CN110522157A - It is a kind of using flowers and plants powder as powder puff of filler and preparation method thereof - Google Patents
It is a kind of using flowers and plants powder as powder puff of filler and preparation method thereof Download PDFInfo
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- CN110522157A CN110522157A CN201910879565.4A CN201910879565A CN110522157A CN 110522157 A CN110522157 A CN 110522157A CN 201910879565 A CN201910879565 A CN 201910879565A CN 110522157 A CN110522157 A CN 110522157A
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- 239000000843 powder Substances 0.000 title claims abstract description 84
- 241001477893 Mimosa strigillosa Species 0.000 title claims abstract description 60
- 241000196324 Embryophyta Species 0.000 title claims abstract description 47
- 239000000945 filler Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims abstract description 54
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229920005682 EO-PO block copolymer Polymers 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000004615 ingredient Substances 0.000 claims abstract description 18
- PHQOGHDTIVQXHL-UHFFFAOYSA-N n'-(3-trimethoxysilylpropyl)ethane-1,2-diamine Chemical compound CO[Si](OC)(OC)CCCNCCN PHQOGHDTIVQXHL-UHFFFAOYSA-N 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- -1 Bis(hydroxymethyl)imidazolidinyl urea methylparaben Chemical compound 0.000 claims abstract description 10
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 9
- 239000012948 isocyanate Substances 0.000 claims abstract description 9
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 9
- 229920000642 polymer Polymers 0.000 claims abstract description 9
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 5
- 235000012054 meals Nutrition 0.000 claims abstract description 5
- 241001164374 Calyx Species 0.000 claims abstract description 4
- 239000006185 dispersion Substances 0.000 claims description 36
- 240000002853 Nelumbo nucifera Species 0.000 claims description 21
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims description 21
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 19
- 238000005187 foaming Methods 0.000 claims description 14
- 241000220317 Rosa Species 0.000 claims description 8
- 244000269722 Thea sinensis Species 0.000 claims description 6
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 5
- 240000005385 Jasminum sambac Species 0.000 claims description 5
- 230000018044 dehydration Effects 0.000 claims description 5
- 238000006297 dehydration reaction Methods 0.000 claims description 5
- 241000213006 Angelica dahurica Species 0.000 claims description 3
- 240000004784 Cymbopogon citratus Species 0.000 claims description 3
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims description 3
- 240000000249 Morus alba Species 0.000 claims description 3
- 235000008708 Morus alba Nutrition 0.000 claims description 3
- 244000141698 Prunus lannesiana Species 0.000 claims description 3
- 235000014001 Prunus serrulata Nutrition 0.000 claims description 3
- 235000006468 Thea sinensis Nutrition 0.000 claims description 3
- 235000020279 black tea Nutrition 0.000 claims description 3
- 235000013312 flour Nutrition 0.000 claims description 3
- 235000009569 green tea Nutrition 0.000 claims description 3
- 239000006260 foam Substances 0.000 abstract description 12
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 5
- 239000011707 mineral Substances 0.000 abstract description 5
- 239000000049 pigment Substances 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 238000004040 coloring Methods 0.000 abstract description 2
- 244000178870 Lavandula angustifolia Species 0.000 description 9
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 9
- 239000001102 lavandula vera Substances 0.000 description 9
- 235000018219 lavender Nutrition 0.000 description 9
- 229920000459 Nitrile rubber Polymers 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229920002635 polyurethane Polymers 0.000 description 6
- 239000004814 polyurethane Substances 0.000 description 6
- 244000043261 Hevea brasiliensis Species 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000341 volatile oil Substances 0.000 description 5
- 229920003052 natural elastomer Polymers 0.000 description 4
- 229920001194 natural rubber Polymers 0.000 description 4
- 239000010456 wollastonite Substances 0.000 description 4
- 229910052882 wollastonite Inorganic materials 0.000 description 4
- 241000628997 Flos Species 0.000 description 3
- 241000698291 Rugosa Species 0.000 description 3
- 230000003213 activating effect Effects 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000002087 whitening effect Effects 0.000 description 3
- 239000005995 Aluminium silicate Substances 0.000 description 2
- 229920005830 Polyurethane Foam Polymers 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 230000008821 health effect Effects 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000000474 nursing effect Effects 0.000 description 2
- 239000011496 polyurethane foam Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 1
- 241000243142 Porifera Species 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940099352 cholate Drugs 0.000 description 1
