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CN110387331B - Ethanol blasting method, ethanol blasting device and ganoderma lucidum spore wall breaking equipment - Google Patents

Ethanol blasting method, ethanol blasting device and ganoderma lucidum spore wall breaking equipment Download PDF

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CN110387331B
CN110387331B CN201810364116.1A CN201810364116A CN110387331B CN 110387331 B CN110387331 B CN 110387331B CN 201810364116 A CN201810364116 A CN 201810364116A CN 110387331 B CN110387331 B CN 110387331B
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ethanol
pressure tank
blasting
vapor
ganoderma lucidum
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CN110387331A (en
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曹佐武
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Guangzhou Laifugao Biotechnology Co ltd
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    • C12M47/00Means for after-treatment of the produced biomass or of the fermentation or metabolic products, e.g. storage of biomass
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Abstract

The invention relates to an ethanol blasting method, an ethanol blasting device and ganoderma lucidum spore wall breaking equipment. The ethanol explosion method is a method for initiating explosion by heating ethanol to form high-pressure ethanol vapor. The ethanol blasting device comprises a high-pressure tank for blasting, wherein the high-pressure tank is provided with a heating device for heating ethanol in the high-pressure tank into ethanol vapor, and a large-caliber gate is also arranged on the high-pressure tank for releasing the ethanol vapor to trigger blasting. When the ethanol blasting device is used for breaking the wall of the ganoderma lucidum spores, a vacuum pump is used for pumping out gas in the high-pressure tank, then ethanol and articles to be blasted are added from a sample inlet, then the ethanol in the high-pressure tank is heated to generate ethanol vapor, and when the ethanol vapor pressure of the high-pressure tank reaches a set value, a gate of the high-pressure tank is opened to release the vapor to initiate blasting. The explosion is carried out by utilizing the characteristic of low boiling point of ethanol, so that the active substances of the ganoderma lucidum spores are reduced to be degraded at high temperature in the explosion process, and the active ingredients of the ganoderma lucidum spores are protected.

