CN110441163B - High temperature ultrasonic fatigue in-situ testing instrument and testing method - Google Patents
High temperature ultrasonic fatigue in-situ testing instrument and testing method Download PDFInfo
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Abstract
本发明涉及一种高温超声疲劳原位测试仪器及测试方法,属于精密科学仪器领域。仪器由整体框架模块、机械加载模块、高温加载模块和原位监测模块组成,整体框架模块用于对各功能模块精确定位,同时提供稳定支撑和有效隔振;机械加载模块用于对被测试样两端同步施加静态拉伸/压缩载荷,依据测试需要施加超声疲劳载荷,并可实现轴向的精确转位;高温加载模块用于对被测试样施加高温载荷;原位监测模块用于对被测试样的表面变形损伤与内部损伤缺陷实施并行原位监测。可实现对被测试样缺陷信息由内而外、由表及里的同步表征及三维重构。具有载荷环境复杂、测试精度高、同时能动态监测材料力学行为与变形损伤机制的特点。
The invention relates to a high-temperature ultrasonic fatigue in-situ testing instrument and a testing method, and belongs to the field of precision scientific instruments. The instrument consists of an overall frame module, a mechanical loading module, a high-temperature loading module and an in-situ monitoring module. The overall frame module is used for precise positioning of each functional module, while providing stable support and effective vibration isolation; the mechanical loading module is used for the test sample. Static tensile/compression loads are applied simultaneously at both ends, ultrasonic fatigue loads are applied according to the test requirements, and accurate axial indexing can be achieved; the high temperature loading module is used to apply high temperature loads to the tested sample; the in-situ monitoring module is used to apply high temperature loads to the tested sample. The surface deformation damage and internal damage defects of the test samples were monitored in situ in parallel. It can realize the synchronous characterization and three-dimensional reconstruction of the defect information of the tested sample from the inside to the outside and from the outside to the inside. It has the characteristics of complex load environment, high test accuracy, and dynamic monitoring of material mechanical behavior and deformation damage mechanism.
Description
技术领域technical field
本发明涉及精密科学仪器领域,特别涉及一种高温超声疲劳原位测试仪器及测试方法。在真空或惰性气体氛围下实现被测材料试样的高温加载,同时可实现对被测试样缺陷信息由内而外、由表及里的同步表征及三维重构。为航空航天、装备制造等领域材料在高温、超声载荷作用下的疲劳性能及变形损伤机制研究提供了一种可靠手段。The invention relates to the field of precision scientific instruments, in particular to a high-temperature ultrasonic fatigue in-situ testing instrument and a testing method. The high-temperature loading of the tested material sample can be realized in a vacuum or inert gas atmosphere, and at the same time, the synchronous characterization and three-dimensional reconstruction of the defect information of the tested sample from the inside to the outside and from the outside to the inside can be realized. It provides a reliable method for studying the fatigue performance and deformation damage mechanism of materials in the fields of aerospace and equipment manufacturing under high temperature and ultrasonic loads.
背景技术Background technique
结合原位监测手段,开展力热耦合疲劳测试是获取材料在高温下的服役性能、探究其疲劳性能演化规律的重要手段。在航空航天、装备制造等领域,一些关键结构材料如航空发动机涡轮叶片、汽车发动机活塞等常在高温、高频的工况下服役,疲劳失效时有发生,对国家造成了严重的经济损失。如何实现高温温度场及高频机械载荷的高精度加载,模拟材料接近实际服役工况,并结合原位监测装置开展材料接近实际服役工况下的原位监测,是评估材料高温疲劳性能和服役安全性的关键。Combining in-situ monitoring methods, carrying out mechanical-thermal coupled fatigue testing is an important method to obtain the service performance of materials at high temperature and to explore the evolution law of fatigue performance. In the fields of aerospace and equipment manufacturing, some key structural materials, such as aero-engine turbine blades, automobile engine pistons, etc., often serve under high temperature and high frequency conditions, and fatigue failures often occur, causing serious economic losses to the country. How to achieve high-precision loading of high-temperature temperature field and high-frequency mechanical load, simulate materials close to actual service conditions, and combine in-situ monitoring devices to carry out in-situ monitoring of materials close to actual service conditions, is to evaluate the high-temperature fatigue performance and service conditions of materials. The key to safety.
万能试验机、超声疲劳试验机、低频疲劳试验机、集成马弗炉的疲劳试验机等是目前市面上比较常见的材料试验机,这些试验机结构简单、功能单一,难以构建真空或惰性气体氛围,无法实现对被测试样高温温度场及高频机械载荷的高精度加载,并且由于缺乏原位监测装置,在试验过程中也难以开展对被测试样的原位监测。受制于现有材料测试装置,现有的测试方法也相对单一,难以实现对航空、航天及汽车等关键领域材料在高温、超声疲劳作用下疲劳性能及变形损伤机制的研究。Universal testing machines, ultrasonic fatigue testing machines, low-frequency fatigue testing machines, and fatigue testing machines with integrated muffle furnaces are relatively common material testing machines on the market. These testing machines are simple in structure and single in function, making it difficult to build a vacuum or inert gas atmosphere. , it is impossible to achieve high-precision loading of the high-temperature temperature field and high-frequency mechanical load of the tested sample, and due to the lack of an in-situ monitoring device, it is difficult to carry out in-situ monitoring of the tested sample during the test. Restricted by the existing material testing equipment and the existing testing methods are relatively simple, it is difficult to realize the research on the fatigue performance and deformation damage mechanism of materials in key fields such as aviation, aerospace and automobiles under the action of high temperature and ultrasonic fatigue.