- BHQCQFFYRZLCQQ-OELDTZBJSA-N cholic acid Chemical compound C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(O)=O)C)[C@@]2(C)[C@@H](O)C1 BHQCQFFYRZLCQQ-OELDTZBJSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000008101 lactose Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000002906 microbiologic effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000012459 muffins Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000004224 protection Effects 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D33/00—Containers or accessories specially adapted for handling powdery toiletry or cosmetic substances
- A45D33/34—Powder-puffs, e.g. with installed container
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of using flowers and plants powder as powder puff of filler and preparation method thereof, the component A and B component for being 2:1 including mass ratio, component A includes the ingredient of following mass percent: a1: water 55%-57.15%, a2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.15%-0.3%, a3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%-1.4%, a4: ethylene oxide propylene oxide block copolymer 0.05%-0.07%, a5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%-1%, a6: ethylene oxide-propylene oxide block copolymer 1%-1.2%, a7: flowers and plants powder: flower class includes petal calyx, careless class is included as axis and leaf 40%-4 2%；B component includes the ingredient of following mass percent: b1: polyethylene glycol, polymer >=90.0% of toluene di-isocyanate(TDI), b2:2.0%≤1,3- diisocyanate base toluene≤5.0%.The present invention uses natural plant flowers grass meal to substitute conventional mineral type filler for filler, while colouring and assigning fragrant, good anti-bacterial effect to foam with the included smell of natural plant pigment and flowers and plants powder, and service life is longer.
Description
Technical field
The present invention relates to powder puff technical fields, a kind of using flowers and plants powder as the powder puff of filler and its preparation side in particular
Method.
Background technique
Powder puff is one kind of cosmetic applicators, all can include powder puff, mostly cotton and velvet material in general loose powder and compact case
Material, for picking foundation cream and modification dressing.According to the different type of powder puff, mainly have following effect: sponge powder puff is relatively suitble to wet
Water uses, convenient equably to push liquid foundation cream open；Triangle is then convenient for the smearing positions such as canthus and the wing of nose.Wet-dry powder
It flutters and is typically round or Wet-dry muffin can be applied on the face by rectangle regardless of whether getting use wet.No matter selecting sea
Continuous powder puff or Wet-dry powder puff, or be preferred so that pliability is moderate.
Common color make-up air cushion powder puff substantially has two major classes from the point of view of foamed material: rubber pange powder puff and poly- ammonia
Ester foaming powder puff.Rubber pange powder puff is divided into natural rubber (NR), nitrile rubber (NBR), the foaming of butadiene-styrene rubber (SBR) three categories
Material.The have drawn from latex of rubber tree of natural rubber (NR) powder puff is made, and emerges earliest.Nitrile rubber (NBR) powder puff is
The rubber pange class powder puff of the comparison mainstream to circulate in the market.Butadiene-styrene rubber (SBR) powder puff oil resistant, ageing-resistant performance are all less than
Nitrile rubber (NBR) powder puff, but because cheap, it is mostly individually sold as cosmetic applicators, on the market multiple dress triangular forms, it is special-shaped
Powder puff is mostly butadiene-styrene rubber (SBR) material.Polyurethane foam powder puff is divided into polyether-polyurethane foaming, polyester-polyurethane foaming and gathers
Ether/polyester-polyurethane mixed foaming three classes material, foam process are broadly divided into dry type foaming and wet type foaming two ways.
Traditional hydrophilic polyurethane foaming is often used wollastonite, and kaolin etc. is main stuffing, with mineral type mill base or tree
Epoxy-type mill base is coloured to foam, assigns perfume to foam with essence.The fillers such as wollastonite kaolin can be such that foam quality increases, mill base class
Easily decolourizes and contain heavy metal element, such as Pb compound.Essence class is volatile, cannot lasting lasting, and easily cause skin mistake
It is quick.Current existing powder puff uses wollastonite as filler in the preparation, and adverse environment protection, antibacterial effect is poor, uses week
Phase is short.
Summary of the invention
Natural plant flowers grass meal is used to substitute conventional mineral type filler for filler the purpose of the present invention is to provide a kind of, together
When with the included smell of natural plant pigment and flowers and plants powder give foam coloring, assign fragrant, good anti-bacterial effect, the longer powder of service life
Flutter and preparation method thereof.