Description

Ethanol blasting method, ethanol blasting device and ganoderma lucidum spore wall breaking equipment
Technical Field
The invention relates to a blasting technology and a blasting device, in particular to a method and a device for blasting ethanol and ganoderma lucidum spore wall breaking equipment.
Background
In China, ganoderma lucidum has about 2000 years of history of medication, and has the effects of tonifying qi and soothing nerves, and relieving cough and asthma. Modern medicine research proves that it has certain curative effect on chronic trachitis, acute hepatitis, nephritis, coronary heart disease, neurasthenia, etc. In recent years, ganoderma lucidum has been paid attention to as a new anticancer drug.
Ganoderma spore is Ganoderma seed ejected when fruiting body of Ganoderma grows and matures. The research shows that the active ingredients of ganoderma lucidum are mainly concentrated in ganoderma lucidum spores. However, the traditional ganoderma lucidum stewing method cannot break the ganoderma lucidum spore shell because the outer parts of the ganoderma lucidum spore shells are wrapped with two layers of hard cell wall shells, so that the digestion and absorption of the human body on the contents are prevented. Only the wall-broken ganoderma lucidum spores can fully show the unique medicinal value and the nutritional value. Therefore, the wall breaking of the ganoderma lucidum spores becomes a key link in the ganoderma lucidum powder production process.
At present, the wall breaking process of the ganoderma lucidum spore powder has a plurality of biological methods, chemical methods, physical methods, mechanical methods and the like, but many methods have unsatisfactory wall breaking effects, and some advanced methods with good effects have complex procedures, expensive equipment and high energy consumption.
The air explosion is a familiar and simple blasting method and can also be used for breaking the spore wall of ganoderma lucidum. However, because steam explosion needs to occur at high temperature, some active ingredients in the steam explosion are easy to be denatured and inactivated, for example, the anticancer component ganoderma lucidum triterpenes in ganoderma lucidum are easy to be degraded at high temperature, and researches show that the stability of ganoderma lucidum triterpenes is inversely related to temperature and time. After 5h of preservation, at 50 ℃, the triterpene acid is degraded by about 4%; degradation at 75 ℃ of about 8%; and the degradation amount of the triterpenic acid reaches 15% at 100 ℃. Conventional steam explosion therefore has an adverse effect in the extraction and separation of biologically active substances.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention provides an ethanol blasting method, an ethanol blasting device and ganoderma lucidum spore wall breaking equipment. The boiling point of the ethanol is low, the ethanol can be gasified at 78.5 ℃, and the boiling point of the ethanol is lower under the vacuum condition, for example, the boiling point of the ethanol is as low as 42 ℃ under the condition of 0.02MPa, and the ethanol is also a good solvent, so that the ethanol can be used for extracting active ingredients in ganoderma lucidum spores. Therefore, by manufacturing an ethanol blasting environment, the blasting temperature can be reduced, so that the problem that the blasted objects are likely to be degraded at high temperature in the conventional blasting technology is solved.
The invention provides an ethanol blasting method, which comprises the steps of firstly adding an object to be blasted and ethanol into a blasting container, then heating the ethanol to form ethanol vapor in the blasting container, and opening a gate of the blasting container to initiate blasting when the ethanol vapor pressure reaches a set value.
In an embodiment of the invention, an ethanol explosion device is provided. The ethanol blasting device comprises a high-pressure tank for blasting, wherein the high-pressure tank is used for containing ethanol and objects to be blasted; the high-pressure tank is provided with a heating device for heating the ethanol in the high-pressure tank into ethanol vapor; the high-pressure tank is also provided with a large-caliber gate for releasing ethanol vapor to initiate explosion.
Preferably, the high-pressure tank is connected with a vacuum pump, and the vacuum pump is used for pumping the gas in the high-pressure tank to reach a vacuum state so as to reduce the boiling point of the ethanol.
Preferably, the high-pressure tank is provided with a sample inlet for adding ethanol and the articles to be blasted to the high-pressure tank.
Preferably, the high pressure tank is provided with a fluid heater which heats the ethanol in the high pressure tank to form vapor by delivering a flowing liquid at a set temperature.
Preferably, the caliber of the gate of the high-pressure tank is the same as the diameter of the high-pressure tank, the gate is provided with a cartridge button valve, and the cartridge button valve is used for rapidly opening the gate of the high-pressure tank in one step to release ethanol vapor.
Preferably, the gate of the high pressure tank is connected with a decompression bin, and the decompression bin is vacuumized first and is used for receiving vapor of the high pressure tank and the exploded articles and resolving the vapor pressure of the ethanol to negative pressure.
Preferably, the high pressure tank is provided with a pressure measuring device for measuring and displaying the air pressure value in the high pressure tank.
Preferably, the high pressure tank is provided with a temperature measuring device for measuring and displaying the temperature inside the high pressure tank.
The embodiment of the invention provides ganoderma lucidum spore wall breaking equipment, which comprises any one of the ethanol explosion devices.
Preferably, the ganoderma lucidum spore wall breaking equipment comprises a high-pressure tank, wherein the high-pressure tank is made of 304 # stainless steel, so that the problems of heavy metal pollution and the like in the high-temperature blasting process are avoided.
The invention provides an ethanol blasting method, which is a method for blasting by utilizing ethanol vapor. Because the boiling point of ethanol is lower than that of water, the ethanol can be heated to a lower temperature to generate steam, and when the ethanol steam reaches a certain pressure, the steam is released rapidly to initiate explosion. Thus, the blasting is carried out at a lower temperature, and the high-temperature degradation of bioactive substances in the blasting process is reduced, so that the effective components of the blasted objects are protected.