随着光学显微成像技术、红外热成像技术、X射线晶体衍射技术等在材料微观力学性能测试领域的广泛应用,基于多种原位监测手段并行监测的原位力学测试技术在关键领域材料高温疲劳性能及变形损伤机制研究中的作用愈发突出。如:采用CT扫描成像技术和光学显微成像技术同步表征,可直观获取被测试样内部三维形貌及表面微区形貌;采用CT扫描成像技术和红外热成像技术同步表征,可直观获取被测试样内部损伤的三维形貌及试样标距段全局温度分布信息。With the wide application of optical microscopy imaging technology, infrared thermal imaging technology, X-ray crystal diffraction technology, etc. in the field of material micromechanical property testing, the in situ mechanical testing technology based on parallel monitoring of multiple in situ monitoring methods is used in key areas of high temperature materials. The role of fatigue performance and deformation damage mechanism research has become more and more prominent. For example, by using CT scanning imaging technology and optical microscopic imaging technology for simultaneous characterization, the internal three-dimensional topography and surface micro-region topography of the test sample can be intuitively obtained; by using CT scanning imaging technology and infrared thermal imaging technology for simultaneous characterization, the test sample can be visually obtained. The three-dimensional morphology of the internal damage of the test sample and the global temperature distribution information of the sample gauge section.
综上所述,面向国家航空航天、装备制造等领域关键结构材料的重大测试需求,结合现有的原位监测技术,研制一种高温超声疲劳原位测试仪器,并提供一种高温超声疲劳原位测试方法是十分必要的。To sum up, in order to meet the major testing requirements of key structural materials in the fields of national aerospace and equipment manufacturing, combined with the existing in-situ monitoring technology, a high-temperature ultrasonic fatigue in-situ testing instrument is developed, and a high-temperature ultrasonic fatigue test instrument is provided. A bit test method is necessary.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种高温超声疲劳原位测试仪器及测试方法,弥补现有测试方法及测试技术的不足。本发明仪器采用液压伺服驱动技术、电伺服驱动技术、压电超声驱动技术,并结合电阻丝辐射加热技术,可构建真空或惰性气体氛围,实现对被测试样在高温环境下的超声疲劳测试。同时,采用高景深显微成像装置、红外热成像装置、CT扫描装置,可实现对被测试样缺陷信息由内而外、由表及里的同步表征及三维重构;基于高温超声疲劳原位测试仪器,提供了一种高温超声疲劳原位测试方法,面向国家航空航天、装备制造等领域关键结构材料的重大测试需求,为其在高温、超声疲劳作用下疲劳性能及变形损伤机制的研究提供了可靠手段。The purpose of the present invention is to provide a high-temperature ultrasonic fatigue in-situ testing instrument and a testing method to make up for the deficiencies of the existing testing methods and testing techniques. The instrument of the invention adopts hydraulic servo drive technology, electric servo drive technology, piezoelectric ultrasonic drive technology, combined with resistance wire radiation heating technology, can construct vacuum or inert gas atmosphere, and realize ultrasonic fatigue test of the tested sample under high temperature environment. At the same time, the high-depth-of-field microscopic imaging device, infrared thermal imaging device, and CT scanning device can be used to realize the simultaneous characterization and three-dimensional reconstruction of the defect information of the tested sample from the inside to the outside, from the outside to the inside; based on high-temperature ultrasonic fatigue in situ The test instrument provides a high-temperature ultrasonic fatigue in-situ test method for the major testing needs of key structural materials in the fields of national aerospace and equipment manufacturing. reliable means.
本发明的上述目的通过以下技术方案实现:The above-mentioned purpose of the present invention is achieved through the following technical solutions:
高温超声疲劳原位测试仪器,包括整体框架模块1、机械加载模块2、原位监测模块3、高温加载模块4,整体框架模块1采用四立柱式结构,实现对机械加载模块2、原位监测模块3、高温加载模块4的牢固支撑,机械加载模块2分别通过商业化电机驱动组件40的支撑外壳、上液压缸43的连接法兰与整体框架模块1中的上支撑板9、安装平台5刚性连接,实现对被测试样的两端同步施加静态拉伸/压缩载荷,原位监测模块3分别通过固定底板67、固定座60、导轨座61和安装架58与整体框架模块1中的安装平台5、CT固定板Ⅱ14、立柱连接块8、CT固定板Ⅰ7刚性连接,实现对被测试样缺陷信息进行由内而外、由表及里的同步表征及三维重构;高温加载模块4通过“L”型支座75与整体框架模块1的安装平台5刚性连接,并通过上、下动密封波纹管71、77与机械加载模块2中的上、下超声探头上33、35连接,构建真空或惰性气体氛围以隔绝氧气,实现对被测试样的高温加载。High-temperature ultrasonic fatigue in-situ testing instrument, including overall frame module 1,
所述的机械加载模块2包含液压加载子模块15、超声加载子模块16和试样转位子模块17,超声加载子模块16实现对被测试样的超声疲劳加载,液压加载子模块15分别通过上、下活塞杆46、47与试样转位子模块17的胀紧套Ⅱ41及超声加载子模块16的胀紧套Ⅰ38刚性连接;试样转位子模块17通过胀紧套Ⅲ42与超声加载子模块16的中间连接杆27刚性连接,在一次测试试验中,同时实现对被测试样进行双端同步静态拉伸载荷加载、超声疲劳载荷加载与轴向精确转位。The
