURFACE EFFECTS OR FINISHES
- B44D2/00—Special techniques in artistic painting or drawing, e.g. oil painting, water painting, pastel painting, relief painting
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
- C09D171/02—Polyalkylene oxides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
- C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention relates to the technical field of industrial art, in particular to a method for manufacturing a cinnabar mosaic picture, which comprises the following steps: (1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials; (2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished; (3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified. According to the manufacturing method of the cinnabar inlaid picture, the cinnabar and the inlaid base surface are firmly adhered together by the adhesive and the curing agent, are not easy to fall off and are permanently stored; the color protecting liquid can effectively prevent cinnabar from fading and cracking caused by high temperature, high humidity, ultraviolet light, microorganisms and the like, so that the prepared mosaic picture can keep bright color and bright luster for a long time.
Description
Technical Field
The invention relates to the technical field of industrial art, in particular to a method for manufacturing a cinnabar mosaic.
Background
Cinnabar is also called sand, cinnabar, red lead and mercurous chloride, is natural ore of mercurous sulfide, is bright red, has diamond luster to metallic luster, belongs to a trigonal crystal system, has plate-shaped or soil-shaped crystals, and often has rhombic double crystals and large-particle single crystals, and is semitransparent or opaque. The light-sensitive adhesive is crisp in nature, sensitive to light, high in refractive index, 2-2.5 in hardness, 8.09-8.2 in specific gravity, light in weight and crisp in texture, flaky people are easy to break, and powdery people have glittering luster and are tasteless. The main component of cinnabar is mercuric sulfide, but it is often mixed with realgar, apatite, asphaltene, etc. Cinnabar has the name of 'soft ruby', and the cinnabar painting is the traditional handicraft in China. However, the cinnabar painting on the market is mainly drawn by cinnabar ink or cinnabar color or made by simple cinnabar powder. The pattern is simple and the visual effect is poor.
The mosaic picture is made of colored stones, ceramic pieces, enamel or colored glass blocks. The mosaic painting takes hard materials as the mosaic raw materials, the texture and the sense of quality of the hard materials and the shape, the color and the light effects generated by the mosaic technology make the mosaic painting appear rugged and colorful in the aspects of color, quality and sense of quality. The cinnabar is bright in color and hard in texture and can be used as an inlaying raw material for inlaying pictures. For example, CN97114410.9 discloses a method for making an inlaid picture, which comprises pouring a gypsum board on a base surface of the inlaid picture, engraving a pattern on the gypsum board, inlaying with natural materials (such as cinnabar, realgar, iron red, iron blue and carbon black), solidifying, and coating 2-3 layers of unsaturated polyester resin with a curing agent. The cinnabar is directly inlaid on the gypsum board, and the cinnabar and the gypsum board are poor in cohesiveness and easy to fall off.
Disclosure of Invention
In order to solve the technical problems in the prior art, the invention provides a method for making a cinnabar mosaic picture, which is realized by the following technical scheme:
a method for making a cinnabar mosaic picture comprises the following steps:
(1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials;
(2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished;
(3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified.
Preferably, the adhesive is prepared by mixing 20-30 parts of modified soybean protein, 10-16 parts of epoxy resin, 4-5 parts of pentaerythritol tetraester, 12-15 parts of cross-linking agent, 6-8 parts of reinforcing agent and 80-100 parts of water in parts by weight.
Preferably, the modified soy protein is synthesized by grafting modified soy protein with vinyl acetate resin.
Preferably, the cross-linking agent is a glycidyl ester; the reinforcing agent is hydroxy acrylic resin.
Preferably, the curing agent is prepared by mixing 6-8 parts of epoxy resin and 4-5 parts of pentaerythritol tetraester in parts by weight.
Preferably, the protective solution is prepared by mixing 3-5 parts of boric acid, 8-10 parts of polyethylene glycol, 10-16 parts of acrylic resin, 4-6 parts of silicone oil, 0.1-0.2 part of dispersing agent, 0.1-0.2 part of surfactant and 80-100 parts of water in parts by weight.
Preferably, the dispersant is water glass; the surfactant is sodium dodecyl benzene sulfonate.
The invention has the beneficial effects that: adopting modified soy protein, epoxy resin and pentaerythritol tetrapotate as main raw materials to prepare an adhesive; the adhesive has stronger binding power with the veneers with the inlaid base surfaces, meanwhile, the modified soy protein and pentaerythritol tetraester in the adhesive contain a large amount of sulfydryl, and the sulfydryl has good affinity with the main component mercuric sulfide in the cinnabar, so that the cinnabar and the three-ply board can be tightly adhered together; the curing agent further enhances the bonding firmness of the cinnabar and the three-ply board, is not easy to fall off and can be stored permanently. The color protecting liquid prepared from boric acid, polyethylene glycol, acrylic resin, silicone oil, a dispersing agent, a surfactant and water has good antibacterial, cooling, waterproof and weather-resistant properties, and can form a layer of almost colorless transparent film on the surface of cinnabar white, so that cinnabar can be effectively prevented from fading and cracking caused by high temperature, high humidity, ultraviolet light, microorganisms and the like, and the prepared mosaic can keep bright color and bright luster for a long time.