The invention provides an ethanol blasting device which comprises a high-pressure tank for blasting, wherein the high-pressure tank is used for containing ethanol and objects to be blasted; the high-pressure tank is provided with a heating device for heating the ethanol in the high-pressure tank into ethanol vapor; the high pressure tank also has a large caliber gate for releasing vapor to initiate a burst.
When the ethanol blasting device provided by the invention is used, a user firstly closes a gate of the high-pressure tank, uses a vacuum pump to pump out gas in the high-pressure tank, then closes the vacuum pump, opens a sample inlet, adds ethanol and an object to be blasted, then opens a fluid heater to convey liquid with set temperature to heat the ethanol in the high-pressure tank to generate ethanol vapor, and when the ethanol vapor pressure of the high-pressure tank reaches a set value, opens the gate of the high-pressure tank to release the vapor to initiate blasting.
The invention provides ganoderma lucidum spore wall breaking equipment which comprises the ethanol blasting device. According to the characteristics of ganoderma lucidum spores, the equipment adopts a water bath heater to heat the ethanol to generate ethanol vapor. When the ganoderma lucidum spore wall breaking equipment provided by the invention is used, a user firstly pumps out the gas in the high-pressure tank by using the vacuum pump, so that the high-pressure tank is in a negative pressure state. And closing a vacuum pump, adding ethanol and ganoderma lucidum spores to be exploded from a sample inlet, opening a water bath heater, gradually raising the temperature in the high-pressure tank through flowing hot water surrounding the high-pressure tank to generate ethanol vapor, closing the heater when the vapor pressure in the high-pressure tank reaches a set value, opening a valve of the high-pressure tank, releasing the high-pressure ethanol vapor to enter a vacuum decompression bin, dissolving the high-pressure vapor to negative pressure, and causing the explosion of ganoderma lucidum spores by obvious pressure difference. Compared with the conventional blasting device, the temperature in the high-pressure tank of the ethanol blasting is obviously reduced, so that the degradation of active ingredients in the ganoderma lucidum spores is greatly reduced, and the protection of the active ingredients of the ganoderma lucidum spores in the blasting process is facilitated.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the following description will briefly explain the drawings needed in the embodiments or the prior art description, and it is obvious that the drawings in the following description are some embodiments of the present invention, and other drawings can be obtained according to the drawings without inventive effort for a person skilled in the art.
Fig. 1 is a schematic diagram of a first structure of an ethanol explosion apparatus provided by the present invention;
fig. 2 is a schematic diagram of a second structure of the ethanol explosion apparatus provided by the present invention;
FIG. 3 is a schematic diagram of a third embodiment of a ganoderma lucidum spore wall breaking apparatus according to the present invention;
fig. 4 is a schematic diagram of a fourth structure of the ethanol explosion apparatus provided by the present invention;
fig. 5 is a schematic diagram of a fifth structure of the ethanol explosion apparatus provided by the present invention;
fig. 6 is a schematic structural diagram of a ganoderma lucidum spore wall breaking device provided by the invention.
Icon: 10 sample tanks, 110 sample feeding ports, 120 sample feeding ports, 20 high-pressure tanks, 210 snap-on valves, 220 vent pipes, 30 liquid storage bottles, 40 decompression bins, 50 vacuum pumps, 510 exhaust pipes, 60 inert gas tanks, 610 inert gas conveying pipes, 70 air pressure measuring probes, 80 temperature measuring probes and 90 heaters
Detailed Description
The following description of the embodiments of the present invention will be made apparent, and it is intended, in view of the accompanying drawings, to provide a clear and complete description of the embodiments of the present invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In the description of the present invention, it should be noted that terms such as "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," "outer," and the like are used merely for convenience in describing the present invention based on the orientation or positional relationship shown in the drawings, and do not denote or imply that the apparatus or element in question must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as limiting the present invention. Furthermore, the terms "first," "second," "third," and the like, as used herein, are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should be noted that, unless explicitly specified and limited otherwise, the terms "connected," "connected," and "coupled" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communication between two elements. The specific meaning of the above terms in the present invention will be understood in specific cases by those of ordinary skill in the art.
The invention provides an ethanol blasting method, an ethanol blasting device and ganoderma lucidum spore wall breaking equipment, and provides an implementation mode thereof.
The invention provides an ethanol blasting method, which is a blasting method by utilizing ethanol vapor. Firstly adding the object to be blasted and the ethanol into a blasting container, heating the ethanol in the blasting container by using flowing liquid with a set temperature to form ethanol vapor, and opening a gate to release high-pressure vapor for blasting when the ethanol vapor pressure in the blasting container reaches a set value.
(embodiment 1) the ethanol explosion device provided by the invention comprises a high-pressure tank 20 for explosion, as shown in fig. 1, wherein the high-pressure tank 20 comprises a sample inlet 120 and a gate 210, the sample inlet is used for placing ethanol and an object to be exploded into the high-pressure tank, and the gate is provided with a button valve for rapidly opening the gate to release ethanol vapor in the high-pressure tank. The high-pressure tank is connected to an exhaust pipe 510 connected to the vacuum pump 50 for exhausting the gas from the high-pressure tank. The high pressure tank is also provided with a fluid heater 90 for raising the temperature in the high pressure tank. Specifically, a fluid line 910 surrounds the outside of the high pressure tank and a fluid circulating within the fluid line heats the ethanol within the high pressure tank to form a vapor. The high pressure tank is also connected with a temperature probe 80 for measuring the temperature in the high pressure tank and an air pressure probe 70 for measuring the air pressure in the high pressure tank.