所述的超声加载子模块16中的上、下高温连杆23、22的尺寸超声系统匹配,在20kHz下达到纵振;上、下高温连杆23、22中开有对称分布的“H”型冷却流道,且冷却流道的出/入口均设置在其振动位移节点,以减小冷却水管对上、下高温连杆23、22振动的干扰。The dimensions of the upper and lower high-
所述的原位监测模块3包含三维红外热成像子模块51、高景深显微成像子模块52、CT扫描成像子模块53,所述三维红外热成像子模块51的两个红外热成像装置69均放置在“H”型安装板62上,实现对被测试样标距段全局温度信息的三维重构;所述高景深显微成像子模块52是:高景深显微成像装置65固定在显微镜安装板64上,显微镜安装板64固定在显微镜三自由度定位平台66上,在显微镜三自由度定位平台66的驱动下,高景深显微成像装置65相对被测试样的轴向及径向位置进行快速、精确调整,实现对被测试样标距中心微区表面形貌、缺陷的随动监测;所述CT扫描成像子模块53是:CT主机55固定在支撑板59上,支撑板59固定在CT三自由度定位平台54上,CT三自由度定位平台54固定在固定座60上,高分辨率接收板56固定在接收板Z向定位平台57上,接收板Z向定位平台57固定在安装架58上,在CT三自由度定位平台54的驱动下,CT主机55相对被测试样的轴向及径向位置进行快速、精确调整;在接收板Z向定位平台57的驱动下,高分辨率接收板56相对被测试样的轴向进行快速、精确调整,CT主机55与高分辨率接收板56配合使用,实现对被测试样标距段的逐层扫描、成像。The in-situ monitoring module 3 includes a three-dimensional infrared
所述的“H”型安装板62与滑块组件Ⅰ68连接,滑块组件Ⅰ68与导轨组件Ⅰ63配合,导轨组件Ⅰ63与导轨座61刚性连接,“H”型安装板62上加工有螺纹孔,导轨座61的相应位置加工有盲孔,“H”型安装板62沿着导轨组件163上下移动,并通过螺栓实现与导轨座61的固定。The "H"
所述的高温加载模块4中,气体弹簧组件82与上动密封波纹管71的法兰刚性连接,限制波纹管的轴向转动自由度,防止波纹管受扭破坏。In the above-mentioned high temperature loading module 4, the
所述的高温加载模块4中,旋转密封组件Ⅰ、Ⅱ87、91包含密封圈Ⅰ94、密封圈组件95、密封圈Ⅱ96、密封轴套97、密封法兰98,密封圈组件95嵌入上超声探头33轴肩的密封槽内,密封圈Ⅰ94嵌入密封法兰98的密封槽内,密封圈Ⅱ96嵌入上动密封波纹管71法兰上的密封槽内,旋转密封组件Ⅰ、Ⅱ87、91与上、下超声探头33、35配合,实现旋转密封。In the high temperature loading module 4, the rotary seal assemblies I, II 87, and 91 include a
所述的高温加载模块4中,内嵌式石英观测窗组件89为独立的模块,通过螺栓固定在真空腔72外壁上;内嵌式石英观测窗组件89由内外两层石英玻璃组成,内外两层石英玻璃间有间隙,通入循环冷却水实现冷却,外层石英玻璃的底部紧靠加热炉78的炉壁,内层石英玻璃内径大于高景深显微成像装置65的镜头外径,试验时高景深显微成像装置65的镜头探入内嵌式石英观测窗组件89中,以满足其显微成像距离要求。In the high temperature loading module 4, the built-in quartz
所述的高温加载模块4中,腔体支撑座74焊接在真空腔72侧壁上,并通过螺栓与滑块组件Ⅱ86刚性连接,滑块组件Ⅱ86与导轨组件Ⅱ79配合,导轨组件Ⅱ79通过螺栓与“L”型支座75刚性连接,“L”型支座75与安装平台5刚性连接,当进行常温试验时,真空腔72沿着导轨移动,为试验人员提供充足的操作空间。In the above-mentioned high temperature loading module 4, the
本发明的另一目的在于提供一种高温超声疲劳原位测试方法,具体步骤如下:Another object of the present invention is to provide a high-temperature ultrasonic fatigue in-situ testing method, the specific steps are as follows:
步骤一、超声试样34的装夹:将“H”型安装板62沿着导轨组件Ⅰ63移动至上极限位置,并用螺栓固定;打开真空腔门83,将超声试样34通过双头螺柱与上、下高温连杆23、22刚性连接;Step 1. Clamping of the ultrasonic sample 34: Move the "H"
步骤二、超声试样34的高温加载:真空腔72内构建真空环境,或向真空腔72内持续通入惰性气体构建惰性气体氛围;温度控制器向加热炉78内的电阻丝通入不同大小的电压使其发热,并通过热辐射的方式实现超声试样34不同温度的高温加载;红外测温计Ⅰ、Ⅱ92、93实时监测超声试样34标距段的温度,并反馈至温度控制器,形成闭环控制;
步骤三、超声试样34的静态拉伸/压缩载荷加载:超声试样34的静态拉伸/压缩载荷加载由机械加载模块2来实现,上、下高压油驱动活塞杆46、47相向运动,将动力传递给超声加载子模块16,带动上、下高温连杆23、22相向运动,实现对超声试样34的静态拉伸/压缩载荷加载;Step 3. Static tensile/compressive load loading of the ultrasonic sample 34: The static tensile/compressive load loading of the
步骤四、超声试样34的超声疲劳载荷加载:超声试样34的超声疲劳载荷加载由超声加载子模块16来实现,超声换能器26输出的微弱机械振动经上超声连接器25、上超声探头33的两极放大后,依次传递给上高温连杆23、超声试样34、下高温连杆22、下超声探头35、下超声连接器21,激励这些零件对在20 kHz形成稳定的共振,实现超声试样34的超声疲劳载荷加载;Step 4. Ultrasonic fatigue load loading of the ultrasonic sample 34: The ultrasonic fatigue load loading of the
步骤五、超声试样34的轴向转位:超声试样34的轴向转位由试样转位子模块17来实现,商业化电机驱动组件40中伺服电机输出的动力,经减速器传递给花键轴39,带动超声加载子模块16旋转,实现超声试样34的轴向转位;
步骤六、超声试样34的并行原位监测:超声试样34的并行原位监测由原位监测模块3来实现,在三维红外热成像子模块51中,两个红外热成像装置69均放置在“H”型安装板62上,实现对被测试样标距段温度信息的三维重构;在高景深显微成像子模块52中,显微镜三自由度定位平台66的驱动高景深显微成像装置65相对被测试样的轴向及径向位置进行快速、精确调整,实现对被测试样标距中心微区表面形貌、缺陷的随动监测;在CT扫描成像子模块53中,CT三自由度定位平台54的驱动CT主机55对被测试样标距段进行逐层扫描、成像,实现对被测试样标距段全局缺陷信息三维重构;三维红外热成像子模块51、高景深显微成像子模块52、CT扫描成像子模块53可同时使用,或两两组合使用,或单个使用,实现试验过程中对超声试样34的动态原位监测。Step 6. Parallel in-situ monitoring of the ultrasonic sample 34: The parallel in-situ monitoring of the
本发明的有益效果在于:The beneficial effects of the present invention are:
1、采用多因素耦合模块化设计思路。本仪器由整体框架模块、机械加载模块、原位监测模块、高温加载模块组成,其中机械加载模块包含液压加载子模块、超声加载子模块和试样转位子模块,原位监测模块包含三维红外热成像子模块、高景深显微成像子模块、CT扫描成像子模块。使设备标准化、模块化,便于维护保养。1. Adopt multi-factor coupled modular design ideas. The instrument consists of an overall frame module, a mechanical loading module, an in-situ monitoring module, and a high-temperature loading module. The mechanical loading module includes a hydraulic loading sub-module, an ultrasonic loading sub-module and a sample transposition sub-module, and the in-situ monitoring module includes a three-dimensional infrared thermal Imaging sub-module, high-depth microscopic imaging sub-module, CT scanning imaging sub-module. Standardize and modularize equipment for easy maintenance.
