CN110357558A - A kind of ceramic tile bond and preparation method thereof - Google Patents
A kind of ceramic tile bond and preparation method thereof Download PDFInfo
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- CN110357558A CN110357558A CN201910649726.0A CN201910649726A CN110357558A CN 110357558 A CN110357558 A CN 110357558A CN 201910649726 A CN201910649726 A CN 201910649726A CN 110357558 A CN110357558 A CN 110357558A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
- C04B28/065—Calcium aluminosulfate cements, e.g. cements hydrating into ettringite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
- C04B28/16—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing anhydrite, e.g. Keene's cement
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00637—Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/40—Porous or lightweight materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Finishing Walls (AREA)
Abstract
The invention discloses a kind of ceramic tile bonds and preparation method thereof, which includes the following raw material: 80~120 parts of portland cement, 0~15 part of land plaster, 0~15 part of sulphate aluminium cement, 50~150 parts of quartz sand, 8~25 parts of wollastonite in powder, 0~3 part of calcium carbonate superfine powder, 2~7 parts of redispersable latex powder, 0.2~0.6 part of cellulose ether, 0.05~0.5 part of water-reducing agent, 0.03~0.06 part of defoaming agent, 1~4 part of sodium bentonite, 4.5~20 parts of glass bead, 3~15 parts of swelling perlite powder.In the above manner, ceramic tile bond adhesion strength of the present invention is high, stability is strong, and heat resistance and resistance to ag(e)ing are good, and durability is strong, and have the function of lightweight, heat preservation energy-saving.
Description
Technical field
The present invention relates to building material technical fields, and in particular to a kind of ceramic tile bond and preparation method thereof.
Background technique
Ceramic tile bond is a kind of high-quality environment protective type polyalcohol cement basis compoiste adhering material, is mainly used for pasting porcelain
The ornament materials such as brick, face brick, floor tile.Traditional ceramic tile bond is generally based on cement and quartz sand and polymer adhesive
Material is equipped with multiple additives and forms through mixing machine stirring is mixed, also known as glue for tile；Its cohesive force is mainly embedded in ceramic tile hole by mortar
The chemically and physically cohesive force composition that the mechanical snap power and polymeric compositions that gap is formed are formed at bonding interface, compared to common
Cement mortar binder, glue for tile have adhesion strength is higher, setting rate faster, application property better characteristics, it is generally applicable
In the facing decoration places of the buildings such as inside and outside metope, ground, bathroom, kitchen, beautiful luxurious cleaning.But major part ceramic tile is viscous at present
Agent is tied since the stability of formula is not strong, adhesion strength is still to be improved；Some manufacturers are in order to reach ceramic tile bond
To higher adhesion strength, polymer adhesive doping is big, although in construction, adhesion strength is higher in this way, polymer latex
Stick is met water and can be swollen, and intensity reduces rapidly, and polymer adhesive category organic matter, and resistance to ag(e)ing is poor, not durable；In addition, existing
There are many some general quartz sand volumes of ceramic tile bond, and weight of binder is big, and manual operation is hard, and does not have heat preservation energy-saving function
Energy.
Summary of the invention
In order to solve the above technical problem, the present invention provides a kind of ceramic tile bonds and preparation method thereof.
The technical scheme adopted by the invention is that: a kind of ceramic tile bond, the raw material including following parts by weight: silicate cement
80~120 parts of mud, 0~15 part of land plaster, 0~15 part of sulphate aluminium cement, 50~150 parts of quartz sand, wollastonite in powder 8~25
Part, 0~3 part of calcium carbonate superfine powder, 2~7 parts of redispersable latex powder, 0.2~0.6 part of cellulose ether, water-reducing agent 0.05~0.5
Part, 0.03~0.06 part of defoaming agent, 1~4 part of sodium bentonite, 4.5~20 parts of glass bead, 3~15 parts of swelling perlite powder；
The partial size of the calcium carbonate superfine powder is 0.02~0.1 μm.
In the weight proportion of the above raw material, the weight of every parts by weight is unified, can be 1g, 2g, 5g, 10g, 50g, 100g etc..
