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CN110468369A - 300 series stainless steel screw fasteners nitridation heat treatment processing procedure - Google Patents

300 series stainless steel screw fasteners nitridation heat treatment processing procedure Download PDF

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Publication number
CN110468369A
CN110468369A CN201810568574.7A CN201810568574A CN110468369A CN 110468369 A CN110468369 A CN 110468369A CN 201810568574 A CN201810568574 A CN 201810568574A CN 110468369 A CN110468369 A CN 110468369A
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screw
stainless steel
series stainless
heat treatment
processing procedure
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郭渊源
朱东德
陈胜渊
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Guolian Screw Industry Co ltd
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Guolian Screw Industry Co ltd
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/08Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
    • C23C8/24Nitriding
    • C23C8/26Nitriding of ferrous surfaces

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatment Of Articles (AREA)

Abstract

A kind of 300 series stainless steel screw fasteners nitridation heat treatment processing procedure includes: forming step is carried out to the disk member of 300 series stainless steel materials, so that the disk member has screw terminal and screw rod;It carries out rolling over tooth step, so that at least one portion of the screw rod becomes screw thread portion, thus forms screw;Nitridation process step is carried out to the screw, to increase the hardness of the screw surface;And surface treatment step is carried out to the screw, to form antirust coat in the screw surface.

Description

300系列不锈钢螺丝扣件氮化热处理制程Nitriding heat treatment process for 300 series stainless steel screw fasteners

技术领域technical field

本发明涉及一种螺丝扣件的热处理制程,特别是涉及一种300系列不锈钢螺丝扣件氮化热处理制程。The invention relates to a heat treatment process for screw fasteners, in particular to a nitriding heat treatment process for 300 series stainless steel screw fasteners.

背景技术Background technique

钻尾螺丝由于其特殊的钻尾端设计,让钻尾螺丝同时集「钻」、「攻」、「锁」三大功能于一身:钻—钻头外形的尾端部份(简称钻尾),可直接在对锁件表面钻孔;攻—钻头以外的自攻牙部份,可直接在孔内攻牙形成内螺纹;锁—不必预先开孔攻牙,便能达到螺丝最主要的用途:锁付物件。Due to its special design of the drill tail end, the drill tail screw integrates the three functions of "drilling", "tapping" and "locking" at the same time: Drilling - the tail end part of the drill bit shape (referred to as the drill tail), It can directly drill holes on the surface of the lock; tapping—the self-tapping part other than the drill bit, which can be directly tapped in the hole to form an internal thread; lock—the main purpose of the screw can be achieved without pre-drilling and tapping: Lock payment objects.

钻尾螺丝可利用各种不同材质和制程制成。例如,钻尾头的材质使用碳钢,而螺丝杆部分则使用不锈钢,且两者是以焊接方式加以接合。然而,此种复合式钻尾螺丝的缺点在于,工序繁多、成本高昂,且焊接点容易断裂。Drilling screws are available in a variety of materials and processes. For example, carbon steel is used for the material of the drill tail, and stainless steel is used for the screw shaft, and the two are joined by welding. However, the disadvantages of this kind of compound drill end screw are that the process is complicated, the cost is high, and the welding point is easy to break.

或者,也可使用400系列不锈钢来一体式地制造出钻尾螺丝。然而,400系列不锈钢钻尾螺丝虽说有足够的硬度以贯穿对锁件,但是却有容易锈蚀的缺点。Alternatively, 400 series stainless steel can be used to manufacture the drill end screws in one piece. However, although the 400 series stainless steel drill tail screw has enough hardness to penetrate the lock, it has the disadvantage of being easy to rust.

