CN110655986A - Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof - Google Patents
Honey and grapefruit compound-flavor electronic cigarette oil and preparation method thereof Download PDFInfo
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- CN110655986A CN110655986A CN201910909298.0A CN201910909298A CN110655986A CN 110655986 A CN110655986 A CN 110655986A CN 201910909298 A CN201910909298 A CN 201910909298A CN 110655986 A CN110655986 A CN 110655986A
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- phenylacetate
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 52
- 240000000560 Citrus x paradisi Species 0.000 title claims abstract description 30
- 235000012907 honey Nutrition 0.000 title claims abstract description 29
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000003921 oil Substances 0.000 claims abstract description 31
- 235000019198 oils Nutrition 0.000 claims abstract description 31
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 20
- CRZQGDNQQAALAY-UHFFFAOYSA-N Methyl benzeneacetate Chemical compound COC(=O)CC1=CC=CC=C1 CRZQGDNQQAALAY-UHFFFAOYSA-N 0.000 claims abstract description 20
- LRVLBFSVAFUOGO-UHFFFAOYSA-N amyl phenylacetate Chemical compound CCCCCOC(=O)CC1=CC=CC=C1 LRVLBFSVAFUOGO-UHFFFAOYSA-N 0.000 claims abstract description 20
- MMXKVMNBHPAILY-UHFFFAOYSA-N ethyl laurate Chemical compound CCCCCCCCCCCC(=O)OCC MMXKVMNBHPAILY-UHFFFAOYSA-N 0.000 claims abstract description 20
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 claims abstract description 18
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims abstract description 11
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 10
- JLIDRDJNLAWIKT-UHFFFAOYSA-N 1,2-dimethyl-3h-benzo[e]indole Chemical compound C1=CC=CC2=C(C(=C(C)N3)C)C3=CC=C21 JLIDRDJNLAWIKT-UHFFFAOYSA-N 0.000 claims abstract description 10
- RJASFPFZACBKBE-UHFFFAOYSA-N 2-Methylpropyl phenylacetate Chemical compound CC(C)COC(=O)CC1=CC=CC=C1 RJASFPFZACBKBE-UHFFFAOYSA-N 0.000 claims abstract description 10
- WLJVXDMOQOGPHL-PPJXEINESA-N 2-phenylacetic acid Chemical compound O[14C](=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-PPJXEINESA-N 0.000 claims abstract description 10
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 10
- CDJJKTLOZJAGIZ-UHFFFAOYSA-N Tolylacetate Chemical compound CC(=O)OC1=CC=C(C)C=C1 CDJJKTLOZJAGIZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000001416 apis mellifera l. absolute Substances 0.000 claims abstract description 10
- DULCUDSUACXJJC-UHFFFAOYSA-N benzeneacetic acid ethyl ester Natural products CCOC(=O)CC1=CC=CC=C1 DULCUDSUACXJJC-UHFFFAOYSA-N 0.000 claims abstract description 10
- MDHYEMXUFSJLGV-UHFFFAOYSA-N phenethyl acetate Chemical compound CC(=O)OCCC1=CC=CC=C1 MDHYEMXUFSJLGV-UHFFFAOYSA-N 0.000 claims abstract description 10
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims abstract description 10
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000012141 vanillin Nutrition 0.000 claims abstract description 10
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 claims abstract description 10
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims abstract description 9
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims abstract description 9
- 229940093503 ethyl maltol Drugs 0.000 claims abstract description 9
- 239000001327 prunus amygdalus amara l. extract Substances 0.000 claims abstract description 9
- 229930007850 β-damascenone Natural products 0.000 claims abstract description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 23
- 150000001875 compounds Chemical class 0.000 claims description 9
- 239000010622 buchu oil Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- 150000002576 ketones Chemical class 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 abstract description 27
- 235000019634 flavors Nutrition 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 5
- WTOYNNBCKUYIKC-JMSVASOKSA-N (+)-nootkatone Chemical compound C1C[C@@H](C(C)=C)C[C@@]2(C)[C@H](C)CC(=O)C=C21 WTOYNNBCKUYIKC-JMSVASOKSA-N 0.000 abstract description 2
- 244000061176 Nicotiana tabacum Species 0.000 abstract description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 2