Preferably, the ceramic tile bond includes the raw material of following parts by weight: 90~100 parts of portland cement, land plaster 3
~6 parts, 8~12 parts of sulphate aluminium cement, 80~120 parts of quartz sand, 15~20 parts of wollastonite in powder, 1~3 part of calcium carbonate superfine powder,
3~6 parts of redispersable latex powder, 0.3~0.5 part of cellulose ether, 0.1~0.4 part of water-reducing agent, 0.04~0.05 part of defoaming agent,
2~4 parts of sodium bentonite, 10~15 parts of glass bead, 3~10 parts of swelling perlite powder.
It is further preferred that the ceramic tile bond includes the raw material of following parts by weight: 100 parts of portland cement, gypsum
6 parts of powder, 8 parts of sulphate aluminium cement, 100 parts of quartz sand, 20 parts of wollastonite in powder, 3 parts of calcium carbonate superfine powder, redispersable latex powder 5
Part, 0.5 part of cellulose ether, 0.3 part of water-reducing agent, 0.05 part of defoaming agent, 4 parts of sodium bentonite, 10 parts of glass bead, expanded pearlite
5 parts of rock powder.
Preferably, the water-reducing agent is selected from least one of polycarboxylate water-reducer, melamine water reducing agent.
When water-reducing agent can be mixed by improving ceramic tile bond use process the effects of electrostatic repulsion and steric hindrance with water
Dispersibility between cement granules improves the mobility of cement matrix, to greatly reduce water consumption, increases the closely knit of binder
Degree.In addition, showing that the performance of composite water-reducing agent is substantially better than single type water-reducing agent through test.Preferably, the water-reducing agent is
The combination of polycarboxylate water-reducer and melamine water reducing agent significantly improves space steric effect by the way that the two is compound, to cement
The enhancement effect of sill, which is greater than, solely uses any one of them high efficiency water reducing agent.It is further preferred that the polycarboxylic acids subtracts
The mass ratio of aqua and melamine water reducing agent is 1:1.
Preferably, the partial size of the quartz sand is 120~380 μm (i.e. 40~120 mesh)；The partial size of the glass bead is
180~380 μm (i.e. 40~80 mesh)；The partial size of the swelling perlite powder is 120~250 μm (i.e. 60~120 mesh).
Preferably, the ceramic tile bond further includes the raw material of following parts by weight: 1~12 part of floating bead.
Floating bead is in powder coal ash glass-microballons, and density is less than 1g/cm3Microballon, thermal coefficient is lower, high temperature resistant, hardness
With isostatic pressing strength height.The floating bead that a small amount of ratio is mixed in the raw material of ceramic tile bond, not only plays the role of light thermal-insulation, but also can be with
The intensity for enhancing thermal insulation material, makes material reach the standard of A grades of fireproof and heat-insulating materials.It is further preferred that the grain of the floating bead
Diameter is 150~250 μm, i.e. 60~100 mesh.
The present invention also provides the preparation methods of more than one ceramic tile bonds, comprising the following steps: matches by the above weight
Than taking each raw material；Then by portland cement, land plaster, sulphate aluminium cement, wollastonite in powder, calcium carbonate superfine powder, redispersible
Latex powder, cellulose ether, water-reducing agent, defoaming agent and sodium bentonite are mixed and stirred for uniformly；Add quartz sand, glass bead
And swelling perlite powder, it stirs evenly.
The above ceramic tile bond generally mixes when in use with suitable water again and stirs evenly use, and the usage amount of water is generally 60
~120 parts by weight, the weight of every parts by weight water and the weight of the every parts by weight of each raw material of ceramic tile bond are unified.
In the raw material of ceramic tile bond of the present invention, portland cement has fast solidifying, intensity height, frost resistance good, resistance to
Mill property it is good, be applied to ceramic tile bond can accelerated material hardening, improve mechanical strength.Suitable land plaster and portland cement are ripe
Expect that mineral reaction produces single sulfur type hydrated calcium aluminate sulfate (AFm) and calcium trisulphoaluminate hydrate (AFt), and then water can be improved
The early strength and the comprehensive performance after improvement hardening of cement of cement-based material.And suitable sulphate aluminium cement and portland cement
Compounding can play the role of microdilatancy, increase the compactness of cement base ability material.It is preferred that using portland cement, sulphur aluminic acid
Salt cement and land plaster combination compounding, portland cement-sulphate aluminium cement-gypsum three-component compound system gel rubber material has early
Play the feature that intensity is high, adhesive property is good.
