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CN110526556A - A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method - Google Patents

A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method Download PDF

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Publication number
CN110526556A
CN110526556A CN201910918273.7A CN201910918273A CN110526556A CN 110526556 A CN110526556 A CN 110526556A CN 201910918273 A CN201910918273 A CN 201910918273A CN 110526556 A CN110526556 A CN 110526556A
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CN
China
Prior art keywords
extrusion die
glass
glass pipe
manufacturing apparatus
semiconducting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910918273.7A
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Chinese (zh)
Inventor
曹发忠
汪贵华
易家良
潘守芹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nanjing Hengxin Photoelectric Technology Co Ltd
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Nanjing Hengxin Photoelectric Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nanjing Hengxin Photoelectric Technology Co Ltd filed Critical Nanjing Hengxin Photoelectric Technology Co Ltd
Priority to CN201910918273.7A priority Critical patent/CN110526556A/en
Publication of CN110526556A publication Critical patent/CN110526556A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B17/00Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
    • C03B17/04Forming tubes or rods by drawing from stationary or rotating tools or from forming nozzles

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Extrusion Of Metal (AREA)

Abstract

The present invention provides a kind of manufacturing method of semiconducting glass pipe, corresponding glass tube production temperature and viscosity, and except devitrification of glass range, and forming temperature is lower than the operation temperature of usual tuber.The technical solution that this method is implemented is to be squeezed the frit block of heating by turbine lift, compression bar, stripper plate, passes through extrusion die extrusion molding.Flow behavior of the glass flow under squeezed state in channel determines the geometric parameter and running parameter of extrusion die.The vitreum of tubulose is shaped to due to viscid elastic characteristic, the free wxpansion when leaving extrusion die overcomes this deformation after unloading effect by forming auxiliary device.The beneficial effects of the present invention are: for manufacturing accurate in size extraordinary semiconducting glass pipe, it is also applied for other and is easy to crystallization and the narrow special glass manufacture glass tube of forming temperature scope.