- WTOYNNBCKUYIKC-UHFFFAOYSA-N dl-nootkatone Natural products C1CC(C(C)=C)CC2(C)C(C)CC(=O)C=C21 WTOYNNBCKUYIKC-UHFFFAOYSA-N 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- ZOZIRNMDEZKZHM-UHFFFAOYSA-N Phenethyl phenylacetate Chemical compound C=1C=CC=CC=1CCOC(=O)CC1=CC=CC=C1 ZOZIRNMDEZKZHM-UHFFFAOYSA-N 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 7
- 235000011187 glycerol Nutrition 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- 235000019504 cigarettes Nutrition 0.000 description 5
- 239000002131 composite material Substances 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 5
- 238000005303 weighing Methods 0.000 description 4
- 238000007865 diluting Methods 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 102000004316 Oxidoreductases Human genes 0.000 description 2
- 108090000854 Oxidoreductases Proteins 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 229960002715 nicotine Drugs 0.000 description 2
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 2
- IXQGCWUGDFDQMF-UHFFFAOYSA-N o-Hydroxyethylbenzene Natural products CCC1=CC=CC=C1O IXQGCWUGDFDQMF-UHFFFAOYSA-N 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- ROTNQFPVXVZSRL-UHFFFAOYSA-N 4,4,6-trimethyl-7-oxabicyclo[4.1.0]heptan-2-one Chemical compound C1C(C)(C)CC(=O)C2OC21C ROTNQFPVXVZSRL-UHFFFAOYSA-N 0.000 description 1
- BGTBFNDXYDYBEY-FNORWQNLSA-N 4-(2,6,6-Trimethylcyclohex-1-enyl)but-2-en-4-one Chemical compound C\C=C\C(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-FNORWQNLSA-N 0.000 description 1
- 235000019489 Almond oil Nutrition 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 244000276331 Citrus maxima Species 0.000 description 1
- 235000001759 Citrus maxima Nutrition 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000008168 almond oil Substances 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002608 insulinlike Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- -1 paraquat ketone Chemical class 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the technical field of tobacco essence and flavor, in particular to honey pomelo compound-flavor electronic cigarette oil and a preparation method thereof. The electronic cigarette oil comprises, by mass, 0.5-3 parts of phenethyl acetate, 0.1-0.5 part of phenylacetic acid, 0.2-1.0 part of p-cresol acetate, 0.5-3 parts of methyl phenylacetate, 0.1-0.5 part of menthyl acetate, 1.5-5.0 parts of isobutyl phenylacetate, 0.2-0.8 part of ethyl phenylacetate, 0.5-3.5 parts of damascenone, 0.2-0.8 part of natural citral, 0.5-3 parts of beeswax absolute, 0.3-1 part of amyl phenylacetate, 0.2-1.0 part of vanillin, 10-20 parts of benzyl alcohol, 1-5 parts of ethyl laurate, 0.5-3 parts of oxidized isophorone, 2-8 parts of nootkatone, 0.2-1.0 part of bruton oil, 0.2-0 part of bitter almond oil, 1.5-5.5 parts of ethyl maltol and 850 parts of propylene glycol. The electronic cigarette oil with the fragrance of honey pomelo, harmonious and natural fragrance, soft and exquisite smoke and comfortable mouthfeel is obtained by matching a plurality of components, and the electronic cigarette oil is simple in preparation method, low in cost and applicable to large-scale industrial production.
Description
Technical Field
The invention relates to the technical field of tobacco essence and flavor, in particular to honey pomelo compound-flavor electronic cigarette oil and a preparation method thereof.
Background
The electronic cigarette is an electronic product simulating a cigarette, and has the same appearance, smoke, taste and sensation as the cigarette. It is a product which is absorbed by users after nicotine and the like are changed into steam by means of atomization and the like.
The electronic cigarette liquid is electronic atomized liquid used in cooperation with an electronic cigarette, is also a food additive, and can generate mist like cigarettes by heating through an electronic cigarette atomizer. The components are as follows: propylene glycol, vegetable glycerin, flavoring essence and natural extract and nicotine.
At present, the electronic cigarette still has certain deficiencies in the aspects of smoking quality, aroma style characteristics and the like, the development of an essence product suitable for the electronic cigarette is delayed, and a novel essence suitable for the electronic cigarette is urgently needed to solve the problems, so that the aroma amount is increased, the personalized requirements of consumers on aroma are met, and the problems are avoided.