又或者,也可使用300系列不锈钢来一体式地制造出钻尾螺丝。然而,300系列不锈钢钻尾螺丝虽然耐腐蚀性佳,但是由于无法对其施以一般的热处理制程,所以硬度较低,因而其无法贯穿硬度较高的对锁件,例如,现有300系列不锈钢钻尾螺丝并无法贯穿洛氏硬度B尺度(HRB)80±5且厚度为3毫米至6毫米的型钢。所以,有必要寻求解决方案。Alternatively, 300 series stainless steel can be used to manufacture the drill end screws in one piece. However, although 300 series stainless steel drill tail screws have good corrosion resistance, they have low hardness because they cannot be subjected to a general heat treatment process, so they cannot penetrate through the relatively high-hardness locking parts. For example, the existing 300 series stainless steel Drilling screws cannot penetrate steel sections with a Rockwell hardness B scale (HRB) of 80±5 and a thickness of 3 mm to 6 mm. So, it is necessary to find a solution.

发明内容Contents of the invention

本发明的目的在于提供一种300系列不锈钢螺丝扣件氮化热处理制程。The object of the present invention is to provide a nitriding heat treatment process for 300 series stainless steel screw fasteners.

本发明300系列不锈钢螺丝扣件氮化热处理制程,包含:(a)对300系列不锈钢材质的盘元进行成型步骤,使得所述盘元具有螺丝头及螺丝杆;(b)进行辗牙步骤,使得所述螺丝杆的至少一个部分成为螺丝牙部,因而形成螺丝;(c)对所述螺丝进行氮化处理步骤,以增加所述螺丝表面的硬度;及(d)对所述螺丝进行表面处理步骤,以在所述螺丝表面形成防锈层。The 300 series stainless steel screw fastener nitriding heat treatment process of the present invention includes: (a) forming a disc element made of 300 series stainless steel, so that the disc element has a screw head and a screw shaft; (b) performing a tooth rolling step, making at least one portion of the screw shank a screw thread, thereby forming a screw; (c) subjecting the screw to a nitriding treatment step to increase the hardness of the surface of the screw; and (d) subjecting the screw to a surface A treatment step to form an anti-rust layer on the surface of said screw.

本发明300系列不锈钢螺丝扣件氮化热处理制程,还包含在所述(b)步骤及所述(c)步骤间的(e)步骤,是以酸剂清洗所述螺丝的表面,进行抛光,以提高所述螺丝表面的亮度。The 300 series stainless steel screw fastener nitriding heat treatment process of the present invention also includes the (e) step between the (b) step and the (c) step, which is to clean the surface of the screw with an acid agent and polish it. To improve the brightness of the screw surface.

本发明300系列不锈钢螺丝扣件氮化热处理制程,在所述(c)步骤中,是将所述螺丝置于真空箱型炉中进行氮化处理步骤。In the 300 series stainless steel screw fastener nitriding heat treatment process of the present invention, in the step (c), the screw is placed in a vacuum box furnace for nitriding treatment.

本发明300系列不锈钢螺丝扣件氮化热处理制程,在所述(c)步骤中,是以700℃±50℃的温度进行氮化处理步骤达90分钟至120分钟,再冷却至常温,使得渗氮深度达到3微米至4微米。In the nitriding heat treatment process of the 300 series stainless steel screw fasteners of the present invention, in the (c) step, the nitriding treatment step is carried out at a temperature of 700°C ± 50°C for 90 minutes to 120 minutes, and then cooled to normal temperature, so that the nitriding The nitrogen depth reaches 3 microns to 4 microns.

本发明300系列不锈钢螺丝扣件氮化热处理制程,在所述(c)步骤中,是先将所述螺丝置于真空箱型炉中,以700℃±50℃的温度进行氮化处理步骤达90分钟至120分钟,再冷却至常温,使得渗氮深度达到3微米至4微米。The 300 series stainless steel screw fastener nitriding heat treatment process of the present invention, in the (c) step, first place the screw in a vacuum box furnace, and carry out the nitriding treatment step at a temperature of 700°C ± 50°C. 90 minutes to 120 minutes, and then cooled to normal temperature, so that the nitriding depth reaches 3 microns to 4 microns.

本发明300系列不锈钢螺丝扣件氮化热处理制程,在所述(d)步骤中,所述防锈层需进行超过1000小时的盐雾试验。In the nitriding heat treatment process of the 300 series stainless steel screw fasteners of the present invention, in the step (d), the anti-rust layer needs to be subjected to a salt spray test for more than 1000 hours.