In order to achieve the above object the present invention adopts the following technical scheme:
It is a kind of using flowers and plants powder as the powder puff of filler, including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 55%-57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.15%-0.3%；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%-1.4%；
A4: ethylene oxide propylene oxide block copolymer 0.05%-0.07%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%-1%；
A6: ethylene oxide-propylene oxide block copolymer 1%-1.2%；
A7: flowers and plants powder: flower class includes petal calyx, and careless class is included as axis and leaf 40%-42%；
The B component includes the ingredient of following mass percent:
B1: polymer >=90.0% of polyethylene glycol, toluene di-isocyanate(TDI)；
B2:2.0%≤1,3- diisocyanate base toluene≤5.0%.
Preferably, the flowers and plants powder is lotus leaf powder, rose powder, jasmine powder, one of lemongrass powder and mulberry leaf powder or a variety of.
The flowers and plants powder uses rose powder, and the rare essential oil in Flos Rosae Rugosas pollen can be with whitening activating skin.
Preferably, the flowers and plants powder is lavender powder, green tea powder, black tea powder, oriental cherry powde, one in yam flour and angelica dahurica powder
Kind is a variety of.The flowers and plants powder uses lavender powder, and the Lavender in lavender powder has sleeping effect.
Preferably, the component A includes the ingredient of following mass percent:
A1: water 57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.3%；CAS number 1760-24-3；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%；
A4: ethylene oxide propylene oxide block copolymer 0.05%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%；
A6: ethylene oxide-propylene oxide block copolymer 1%；
A7: flowers and plants powder: the lotus leaf powder 40% of dehydration；
The B component includes the ingredient of following mass percent:
B1: polymer >=90.0% of polyethylene glycol, toluene di-isocyanate(TDI)；
B2:2.0%≤1,3- diisocyanate base toluene≤5.0%.
Preferably, the granular size of the lotus leaf powder is 300 mesh.
The present invention also provides a kind of using flowers and plants powder as the preparation method of the powder puff of filler, includes the following steps:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in a mixing bowl, pressure is normal pressure, obtains dispersion liquid；
Step 2): the a3 in the component A is melted under conditions of temperature is 80 DEG C, is added in the dispersion liquid of step 1)
Completely with the mixing speed dispersion of 180 turns/min, pressure is normal pressure；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added and passes through step 1) and step
2) complete with the mixing speed dispersion of 180 turns/min in the dispersion liquid formed, pressure is normal pressure；By step 1), step 2) and
Three steps of step 3), are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): by step 4) obtain component A and step 5) obtain component B with 2:1 ratio mix, under normal pressure with
The revolving speed of 4500 turns/min is uniformly mixed；Finished product can be obtained completely by standing foaming in 6 minutes.
Beneficial effects of the present invention: the present invention is using natural plant flowers grass meal (lotus leaf powder, rose powder, jasmine pollen etc.)
While filler substitutes conventional mineral type filler, is coloured, assigned fragrant to foam with the smell that natural plant pigment and flowers and plants powder are included.
It solves conventional filler and uses mill base, essence etc. may lead to the problem of adverse effect to atmosphere, water body, while assign one to foam
Fixed nursing health effect (the rare essential oil in such as Flos Rosae Rugosas pollen can have sleeping effect with whitening activating skin, Lavender).
The weight for alleviating traditional hydrophilic polyurethane powder puff avoids the possibility polluted using traditional mill base water supply body, increases
Foam fragrance remaining time avoids mill base and essence from causing the bad phenomenon of stimulation to skin.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail, herein with illustrative examples and explanation of the invention
For explaining the present invention, but it is not as a limitation of the invention.
It is a kind of using flowers and plants powder as the powder puff of filler, including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 55%-57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.15%-0.3%；CAS number 1760-24-3；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%-1.4%；
A4: ethylene oxide propylene oxide block copolymer 0.05%-0.07%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%-1%；
A6: ethylene oxide-propylene oxide block copolymer 1%-1.2%；
A7: flowers and plants powder: flower class includes petal calyx, and careless class is included as axis and leaf 40%-42%；
The B component includes the ingredient of following mass percent:
B1: polymer >=90.0% of polyethylene glycol, toluene di-isocyanate(TDI)；CASRN:9042-77-7；
B2:2.0%≤1,3- diisocyanate base toluene≤5.0%；CASRN:26471-62-5.
