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CN110668880A - Method for producing carrot liquid organic fertilizer from pomace after apple pectin extraction - Google Patents

Method for producing carrot liquid organic fertilizer from pomace after apple pectin extraction Download PDF

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Publication number
CN110668880A
CN110668880A CN201911091487.8A CN201911091487A CN110668880A CN 110668880 A CN110668880 A CN 110668880A CN 201911091487 A CN201911091487 A CN 201911091487A CN 110668880 A CN110668880 A CN 110668880A
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China
Prior art keywords
pomace
organic fertilizer
liquid organic
fermentation
carrots
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CN201911091487.8A
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Chinese (zh)
Inventor
王琴
常晓明
刑子刚
刘巍
李印朝
贾振领
杨慧
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Dangshan Haisheng Pectin Co Ltd
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Dangshan Haisheng Pectin Co Ltd
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Priority to CN201911091487.8A priority Critical patent/CN110668880A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

A method for producing a carrot liquid organic fertilizer by using pomace after apple pectin extraction is characterized in that auxiliary materials, microbial inoculum types and addition proportions are reasonably configured to achieve the effect of promoting liquid fermentation of pomace waste, and the pomace is used as an organic material rich in nutrient substances to produce the liquid organic fertilizer through microbial liquid fermentation. The invention has the beneficial effects that: (1) according to the invention, the liquid organic fertilizer required by growth of carrots is prepared by fully utilizing apple pomace, so that the beneficial effect of changing waste into valuable is achieved; (2) the carrot-containing compound fertilizer is rich in various amino acids and physiological active substances which are necessary for the growth of carrots, is applied to a carrot field, obviously promotes the growth of the carrots, and meanwhile, the carrots are more bright red in color.