Detailed Description
The technical solution of the present invention is further defined below with reference to the specific embodiments, but the scope of the claims is not limited to the description.
Example 1
A method for making a cinnabar mosaic picture comprises the following steps:
(1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials;
(2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished;
(3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified.
The adhesive is prepared by mixing 20g of modified soybean protein, 10g of epoxy resin, 4g of pentaerythritol tetraester, 12g of cross-linking agent, 6g of reinforcing agent and 80g of water in parts by weight.
The modified soybean protein is synthesized by grafting modified soybean protein with vinyl acetate resin.
The cross-linking agent is glycidyl ester; the reinforcing agent is hydroxy acrylic resin.
The curing agent is prepared by mixing 6g of epoxy resin and 4g of pentaerythritol tetraester in parts by weight.
The protective solution is prepared by mixing 3g of boric acid, 8g of polyethylene glycol, 10g of acrylic resin, 4g of silicone oil, 0.1g of dispersing agent, 0.1g of surfactant and 80g of water in parts by weight.
The dispersing agent is water glass; the surfactant is sodium dodecyl benzene sulfonate.
Example 2
A method for making a cinnabar mosaic picture comprises the following steps:
(1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials;
(2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished;
(3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified.
The adhesive is prepared by mixing 24g of modified soybean protein, 12g of epoxy resin, 4g of pentaerythritol tetraester, 14g of cross-linking agent, 7g of reinforcing agent and 90g of water in parts by weight.
The modified soybean protein is synthesized by grafting modified soybean protein with vinyl acetate resin.
The cross-linking agent is glycidyl ester; the reinforcing agent is hydroxy acrylic resin.
The curing agent is prepared by mixing 7g of epoxy resin and 5g of pentaerythritol tetraester in parts by weight.
The protective solution is prepared by mixing 4g of boric acid, 8g of polyethylene glycol, 12g of acrylic resin, 5g of silicone oil, 0.15g of dispersing agent, 0.5g of surfactant and 90g of water in parts by weight.
The dispersing agent is water glass; the surfactant is sodium dodecyl benzene sulfonate.
Example 3
A method for making a cinnabar mosaic picture comprises the following steps:
(1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials;
(2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished;
(3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified.
The adhesive is prepared by mixing 30g of modified soybean protein, 16g of epoxy resin, 5g of pentaerythritol tetraester, 15g of cross-linking agent, 8g of reinforcing agent and 100g of water in parts by weight.
The modified soybean protein is synthesized by grafting modified soybean protein with vinyl acetate resin.
The cross-linking agent is glycidyl ester; the reinforcing agent is hydroxy acrylic resin.
The curing agent is prepared by mixing 6-8 parts of epoxy resin and 4-5 parts of pentaerythritol tetraester in parts by weight.
The protective solution is prepared by mixing 5g of boric acid, 10g of polyethylene glycol, 16g of acrylic resin, 6g of silicone oil, 0.2g of dispersing agent, 0.2g of surfactant and 100g of water in parts by weight.
The dispersing agent is water glass; the surfactant is sodium dodecyl benzene sulfonate.
Comparative example 1
Comparative example 1 is different from example 1 in that the pattern formation is completed without coating a color protection liquid.
Comparative example 2
The difference between the comparative example 2 and the example 1 is that the conventional fixing solution, not the color protection solution, is coated after the pattern is formed.
Comparative example 3
Comparative example 3 differs from example 1 in that the curing agent is applied after the setting is completed.
Comparative example 4
Comparative example 4 a mosaic was made as disclosed in CN 97114410.9.
The mosaic paintings made in examples 1 to 3 and comparative examples 1 to 4 were left in an environment of high temperature (60 ℃ C. -65 ℃ C.) and high humidity (80% or more) for 40 days. The results show that the paintings made in examples 1-3 still remained pure red, and had uniform color, bright luster, and no cracks, looseness, or falling of cinnabar. The painting of comparative example 1 showed small-area fading, dull luster, few cracks of cinnabar, and no loosening or falling of cinnabar. The painted surface of comparative example 2 had very little discoloration of cinnabar, dull luster, and no cracking, loosening, or falling of cinnabar. The painting of comparative example 3 kept pure red, and had uniform color and luster, and had the condition that very little cinnabar was loose, and no cinnabar was cracked and dropped. The painting of comparative example 4 remained red, had a uniform color and a dull luster, and exhibited loosening and cracking of very few vermilion and no shedding of vermilion;
it should be noted that the above examples and test examples are only for further illustration and understanding of the technical solutions of the present invention, and are not to be construed as further limitations of the technical solutions of the present invention, and the invention which does not highlight essential features and significant advances made by those skilled in the art still belongs to the protection scope of the present invention.