2、可有效防止被测试样的表面氧化。可利用机械泵(外部装置)配合分子泵(外部装置)两级抽真空的方式抽取真空腔内的空气(氧气)或向真空腔内持续通入惰性气体排除空气(氧气),构建真空或惰性气体氛围,防止被测试样表面氧化。2. It can effectively prevent the surface oxidation of the tested sample. The mechanical pump (external device) and the molecular pump (external device) can be used to extract the air (oxygen) in the vacuum chamber by two-stage vacuuming, or continuously pass inert gas into the vacuum chamber to remove the air (oxygen), and build a vacuum or inert gas. Gas atmosphere to prevent oxidation of the surface of the test sample.
3、可真实模拟材料实际服役工况。本发明采用液压伺服驱动技术、电伺服驱动技术、压电超声驱动技术、电阻丝辐射加热技术,可实现对被测试样高温温度场及高频机械载荷的高精度加载,真实模拟航空、航天及汽车等关键领域材料的实际服役工况。3. It can realistically simulate the actual service conditions of materials. The invention adopts hydraulic servo drive technology, electric servo drive technology, piezoelectric ultrasonic drive technology, and resistance wire radiation heating technology, which can realize high-precision loading of the high-temperature temperature field and high-frequency mechanical load of the tested sample, and truly simulate aviation, aerospace and other industries. Actual service conditions of materials in key fields such as automobiles.
4、可实现试样内部损伤信息的并行原位监测。本发明集成高景深显微成像装置、红外热成像装置、CT扫描装置,可实现对被测试样缺陷信息由内而外、由表及里的同步表征及三维重构,为航空、航天及汽车等关键领域材料在高温、超声疲劳作用下的疲劳性能及变形损伤机制研究提供了一种可靠手段。4. Parallel in-situ monitoring of damage information inside the sample can be realized. The invention integrates a high-depth-of-field microscopic imaging device, an infrared thermal imaging device, and a CT scanning device, and can realize the synchronous characterization and three-dimensional reconstruction of the defect information of the tested sample from the inside to the outside, from the outside to the inside, and is suitable for aviation, aerospace and automobiles. It provides a reliable method to study the fatigue performance and deformation damage mechanism of materials in key fields such as high temperature and ultrasonic fatigue.
附图说明Description of drawings
此处所说明的附图用来提供对本发明的进一步理解,构成本申请的一部分,本发明的示意性实例及其说明用于解释本发明,并不构成对本发明的不当限定。The accompanying drawings described herein are used to provide a further understanding of the present invention and constitute a part of the present application. The schematic examples of the present invention and their descriptions are used to explain the present invention and do not constitute an improper limitation of the present invention.
图1为本发明的整体外观结构示意图;Fig. 1 is the overall appearance structure schematic diagram of the present invention;
图2为本发明的整体框架模块的结构示意图;Fig. 2 is the structural schematic diagram of the overall frame module of the present invention;
图3为本发明的机械加载模块的结构示意图;3 is a schematic structural diagram of a mechanical loading module of the present invention;
图4为本发明的超声加载子模块的结构示意图;4 is a schematic structural diagram of an ultrasonic loading sub-module of the present invention;
图5为本发明的试样转位子模块的结构示意图;5 is a schematic structural diagram of a sample transposition sub-module of the present invention;
图 6为本发明的液压加载子模块的结构示意图;6 is a schematic structural diagram of a hydraulic loading sub-module of the present invention;
图 7为本发明的原位监测模块的结构示意图;7 is a schematic structural diagram of an in-situ monitoring module of the present invention;
图8为本发明的CT扫描成像子模块的结构示意图;8 is a schematic structural diagram of a CT scanning imaging sub-module of the present invention;
图9为本发明的三维红外热成像子模块、高景深显微成像子模块的结构示意图;9 is a schematic structural diagram of a three-dimensional infrared thermal imaging sub-module and a high-depth-of-field microscopic imaging sub-module of the present invention;
图10为本发明的高温加载模块的主视图;10 is a front view of the high temperature loading module of the present invention;
图11为本发明的高温加载模块的后视图;Figure 11 is a rear view of the high temperature loading module of the present invention;
图12为本发明的测温组件的结构示意图;12 is a schematic structural diagram of the temperature measuring assembly of the present invention;
图13为本发明的旋转密封组件的结构示意图;13 is a schematic structural diagram of the rotary seal assembly of the present invention;
图14为本发明的超声加载子模块振动位移与应力的分布图;Fig. 14 is the distribution diagram of the vibration displacement and stress of the ultrasonic loading sub-module of the present invention;
图15为本发明的高温连杆振动位移与应力的分布图;Fig. 15 is the distribution diagram of the vibration displacement and stress of the high-temperature connecting rod of the present invention;
图16为本发明的并行原位监测原理图;16 is a schematic diagram of the parallel in-situ monitoring of the present invention;
图17为本发明的内嵌式石英观测窗组件的结构示意图;17 is a schematic structural diagram of the embedded quartz observation window assembly of the present invention;
图18为本发明的载荷加载、原位测试原理图;18 is a schematic diagram of load loading and in-situ testing of the present invention;
图19为沙漏型超声试样的结构示意图。FIG. 19 is a schematic structural diagram of an hourglass-shaped ultrasonic sample.