Honey is produced by natural fermentation of honey in honeycomb, and is a yellow-white sticky liquid which contains various inorganic salts with similar concentration to human serum, various organic acids such as vitamins, iron, calcium, copper, manganese, potassium and phosphorus, trace elements beneficial to human health, fructose, glucose, amylase, oxidase, reductase and the like, has the effects of nourishing, moistening dryness, detoxifying, whitening, beautifying and relaxing bowel, and is known as the most perfect nutritional food in nature. The pomelo is a tree of Citrus of Rutaceae, contains abundant nutritional values, contains a large amount of nutritional elements, including protein, organic acid, multiple vitamins, calcium, phosphorus, magnesium, sodium and other trace elements necessary for human body, and the pomelo meat contains abundant vitamin C, insulin-like and other components, so that the pomelo has the effects of reducing blood sugar, blood fat, weight, skin care and beautifying. The honey and grapefruit composite flavor type electronic cigarette oil can endow the electronic cigarette with new flavor type in the application of the electronic cigarette, increase the fragrance amount, improve the smoking quality of the electronic cigarette, and meet the personalized requirements of consumers.
Disclosure of Invention
The invention aims to solve the problems and provides the electronic cigarette oil which has the fragrance of honey pomelo, harmonious and natural fragrance, soft and exquisite smoke and comfortable mouthfeel and the preparation method thereof.
The technical scheme for solving the problems is to provide honey pomelo compound-flavor electronic cigarette oil which comprises, by mass, 0.5-3 parts of phenethyl phenylacetate, 0.1-0.5 part of phenylacetic acid, 0.2-1.0 part of p-cresol acetate, 0.5-3 parts of methyl phenylacetate, 0.1-0.5 part of menthyl acetate, 1.5-5.0 parts of isobutyl phenylacetate, 0.2-0.8 part of ethyl phenylacetate, 0.5-3.5 parts of damascenone, 0.2-0.8 part of natural citral, 0.5-3 parts of beeswax absolute, 0.3-1 part of amyl phenylacetate, 0.2-1.0 part of vanillin, 10-20 parts of benzyl alcohol, 1-5 parts of ethyl laurate, 0.5-3 parts of oxidized isophorone, 2-8 parts of parapomelo ketone, 0.2-1.0 part of buchu oil, 0.2-0.8 part of almond oil and 1.5-5 parts of ethyl phenol, 750 portions of propylene glycol and 850 portions of propylene glycol.
Preferably, the cleaning agent comprises, by mass, 2 parts of phenylethyl phenylacetate, 0.8 part of phenylacetic acid, 0.6 part of p-cresol acetate, 2 parts of methyl phenylacetate, 0.3 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.6 part of ethyl phenylacetate, 2.2 parts of damascenone, 0.5 part of natural citral, 1.2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.7 part of vanillin, 15 parts of benzyl alcohol, 3.2 parts of ethyl laurate, 1.8 parts of oxidized isophorone, 6 parts of paraquat ketone, 0.6 part of brunaxseed oil, 0.6 part of bitter almond oil, 3 parts of ethyl maltol and 785 parts of propylene glycol.
The invention also aims to provide a preparation method of the honey pomelo compound-flavor electronic cigarette oil, which comprises the following steps: the components are evenly mixed according to the mass portion and then diluted to 900-1100 portions.
Preferably, it is diluted with glycerol.
The invention has the beneficial effects that:
1. the natural honey fragrance is prepared by matching and using raw materials such as phenethyl phenylacetate, phenylacetic acid, p-cresol acetate, methyl phenylacetate, menthyl acetate, isobutyl phenylacetate, ethyl phenylacetate, damascenone, natural citral, beeswax absolute, amyl phenylacetate, vanillin, benzyl alcohol, ethyl laurate, isophorone oxide and the like, and the natural honey fragrance is natural, and is transparent and lasting. The main fragrance of the grapefruit is prepared by reasonably matching and using the raw materials such as natural citral, 6 parts of paraguazone, 0.6 part of buchu oil, 0.6 part of bitter almond oil, fruit fragrance such as ethyl maltol and the like, herb fragrance and the like, and the use of the raw materials can improve the overall quality of the essence to different degrees. The essence has high quality, no impurity is separated out during suction, and the feasibility is reliably guaranteed through production verification.