Description

A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method
Technical field
The present invention relates to semiconducting glass pipe manufacturing fields, manufacture and fill more specifically to a kind of semiconducting glass pipe It sets.
Background technique
Semiconducting glass pipe needed for manufacturing body conductance microchannel plate, the molding technical requirements of high temperature tubulation are harsher. Because the forming temperature scope of the glass is narrower, and surface volatilization easily causes crystallization during molding making, it is difficult to adopt This glass tube is manufactured with general tuber.
Summary of the invention
The present invention overcomes deficiencies in the prior art, provide a kind of semiconducting glass pipe manufacturing apparatus, utilize glass Thermoplastic property, allow frit to squeeze out by mold with annular channel in the case where being heated and pressurizeed, to obtain accurate in size Semiconducting glass pipe, corresponding glass tube production temperature and viscosity, except devitrification of glass range.
The purpose of the present invention is achieved by following technical proposals.
A kind of semiconducting glass pipe manufacturing apparatus, including rack, pressure unit, hot briquetting portion, molding assisted parts and traction The top of the rack is arranged in portion, the pressure unit, and the hot briquetting portion is arranged in the pressure unit bottom, the traction The lower section in the rack and corresponding to the extrusion die in the hot briquetting portion is arranged in portion, and the molding assisted parts is located at described Between hot briquetting portion and the tractive unit;The molding assisted parts is water-cooling ring and positioning pin, and the stack shell configures bottom-detachable Plate is the pedestal of heating furnace below the bottom plate, and the bottom of the bottom plate is equipped with discharging cooling ring, utilizes institute by the bottom plate State the relative position that positioning pin is aligned between the extrusion die and the screw slider.
Further, the pressure unit includes turbine lift structure, reduction gearbox, compression bar, stripper plate and stack shell, the turbine liter Descending mechanism and reduction gearbox transmission cooperate, and the reduction gearbox is arranged in the frame top, and the turbine lift passes through pressure Bar is connected with the stripper plate, and the stripper plate rises to except the stack shell when frit is added;It is arranged when pressure in institute It states in stack shell, realization is pressed down against the frit heated.
Further, the hot briquetting portion is equipped with heating furnace and the extrusion die, and the heating furnace is for heating stack shell, glass Glass block and extrusion die, the extrusion die include mould body and mold core, form circular passage between the mould body and the mold core, described Circular passage top expands into horn mouth, and the detachable bottom plate of the stack shell is located at below the extrusion die, frit when pressure It is squeezed out via the horn mouth by the circular passage, forms glass tube.
Further, the bell-mouthed subtended angle is 90-150 °.
Further, the ratio of the length and equivalent diameter of the circular passage is 0.5-2.5.
Further, the traction mechanism is made of screw slider and Pneumatic clamping mechanism, the Pneumatic clamping mechanism setting Realize that the glass tube of clamping extrusion molding moves downward on the screw slider.
Further, the stripper plate and the stack shell are made of nichrome.
Further, the compression bar and the bottom plate are made of heat-resistant steel.
Further, the extrusion die is made of aluminium bronze.
A kind of method that glass pipe manufacturing apparatus prepares semiconducting glass pipe:
The frit block of heating is squeezed by turbine lift structure, compression bar, stripper plate, is existed according to glass flow by the first step Flow behavior under squeezed state determines the geometric parameter and running parameter of extrusion die, thus by extrusion die extrusion molding;
Second step is shaped to the vitreum of tubulose in the first step by forming auxiliary device, overcome frit from Free wxpansion bring deformation after unloading effect and molding glass tube is made to precisely align traction device when opening extrusion die.
The invention has the benefit that
The present invention is also applied for other and is easy to crystallization and molding temperature for manufacturing accurate in size extraordinary semiconducting glass pipe The special glass for spending narrow scope manufactures glass tube.
This method utilizes the thermoplastic property of glass, and frit is allowed to squeeze by the mold with annular channel in the case where being heated and pressurizeed Out, to obtain accurate in size semiconducting glass pipe;Corresponding glass tube production temperature and viscosity, are in devitrification of glass model Except enclosing.
Detailed description of the invention
Fig. 1 a, Fig. 1 b are that the experimental model of glass flow Extrusion Flow form is shown;
Fig. 2 is the basic molding equipment schematic diagram of glass tube;