图中:1、整体框架模块;2、机械加载模块;3、原位监测模块;4、高温加载模块; 5、安装平台;6、立柱固定套筒;7、CT固定板Ⅰ;8、立柱连接块;9、上支撑板;10、锁紧螺钉;11、吊环螺钉;12、立柱;13、冷风枪支撑板;14、CT固定板Ⅱ;15、液压加载子模块;16、超声加载子模块;17、试样转位子模块;18、中间连接板;19、下连接器固定板Ⅰ;20、下螺母;21、下超声连接器;22、下高温连杆;23、上高温连杆;24、上连接器固定板Ⅰ;25、上超声连接器;26、超声换能器;27、中间连接杆;28、力传感器;29、力传感器固定板;30、上传力杆;31、上连接器固定板Ⅱ;32、上螺母;33、上超声探头;34、超声试样;35、下超声探头;36、下连接器固定板Ⅱ;37、下传力杆;38、胀紧套Ⅰ;39、花键轴;40、商业化电机驱动组件;41、胀紧套Ⅱ;42、胀紧套Ⅲ;43、上液压缸;44、上蓄能器;45、上阀板组件;46、上活塞杆;47、下活塞杆;48、下阀板组件;49、下蓄能器;50、下液压缸;51、三维红外热成像子模块;52、高景深显微成像子模块;53、CT扫描成像子模块;54、CT三自由度定位平台;55、CT主机;56、高分辨率接收板;57、接收板Z向定位平台;58、安装架;59、支撑板;60、固定座;61、导轨座;62、“H”型安装板;63、导轨组件Ⅰ;64、显微镜安装板;65、高景深显微成像装置;66、显微镜三自由度定位平台;67、固定底板;68、滑块组件Ⅰ;69、红外热成像装置;70、制冷组件;71、上动密封波纹管;72、真空腔;73、左石英观测窗;74、腔体支撑座;75、“L”型支座;76、腔门锁紧器;77、下动密封波纹管;78、加热炉;79、导轨组件Ⅱ;80、前石英观测窗;81、真空压力表;82、气体弹簧组件;83、真空腔门;84、腔门把手;85、铰链;86、滑块组件Ⅱ;87、旋转密封组件Ⅰ;88、右石英观测窗;89、内嵌式石英观测窗组件;90、真空波纹管组件;91、旋转密封组件Ⅱ;92、红外测温计Ⅰ;93、红外测温计Ⅱ;94、密封圈Ⅰ;95、密封圈组件;96、密封圈Ⅱ;97、密封轴套;98、密封法兰。In the figure: 1. Overall frame module; 2. Mechanical loading module; 3. In-situ monitoring module; 4. High temperature loading module; 5. Installation platform; 6. Upright column fixing sleeve; 7. CT fixing plate I; 8. Upright column Connection block; 9. Upper support plate; 10. Locking screw; 11. Lifting ring screw; 12. Upright column; 13. Cold air gun support plate; 14. CT fixing plate II; 15. Hydraulic loading sub-module; 16. Ultrasonic loading sub-module Module; 17. Sample transposition sub-module; 18. Intermediate connecting plate; 19. Lower connector fixing plate I; 20. Lower nut; 21. Lower ultrasonic connector; 22. Lower high-temperature connecting rod; 23. Upper high-temperature connecting rod ; 24, upper connector fixing plate I; 25, upper ultrasonic connector; 26, ultrasonic transducer; 27, middle connecting rod; 28, force sensor; 29, force sensor fixing plate; 30, uploading force rod; 31, Upper connector fixing plate II; 32. Upper nut; 33. Upper ultrasonic probe; 34. Ultrasonic sample; 35. Lower ultrasonic probe; 36. Lower connector fixing plate II; 37. Lower dowel rod; 38. Expansion Sleeve I; 39, Spline Shaft; 40, Commercial Motor Drive Components; 41, Expansion Sleeve II; 42, Expansion Sleeve III; 43, Upper Hydraulic Cylinder; 44, Upper Accumulator; 45, Upper Valve Plate Assembly ;46, upper piston rod; 47, lower piston rod; 48, lower valve plate assembly; 49, lower accumulator; 50, lower hydraulic cylinder; 51, 3D infrared thermal imaging sub-module; 52, high depth of field microscopy imaging sub Module; 53, CT scanning imaging sub-module; 54, CT three-degree-of-freedom positioning platform; 55, CT host; 56, high-resolution receiving plate; 57, receiving plate Z-direction positioning platform; 58, mounting frame; 59, support plate ;60, fixed seat; 61, guide rail seat; 62, "H" type mounting plate; 63, guide rail assembly I; 64, microscope mounting plate; 65, high depth of field microscope imaging device; 66, microscope three-degree-of-freedom positioning platform; 67, fixed bottom plate; 68, slider assembly I; 69, infrared thermal imaging device; 70, refrigeration assembly; 71, upper dynamic sealing bellows; 72, vacuum chamber; 73, left quartz observation window; 74, cavity support seat ;75, "L" type support; 76, cavity door lock; 77, lower dynamic sealing bellows; 78, heating furnace; 79, guide rail assembly II; 80, front quartz observation window; 81, vacuum pressure gauge; 82, gas spring assembly; 83, vacuum chamber door; 84, chamber door handle; 85, hinge; 86, slider assembly II; 87, rotary seal assembly I; 88, right quartz observation window; 89, embedded quartz observation Window assembly; 90, vacuum bellows assembly; 91, rotary seal assembly II; 92, infrared thermometer I; 93, infrared thermometer II; 94, sealing ring I; 95, sealing ring assembly; 96, sealing ring II ; 97, sealing sleeve; 98, sealing flange.
具体实施方式Detailed ways
下面结合附图进一步说明本发明的详细内容及其具体实施方式。The details of the present invention and the specific implementations thereof will be further described below with reference to the accompanying drawings.