Description

Method for producing carrot liquid organic fertilizer from pomace after apple pectin extraction
Technical Field
The invention belongs to the field of pectin preparation, and particularly relates to a method for producing a carrot liquid organic fertilizer by extracting apple pectin residues.
Background
Pectin is a natural high molecular compound, has good gelling and emulsifying stabilizing effects, and is widely used in food, medicine, daily chemical and textile industries. The pomelo peel is rich in pectin, the content of the pomelo peel reaches about 6 percent, and the pomelo peel is an ideal raw material for preparing pectin. Pectin is divided into pectin liquid, pectin powder and low methoxyl pectin, wherein the pectin powder is most commonly applied. Pectin powder and low methoxyl pectin can be prepared from pericarpium Citri Grandis. Pectin extracted from apple is also rich.
Liquid fertilizer, liquid fertilizer for short. Refers to a fertilizer that is fluid without a certain shape. The liquid fertilizer mainly comprises a clear liquid type and a suspension type, and is mainly produced in China, for example, ammonium phosphate solutions with different concentrations, which are produced by neutralizing liquid ammonia with phosphoric acid, superphosphoric acid and polyphosphoric acid, are commonly used liquid fertilizers. If it is dissolved in other nitrogen fertilizer, potassium chloride and medium and trace elements, the multi-element liquid compound fertilizer can be produced.
The apple has pomace waste after being prepared into pectin, and if the pomace waste is directly discarded, unnecessary waste is caused, and the post-treatment is also a burden.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides a method for producing a carrot liquid organic fertilizer by using pomace after apple pectin is extracted.
In order to solve the technical problems, the technical scheme of the invention is as follows:
a method for producing a carrot liquid organic fertilizer by using pomace after apple pectin extraction comprises the following steps:
① adding a certain amount of bean pulp, brown sugar, rice bran, brewer's grains and pure water into the fruit residues according to the water content, organic matter and total nitrogen, phosphorus and potassium content of the fruit residues, and stirring and mixing to obtain a mixed material A;
②, adding an acid-base adjusting material according to 0.72mol (NH 3)/kg dry matter amount so as to adjust the pH value of the mixed material to 6.5-7.5;
③, after adjusting the pH value, adding a fermentation inoculum into the material obtained in the step ② according to the proportion of 2-10 g/kg dry material amount, and spraying or spreading to obtain a mixed material B;
④, stirring the mixed material B by a pneumatic stirring device, and adding oxygen for 5 minutes;
⑤, passing the material obtained in the step ④ through a clean gauze, covering with double layers, fastening, and fermenting at room temperature in a cool and ventilated place for 20-30 days;
⑥ stirring and oxygenating the ④ materials every day for 5-10 minutes during daily fermentation, timely performing covering operation, measuring the fermentation temperature every day, and periodically monitoring the pH and the EC so as to accurately control the fermentation process of the materials;
⑦ at the later stage of fermentation, layering the clear liquid and the residue of the materials, filtering the supernatant to obtain a filtrate, distilling the filtrate at 83-86 ℃ for 20-30 minutes, discarding the distillate, adding potassium fulvate, polyacrylamide, potassium dihydrogen phosphate, sodium tetraborate, ammonium molybdate, ferrous sulfate, gibberellin, magnesium chloride and citric acid into the distilled filtrate, and uniformly mixing to obtain the liquid organic fertilizer.
Preferably, the C/N ratio of the mixture obtained in step ① is 25:1, the moisture content is 94%, and the dry matter is 6%.
Preferably, the acid-base adjusting material in step ② is a potassium hydroxide solution.
Preferably, the zymophyte agent in the step ③ is specifically an EM agent.
Preferably, the stirring speed in the step ④ is 600-800 r/min.
The invention has the beneficial effects that: (1) according to the invention, the liquid organic fertilizer required by growth of carrots is prepared by fully utilizing apple pomace, so that the beneficial effect of changing waste into valuable is achieved; (2) the carrot-containing compound fertilizer is rich in various amino acids and physiological active substances which are necessary for the growth of carrots, is applied to a carrot field, obviously promotes the growth of the carrots, and meanwhile, the carrots are more bright red in color.
Detailed Description
In order to provide a further understanding and appreciation for the structural features and advantages achieved by the present invention, the following detailed description of the preferred embodiments is provided:
example 1
A method for producing a carrot liquid organic fertilizer by using pomace after apple pectin extraction comprises the following steps:
① adding a certain amount of bean pulp, brown sugar, rice bran, brewer's grains and pure water into the fruit residues according to the water content, organic matter and total nitrogen, phosphorus and potassium content of the fruit residues, and stirring and mixing to obtain a mixed material A;
②, adding an acid-base adjusting material according to 0.72mol (NH 3)/kg dry matter amount so as to adjust the pH value of the mixed material to 6.5-7.5;
③, after adjusting the pH value, adding a zymophyte agent into the material obtained in the step ② according to the proportion of 2g/kg dry material amount, and spraying or spreading to obtain a mixed material B;
④, stirring the mixed material B by a pneumatic stirring device, and adding oxygen for 5 minutes;
⑤ passing the material obtained in step ④ through clean gauze, covering with double layers, fastening, and fermenting at room temperature for 20 days;
⑥ stirring the ④ materials every day, adding oxygen for 5 minutes, covering in time, measuring the fermentation temperature every day, and monitoring pH and EC regularly to control the fermentation process of the materials accurately;
⑦ at the later stage of fermentation, layering the clear liquid and the residue, filtering the supernatant to obtain a filtrate, distilling the filtrate at 83 deg.C for 20 min and discarding the distillate, adding potassium fulvate, polyacrylamide, potassium dihydrogen phosphate, sodium tetraborate, ammonium molybdate, ferrous sulfate, gibberellin, magnesium chloride and citric acid into the distilled filtrate, and mixing to obtain the liquid organic fertilizer.
The content of C/N in the mixed material obtained in the step ① is 25:1, the content of water is 94%, and the content of dry materials is 6%. the acid-base adjusting material in the step ② is a potassium hydroxide solution, the fermentation microbial inoculum in the step ③ is an EM microbial inoculum, and the stirring speed in the step ④ is 600 r/min.
Example 2
A method for producing a carrot liquid organic fertilizer by using pomace after apple pectin extraction comprises the following steps:
① adding a certain amount of bean pulp, brown sugar, rice bran, brewer's grains and pure water into the fruit residues according to the water content, organic matter and total nitrogen, phosphorus and potassium content of the fruit residues, and stirring and mixing to obtain a mixed material A;
②, adding an acid-base adjusting material according to 0.72mol (NH 3)/kg dry matter amount so as to adjust the pH value of the mixed material to 6.5-7.5;
③, after adjusting the pH value, adding a zymophyte agent into the material obtained in the step ② according to the proportion of 10g/kg dry material amount, and spraying or spreading to obtain a mixed material B;
④, stirring the mixed material B by a pneumatic stirring device, and adding oxygen for 5 minutes;
⑤ passing the material obtained in step ④ through clean gauze, covering with double layers, fastening, and fermenting at room temperature in a cool and ventilated place for 30 days;
⑥ stirring the ④ materials every day, adding oxygen for 10 minutes, covering in time, measuring the fermentation temperature every day, and monitoring pH and EC regularly to control the fermentation process of the materials accurately;
⑦ at the later stage of fermentation, layering the clear liquid and the residue, filtering the supernatant to obtain a filtrate, distilling the filtrate at 86 deg.C for 30 min and discarding the distillate, adding potassium fulvate, polyacrylamide, potassium dihydrogen phosphate, sodium tetraborate, ammonium molybdate, ferrous sulfate, gibberellin, magnesium chloride and citric acid into the distilled filtrate, and mixing to obtain the liquid organic fertilizer.
The content of C/N in the mixed material obtained in the step ① is 25:1, the content of water is 94%, and the content of dry materials is 6%. the acid-base adjusting material in the step ② is a potassium hydroxide solution, the fermentation microbial inoculum in the step ③ is an EM microbial inoculum, and the stirring speed in the step ④ is 800 r/min.
Example 3
A method for producing a carrot liquid organic fertilizer by using pomace after apple pectin extraction comprises the following steps:
① adding a certain amount of bean pulp, brown sugar, rice bran, brewer's grains and pure water into the fruit residues according to the water content, organic matter and total nitrogen, phosphorus and potassium content of the fruit residues, and stirring and mixing to obtain a mixed material A;
②, adding an acid-base adjusting material according to 0.72mol (NH 3)/kg dry matter amount so as to adjust the pH value of the mixed material to 6.5-7.5;
③, after adjusting the pH value, adding a zymophyte agent into the material obtained in the step ② according to the proportion of 6g/kg dry material amount, and spraying or spreading to obtain a mixed material B;
④, stirring the mixed material B by a pneumatic stirring device, and adding oxygen for 5 minutes;
⑤ passing the material obtained in step ④ through clean gauze, covering with double layers, fastening, and fermenting at room temperature in a cool and ventilated place for 25 days;
⑥ stirring the ④ materials every day, adding oxygen for 8 minutes, covering in time, measuring the fermentation temperature every day, and monitoring pH and EC regularly to control the fermentation process of the materials accurately;
⑦ at the later stage of fermentation, layering the clear liquid and the residue, filtering the supernatant to obtain a filtrate, distilling the filtrate at 85 deg.C for 25 min and discarding the distillate, adding potassium fulvate, polyacrylamide, potassium dihydrogen phosphate, sodium tetraborate, ammonium molybdate, ferrous sulfate, gibberellin, magnesium chloride and citric acid into the distilled filtrate, and mixing to obtain the liquid organic fertilizer.
The content of C/N in the mixed material obtained in the step ① is 25:1, the content of water is 94%, and the content of dry materials is 6%. the acid-base adjusting material in the step ② is a potassium hydroxide solution, the fermentation microbial inoculum in the step ③ is an EM microbial inoculum, and the stirring speed in the step ④ is 700 r/min.
The method achieves the effect of promoting the liquid fermentation of the pomace waste by reasonably configuring the types and the adding proportion of the auxiliary materials, the microbial inoculum and the microbial inoculum, and achieves the purpose of changing waste into valuable by utilizing pomace as an organic material rich in nutrient substances and producing a liquid organic fertilizer through microbial liquid fermentation.
The effects of the liquid organic fertilizer obtained in examples 1 to 3 are shown in the following tables 1 and 2:
Figure 647972DEST_PATH_IMAGE001
Figure 240758DEST_PATH_IMAGE002
the foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are merely illustrative of the principles of the invention, but that various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (5)