Preferably, the flowers and plants powder is lotus leaf powder, rose powder, jasmine powder, one of lemongrass powder and mulberry leaf powder or a variety of.
Preferably, the flowers and plants powder is lavender powder, green tea powder, black tea powder, oriental cherry powde, one in yam flour and angelica dahurica powder
Kind is a variety of.
Preferably, the granular size of the lotus leaf powder is 300 mesh.
The present invention also provides a kind of using flowers and plants powder as the preparation method of the powder puff of filler, includes the following steps:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in a mixing bowl, pressure is normal pressure, obtains dispersion liquid；
Step 2): the a3 in the component A is melted under conditions of temperature is 80 DEG C, is added in the dispersion liquid of step 1)
Completely with the mixing speed dispersion of 180 turns/min, pressure is normal pressure；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added and passes through step 1) and step
2) complete with the mixing speed dispersion of 180 turns/min in the dispersion liquid formed, pressure is normal pressure；By step 1), step 2) and
Three steps of step 3), are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): by step 4) obtain component A and step 5) obtain component B with 2:1 ratio mix, under normal pressure with
The revolving speed of 4500 turns/min is uniformly mixed；Finished product can be obtained completely by standing foaming in 6 minutes.
Embodiment 1, it is a kind of using flowers and plants powder as the powder puff of filler, including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.3%；CAS number 1760-24-3；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%；
A4: ethylene oxide propylene oxide block copolymer 0.05%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%；
A6: ethylene oxide-propylene oxide block copolymer 1%；
A7: flowers and plants powder: the lotus leaf powder 40% of dehydration；
The B component includes the ingredient of following mass percent:
B1: the polymer 95.0% of polyethylene glycol, toluene di-isocyanate(TDI)；CASRN:9042-77-7；
B2:1,3- diisocyanate base toluene 5.0%；CASRN:26471-62-5.
Preparation method the following steps are included:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in a mixing bowl, pressure is normal pressure, obtains dispersion liquid；
Step 2): the a3 in the component A is melted under conditions of temperature is 80 DEG C, is added in the dispersion liquid of step 1)
Completely with the mixing speed dispersion of 180 turns/min, pressure is normal pressure；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added and passes through step 1) and step
2) complete with the mixing speed dispersion of 180 turns/min in the dispersion liquid formed, pressure is normal pressure；By step 1), step 2) and
Three steps of step 3), are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): by step 4) obtain component A and step 5) obtain component B with 2:1 ratio mix, under normal pressure with
The revolving speed of 4500 turns/min is uniformly mixed；The powder puff of lotus leaf faint scent can be obtained completely by standing foaming in 6 minutes.
Embodiment 2, it is a kind of using flowers and plants powder as the powder puff of filler, including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 55%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.15%；CAS number 1760-24-3；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1.4%；
A4: ethylene oxide propylene oxide block copolymer 0.05%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 1%；
A6: ethylene oxide-propylene oxide block copolymer 1.2%；
A7: flowers and plants powder: the rose powder 41.2% of dehydration；
The B component includes the ingredient of following mass percent:
B1: the polymer 98.0% of polyethylene glycol, toluene di-isocyanate(TDI)；CASRN:9042-77-7；
B2:1,3- diisocyanate base toluene 2.0%；CASRN:26471-62-5.
Preparation method the following steps are included:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in a mixing bowl, pressure is normal pressure, obtains dispersion liquid；
Step 2): the a3 in the component A is melted under conditions of temperature is 80 DEG C, is added in the dispersion liquid of step 1)
Completely with the mixing speed dispersion of 180 turns/min, pressure is normal pressure；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added and passes through step 1) and step
2) complete with the mixing speed dispersion of 180 turns/min in the dispersion liquid formed, pressure is normal pressure；By step 1), step 2) and
Three steps of step 3), are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): by step 4) obtain component A and step 5) obtain component B with 2:1 ratio mix, under normal pressure with
The revolving speed of 4500 turns/min is uniformly mixed；The powder puff of rose scent can be obtained completely by standing foaming in 6 minutes.