参见图1至图19所示,本发明的高温超声疲劳原位测试仪器及测试方法,仪器由整体框架模块、机械加载模块、高温加载模块和原位监测模块组成。其中:整体框架模块用于对各功能模块精确定位,同时提供稳定支撑和有效隔振;机械加载模块用于对被测试样两端同步施加静态拉伸/压缩载荷,依据测试需要施加超声疲劳载荷,并可实现轴向的精确转位;高温加载模块用于对被测试样施加高温载荷;原位监测模块用于对被测试样的表面变形损伤与内部损伤缺陷实施并行原位监测。本发明面向航空航天、装备制造等领域对关键材料力学性能测试保障方面的重大需求,提供了一种高温超声疲劳原位测试方法,具有载荷环境复杂、测试精度高、同时能动态监测材料力学行为与变形损伤机制的特点。1 to 19, the high temperature ultrasonic fatigue in-situ testing instrument and testing method of the present invention is composed of an overall frame module, a mechanical loading module, a high-temperature loading module and an in-situ monitoring module. Among them: the overall frame module is used to accurately position each functional module, while providing stable support and effective vibration isolation; the mechanical loading module is used to simultaneously apply static tensile/compression loads to both ends of the tested sample, and ultrasonic fatigue loads are applied according to the test requirements. , and can achieve precise axial indexing; the high-temperature loading module is used to apply high-temperature load to the tested sample; the in-situ monitoring module is used to perform parallel in-situ monitoring of the surface deformation damage and internal damage defects of the tested sample. The present invention provides a high-temperature ultrasonic fatigue in-situ testing method in order to meet the major demands of the fields of aerospace, equipment manufacturing and other fields for testing and guaranteeing the mechanical properties of key materials, which has the advantages of complex load environment, high testing accuracy, and can dynamically monitor the mechanical behavior of materials at the same time. Characterization of damage mechanisms with deformation.
参见图1至图13所示,本发明的高温超声疲劳原位测试仪器,包括整体框架模块1、机械加载模块2、原位监测模块3、高温加载模块4,整体框架模块1采用四立柱式结构,用于实现对机械加载模块2、原位监测模块3、高温加载模块4的牢固支撑,并提供精确的安装定位及有效的隔振处理。机械加载模块2分别通过商业化电机驱动组件40的支撑外壳、上液压缸43的连接法兰与整体框架模块1中的上支撑板9、安装平台5刚性连接,用于实现对被测试样的两端同步施加静态拉伸/压缩载荷,依据测试需要施加超声疲劳载荷,并可实现轴向的精确转位。原位监测模块3分别通过固定底板67、固定座60、导轨座61和安装架58与整体框架模块1中的安装平台5、CT固定板Ⅱ14、立柱连接块8、CT固定板Ⅰ7刚性连接,用于实现对被测试样缺陷信息进行由内而外、由表及里的同步表征及三维重构;高温加载模块4通过“L”型支座75与整体框架模块1的安装平台5刚性连接,并通过上、下动密封波纹管71、77与机械加载模块2中的上、下超声探头上33、35连接,可构建真空或惰性气体氛围以隔绝氧气,实现对被测试样的高温加载。1 to 13, the high-temperature ultrasonic fatigue in-situ testing instrument of the present invention includes an overall frame module 1, a
参见图2所示,本发明的整体框架模块1包含安装平台5、立柱固定套筒6、CT固定板Ⅰ7、立柱连接块8、上支撑板9、锁紧螺钉10、吊环螺钉11、立柱12、冷风枪支撑板13、CT固定板Ⅱ14等,安装平台5通过地脚螺钉固定在地面,立柱12下端与立柱固定套筒6过盈配合,立柱12上端通过锁紧螺钉10与上支撑板9刚性连接,CT固定板Ⅰ7、冷风枪支撑板13、CT固定板Ⅱ14通过立柱连接块8与立柱12刚性连接,吊环螺钉11与上支撑板9刚性连接,用于实现对其余各模块的牢固支撑,并提供精确的安装定位及有效的隔振处理。Referring to FIG. 2 , the overall frame module 1 of the present invention includes an
参见图3所示,本发明所述的机械加载模块2包含液压加载子模块15、超声加载子模块16和试样转位子模块17,液压加载子模块15分别通过上、下活塞杆46、47与试样转位子模块17的胀紧套Ⅱ41及超声加载子模块16的胀紧套Ⅰ38刚性连接;试样转位子模块17通过胀紧套Ⅲ42与超声加载子模块16的中间连接杆27刚性连接,在一次测试试验中,可同时实现对被测试样进行双端同步静态拉伸载荷加载、超声疲劳载荷加载与轴向精确转位。Referring to FIG. 3, the