本发明300系列不锈钢螺丝扣件氮化热处理制程,还包含在所述(a)步骤及所述(b)步骤间的(f)步骤,进行夹尾步骤,使得所述螺丝杆远离所述螺丝头的端部成为钻尾部,所述(b)步骤使得所述钻尾部以外的其余螺丝杆部分成为所述螺丝牙部。The nitriding heat treatment process of the 300 series stainless steel screw fasteners of the present invention also includes the (f) step between the (a) step and the (b) step, performing the tail clamping step so that the screw rod is far away from the screw The end of the head becomes the drill tail, and the step (b) makes the rest of the screw shaft except the drill tail become the screw thread.

本发明300系列不锈钢螺丝扣件氮化热处理制程,所述螺丝的成品的表面硬度为维氏硬度600以上,且能贯穿洛氏硬度B尺度80±5且厚度为3毫米至6毫米的型钢。According to the nitriding heat treatment process of the 300 series stainless steel screw fasteners of the present invention, the surface hardness of the finished product of the screws is above 600 Vickers hardness, and can penetrate the section steel with a Rockwell hardness B scale of 80±5 and a thickness of 3 mm to 6 mm.

本发明的有益效果在于:由于利用「氮化处理」步骤突破现有300系列不锈钢螺丝扣件原本无法热处理的限制,因而能大幅提高螺丝表面的硬度。The beneficial effect of the present invention is that the hardness of the surface of the screw can be greatly improved due to the use of the "nitriding treatment" step to break through the limitation that the existing 300 series stainless steel screw fasteners cannot be heat-treated.

附图说明Description of drawings

图1是一流程图,说明本发明300系列不锈钢螺丝扣件氮化热处理制程的实施例;Fig. 1 is a flow chart, illustrates the embodiment of the nitriding heat treatment process of 300 series stainless steel screw fasteners of the present invention;

图2是一侧视图,说明本实施例中当对300系列不锈钢材质的盘元进行成型步骤后,该盘元具有螺丝头及螺丝杆;Fig. 2 is a side view, illustrating that in this embodiment, after the forming step is performed on the disc unit made of 300 series stainless steel, the disc unit has a screw head and a screw shaft;

图3是一侧视图,说明本实施例中对该螺丝杆进行夹尾步骤,使得螺丝杆远离螺丝头的端部成为钻尾部;及Fig. 3 is a side view, illustrating the step of clamping the tail of the screw rod in this embodiment, so that the end of the screw rod away from the screw head becomes the tail of the drill; and

图4是一侧视图,说明本实施例中进行辗牙步骤,使得钻尾部以外的其余螺丝杆部分成为螺丝牙部。Fig. 4 is a side view illustrating the thread rolling step in this embodiment, so that the rest of the screw shaft except the tail of the drill becomes the thread portion.

具体实施方式Detailed ways

下面结合附图及实施例对本发明进行详细说明。The present invention will be described in detail below in conjunction with the accompanying drawings and embodiments.

参阅图1至4,本发明300系列不锈钢(即SUS300)螺丝扣件氮化热处理制程,适用于对300系列不锈钢材质的盘元进行氮化热处理制程,以形成表面硬度较高的300系列不锈钢螺丝扣件。Referring to Figures 1 to 4, the nitriding heat treatment process for 300 series stainless steel (i.e. SUS300) screw fasteners of the present invention is suitable for carrying out the nitriding heat treatment process for 300 series stainless steel disk elements to form 300 series stainless steel screws with higher surface hardness fasteners.

如图1步骤21及图2所示,在本实施例中,是先对300系列不锈钢材质的盘元进行成型步骤,使得该盘元具有螺丝头11及螺丝杆12。此时,由于尚未进行辗牙步骤,所以该螺丝杆12上尚无螺牙。As shown in step 21 of FIG. 1 and FIG. 2 , in this embodiment, the disc unit made of 300 series stainless steel is formed first, so that the disc unit has a screw head 11 and a screw rod 12 . At this moment, because the thread rolling step has not been carried out, there is no thread on the screw rod 12 yet.