Fig. 3 is the extrusion die and assistant formation structural scheme of mechanism of shaping glass tubes;
In figure:
1, turbine lift structure;2, reduction gearbox;3, compression bar;4, stripper plate;5, stack shell;
6, detachable bottom plate;7, pedestal;8, heating furnace;9, extrusion die;10, mold core;11, horn mouth;
12, circular passage;13, positioning pin;14, cooling ring;15, screw slider;16, clamping device;
17, rack.
Specific embodiment
Below by specific embodiment, further description of the technical solution of the present invention.
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention In attached drawing, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is A part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art Every other embodiment obtained without creative efforts, shall fall within the protection scope of the present invention.
Semiconducting glass pipe manufacturing method in the present invention, corresponding glass tube production temperature and viscosity, are analysed in glass Except brilliant range.The technical solution that this method is implemented is: by turbine lift structure, compression bar, stripper plate by the frit block of heating It squeezes, passes through extrusion die extrusion molding;According to flow behavior of the glass flow under squeezed state, the geometry of extrusion die is determined Parameter and running parameter;The vitreum of tubulose is shaped to due to viscid elastic characteristic, the free wxpansion when leaving extrusion die, by Type auxiliary device overcomes this deformation after unloading effect.
A kind of semiconducting glass pipe manufacturing apparatus as shown in Figure 2,3, including rack 17, pressure unit, hot briquetting portion, molding Assisted parts and tractive unit, the pressure unit are arranged in the top of the rack and extend in the stack shell in the hot briquetting portion, The lower section in the rack and corresponding to hot briquetting portion extrusion die is arranged in the tractive unit, and the molding assists position Between the hot briquetting and the tractive unit, the molding assisted parts adjusts the glass tube that the hot briquetting portion squeezes out Temperature, and molding glass tube is made to precisely align traction device;
The pressure unit includes turbine lift structure 1, reduction gearbox 2, compression bar 3, stripper plate 4 and stack shell 5, turbine lift structure 1 cooperates with the transmission of reduction gearbox 2, and the setting of reduction gearbox 2 is connected by compression bar 3 with stripper plate 4 in 17 top of rack, turbine lift 1, The setting of stripper plate 4 squeezes frit, 5 internal diameter < 100 millimeter of stack shell in stack shell 5, and the pressure of turbine lift structure 1 is 3-10 tons. Turbine lift structure 1 has additional deceleration case 2;Adjust turbine lift structure 1 moves down speed, so that frit passes through extrusion die Speed when lower passage 12 is 2-50 milli m/min.Stripper plate 4 and stack shell 5 are made of nichrome;Compression bar 3 and bottom plate 6 are by resistance to Hot steel is made;
The hot briquetting portion is equipped with heating furnace 8, stack shell 5 and extrusion die, and stack shell 5 is arranged in heating furnace 8, heating furnace 8 Bottom is equipped with extrusion die, and the extrusion die includes mould body and mold core 10, forms circular passage 12 between mould body and mold core 10, squeezes out Mould 9 and mold core 10 are made of aluminium bronze, and the top of circular passage 12 expands into horn mouth 11;The temperature of heating furnace 8 is adjusted, with control The forming temperature of frit processed, so that viscosity when frit is by circular passage 12 is 106.5~8.5Pool.
The subtended angle of horn mouth 11 is 90-150 °, and the length of circular passage 12 and the ratio of equivalent diameter are 0.5-2.5.
The traction mechanism is made of screw slider 15 and Pneumatic clamping mechanism 16, and the Pneumatic clamping mechanism is arranged in silk Realize that the glass tube of clamping extrusion molding moves downward on thick stick sliding block 15, the motor driver speed letter of screw slider mechanism 15 Number, match with the motor driver speed signal of turbine lift structure 1 according to frit flow.16 conduct of Pneumatic clamping mechanism The clamping device of glass tube, it makes the movement for clamping glass tube with flexible, can easily be accommodated.
The molding assisted parts setting water-cooling ring 14 and positioning pin 13, glass tube is from the temperature after the extrusion of extrusion die 9, by water Cold 14 auxiliary adjustment of ring, to reach required glass tube annealing temperature.Stack shell 5 configures detachable bottom plate 6, and bottom plate 6 is to add below The pedestal 7 of hot stove 8, the bottom of bottom plate 6 are equipped with discharging cooling ring 14;Extrusion die 9 and silk are directed at using positioning pin 13 by bottom plate 6 Relative position between thick stick sliding block 15.