2. Presents the fragrance of the compound honey and the grapefruit and is suitable for the field of electronic cigarette manufacture. The honey pomelo composite fragrance type fruit and fruit vinegar contains various fragrance components including fruity, sour, burnt, sweet, baking, herbal and other fragrance notes, is rich in fragrance note and natural in transition, can better highlight the main fragrance note of the honey pomelo composite fragrance type, is harmonious and natural in fragrance note, soft and fine in smoke and comfortable in taste, improves sensory experience, and meets the individual requirements of consumers.
3. The preparation method is simple and convenient, has low cost, can be used for large-scale industrial production, and has strong practicability.
Detailed Description
The following are specific embodiments of the present invention and further describe the technical solutions of the present invention, but the present invention is not limited to these examples.
Example 1
Weighing the following raw materials in parts by weight: 0.6 part of phenethyl acetate, 0.2 part of phenylacetic acid, 0.3 part of p-cresol acetate, 0.6 part of methyl phenylacetate, 0.2 part of menthyl acetate, 1.8 parts of isobutyl phenylacetate, 0.3 part of ethyl phenylacetate, 0.9 part of damascenone, 0.3 part of natural citral, 0.6 part of beeswax absolute, 0.4 part of amyl phenylacetate, 0.3 part of vanillin, 12 parts of benzyl alcohol, 1.2 parts of ethyl laurate, 0.6 part of oxidized isophorone, 3 parts of naringenone, 0.3 part of buchu oil, 0.3 part of bitter almond oil, 1.7 parts of ethyl maltol and 760 parts of propylene glycol, and then the components are diluted to 1000 parts by glycerol and uniformly stirred to prepare the honey and pomelo compound fragrance electronic cigarette oil 1 for standby.
According to the procedure of adding electronic cigarette oil in the production of electronic cigarettes, the honey pomelo compound fragrance type electronic cigarette oil 1 is added to prepare an electronic cigarette product A.
Example 2
Weighing the following raw materials in parts by weight: 2.9 parts of phenethyl phenylacetate, 0.45 part of phenylacetic acid, 0.9 part of p-cresol acetate, 2.8 parts of methyl phenylacetate, 0.4 part of menthyl acetate, 4.7 parts of isobutyl phenylacetate, 0.7 part of ethyl phenylacetate, 3.3 parts of damascenone, 0.7 part of natural citral, 2.8 parts of beeswax absolute, 0.9 part of amyl phenylacetate, 0.8 part of vanillin, 18 parts of benzyl alcohol, 4.5 parts of ethyl laurate, 2.8 parts of oxidized isophorone, 7.4 parts of pomelo garden ketone, 0.9 part of buchu oil, 0.75 part of bitter almond oil, 5.3 parts of ethyl maltol and 835 parts of propylene glycol, then diluting to 1000 parts by using glycerol, and stirring uniformly to prepare the shaddock compound flavor electronic cigarette oil 2 for later use.
According to the procedure of adding electronic cigarette oil in the production of electronic cigarettes, the honey pomelo compound fragrance type electronic cigarette oil 2 is added to prepare an electronic cigarette product B.
Example 3
Weighing the following raw materials in parts by weight: 1.8 parts of phenethyl phenylacetate, 0.8 part of phenylacetic acid, 0.65 part of p-cresol acetate, 1.6 parts of methyl phenylacetate, 0.35 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.45 part of ethyl phenylacetate, 2 parts of damascenone, 0.65 part of natural citral, 2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.6 part of vanillin, 15 parts of benzyl alcohol, 3 parts of ethyl laurate, 1.7 parts of oxidized isophorone, 5 parts of parapummelone, 0.65 part of buchu oil, 0.5 part of bitter almond oil, 3.6 parts of ethyl maltol and 800 parts of propylene glycol, then diluting the mixture to 1000 parts by using glycerol, and stirring the mixture uniformly to prepare the honey and grapefruit composite flavor type electronic cigarette oil 3 for later use.
And (3) adding the honey pomelo compound-flavor electronic cigarette oil 3 according to the procedure of adding electronic cigarette oil in the electronic cigarette production to prepare an electronic cigarette product C.