Embodiment 3, it is a kind of using flowers and plants powder as the powder puff of filler, including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 56.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.25%；CAS number 1760-24-3；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1.2%；
A4: ethylene oxide propylene oxide block copolymer 0.06%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 1.1%；
A6: ethylene oxide-propylene oxide block copolymer 1.2%；
A7: flowers and plants powder: the lavender powder 40.44% of dehydration；
The B component includes the ingredient of following mass percent:
B1: the polymer 96.5% of polyethylene glycol, toluene di-isocyanate(TDI)；CASRN:9042-77-7；
B2:1,3- diisocyanate base toluene 3.5%；CASRN:26471-62-5.
Preparation method the following steps are included:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in a mixing bowl, pressure is normal pressure, obtains dispersion liquid；
Step 2): the a3 in the component A is melted under conditions of temperature is 80 DEG C, is added in the dispersion liquid of step 1)
Completely with the mixing speed dispersion of 180 turns/min, pressure is normal pressure；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added and passes through step 1) and step
2) complete with the mixing speed dispersion of 180 turns/min in the dispersion liquid formed, pressure is normal pressure；By step 1), step 2) and
Three steps of step 3), are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): by step 4) obtain component A and step 5) obtain component B with 2:1 ratio mix, under normal pressure with
The revolving speed of 4500 turns/min is uniformly mixed；The powder puff of lavender faint scent can be obtained completely by standing foaming in 6 minutes.
Tradition is using wollastonite as filler hydrophilic polyurethane foam and product of the present invention parameter comparison:
1. volume is all 15cm3The quality versus of product of the present invention and traditional powder puff: the powder puff of lotus leaf faint scent is 8.2 grams,
Traditional powder puff is 9.6 grams, and the more traditional powder puff quality of the powder puff of the present invention of same volume about lacks 15%.
2. being all that the cylindrical body of 4cm diameter 6cm height does pulling force comparison: traditional powder puff is 8.2kgf, the powder of lotus leaf faint scent
It flutters as 9.4kgf；The more traditional powder puff of the value of thrust of powder puff of the present invention improves about 10%.
3. color contrast: traditional powder puff is white, and the powder puff of lotus leaf faint scent of the present invention is light green color.The powder of lotus leaf faint scent
The anti-decoloring ability flutterred is strong, and under the conditions of 45 DEG C, 0.5% detergent presses 100 times without obvious decoloration phenomenon repeatedly.
4. smell compares: traditional powder puff is that tasteless, of the invention powder puff has lotus leaf faint scent.Lotus leaf faint scent of the present invention
The powder puff powder puff that fragrance remaining time is more traditional at 60 DEG C adds twice of essence product extension or more.In normal use, the present invention is adopted
It is increased more than twice with the more traditional addition essential oil class product retention time of volatile oil content in flowers and plants powder.
5. anti-mildew test: configuring culture solution with lactose cholate fermentation medium, take traditional powder puff and lotus leaf faint scent
Each 3, powder puff sample.Test within 72 hours for 35 DEG C in microbiological incubator, obvious mould spot, lotus occurs in traditional powder puff
The powder puff of leaf faint scent does not occur.
6. the test of ultraviolet tolerance: take be all 4cm diameter 6cm height cylindrical body, at the ultraviolet light irradiation of 24W 144 hours,
The powder puff of the significant yellow of traditional powder puff, lotus leaf faint scent occurs without aetiolation.
The present invention is that filler substitutes conventional mineral using natural plant flowers grass meal (lotus leaf powder, rose powder, jasmine pollen etc.)
While type filler, is coloured, assigned fragrant to foam with the smell that natural plant pigment and flowers and plants powder are included.Conventional filler is solved to use
Mill base, essence etc. may lead to the problem of adverse effect to atmosphere, water body, while certain nursing health effect is assigned to foam
(the rare essential oil in such as Flos Rosae Rugosas pollen can have sleeping effect with whitening activating skin, Lavender).Alleviate traditional hydrophily
The weight of polyurethane powder puff is avoided the possibility polluted using traditional mill base water supply body, increases foam fragrance remaining time, keep away
Exempt from the bad phenomenon that mill base and essence cause stimulation to skin.
It is provided for the embodiments of the invention technical solution above to be described in detail, specific case used herein
The principle and embodiment of the embodiment of the present invention are expounded, the explanation of above embodiments is only applicable to help to understand this
The principle of inventive embodiments；At the same time, for those skilled in the art, according to an embodiment of the present invention, in specific embodiment party
There will be changes in formula and application range, in conclusion the contents of this specification are not to be construed as limiting the invention.