Semiconducting glass pipe is manufactured by extrusion molding apparatus shown in Fig. 2,3;Tube outer diameter is 30 millimeters, and pipe thickness is 3 millimeters.The softening point of used glass is 600 DEG C, and annealing point is 480 DEG C.Frit block is placed on 75 millimeters of internal diameter, 10 milli of wall thickness It is heated and softened in the kuromore extrusion cylinder of rice.Extruding force < 3 ton of compression bar;The corresponding viscosity of forming temperature is 107.5Pool, Shaping speed is 10 millis m/min.Pipe mold is squeezed out using aluminium bronze or the manufacture of nickel plating aluminum-bronze material.Extrusion die lower annular is logical The equivalent diameter D in roadeIt is 6 millimeters;Take L/De=1.5, then the circular passage length L of extrusion die is 9 millimeters.
The extrusion equipment of this method is as shown in Figures 2 and 3.Frit block is placed in stack shell 5 and heats and softens, stack shell 5 Bottom plate 6 it is detachable.Turbine lift structure 1 is pressed by compression bar 3 and stripper plate 4 to the frit of heating;Under pressure Frit is squeezed out by extrusion die 9, is formed tubulose, is then cooled and shaped;The glass being made of screw slider 15 and clamper 16 Pipe traction mechanism pulls downwards glass pipe.
The Extrusion Flow characteristic of frit under heat, is shown by the experimental model of Fig. 1 a, Fig. 1 b.The glass being laminated in Fig. 1 a Glass piece (tinting on surface) is placed in similar container model, and mould tube passage is squeezed into after heating and pressure, and at this moment glass is in mould pipe Radially (tube hub speed is maximum, and at tube wall zero) speed is for parabolic distribution for interior flowing velocity.This shows that frit is logical When crossing extrusion die 9, characteristic is the newton-type viscous fluid of Laminar Flow, squeezes out the mean flow rate Vm of fluid in channel 12, clothes From Hagen-Poiseuille formula: Vm=Δ pD2(wherein Δ p, η, D, L is the pressure, viscosity and channel of fluid respectively to/32 η L Internal diameter and length).
When glass flows in the circular passage of extrusion die, D should be that (equivalent diameter De is equivalent diameter De in above formula The external diameter minus internal diameter of circular passage).In addition, the mobile frictional resistance between glass and conduit wall, related with channel material, it is general Frictional resistance when logical stainless steel mould high temperature between glass is greater than nickel-chrome alloy steel, and between nickel-chrome alloy steel and glass Frictional resistance is greater than aluminium bronze;Therefore, the flow resistance of glass in the channel, in addition to glass viscosity and the geometrical factor in channel with Outside, it is contemplated that mobile friction between glass and conduit wall, actual fluid resistance should also be in above formula plus being greater than 1 Empirical correction factor C (so that Ve=Vm/C).Then it obtains: Ve=Δ pDe 2/ C32 η L, this formula show extrusion tubulation Relationship between each main technologic parameters.
The forming temperature and viscosity of this manufacturing method are in other than the crystallization range of glass, and frit passes through extrusion die lower part There is viscosities il (10 more higher than general tubulation method when 126.5-8.5Pool).Which dictates that lower molding extruded velocity Ve (2-50 Milli m/min);Thus the higher extruding force Δ p needed for, by the 1 (rated pressure of turbine lift structure for having additional deceleration case 2 3-10 tons) Lai Shixian.With this cooperation, the main geometric parameters of extrusion die 9, i.e. the length L and equivalent in lower annular channel 12 The ratio between diameter De is L/De=0.5-2.5 and the subtended angle of top horn mouth 11 is 90 ° -150 °.
From the shape of the glass tube after mold extrusion, need to continue to control;At this moment glass is in viscid elastic characteristic, In Free wxpansion when leaving extrusion die overcomes this deformation after unloading effect by forming auxiliary device.At this moment glass is from viscous flow shape State is transformed into rigid solid state.The forming temperature that glass is squeezed out from extrusion die 9, in the case where the temperature of cooling ring 14 is adjusted, drop Temperature arrives the annealing temperature of glass, corresponds to glass viscosity 1013-14.5Pool.
In previous glass producing tubes by squeezing method patent, some measures were once used, for preventing the glass tube after squeezing out Correct geometric dimension needed for deviateing.Reinforce cooling (US Patent:4,350,513) for example, squeezing out position in mold, or Mobile adjustment die orifice position (US Patent:5,743,928) is inclined to the bending for compensating extruding pipe.However, this extrusion method Feature is operated under higher glass viscosity and lower forming temperature, and more direct, more effective assistant formation is taken Calibrating installation, to obtain geometric dimension accurately satisfactory glass tube.
One embodiment of the present invention has been described in detail above, but the content is only preferable implementation of the invention Example, should not be considered as limiting the scope of the invention.It is all according to all the changes and improvements made by the present patent application range Deng should still be within the scope of the patent of the present invention.