Wollastonite is a kind of natural chain metasilicate mineral, structural formula Ca3(Si3O9)；In wollastonite crystalline texture
In, SiO4Skeletal chain and CaO6The compound single-stranded basic unit as wollastonite crystalline texture that octahedra column is formed, it is this special
Crystal structure determines its property, when being ground into fine particle, can still keep acicular morphology.Due to this uniqueness
High length-diameter ratio powder fibre property, wollastonite in powder can be used to improve the hardness of material, bending strength, hits resistance, thermostabilization
Property and corrosion resistance.Wollastonite in powder is added in the raw material of ceramic tile bond, the mechanical strength of binder and heat-resisting, resistance to can be improved
Corrosivity.
Calcium carbonate superfine powder refers to calcium carbonate of the primary partical partial size between 0.02~0.1 μm, is a kind of most cheap receive
Rice material, special quantum size effect, small-size effect, skin effect, make itself and conventional powder material phase possessed by it
Than toughened and reinforced property, dispersibility, thixotropy and in terms of all show apparent advantage.It is added as raw material
It in ceramic tile bond, can penetrate into the micro-pore that portland cement particle can not penetrate into, enhance the compactness of binder, glue
Knot property and thermal stability.
Sodium bentonite belongs to natural inorganic mineral material, and the sodium ion between microstructure synusia can adsorption moisture
Son, and it is full of hydrone between layer and layer, these synusia are separated, swelling is generated.Bentonite surface by aquation,
After a certain amount of hydrone of Cation adsorption, bentonite becomes gel-like state, can effectively prevent hydrone by when this layer
Gel can form excellent waterproof layer, durability is made to reach a century or more in the case where two sides is by uniform limitation.
Glass bead have the characteristics that it is light, heat preservation, it is heat-insulated it is good, electrical insulation capability is good, wear-resisting, corrosion-resistant, be thermal insulation separation
The good material of heat, but vitreous degree is inadequate, sphericity is poor, closed pore is few, water absorption rate is higher mostly.And vitreous degree is larger, sphericity
Then density is larger for good microballon, is not able to satisfy the requirement of thermal insulation mortar dry density, this disadvantage becomes vitrified microsphere insulating material
Weakness.Expanded perlite has relatively large partial size and wider grain composition range, utilizes expanded perlite and vitreous
Microballon progress is compound, can form more reasonable grain composition, while can reducing ceramic tile bond weight, realizes insulation
The optimization of material comprehensive performance.
The method have the benefit that: the present invention provides a kind of ceramic tile bond and preparation method thereof, and the ceramic tile is viscous
Knot agent can reduce the usage amount of polymer latex binder and quartz sand by each raw material coordinated, while guarantee tile bonding
Agent has high bond strength, and stability is strong, and heat resistance and resistance to ag(e)ing are good, and durability is strong, has lightweight, heat preservation energy-saving function
Energy.
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
Embodiment 1
A kind of ceramic tile bond, the raw material including following parts by weight: 100 parts of portland cement, 2 parts of anhydrous plaster powder, sulphur
(partial size is 0.02~0.1 μ for 3 parts of aluminate cement, 150 parts of quartz sand (40~120 mesh), 10 parts of wollastonite in powder, calcium carbonate superfine powder
M) 1 part, 2 parts of redispersable latex powder, 0.3 part of cellulose ether, 0.05 part of polycarboxylate water-reducer, melamine water reducing agent 0.05
Part, 0.03 part of defoaming agent, 2 parts of sodium bentonite, 8 parts of glass bead (40~80 mesh), swelling perlite powder (60~120 mesh) 6
Part, 2 parts of floating bead (60~100 mesh)；Every parts by weight are based on 1g.
The preparation method of the above ceramic tile bond the following steps are included:
1) by portland cement, anhydrous plaster powder, sulphate aluminium cement, wollastonite in powder, calcium carbonate superfine powder, redispersible cream
Rubber powder, cellulose ether, polycarboxylate water-reducer, melamine water reducing agent, defoaming agent and sodium bentonite mix in proportion, and sufficiently
It stirs evenly spare；
2) quartz sand is proportionally added into the resulting stirring material of step 1), continues to stir evenly；Then it is proportionally added into
Glass bead, swelling perlite powder and floating bead, stir, and obtain ceramic tile bond.