When the ethanol explosion device provided by the invention is used, a user can close the sample inlet 120 and the gate 210 of the high-pressure tank 20, pump the gas in the high-pressure tank 20 by using the vacuum pump 50, as shown in fig. 2, so that the gas pressure in the high-pressure tank 20 is lower than 0.1 atmosphere, and then close the vacuum pump, and add ethanol and an object to be exploded from the sample inlet 120, as shown in fig. 3. The fluid heater 90 is turned on and the ethanol in the high pressure tank is heated by the flowing liquid to form a vapor, as shown in fig. 4. When the air pressure in the high-pressure tank reaches a set value, the gate of the high-pressure tank is opened to burst.
(example 2) the apparatus for breaking wall of Ganoderma lucidum spores provided by the invention comprises the ethanol blasting device, according to the characteristics of Ganoderma lucidum spores, the apparatus is heated by a water bath heater, and ethanol vapor is generated by heating ethanol through a hot water pipe surrounding the outside of a high-pressure tank. The ethanol explosion device comprises a high-pressure tank 20 for explosion, as shown in fig. 1. In order to avoid the problems of heavy metal pollution and the like in the blasting process, the high-pressure tank is made of 304 stainless steel. The high pressure tank is connected to an exhaust pipe 510 connected to the vacuum pump 50 for exhausting the gas in the high pressure tank to generate ethanol vapor in a vacuum state. The high pressure tank 20 is provided with an air pressure measuring probe 70 for monitoring the air pressure value inside the high pressure tank 20. The gate 210 of the high pressure tank is connected with the decompression chamber 40, and the volume of the decompression chamber is 100 times that of the high pressure tank, so as to quickly dissolve the vapor pressure of the ethanol and increase the burst pressure difference.
When the ganoderma lucidum spore wall breaking device provided by the invention is used for breaking ganoderma lucidum spores, a user firstly closes the gate 210 of the high-pressure tank 20 and uses the vacuum pump 50 to pump out gas in the high-pressure tank 20, as shown in fig. 2. Specifically, the vacuum pump 50 pumps out the air in the high-pressure tank 20 so that the air pressure value in the high-pressure tank is reduced to below 0.01Mpa or below 0.1 atm. Ganoderma lucidum spores immersed in ethanol were added from the sample inlet 120, and the ratio of ethanol to ganoderma lucidum spores was 2:1 as shown in fig. 3. The water bath heater 90 is turned on, the water temperature is adjusted to gradually rise from 40 ℃ to 90 ℃, and the ethanol in the high-pressure tank is heated by flowing hot water to form vapor, as shown in fig. 4. The air pressure is gradually increased. Before blasting, the air in the decompression bin is pumped by a vacuum pump, so that the air pressure in the decompression bin is reduced to 0.05 atmosphere, and the temperature of the bin body is reduced to 4 ℃. When the air pressure in the high-pressure tank reaches 5 atmospheres, the valve of the high-pressure tank is opened in one step, the ethanol vapor in the high-pressure tank 20 is rapidly sprayed into the decompression bin 40, the air pressure is rapidly reduced, the high-pressure vapor is decomposed to negative pressure, a significant pressure difference is formed, and therefore the explosion of ganoderma lucidum spores is initiated. As shown in fig. 6.
In summary, the ethanol blasting device provided by the invention comprises a high-pressure tank 20 for blasting, wherein the high-pressure tank 20 comprises a sample inlet 120 and a cartridge button valve 210, the sample inlet is used for placing ethanol and articles to be blasted into the high-pressure tank, and the cartridge button valve is used for rapidly releasing ethanol vapor in the high-pressure tank. The high-pressure tank is connected with an exhaust pipe, the exhaust pipe is connected with a vacuum pump and used for exhausting gas in the high-pressure tank, the high-pressure tank further comprises a fluid heater 90, the heater is used for raising the temperature in the high-pressure tank, and ethanol vapor is generated in the high-pressure tank; the high-pressure tank is also connected with a temperature probe 80 and an air pressure probe 70, the temperature probe is used for measuring the temperature in the high-pressure tank, and the air pressure probe is used for measuring the air pressure in the high-pressure tank.
When the ethanol explosion device provided by the invention is used, a user pumps out the gas in the high-pressure tank 20 by using the vacuum pump 50, so that the gas pressure in the high-pressure tank 20 is lower than 0.1 atmosphere, then the vacuum pump is closed, ethanol and a sample to be exploded are added from the sample inlet 120, the fluid heater is opened, ethanol vapor is generated in the high-pressure tank, and when the gas pressure in the high-pressure tank reaches a set value, the high-pressure tank gate 210 is opened to explode the object to be exploded.
The invention provides ganoderma lucidum spore wall breaking equipment which comprises the ethanol blasting device. Specifically, the equipment adopts a water bath heater, a hot water pipe is arranged outside the high-pressure tank to surround the high-pressure tank, and circulating hot water is arranged in the hot water pipe to heat the ethanol in the high-pressure tank to form vapor. Compared with the conventional blasting method, the ethanol blasting device greatly reduces the blasting temperature in the high-pressure tank 20, and can reduce degradation and inactivation of the active ingredients of the ganoderma lucidum spores after blasting.
And finally, it should be explained that: the above embodiments are only for illustrating the technical solution of the present invention, and not for limiting the same; although the invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical scheme described in the foregoing embodiments can be modified or some or all of the technical features thereof can be replaced by equivalents; such modifications and substitutions do not depart from the spirit of the invention.