参见图4所示,本发明的超声加载子模块16用于实现对被测试样的超声疲劳加载,由中间连接板18、下连接器固定板Ⅰ19、下螺母20、下超声连接器21、下高温连杆22、上高温连杆23、上连接器固定板Ⅰ24、上超声连接器25、超声换能器26、中间连接杆27、力传感器28、力传感器固定板29、上传力杆30、上连接器固定板Ⅱ31、上螺母32、上超声探头33、超声试样34、下超声探头35、下连接器固定板Ⅱ36、下传力杆37、胀紧套Ⅰ38等组成,中间连接杆27与力传感器28刚性连接,力传感器28与力传感器固定板29刚性连接,力传感器固定板29与上传力杆30刚性连接,上传力杆30通过上连接器固定板Ⅱ31、上连接器固定板Ⅰ24、上螺母32与上超声连接器25刚性连接,胀紧套Ⅰ38与中间连接板18刚性连接,中间连接板18与下传力杆37刚性连接,下传力杆37通过下连接器固定板Ⅰ19、下连接器固定板Ⅱ36、下螺母20与下超声连接器21刚性连接,超声换能器26、上超声连接器25、上超声探头33、上高温连杆23、超声试样34、下高温连杆22、下超声探头35、下超声连接器21间均通过双头螺柱刚性连接,用于实现对被测试样的超声疲劳加载。Referring to FIG. 4 , the
所述的超声加载子模块16中的上、下高温连杆23、22的尺寸经过特殊设计与仿真分析结合,以保证其能够与超声系统匹配,在20 kHz下达到纵振;上、下高温连杆23、22中开有对称分布的“H”型冷却流道,且冷却流道的出/入口均设置在其振动位移节点,以减小冷却水管对上、下高温连杆23、22振动的干扰。The dimensions of the upper and lower high-
参见图5所示,本发明的试样转位子模块17由商业化电机驱动组件40、胀紧套Ⅱ41、胀紧套Ⅲ42等组成,其中商业化电机驱动组件40中,与胀紧套Ⅱ41、胀紧套Ⅲ42相连的轴为花键轴39,在试验过程中,液压加载子模块15能够驱动花键轴39进行直线运动,试样转位子模块17能够驱动花键轴39进行旋转运动,从而同时实现对被测试样的静态拉伸加载及精确轴向转位。Referring to FIG. 5 , the sample indexing sub-module 17 of the present invention is composed of a commercial
参见图6所示,本发明的液压加载子模块15由上液压缸43、上蓄能器44、上阀板组件45、上活塞杆46、下活塞杆47、下阀板组件48、下蓄能器49、下液压缸50等组成,上蓄能器44安装在上阀板组件45上,上阀板组件45通过螺栓与上液压缸43刚性连接;下蓄能器49安装在下阀板组件48上,下阀板组件48通过螺栓与下液压缸50刚性连接,用于实现对被测试样的双端静态拉伸/压缩载荷同步加载。6 , the
参见图7所示,本发明的原位监测模块3分别通过固定底板67、固定座60、导轨座61和安装架58与整体框架模块1中的安装平台5、CT固定板Ⅱ14、立柱连接块8、CT固定板Ⅰ7刚性连接,用于实现对被测试样缺陷信息进行由内而外、由表及里的同步表征及三维重构。Referring to FIG. 7 , the in-situ monitoring module 3 of the present invention is connected to the mounting
参见图8、图9所示,本发明所述的原位监测模块3包含三维红外热成像子模块51、高景深显微成像子模块52、CT扫描成像子模块53,其中三维红外热成像子模块51用于实现对被测试样标距段温度信息的三维重构,包含导轨座61、“H”型安装板62、导轨组件Ⅰ63、滑块组件Ⅰ68、红外热成像装置69等,两个红外热成像装置69均放置在“H”型安装板62上,并且二者呈一定角度,以实现对被测试样标距段全局温度信息的三维重构;所述高景深显微成像子模块52用于实现对被测试样表面缺陷信息显微观测,包含显微镜安装板64、高景深显微成像装置65、显微镜三自由度定位平台66、固定底板67等,高景深显微成像装置65通过螺栓固定在显微镜安装板64上,显微镜安装板64通过螺栓固定在显微镜三自由度定位平台66上,在显微镜三自由度定位平台66的驱动下,高景深显微成像装置65可以相对被测试样的轴向及径向位置进行快速、精确调整,实现对被测试样标距中心微区表面形貌、缺陷的随动监测;所述CT扫描成像子模块53用于实现对被测试样标距段全局缺陷信息三维重构,包含CT三自由度定位平台54、CT主机55、高分辨率接收板56、接收板Z向定位平台57、安装架58、支撑板59、固定座60等,CT主机55通过螺栓固定在支撑板59上,支撑板59通过螺栓固定在CT三自由度定位平台54上,CT三自由度定位平台54通过螺栓固定在固定座60上,高分辨率接收板56通过螺栓固定在接收板Z向定位平台57上,接收板Z向定位平台57通过螺栓固定在安装架58上,在CT三自由度定位平台54的驱动下,CT主机55可以相对被测试样的轴向及径向位置进行快速、精确调整;在接收板Z向定位平台57的驱动下,高分辨率接收板56可以相对被测试样的轴向进行快速、精确调整,CT主机55与高分辨率接收板56配合使用,实现对被测试样标距段的逐层扫描、成像。8 and 9, the in-situ monitoring module 3 of the present invention includes a three-dimensional infrared
所述的“H”型安装板62通过螺栓与滑块组件Ⅰ68连接,滑块组件Ⅰ68与导轨组件Ⅰ63配合,导轨组件Ⅰ63通过螺栓与导轨座61刚性连接,“H”型安装板62上加工有螺纹孔,导轨座61的相应位置加工有盲孔,“H”型安装板62可沿着导轨组件163上下移动,并通过螺栓实现与导轨座61的固定。The "H"
参见图10至图12所示,本发明高温加载模块4由制冷组件70、上动密封波纹管71、真空腔72、左石英观测窗73、腔体支撑座74、“L”型支座75、腔门锁紧器76、下动密封波纹管77、加热炉78、导轨组件Ⅱ79、前石英观测窗80、真空压力表81、气体弹簧组件82、真空腔门83、腔门把手84、铰链85、滑块组件Ⅱ86、旋转密封组件Ⅰ87、右石英观测窗88、内嵌式石英观测窗组件89、真空波纹管组件90、旋转密封组件Ⅱ91、红外测温计Ⅰ92、红外测温计Ⅱ93等组成,可构建真空或惰性气体氛围以隔绝氧气,用于实现对被测试样最高1200℃的高温加载。制冷组件70通过螺钉与冷风枪支撑板13刚性连接;左石英观测窗73、前石英观测窗80、右石英观测窗88通过螺钉与真空腔72外壁刚性连接;腔门锁紧器76、腔门把手84通过螺钉与真空腔72外壁刚性连接;铰链85分别与真空腔72、真空腔门83通过螺钉刚性连接;真空波纹管组件90通过螺钉与真空腔72上壁的法兰口刚性连接。10 to 12 , the high-temperature loading module 4 of the present invention is composed of a
所述的高温加载模块4中,气体弹簧组件82通过螺栓与上动密封波纹管71的法兰刚性连接,用于限制波纹管的轴向转动自由度,防止波纹管受扭破坏。In the high temperature loading module 4, the
参见图13所示,本发明的所述的高温加载模块4中,旋转密封组件Ⅰ、Ⅱ87、91包含密封圈Ⅰ94、密封圈组件95、密封圈Ⅱ96、密封轴套97、密封法兰98等,密封圈组件95嵌入上超声探头33轴肩的密封槽内,密封圈Ⅰ94嵌入密封法兰98的密封槽内,密封圈Ⅱ96嵌入上动密封波纹管71法兰上的密封槽内,旋转密封组件Ⅰ、Ⅱ87、91与上、下超声探头33、35配合,实现旋转密封。Referring to FIG. 13 , in the high-temperature loading module 4 of the present invention, the rotary seal assemblies I,