接着,如图1步骤22及图3所示,对该螺丝杆12远离该螺丝头11的端部进行夹尾步骤,使得该螺丝杆12远离该螺丝头11的端部成为钻尾部121。例如,在本实施例中,可利用模具进行锻打,以锻打出3号钻尾。Next, as shown in step 22 of FIG. 1 and FIG. 3 , the end of the screw rod 12 away from the screw head 11 is clamped so that the end of the screw rod 12 away from the screw head 11 becomes a drill tail 121 . For example, in this embodiment, the die can be used for forging to forge the No. 3 drill tail.

接着,如图1步骤23及图4所示,进行辗牙步骤,使得该钻尾部121以外的其余螺丝杆12部分成为螺丝牙部122(粗牙或细牙),因而形成螺丝1。Next, as shown in FIG. 1 step 23 and FIG. 4 , the thread rolling step is carried out so that the rest of the screw rod 12 other than the drill tail portion 121 becomes the screw thread portion 122 (coarse thread or fine thread), thus forming the screw 1 .

由于本实施例在进行前述成型、夹尾、辗牙等步骤时需用到草酸等油脂,所以当步骤23的辗牙步骤完成后,接着需如步骤24所示,以酸剂清洗螺丝1的表面,进行抛光,以提高螺丝1表面的亮度。Since this embodiment needs to use oxalic acid and other oils during the aforementioned steps of molding, tail clamping, and tooth rolling, after the tooth rolling step in step 23 is completed, it is necessary to clean the screw 1 with an acid agent as shown in step 24. The surface is polished to improve the brightness of the screw 1 surface.

接着,如图1步骤25所示,对该螺丝1进行氮化处理步骤,以增加螺丝1表面的硬度。在本实施例中,在进行氮化处理步骤时,是先将螺丝1置于真空箱型炉中,以700℃±50℃的温度进行氮化处理达90分钟至120分钟,再冷却至常温,使得渗氮深度可达到3微米至4微米。因此,本发明以「氮化处理」步骤突破现有300系列不锈钢螺丝扣件原本无法热处理的限制,因而能大幅提高螺丝1表面的硬度。Next, as shown in step 25 of FIG. 1 , a nitriding treatment step is performed on the screw 1 to increase the hardness of the surface of the screw 1 . In this embodiment, when carrying out the nitriding treatment step, the screw 1 is first placed in a vacuum box furnace, and the nitriding treatment is carried out at a temperature of 700 ° C ± 50 ° C for 90 minutes to 120 minutes, and then cooled to room temperature , so that the nitriding depth can reach 3 microns to 4 microns. Therefore, the present invention breaks through the limitation that the existing 300 series stainless steel screw fasteners cannot be heat-treated by using the "nitriding treatment" step, thus greatly improving the hardness of the surface of the screw 1 .

然后,如步骤26所示,对该螺丝1进行表面处理步骤,以在螺丝1表面形成防锈层,因而产生历经氮化热处理的300系列不锈钢螺丝1的成品。在本实施例中,是以涂布(Coating)方式形成该防锈层,且该防锈层需进行超过1000小时的盐雾试验。Then, as shown in step 26 , a surface treatment step is performed on the screw 1 to form an antirust layer on the surface of the screw 1 , thus producing a finished product of the 300 series stainless steel screw 1 undergoing nitriding heat treatment. In this embodiment, the anti-rust layer is formed by coating, and the anti-rust layer needs to be subjected to a salt spray test for more than 1000 hours.

因此,在本实施例中,由于对螺丝1施以700℃±50℃的温度的氮化处理达90分钟至120分钟,再冷却至常温,使得渗氮深度达到3微米至4微米,所以该300系列不锈钢螺丝1的成品的表面硬度可达维氏硬度(HV)600以上,且该300系列不锈钢螺丝1的成品能贯穿洛氏硬度B尺度(HRB)80±5且厚度为3毫米至6毫米的型钢。Therefore, in this embodiment, since the screw 1 is subjected to nitriding treatment at a temperature of 700°C±50°C for 90 minutes to 120 minutes, and then cooled to normal temperature, the nitriding depth reaches 3 microns to 4 microns, so the The surface hardness of the finished 300 series stainless steel screw 1 can reach Vickers hardness (HV) 600 or more, and the finished product of the 300 series stainless steel screw 1 can penetrate the Rockwell hardness B scale (HRB) 80±5 and the thickness is 3 mm to 6 millimeter steel.