1.① adding a certain amount of bean pulp, brown sugar, rice bran, brewer's grains and pure water into the pomace according to the water content, organic matter and total nitrogen, phosphorus and potassium content of pomace waste, stirring and mixing to obtain a mixed material A;
②, adding an acid-base adjusting material according to 0.72mol (NH 3)/kg dry matter amount so as to adjust the pH value of the mixed material to 6.5-7.5;
③, after adjusting the pH value, adding a fermentation inoculum into the material obtained in the step ② according to the proportion of 2-10 g/kg dry material amount, and spraying or spreading to obtain a mixed material B;
④, stirring the mixed material B by a pneumatic stirring device, and adding oxygen for 5 minutes;
⑤, passing the material obtained in the step ④ through a clean gauze, covering with double layers, fastening, and fermenting at room temperature in a cool and ventilated place for 20-30 days;
⑥ stirring and oxygenating the ④ materials every day for 5-10 minutes during daily fermentation, timely performing covering operation, measuring the fermentation temperature every day, and periodically monitoring the pH and the EC so as to accurately control the fermentation process of the materials;
⑦ at the later stage of fermentation, layering the clear liquid and the residue of the materials, filtering the supernatant to obtain a filtrate, distilling the filtrate at 83-86 ℃ for 20-30 minutes, discarding the distillate, adding potassium fulvate, polyacrylamide, potassium dihydrogen phosphate, sodium tetraborate, ammonium molybdate, ferrous sulfate, gibberellin, magnesium chloride and citric acid into the distilled filtrate, and uniformly mixing to obtain the liquid organic fertilizer.
2. The method for producing liquid organic fertilizer for carrot from pomace obtained after apple pectin extraction according to claim 1, wherein C/N in the mixed material obtained in the step ① is 25:1, water content is 94%, and dry matter is 6%.
3. The method for producing liquid organic fertilizer containing carrot extracted from pomace after apple pectin according to claim 1, wherein the acid-base adjusting material in step ② is potassium hydroxide solution.
4. The method for producing the liquid organic fertilizer for carrots from the pomace after apple pectin extraction according to claim 1, wherein the fermentation microbial inoculum in the step ③ is an EM microbial inoculum.
5. The method for producing the liquid organic fertilizer for carrots from the pomace after apple pectin extraction according to claim 1, wherein the stirring speed in the step ④ is 600-800 r/min.
CN201911091487.8A 2019-11-10 2019-11-10 Method for producing carrot liquid organic fertilizer from pomace after apple pectin extraction Pending CN110668880A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022018184A1 (en) * 2020-07-22 2022-01-27 Herbstreith & Fox Gmbh & Co. Kg Pektin-Fabriken Use of an activated carrot fiber for producing products