所述的高温加载模块4中,内嵌式石英观测窗组件89为独立的模块,通过螺栓固定在真空腔72外壁上,便于拆卸;内嵌式石英观测窗组件89由内外两层石英玻璃组成,内外两层石英玻璃间有间隙,用于通入循环冷却水实现冷却,外层石英玻璃的底部紧靠加热炉78的炉壁,内层石英玻璃内径略大于高景深显微成像装置65的镜头外径,试验时高景深显微成像装置65的镜头可以探入内嵌式石英观测窗组件89中,以满足其显微成像距离要求。In the high temperature loading module 4, the built-in quartz
所述的高温加载模块4中,腔体支撑座74焊接在真空腔72侧壁上,并通过螺栓与滑块组件Ⅱ86刚性连接,滑块组件Ⅱ86与导轨组件Ⅱ79配合,导轨组件Ⅱ79通过螺栓与“L”型支座75刚性连接,“L”型支座75通过螺栓与安装平台5刚性连接,当进行常温试验时,真空腔72可沿着导轨移动,为试验人员提供充足的操作空间。In the above-mentioned high temperature loading module 4, the
参见图1至图17所示,本发明的高温超声疲劳原位测试方法,当进行高温超声疲劳原位测试试验时,具体步骤如下:Referring to FIGS. 1 to 17 , in the high-temperature ultrasonic fatigue in-situ test method of the present invention, when the high-temperature ultrasonic fatigue in-situ test is performed, the specific steps are as follows:
步骤一、超声试样34的装夹:将“H”型安装板62沿着导轨组件Ⅰ63移动至上极限位置,并用螺栓固定,此步骤是为了避免真空腔门83开合时与三维红外热成像子模块51发生干涉;打开真空腔门83,将超声试样34通过双头螺柱与上、下高温连杆23、22刚性连接;Step 1. Clamping of the ultrasonic sample 34: Move the "H"-shaped mounting
步骤二、超声试样34的高温加载:利用机械泵(外部装置)配合分子泵(外部装置)两级抽真空的方式抽取真空腔72内的空气(氧气)以构建真空环境,或向真空腔72内持续通入惰性气体排除真空腔72内空气(氧气),构建惰性气体氛围;温度控制器向加热炉78内的电阻丝通入不同大小的电压使其发热,并通过热辐射的方式实现超声试样34不同温度的高温加载;红外测温计Ⅰ、Ⅱ92、93实时监测超声试样34标距段的温度,并反馈至温度控制器,形成闭环控制;
步骤三、超声试样34的静态拉伸/压缩载荷加载:超声试样34的静态拉伸/压缩载荷加载由机械加载模块2来实现,上、下高压油驱动活塞杆46、47相向运动,将动力传递给超声加载子模块16,带动上、下高温连杆23、22相向运动,实现对超声试样34的静态拉伸/压缩载荷加载;Step 3. Static tensile/compressive load loading of the ultrasonic sample 34: The static tensile/compressive load loading of the
步骤四、超声试样34的超声疲劳载荷加载:超声试样34的超声疲劳载荷加载由超声加载子模块16来实现,超声换能器26输出的微弱机械振动经上超声连接器25、上超声探头33的两极放大后,依次传递给上高温连杆23、超声试样34、下高温连杆22、下超声探头35、超声连接器21,激励这些零件对在20 kHz形成稳定的共振,实现超声试样34的超声疲劳载荷加载;Step 4. Ultrasonic fatigue load loading of the ultrasonic sample 34: The ultrasonic fatigue load loading of the
步骤五、超声试样34的轴向转位:超声试样34的轴向转位由试样转位子模块17来实现,商业化电机驱动组件40中伺服电机输出的动力,经减速器传递给花键轴39,带动超声加载子模块16旋转,实现超声试样34的轴向转位;
步骤六、超声试样34的并行原位监测:超声试样34的并行原位监测由原位监测模块3来实现,在三维红外热成像子模块51中,两个红外热成像装置69均放置在“H”型安装板62上,并且二者呈一定角度,实现对被测试样标距段温度信息的三维重构;在高景深显微成像子模块52中,显微镜三自由度定位平台66的驱动高景深显微成像装置65相对被测试样的轴向及径向位置进行快速、精确调整,实现对被测试样标距中心微区表面形貌、缺陷的随动监测;在CT扫描成像子模块53中,CT三自由度定位平台54的驱动CT主机55对被测试样标距段进行逐层扫描、成像,实现对被测试样标距段全局缺陷信息三维重构;三维红外热成像子模块51、高景深显微成像子模块52、CT扫描成像子模块53可同时使用,或两两组合使用,或单个使用,实现试验过程中对超声试样34的动态原位监测。Step 6. Parallel in-situ monitoring of the ultrasonic sample 34: The parallel in-situ monitoring of the
参见图14至图19所示,本发明的原位监测相关公式如下:Referring to Fig. 14 to Fig. 19, the relevant formula of the in-situ monitoring of the present invention is as follows:
CT扫描成像原理公式CT scan imaging principle formula
式中,为穿过被测试样后的射线强度,为射线入射强度,为射线衰减系数,为射线穿过的被测试样厚度。In the formula, is the ray intensity after passing through the test sample, is the ray incident intensity, is the ray attenuation coefficient, It is the thickness of the test sample through which the ray passes.
以上所述仅为本发明的优选实例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡对本发明所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred examples of the present invention, and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and changes. Any modification, equivalent replacement, improvement, etc. made to the present invention shall be included within the protection scope of the present invention.
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