另外,需特别提出的是,在上述实施例中,是以该螺丝1为钻尾螺丝的情况来做说明,然而,本发明不限于此,而是本发明的其他实施例也可省略步骤22的夹尾步骤,也就是说,本发明300系列不锈钢螺丝扣件氮化热处理制程,也可适用于不具有该钻尾部121的一般300系列不锈钢螺丝扣件。In addition, it should be pointed out that, in the above-mentioned embodiment, the description is made with the screw 1 being a drill screw. However, the present invention is not limited thereto, but other embodiments of the present invention can also omit step 22. The tail clamping step, that is to say, the nitriding heat treatment process of the 300 series stainless steel screw fastener of the present invention is also applicable to the general 300 series stainless steel screw fastener without the drill tail 121 .

综上所述,本发明300系列不锈钢螺丝扣件氮化热处理制程,是以「氮化处理」步骤25突破现有300系列不锈钢螺丝扣件原本无法热处理的限制,因而能大幅提高螺丝1表面的硬度,所以确实能达成本发明的目的。To sum up, the nitriding heat treatment process of the 300 series stainless steel screw fasteners of the present invention breaks through the limitation that the existing 300 series stainless steel screw fasteners cannot be heat treated in step 25 of the "nitriding treatment", thus greatly improving the surface hardness of the screw 1. Hardness, so the purpose of the present invention can really be achieved.

Claims (8)

1. a kind of 300 series stainless steel screw fasteners nitridation heat treatment processing procedure, which is characterized in that comprise the steps of
(a) forming step is carried out to the disk member of 300 series stainless steel materials, so that the disk member has screw terminal and screw rod;
(b) it carries out rolling over tooth step, so that at least one portion of the screw rod becomes screw thread portion, thus forms screw;
(c) nitridation process step is carried out to the screw, to increase the hardness of the screw surface;And
(d) surface treatment step is carried out to the screw, to form antirust coat in the screw surface.
2. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: also wrap (e) step being contained between described (b) step and (c) step, is the surface for being cleaned the screw with sour agent, is polished, To improve the brightness of the screw surface.
3. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: in institute It states in (c) step, is that the screw is placed in vacuum box-type furnace to carry out nitridation process step.
4. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: in institute It states in (c) step, is to carry out nitridation process step with 700 DEG C ± 50 DEG C of temperature up to 90 minutes to 120 minutes, is cooled to often Temperature, so that depth of nitration reaches 3 microns to 4 microns.
5. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: in institute It states in (c) step, is that first the screw is placed in vacuum box-type furnace, nitrogen treatment step is carried out with 700 DEG C ± 50 DEG C of temperature Suddenly up to 90 minutes to 120 minutes, it is cooled to room temperature, so that depth of nitration reaches 3 microns to 4 microns.
6. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: in institute It states in (d) step, the antirust coat need to be performed for more than 1000 hours salt spray tests.
7. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 1, it is characterised in that: also wrap (f) step being contained between described (a) step and (b) step carries out folder tail step, so that the screw rod is far from the spiral shell The end of silk head becomes drilling tail portion, and (b) step makes remaining screw bar part other than the drilling tail portion become the spiral shell Silk tooth portion.
8. 300 series stainless steel screw fastener nitridation heat treatment processing procedure according to claim 7, it is characterised in that: described The surface hardness of the finished product of screw is 600 or more Vickers hardness, and can be through Rockwell hardness B scale 80 ± 5 and with a thickness of 3 millimeters To 6 millimeters of fashioned iron.
CN201810568574.7A 2018-05-09 2018-06-05 300 series stainless steel screw fasteners nitridation heat treatment processing procedure Pending CN110468369A (en)

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TW107115669A TWI714846B (en) 2018-05-09 2018-05-09 Nitriding heat treatment process for 300 series stainless steel screw fasteners
TW107115669 2018-05-09

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