Claims (7)
1. The manufacturing method of the cinnabar mosaic picture is characterized by comprising the following steps of:
(1) preparing an adhesive: preparing an adhesive by taking modified soybean protein, epoxy resin, pentaerythritol tetraester, a cross-linking agent, a reinforcing agent and water as raw materials;
(2) pattern making: the plywood is used as an embedding base surface, pattern female patterns are carved on the plywood, after a layer of adhesive is coated on the pattern female patterns, cinnabar is immediately used for embedding, and a layer of curing agent is sprayed after the embedding is finished;
(3) color protection: and coating a layer of protective liquid on the surface of the pattern after the pattern is solidified.
2. The method for making a cinnabar mosaic picture according to claim 1, wherein the adhesive is prepared by mixing, by weight, 20-30 parts of modified soy protein, 10-16 parts of epoxy resin, 4-5 parts of pentaerythritol tetraester, 12-15 parts of a cross-linking agent, 6-8 parts of a reinforcing agent and 80-100 parts of water.
3. The method for making a vermilion mosaic according to claim 1 or 2, wherein said modified soy protein is synthesized by grafting modified soy protein with vinyl acetate resin.
4. The method for manufacturing a vermilion mosaic according to claim 1 or 2, wherein said cross-linking agent is glycidyl ester; the reinforcing agent is hydroxy acrylic resin.
5. The method for making a cinnabar mosaic picture according to claim 1, wherein said curing agent is prepared by mixing 6-8 parts by weight of epoxy resin and 4-5 parts by weight of pentaerythritol tetraester.
6. The method for making a vermilion mosaic according to claim 1, wherein said protective solution is prepared by mixing, by weight, 3-5 parts of boric acid, 8-10 parts of polyethylene glycol, 10-16 parts of acrylic resin, 4-6 parts of silicone oil, 0.1-0.2 part of a dispersing agent, 0.1-0.2 part of a surfactant, and 80-100 parts of water.
7. The method for making a vermilion mosaic according to claim 6, wherein said dispersing agent is water glass; the surfactant is sodium dodecyl benzene sulfonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910859628.XA CN110682721A (en) | 2019-09-11 | 2019-09-11 | Method for making cinnabar inlaid picture |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910859628.XA CN110682721A (en) | 2019-09-11 | 2019-09-11 | Method for making cinnabar inlaid picture |
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| CN110682721A true CN110682721A (en) | 2020-01-14 |
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| CN201910859628.XA Pending CN110682721A (en) | 2019-09-11 | 2019-09-11 | Method for making cinnabar inlaid picture |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113561697A (en) * | 2021-07-27 | 2021-10-29 | 唐秀伟 | Preparation method of cinnabar picture |
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| CN1060259A (en) * | 1991-08-17 | 1992-04-15 | 王新民 | The manufacturing process of glass-inlaid picture |
| CN1204588A (en) * | 1997-07-08 | 1999-01-13 | 刘志赝 | Method for manufacturing mosaic |
| CN101450899A (en) * | 2007-12-01 | 2009-06-10 | 西北师范大学 | Pentaerythrite tetra(2-methyl-1,2-dibromoacrylate) and preparation method thereof |
| DE102011080300A1 (en) * | 2011-08-02 | 2013-02-07 | Surface Technologies Gmbh & Co. Kg | Method of making a decorated wall, ceiling or floor panel |
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| CN105153998A (en) * | 2015-08-28 | 2015-12-16 | 北京林业大学 | Adhesive for artificial board and preparation method of adhesive |
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2019
- 2019-09-11 CN CN201910859628.XA patent/CN110682721A/en active Pending
Patent Citations (7)
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|---|---|---|---|---|
| CN1060259A (en) * | 1991-08-17 | 1992-04-15 | 王新民 | The manufacturing process of glass-inlaid picture |
| CN1204588A (en) * | 1997-07-08 | 1999-01-13 | 刘志赝 | Method for manufacturing mosaic |
| CN101450899A (en) * | 2007-12-01 | 2009-06-10 | 西北师范大学 | Pentaerythrite tetra(2-methyl-1,2-dibromoacrylate) and preparation method thereof |
| DE102011080300A1 (en) * | 2011-08-02 | 2013-02-07 | Surface Technologies Gmbh & Co. Kg | Method of making a decorated wall, ceiling or floor panel |
| CN104532669A (en) * | 2014-12-05 | 2015-04-22 | 鲁继烈 | Water-tolerant light-resistant ozone-proof composition for protection of character image and cultural relics |
| CN105153998A (en) * | 2015-08-28 | 2015-12-16 | 北京林业大学 | Adhesive for artificial board and preparation method of adhesive |
| CN109383181A (en) * | 2018-11-27 | 2019-02-26 | 铜仁市万山区天下红朱砂工艺有限责任公司 | A kind of production method of embossment Cinnabar picture |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113561697A (en) * | 2021-07-27 | 2021-10-29 | 唐秀伟 | Preparation method of cinnabar picture |
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