Claims (10)

1. a kind of semiconducting glass pipe manufacturing apparatus, it is characterised in that: including rack, pressure unit, hot briquetting portion, molding auxiliary The top of the rack is arranged in portion and tractive unit, the pressure unit, and the hot briquetting portion is arranged in the pressure unit bottom, The lower section in the rack and corresponding to the extrusion die in the hot briquetting portion, the molding assisted parts is arranged in the tractive unit Between the hot briquetting portion and the tractive unit;The molding assisted parts is water-cooling ring and positioning pin, and the stack shell is matched Detachable bottom plate is set, is the pedestal of heating furnace below the bottom plate, the bottom of the bottom plate is equipped with discharging cooling ring, the cooling ring The temperature for adjusting the glass tube that the hot briquetting portion squeezes out is directed at the extrusion die using the positioning pin by the bottom plate Relative position between the screw slider.
2. semiconducting glass pipe manufacturing apparatus according to claim 1, it is characterised in that: the pressure unit includes turbine liter Descending mechanism, reduction gearbox, compression bar, stripper plate and stack shell, the turbine lift structure and reduction gearbox transmission cooperate, the deceleration Case setting is connected by compression bar with the stripper plate in the frame top, the turbine lift, and the stripper plate is being added It is risen to when frit except the stack shell;It is arranged in the stack shell when pressure, realization is pressed down against the frit heated.
3. semiconducting glass pipe manufacturing apparatus according to claim 2, it is characterised in that: the hot briquetting portion, which is equipped with, to be added Hot stove and the extrusion die, for the heating furnace for heating stack shell, glass blocks and extrusion die, the extrusion die includes mould body and mould Core forms circular passage between the mould body and the mold core, the circular passage top expands into horn mouth, the stack shell Detachable bottom plate is located at below the extrusion die, and frit is squeezed out via the horn mouth by the circular passage when pressure, Form glass tube.
4. semiconducting glass pipe manufacturing apparatus according to claim 3, it is characterised in that: the bell-mouthed subtended angle is 90-150°。
5. semiconducting glass pipe manufacturing apparatus according to claim 3, it is characterised in that: the length of the circular passage with The ratio of equivalent diameter is 0.5-2.5.
6. semiconducting glass pipe manufacturing apparatus according to claim 3, it is characterised in that: the traction mechanism is slided by lead screw The glass that clamping extrusion molding is realized on the screw slider is arranged in block and Pneumatic clamping mechanism composition, the Pneumatic clamping mechanism Glass pipe moves downward.
7. -6 any semiconducting glass pipe manufacturing apparatus according to claim 1, it is characterised in that: the stripper plate and institute Stack shell is stated to be made of nichrome.
8. semiconducting glass pipe manufacturing apparatus according to claim 7, it is characterised in that: the compression bar and the bottom plate by Heat resisting steel is made.
9. semiconducting glass pipe manufacturing apparatus according to claim 8, it is characterised in that: the extrusion die is by aluminium bronze system At.
10. a kind of method for preparing semiconducting glass using manufacturing device as claimed in claim 9, it is characterised in that:
The frit block of heating is squeezed by turbine lift structure, compression bar, stripper plate, is being squeezed according to glass flow by the first step Flow behavior under state determines the geometric parameter and running parameter of extrusion die, thus by extrusion die extrusion molding;
Second step is shaped to the vitreum of tubulose in the first step by forming auxiliary device, and thus device overcomes vitreum The free wxpansion bring deformation after unloading effect when leaving extrusion die.
CN201910918273.7A 2019-09-26 2019-09-26 A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method Pending CN110526556A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910918273.7A CN110526556A (en) 2019-09-26 2019-09-26 A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method

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Application Number Priority Date Filing Date Title
CN201910918273.7A CN110526556A (en) 2019-09-26 2019-09-26 A kind of semiconducting glass pipe manufacturing apparatus and manufacturing method

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4350513A (en) * 1981-11-23 1982-09-21 Western Electric Company, Inc. Method and apparatus for extruding glass tubes
US5743928A (en) * 1996-12-16 1998-04-28 Pfleiderer; Larry Method and apparatus for extruding glass tubing
JP2001139335A (en) * 1999-10-13 2001-05-22 Shinetsu Quartz Prod Co Ltd Manufacturing method of cylindrical quartz glass part and apparatus for implementing the method
CN2873767Y (en) * 2005-10-25 2007-02-28 北方夜视技术股份有限公司 Intermittent glass pouring material pipe drawing device
CN102936091A (en) * 2012-11-22 2013-02-20 常熟市信立磁业有限公司 Forming device of semiconductor glass pipe for volume conductive microchannel plate
CN108264216A (en) * 2018-04-25 2018-07-10 蚌埠亘乐家庭用品有限公司 A kind of glass pipe trombone slide molding machine

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4350513A (en) * 1981-11-23 1982-09-21 Western Electric Company, Inc. Method and apparatus for extruding glass tubes
US5743928A (en) * 1996-12-16 1998-04-28 Pfleiderer; Larry Method and apparatus for extruding glass tubing
JP2001139335A (en) * 1999-10-13 2001-05-22 Shinetsu Quartz Prod Co Ltd Manufacturing method of cylindrical quartz glass part and apparatus for implementing the method
CN2873767Y (en) * 2005-10-25 2007-02-28 北方夜视技术股份有限公司 Intermittent glass pouring material pipe drawing device
CN102936091A (en) * 2012-11-22 2013-02-20 常熟市信立磁业有限公司 Forming device of semiconductor glass pipe for volume conductive microchannel plate
CN108264216A (en) * 2018-04-25 2018-07-10 蚌埠亘乐家庭用品有限公司 A kind of glass pipe trombone slide molding machine

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
西北轻工业学院: "《玻璃工艺学》", 31 August 2007, 中国轻工业出版社 *
齐齐哈尔轻工学院: "《玻璃机械设备》", 31 May 1981 *

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Application publication date: 20191203

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