The water of 70 parts by weight (every parts by weight are based on 1g) is taken to mix when use with ceramic tile bond obtained by the present embodiment
And it stirs.
Embodiment 2
A kind of ceramic tile bond, the raw material including following parts by weight: 100 parts of portland cement, 6 parts of anhydrous plaster powder, sulphur
(partial size is 0.02~0.1 μ for 8 parts of aluminate cement, 100 parts of quartz sand (40~120 mesh), 20 parts of wollastonite in powder, calcium carbonate superfine powder
M) 3 parts, 5 parts of redispersable latex powder, 0.5 part of cellulose ether, 0.15 part of polycarboxylate water-reducer, melamine water reducing agent 0.15
Part, 0.05 part of defoaming agent, 4 parts of sodium bentonite, 15 parts of glass bead (40~80 mesh), swelling perlite powder (60~120 mesh)
10 parts, 5 parts of floating bead (60~100 mesh)；Every parts by weight are based on 1g.
The preparation method of the preparation method of the above ceramic tile bond is identical as the preparation method of 1 ceramic tile bond of embodiment.
The water of 100 parts by weight (every parts by weight are based on 1g) is taken to mix when use with ceramic tile bond obtained by the present embodiment
And it stirs.
Embodiment 3
A kind of ceramic tile bond, the raw material including following parts by weight: 100 parts of portland cement, 12 parts of anhydrous plaster powder, sulphur
(partial size is 0.02~0.1 μ for 12 parts of aluminate cement, 50 parts of quartz sand (40~120 mesh), 15 parts of wollastonite in powder, calcium carbonate superfine powder
M) 2 parts, 3 parts of redispersable latex powder, 0.4 part of cellulose ether, 0.1 part of polycarboxylate water-reducer, 0.1 part of melamine water reducing agent,
0.04 part of defoaming agent, 4 parts of sodium bentonite, 18 parts of glass bead (40~80 mesh), swelling perlite powder (60~120 mesh) 12
Part, 6 parts of floating bead (60~100 mesh)；Every parts by weight are based on 1g.
The preparation method of the preparation method of the above ceramic tile bond is identical as the preparation method of 1 ceramic tile bond of embodiment.
The water of 112 parts by weight (every parts by weight are based on 1g) is taken to mix when use with ceramic tile bond obtained by the present embodiment
And it stirs.
Embodiment 4
The present embodiment and embodiment 3 the difference is that: include 15 parts by weight of anhydrous plaster powder in raw material, not sulfur-bearing aluminium
Acid salt cement；Other raw materials, preparation method and application method are same as Example 3.
Embodiment 5
The present embodiment and embodiment 3 the difference is that: include 15 parts by weight of sulphate aluminium cement in raw material, be free of nothing
Water land plaster, other raw materials, preparation method and application method are same as Example 3.
Embodiment 6
The present embodiment and embodiment 3 the difference is that: anhydrous plaster powder and sulphate aluminium cement are free of in raw material,
His raw material, preparation method and application method are same as Example 3.
Embodiment 7
The present embodiment and embodiment 3 the difference is that: include 0.5 parts by weight of polycarboxylate water-reducer in raw material, be free of
Melamine water reducing agent, other raw materials, preparation method and application method are same as Example 3.
Embodiment 8
The present embodiment and embodiment 3 the difference is that: include 0.5 parts by weight of melamine water reducing agent in raw material, no
Containing polycarboxylate water-reducer, other raw materials, preparation method and application method are same as Example 3.
Embodiment 9
The present embodiment and embodiment 3 the difference is that: glass bead equivalent replaces floating bead in raw material, other raw materials,
Preparation method and application method are same as Example 3.
Comparative example 1
This comparative example and embodiment 3 the difference is that: quartz sand equivalent replaces glass bead, expanded pearlite in raw material
Rock powder and floating bead, other raw materials, preparation method and application method are same as Example 3.
Comparative example 2
This comparative example is the purchase preferable ceramic tile adhesive of sales volume on the market.