Claims (6)

1. An ethanol blasting method is characterized by comprising the following steps of: firstly pumping out the gas in the blasting container by using a vacuum pump to reduce the air pressure in the high-pressure tank to below 0.01Mpa, then adding the object to be blasted and the ethanol into the blasting container together, heating to form ethanol vapor, and opening a gate of the blasting container to initiate blasting after reaching 5 atmospheres.
2. The ethanol blasting device is characterized by comprising a high-pressure tank for blasting, wherein the high-pressure tank is used for containing ethanol and objects to be blasted; the high-pressure tank is connected with an exhaust pipe, and the exhaust pipe is connected with a vacuum pump and used for pumping out gas in the high-pressure tank so as to form ethanol vapor in a vacuum state; the high-pressure tank is provided with a fluid heater, and the fluid heater heats ethanol in the high-pressure tank to form vapor by conveying flowing liquid with set temperature; the high pressure tank also has a large caliber gate for releasing vapor to initiate a burst.
3. An ethanol blasting apparatus according to claim 2, wherein the high pressure tank is provided with a sample inlet for adding ethanol and the object to be blasted to the high pressure tank.
4. An ethanol bursting device according to claim 2, wherein the gate of the high pressure tank is provided with a cartridge valve for one step rapid opening of the gate of the high pressure tank to release ethanol vapour.
5. An ethanol blasting apparatus according to claim 2, wherein the gate of the high pressure tank is connected to a decompression chamber which is first evacuated to receive ethanol vapour from the high pressure tank and to dissipate the high pressure of the vapour.
6. A ganoderma lucidum spore wall breaking device, characterized in that the ganoderma lucidum spore wall breaking device comprises the ethanol blasting device according to any one of claims 2 to 5.
CN201810364116.1A 2018-04-23 2018-04-23 Ethanol blasting method, ethanol blasting device and ganoderma lucidum spore wall breaking equipment Active CN110387331B (en)

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CN112680275B (en) * 2021-03-22 2021-06-25 南昌之禾生物工程有限公司 Supercritical extraction process of ganoderma lucidum spore oil with high extraction rate

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