Claims (6)
1. a kind of using flowers and plants powder as the powder puff of filler, which is characterized in that including
Mass ratio is the component A and B component of 2:1,
The component A includes the ingredient of following mass percent:
A1: water 55%-57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.15%-0.3%；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%-1.4%；
A4: ethylene oxide propylene oxide block copolymer 0.05%-0.07%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%-1%；
A6: ethylene oxide-propylene oxide block copolymer 1%-1.2%；
A7: flowers and plants powder: flower class includes petal calyx, and careless class is included as axis and leaf 40%-42%；
The B component includes the ingredient of following mass percent:
B1: polymer >=90.0% of polyethylene glycol, toluene di-isocyanate(TDI)；
B2:2.0%≤1,3- diisocyanate base toluene≤5.0%.
2. according to claim 1 a kind of using flowers and plants powder as the powder puff of filler, it is characterised in that: the flowers and plants powder is lotus
Ye Fen, rose powder, jasmine powder, one of lemongrass powder and mulberry leaf powder or a variety of.
3. according to claim 1 a kind of using flowers and plants powder as the powder puff of filler, it is characterised in that: the flowers and plants powder is smoked
Clothing grass meal, green tea powder, black tea powder, oriental cherry powde, one of yam flour and angelica dahurica powder or a variety of.
4. according to claim 1 a kind of using flowers and plants powder as the powder puff of filler, it is characterised in that: the component A includes
The ingredient of following mass percent:
A1: water 57.15%；
A2:N- aminoethyl-γ-aminopropyltrimethoxysilane 0.3%；
A3:C16-18 alcohol/PEG-20 or C16-18 alcohol ether 1%；
A4: ethylene oxide propylene oxide block copolymer 0.05%；
A5: Bis(hydroxymethyl)imidazolidinyl urea methylparaben propylben 0.5%；
A6: ethylene oxide-propylene oxide block copolymer 1%；
A7: flowers and plants powder: the lotus leaf powder 40% of dehydration；
The B component includes the ingredient of following mass percent:
B1: polymer >=90.0% of polyethylene glycol, toluene di-isocyanate(TDI)；
B2:2.0%≤1,3- diisocyanate base toluene≤5.0%.
5. according to claim 4 a kind of using flowers and plants powder as the powder puff of filler, it is characterised in that:
The granular size of the lotus leaf powder is 300 mesh.
6. it is a kind of using flowers and plants powder as the preparation method of the powder puff of filler described in -5 any one according to claim 1, it is special
Sign is, includes the following steps:
Step 1): by a1, a2, a4, a5, a6 in the component A, homogeneous a mixing bowl is added after mixing in proportion, is stirred in homogeneous
Complete with the mixing speed dispersion of 180 turns/min at 25 DEG C in cylinder, pressure is normal pressure, obtains dispersion liquid；
Step 2): by the a3 in the component A temperature be 80 DEG C under conditions of melt, be added step 1) dispersion liquid in
Completely, pressure is normal pressure for the mixing speed dispersion of 180 turns/min；
Step 3): the a7 in the component A is dried under conditions of temperature is 60 DEG C, is added by step 1) and step 2) shape
At dispersion liquid in the dispersion of the mixing speed of 180 turns/min completely, pressure is normal pressure；By step 1), step 2) and step
3) three steps are prepared into component A；
Step 4): the component A that step 3) is prepared is cooled to 12 DEG C, pressure is normal pressure；
Step 5): by the component B by being heated to 28 DEG C, pressure is normal pressure；
Step 6): the component B that the component A and step 5) that step 4) is obtained are obtained is mixed with 2:1 ratio, under normal pressure with 4500
Turn/revolving speed of min is uniformly mixed；Finished product can be obtained completely by standing foaming in 6 minutes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112646358A (en) * | 2020-12-21 | 2021-04-13 | 江门市玫迎蓉化妆品有限公司 | Formula of cool powder puff made of MATE material |