Performance detection
The bulk density thermal coefficient and bonding of ceramic tile bond obtained by above embodiments 1~9 and comparative example 1,2 are measured respectively
Intensity.Adhesion strength test includes the strength test of stretch-bonded original, immersion post-tensioning adhesion strength is tested, heat ageing post-tensioning is glued
Knotting strength test and the test of Frozen-thawed cycled post-tensioning adhesion strength.Referring to national regulation " Ceramic Tiles adhesive " JC/T 547-
2017, the specific test method is as follows:
(1) stretch-bonded original strength test
It ceramic tile bond obtained by each embodiment and comparative example is respectively adopted is mixed by defined application method with water and stirred evenly,
With identical bonding mode, Ceramic Tiles of the same race are bonded on concrete slab of the same race, environment temperature is 23 DEG C, relative humidity is
After conserving 27d under 50% experimental condition, drawing connector is sticked in Ceramic Tiles with suitable high-intensity viscose binder, continues to place
After for 24 hours, tensile bond strength is tested.
(2) the tensile bond strength test after soaking
It ceramic tile bond obtained by each embodiment and comparative example is respectively adopted is mixed by defined application method with water and stirred evenly,
With identical bonding mode, Ceramic Tiles of the same race are bonded on concrete slab of the same race, environment temperature is 23 DEG C, relative humidity is
After conserving 7d under 50% experimental condition, 20d is conserved in 20 DEG C of water.Sample is taken out from water, is dried with a cloth, with suitable
Drawing connector is sticked in Ceramic Tiles by high-intensity viscose binder, after 7h into the water sample, takes out sample testing after 17h from water
Tensile bond strength.
(3) the tensile bond strength test after heat ageing
It ceramic tile bond obtained by each embodiment and comparative example is respectively adopted is mixed by defined application method with water and stirred evenly,
With identical bonding mode, Ceramic Tiles of the same race are bonded on concrete slab of the same race, environment temperature is 23 DEG C, relative humidity is
After conserving 14d under 50% experimental condition, sample is put into 14d in 70 DEG C of convection ovens.It is taken out from baking oven, with suitable height
Drawing connector is sticked in Ceramic Tiles by intensity adhesive.Continue sample environment temperature is 23 DEG C, relative humidity is 50%
After conserving for 24 hours under experimental condition, tensile bond strength is measured.
(4) the tensile bond strength test after Frozen-thawed cycled
It ceramic tile bond obtained by each embodiment and comparative example is respectively adopted is mixed by defined application method with water and stirred evenly,
With identical bonding mode, Ceramic Tiles of the same race are bonded on concrete slab of the same race, environment temperature is 23 DEG C, relative humidity is
7d is conserved under 50% experimental condition, then conserves 21d in 20 DEG C of water.Sample is taken out from water, carries out freezing-thawing test.
Each Frozen-thawed cycled are as follows:
A, sample is taken out from water, -15 DEG C is down in 2h；
B, sample 2h at -15 DEG C is kept；
C, sample is immersed in 20 DEG C of water, is warming up to 15 DEG C, keeps temperature 2h.
Repeat 25 circulations.Last time recycle after take out sample, environment temperature be 23 DEG C, relative humidity 50%
Experimental condition under conserve, drawing connector is sticked in Ceramic Tiles with suitable high-intensity viscose binder.Continue sample in environment
After conserving for 24 hours under the experimental condition that temperature is 23 DEG C, relative humidity is 50%, tensile bond strength is measured.
The performance of ceramic tile bond obtained by Examples 1 to 9 and comparative example 1,2 is detected respectively, acquired results are such as
Shown in the following table 1.
The performance test results of ceramic tile bond obtained by 1 Examples 1 to 9 of table and comparative example 1,2
By upper table 1 it is found that the application ceramic tile bond has high bond strength, and stability is strong, heat resistance and ageing-resistant
Property is good, and durability is strong, while having the function of lightweight, heat preservation energy-saving.
Although specifically showing and describing the present invention in conjunction with preferred embodiment, those skilled in the art should be bright
It is white, it is not departing from the spirit and scope of the present invention defined by described claims, it in the form and details can be right
The present invention makes a variety of changes, and is protection scope of the present invention.