In the case of the example 4, the following examples are given,
weighing the following raw materials in parts by weight: 2 parts of phenethyl acetate, 0.8 part of phenylacetic acid, 0.6 part of p-cresol acetate, 2 parts of methyl phenylacetate, 0.3 part of menthyl acetate, 3 parts of isobutyl phenylacetate, 0.6 part of ethyl phenylacetate, 2.2 parts of damascone, 0.5 part of natural citral, 1.2 parts of beeswax absolute, 0.6 part of amyl phenylacetate, 0.7 part of vanillin, 15 parts of benzyl alcohol, 3.2 parts of ethyl laurate, 1.8 parts of oxidized isophorone, 6 parts of nootkatone, 0.6 part of buchu oil, 0.6 part of bitter almond oil, 3 parts of ethyl maltol and 785 parts of propylene glycol, then diluting the mixture to 1000 parts by using 170.3 parts of glycerol, and stirring the mixture uniformly to prepare the honey and grapefruit composite flavor electronic cigarette oil 4 for later use.
And (3) adding the honey pomelo compound fragrance type electronic cigarette oil 4 according to the procedure of adding electronic cigarette oil in the electronic cigarette production to prepare an electronic cigarette product D.
Comparative example 1
760 parts of propylene glycol is weighed, diluted to 1000 parts by using glycerol and uniformly stirred by adopting the same method as in example 1 to prepare blank electronic cigarette oil, and then the blank electronic cigarette oil is prepared into a blank electronic cigarette control.
The evaluation is carried out according to the national bureau smoking evaluation standard, a smoking evaluation group consists of 7 cigarette sensory evaluation experts, sensory evaluation is carried out and scoring is carried out in a dark evaluation mode according to the cigarette sensory quality evaluation standard in the national standard GB 5606.5-2005, and the sensory evaluation scoring table is shown in the following table 1:
as can be seen from table 1, the electronic cigarette tobacco product prepared by adding the honey pomelo compound-flavor electronic cigarette oil into the electronic cigarette has fresh and natural honey and pomelo fragrance in the smoking process, has lasting fragrance, unique fragrance style, full fragrance, slightly improved texture, soft and fine smoke, reduced miscellaneous gas, reduced irritation, comfortable oral cavity, no influence on fragrance harmony, and improved sensory experience of consumers.
The specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (4)
1. The honey and grapefruit compound aroma type electronic cigarette oil is characterized in that: according to the mass portion, the composition comprises 0.5-3 portions of phenethyl acetate, 0.1-0.5 portion of phenylacetic acid, 0.2-1.0 portion of p-cresol acetate, 0.5-3 portions of methyl phenylacetate, 0.1-0.5 portion of menthyl acetate, 1.5-5.0 portions of isobutyl phenylacetate, 0.2-0.8 portion of ethyl phenylacetate, 0.5-3.5 portions of damascenone, 0.2-0.8 portion of natural citral, 0.5-3 portions of beeswax absolute, 0.3-1 portion of amyl phenylacetate, 0.2-1.0 portion of vanillin, 10-20 portions of benzyl alcohol, 1-5 portions of ethyl laurate, 0.5-3 portions of oxidized isophorone, 2-8 portions of paranarione, 0.2-1.0 portion of buchu oil, 0.2-0.8 portion of bitter almond oil, 1.5-5.5 portions of ethyl maltol and 850 portions of propylene glycol.
2. The honey pomelo compound odor type electronic cigarette oil according to claim 1, characterized in that: according to the mass portion, the composition comprises 2 portions of phenethyl acetate, 0.8 portion of phenylacetic acid, 0.6 portion of p-cresol acetate, 2 portions of methyl phenylacetate, 0.3 portion of menthyl acetate, 3 portions of isobutyl phenylacetate, 0.6 portion of ethyl phenylacetate, 2.2 portions of damascenone, 0.5 portion of natural citral, 1.2 portions of beeswax absolute, 0.6 portion of amyl phenylacetate, 0.7 portion of vanillin, 15 portions of benzyl alcohol, 3.2 portions of ethyl laurate, 1.8 portions of oxidized isophorone, 6 portions of parapomelo ketone, 0.6 portion of buchu oil, 0.6 portion of bitter almond oil, 3 portions of ethyl maltol and 785 portions of propylene glycol.
3. A method for preparing honey pomelo compound scent type electronic cigarette oil according to any one of claims 1 to 2, which is characterized in that: the method comprises the following steps: the components are evenly mixed according to the mass portion and then diluted to 900-1100 portions.
4. The preparation method of the honey pomelo compound-flavor electronic cigarette oil according to claim 3, characterized by comprising the following steps: diluted with glycerol.
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Cited By (1)
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| CN116584637A (en) * | 2023-06-21 | 2023-08-15 | 上海百润投资控股集团股份有限公司 | a honey essence |
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