| CN113736245A (en) * | 2021-09-07 | 2021-12-03 | 广州市达戈彩美容科技有限公司 | Slow-resilience polyurethane foaming pillow containing plant flower and grass powder and preparation method thereof |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5084292A (en) * | 1989-05-25 | 1992-01-28 | Unilever Patent Holdings B.V. | Processing for preparing flavorings and perfumes based on one or more carotenoids as starting material |
| CN1491243A (en) * | 2001-02-15 | 2004-04-21 | 巴斯福股份公司 | Waterborne Polyurethane Dispersion |
| CN1732082A (en) * | 2002-12-27 | 2006-02-08 | 株式会社加平 | Polyurethane foam sheet and method for producing laminate sheet using the same |
| CN103649143A (en) * | 2011-07-22 | 2014-03-19 | Adeka株式会社 | Aqueous polyurethane resin composition, and highly-adhesive polyester film to which said aqueous polyurethane resin composition has been applied |
| CN104219936A (en) * | 2014-08-08 | 2014-12-17 | 太仓欧锐智能化工程有限公司 | Production process for dustproof heat-conducting foam |
| CN106619353A (en) * | 2016-10-17 | 2017-05-10 | 东莞泰康泡绵有限公司 | Skin-care cleansing foam and foaming process thereof |
| CN107151440A (en) * | 2017-05-11 | 2017-09-12 | 东莞泰康泡绵有限公司 | A kind of sandwich bubble silk floss of multifunctional polyurethane and preparation method thereof |
| CN107531993A (en) * | 2015-05-15 | 2018-01-02 | 住友化学株式会社 | Water-borne dispersions mixture |
| CN108484874A (en) * | 2018-03-23 | 2018-09-04 | 惠州市远安新材料有限公司 | A kind of polyurethane material, high-elastic Antibacterial polyurethane class powder puff and preparation method thereof |
| CN108602934A (en) * | 2016-01-26 | 2018-09-28 | 高级软质材料株式会社 | The manufacturing method of polyurethane foam composition containing polyrotaxane, the polyurethane foam from the composition and polyurethane foam |
| CN108641391A (en) * | 2018-05-07 | 2018-10-12 | 东莞市创继荣高分子材料有限公司 | A kind of bamboo fiber hydrophilic non-latex powder puff and preparation method |
-
2019
- 2019-09-18 CN CN201910879565.4A patent/CN110522157A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5084292A (en) * | 1989-05-25 | 1992-01-28 | Unilever Patent Holdings B.V. | Processing for preparing flavorings and perfumes based on one or more carotenoids as starting material |
| CN1491243A (en) * | 2001-02-15 | 2004-04-21 | 巴斯福股份公司 | Waterborne Polyurethane Dispersion |
| CN1732082A (en) * | 2002-12-27 | 2006-02-08 | 株式会社加平 | Polyurethane foam sheet and method for producing laminate sheet using the same |
| CN103649143A (en) * | 2011-07-22 | 2014-03-19 | Adeka株式会社 | Aqueous polyurethane resin composition, and highly-adhesive polyester film to which said aqueous polyurethane resin composition has been applied |
| CN104219936A (en) * | 2014-08-08 | 2014-12-17 | 太仓欧锐智能化工程有限公司 | Production process for dustproof heat-conducting foam |
| CN107531993A (en) * | 2015-05-15 | 2018-01-02 | 住友化学株式会社 | Water-borne dispersions mixture |
| CN108602934A (en) * | 2016-01-26 | 2018-09-28 | 高级软质材料株式会社 | The manufacturing method of polyurethane foam composition containing polyrotaxane, the polyurethane foam from the composition and polyurethane foam |
| CN106619353A (en) * | 2016-10-17 | 2017-05-10 | 东莞泰康泡绵有限公司 | Skin-care cleansing foam and foaming process thereof |
| CN107151440A (en) * | 2017-05-11 | 2017-09-12 | 东莞泰康泡绵有限公司 | A kind of sandwich bubble silk floss of multifunctional polyurethane and preparation method thereof |
| CN108484874A (en) * | 2018-03-23 | 2018-09-04 | 惠州市远安新材料有限公司 | A kind of polyurethane material, high-elastic Antibacterial polyurethane class powder puff and preparation method thereof |
| CN108641391A (en) * | 2018-05-07 | 2018-10-12 | 东莞市创继荣高分子材料有限公司 | A kind of bamboo fiber hydrophilic non-latex powder puff and preparation method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112646358A (en) * | 2020-12-21 | 2021-04-13 | 江门市玫迎蓉化妆品有限公司 | Formula of cool powder puff made of MATE material |
| CN113736245A (en) * | 2021-09-07 | 2021-12-03 | 广州市达戈彩美容科技有限公司 | Slow-resilience polyurethane foaming pillow containing plant flower and grass powder and preparation method thereof |
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