Claims (9)
1. a kind of ceramic tile bond, which is characterized in that the raw material including following parts by weight: 80~120 parts of portland cement, gypsum
0~15 part of powder, 0~15 part of sulphate aluminium cement, 50~150 parts of quartz sand, 8~25 parts of wollastonite in powder, calcium carbonate superfine powder 0~3
Part, 2~7 parts of redispersable latex powder, 0.2~0.6 part of cellulose ether, 0.05~0.5 part of water-reducing agent, defoaming agent 0.03~0.06
Part, 1~4 part of sodium bentonite, 4.5~20 parts of glass bead, 3~15 parts of swelling perlite powder；The grain of the calcium carbonate superfine powder
Diameter is 0.02~0.1 μm.
2. ceramic tile bond according to claim 1, which is characterized in that the raw material including following parts by weight: silicate cement
90~100 parts of mud, 3~6 parts of land plaster, 8~12 parts of sulphate aluminium cement, 80~120 parts of quartz sand, wollastonite in powder 15~20
Part, 1~3 part of calcium carbonate superfine powder, 3~6 parts of redispersable latex powder, 0.3~0.5 part of cellulose ether, 0.1~0.4 part of water-reducing agent,
0.04~0.05 part of defoaming agent, 2~4 parts of sodium bentonite, 10~15 parts of glass bead, 3~10 parts of swelling perlite powder.
3. ceramic tile bond according to claim 2, which is characterized in that the raw material including following parts by weight: silicate cement
100 parts of mud, 6 parts of land plaster, 8 parts of sulphate aluminium cement, 100 parts of quartz sand, 20 parts of wollastonite in powder, 3 parts of calcium carbonate superfine powder, can be again
5 parts of dispersed latex powder, 0.5 part of cellulose ether, 0.3 part of water-reducing agent, 0.05 part of defoaming agent, 4 parts of sodium bentonite, glass bead 10
Part, 5 parts of swelling perlite powder.
4. ceramic tile bond according to any one of claim 1-3, which is characterized in that the water-reducing agent is selected from polycarboxylic acids
At least one of water-reducing agent, melamine water reducing agent.
5. ceramic tile bond according to claim 4, which is characterized in that the water-reducing agent is polycarboxylate water-reducer and trimerization
The mass ratio of the combination of cyanamide water-reducing agent, the polycarboxylate water-reducer and melamine water reducing agent is 1:1.
6. ceramic tile bond according to any one of claim 1-3, which is characterized in that the partial size of the quartz sand is
120~380 μm；The partial size of the glass bead is 180~380 μm；The partial size of the swelling perlite powder is 120~250 μm.
7. ceramic tile bond according to any one of claim 1-3, which is characterized in that further include the original of following parts by weight
Material: 1~12 part of floating bead.
8. ceramic tile bond according to claim 7, which is characterized in that the partial size of the floating bead is 150~250 μm.
9. the preparation method of ceramic tile bond of any of claims 1-8, which comprises the following steps:
Each raw material is taken by weight ratio；Then by portland cement, land plaster, sulphate aluminium cement, wollastonite in powder, calcium carbonate superfine powder,
Redispersable latex powder, cellulose ether, water-reducing agent, defoaming agent and sodium bentonite are mixed and stirred for uniformly；Add quartz sand,
Glass bead and swelling perlite powder, stir evenly.
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| CN112794691A (en) * | 2021-01-11 | 2021-05-14 | 深圳市奇信集团股份有限公司 | Fair-faced concrete panel and preparation method thereof |
| CN113550490A (en) * | 2020-04-24 | 2021-10-26 | 海安南京大学高新技术研究院 | Prefabricated integral structure wallboard of soft porcelain heat preservation PC |
| CN113896485A (en) * | 2021-11-26 | 2022-01-07 | 佛山市卓仕高新型材料有限公司 | High-strength tile glue and preparation method thereof |
| CN114956724A (en) * | 2022-05-17 | 2022-08-30 | 美巢集团股份公司 | Ceramic tile glue and preparation method thereof |
| CN116081980A (en) * | 2022-11-09 | 2023-05-09 | 华润水泥技术研发有限公司 | High-performance concrete decorative material and forming method thereof |
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Application publication date: 20191022 |