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1891677A (en) * 2006-02-10 2007-01-10 中国科学院遗传与发育生物学研究所 Apple residue comprehensive utilizing and treating method
CN1974490A (en) * 2006-12-11 2007-06-06 陈五岭 Process of fermenting waste from farm and sideline product processing to produce fulvic acid bacterial manure
CN102219564A (en) * 2011-04-13 2011-10-19 富县宏佳果贸有限责任公司 Organic potash fertilizer and production method thereof
CN106242758A (en) * 2016-08-03 2016-12-21 桂林实力科技有限公司 The Application way of Fructus Momordicae marc
CN108164315A (en) * 2018-03-21 2018-06-15 合肥师范学院 A kind of preparation method of the special amino acid foliage fertilizer of blueberry
CN108997052A (en) * 2018-07-10 2018-12-14 来安县薜必英家庭农场 A kind of upland rice foliar fertilizer

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1891677A (en) * 2006-02-10 2007-01-10 中国科学院遗传与发育生物学研究所 Apple residue comprehensive utilizing and treating method
CN1974490A (en) * 2006-12-11 2007-06-06 陈五岭 Process of fermenting waste from farm and sideline product processing to produce fulvic acid bacterial manure
CN102219564A (en) * 2011-04-13 2011-10-19 富县宏佳果贸有限责任公司 Organic potash fertilizer and production method thereof
CN106242758A (en) * 2016-08-03 2016-12-21 桂林实力科技有限公司 The Application way of Fructus Momordicae marc
CN108164315A (en) * 2018-03-21 2018-06-15 合肥师范学院 A kind of preparation method of the special amino acid foliage fertilizer of blueberry
CN108997052A (en) * 2018-07-10 2018-12-14 来安县薜必英家庭农场 A kind of upland rice foliar fertilizer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022018184A1 (en) * 2020-07-22 2022-01-27 Herbstreith & Fox Gmbh & Co. Kg Pektin-Fabriken Use of an activated carrot fiber for producing products

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Application publication date: 20200110