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CN110297289B - Indium phosphide-based optical mixer and preparation method thereof - Google Patents

Indium phosphide-based optical mixer and preparation method thereof Download PDF

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CN110297289B
CN110297289B CN201910315599.0A CN201910315599A CN110297289B CN 110297289 B CN110297289 B CN 110297289B CN 201910315599 A CN201910315599 A CN 201910315599A CN 110297289 B CN110297289 B CN 110297289B
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陆子晴
韩勤
叶焓
王帅
肖峰
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    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/10Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type
    • G02B6/12Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type of the integrated circuit kind
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    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/10Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type
    • G02B6/12Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type of the integrated circuit kind
    • G02B6/126Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type of the integrated circuit kind using polarisation effects
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/10Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type
    • G02B6/12Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type of the integrated circuit kind
    • G02B6/13Integrated optical circuits characterised by the manufacturing method
    • G02B6/136Integrated optical circuits characterised by the manufacturing method by etching
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    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/10Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type
    • G02B6/12Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type of the integrated circuit kind
    • G02B6/13Integrated optical circuits characterised by the manufacturing method
    • G02B6/138Integrated optical circuits characterised by the manufacturing method by using polymerisation
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
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Abstract

本发明公开了一种磷化铟基光学混频器及其制备方法,该混频器包括一外延片器件层,形成于一磷化铟衬底之上,用于实现混频;一二氧化硅上包层,形成于所述外延片器件层之上,用于保护外延片器件层,并提高外延片器件层稳定性;以及一金属薄膜,形成于所述二氧化硅上包层之上,用于控制偏振。其中外延片器件层包括由直波导依次连接的模斑转换器、1×2MMI、第一偏振转换器、第二偏振转换器、2×2MMI、第三偏振转换器、波导型偏振器以及4×4MMI。本发明提出的磷化铟基光学混频器具有微型化、低偏振色散、高带宽、高响应度、制备工艺与CMOS工艺兼容、以及易于制备和集成的综合性能。

Figure 201910315599

The invention discloses an indium phosphide-based optical mixer and a preparation method thereof. The mixer includes an epitaxial wafer device layer formed on an indium phosphide substrate for realizing frequency mixing; an oxide a silicon upper cladding layer formed on the epitaxial wafer device layer for protecting the epitaxial wafer device layer and improving the stability of the epitaxial wafer device layer; and a metal thin film formed on the silicon dioxide upper cladding layer , which controls the polarization. The epitaxial wafer device layer includes a mode spot converter, a 1×2MMI, a first polarization converter, a second polarization converter, a 2×2MMI, a third polarization converter, a waveguide-type polarizer, and a 4×2 MMI sequentially connected by a straight waveguide. 4MMI. The indium phosphide-based optical mixer proposed by the invention has the comprehensive performance of miniaturization, low polarization dispersion, high bandwidth, high responsivity, the preparation process is compatible with the CMOS process, and easy to prepare and integrate.

Figure 201910315599

Description

一种磷化铟基光学混频器及其制备方法Indium phosphide-based optical mixer and preparation method thereof

技术领域technical field

本发明属于相干光通讯领域,尤其涉及一种磷化铟基光学混频器及其制备方法。The invention belongs to the field of coherent optical communication, in particular to an indium phosphide-based optical mixer and a preparation method thereof.

背景技术Background technique

面对日益上涨的通信速率和带宽需求,人们逐渐把关注点放在了相干光通信上。相干光通信是在接收端使用一个本振光源对接收信号进行相干解调的一种新型通讯系统。相干光通信系统的发展大大提高了传统光学通信系统的传输速率、传输容量和传输距离,其发展的关键在于相干光接收机的应用。90°光学混频器是相干光接收机中必不可少的核心器件,对于整个相干光接收机的性能起决定性因素。光学混频器通过将输入光与满足相位匹配、偏振匹配的本振光进行光学混频在探测器端得到携带幅度、相位信息的差频信号。输出的差频信号借助数字信号处理模块最终提取出传输信息。其中光学混频器的精度决定了整个相干接收机的灵敏度。In the face of increasing communication speed and bandwidth requirements, people gradually focus on coherent optical communication. Coherent optical communication is a new type of communication system that uses a local oscillator light source to coherently demodulate the received signal at the receiving end. The development of coherent optical communication systems has greatly improved the transmission rate, transmission capacity and transmission distance of traditional optical communication systems. The key to its development lies in the application of coherent optical receivers. The 90° optical mixer is an essential core device in the coherent optical receiver, and it is a decisive factor for the performance of the entire coherent optical receiver. The optical mixer obtains a difference frequency signal carrying amplitude and phase information at the detector end by optically mixing the input light with the local oscillator light that satisfies the phase matching and polarization matching. The output difference frequency signal finally extracts the transmission information by means of the digital signal processing module. The precision of the optical mixer determines the sensitivity of the entire coherent receiver.

评价90°混频器性能优良的三个重要指标是传输损耗,共模抑制比和相位误差。其中,相位误差是三者中最为关键的一项参数。目前主流的光学混频器是基于4×4多模干涉耦合器(multimode interference,MMI)完成混频的,也就意味着其输入光必须为单一偏振模式,并且目前尚且没有一款激光光源是单偏振模式输出。也就是说,目前的所有光学混频器都存在着或多或少的偏振模式色散,从而严重影响混频器的相位误差,最终导致器件性能下降,为后续的信号补偿模块增加了设计难度。Three important indicators to evaluate the excellent performance of a 90° mixer are transmission loss, common mode rejection ratio and phase error. Among them, the phase error is the most critical parameter among the three. The current mainstream optical mixers are based on 4 × 4 multimode interference couplers (multimode interference, MMI) to complete the mixing, which means that the input light must be in a single polarization mode, and there is currently no laser light source that is Single polarization mode output. That is to say, all current optical mixers have more or less polarization mode dispersion, which seriously affects the phase error of the mixer, and eventually leads to the degradation of device performance, which increases the design difficulty for subsequent signal compensation modules.

目前,在相干光通讯领域中,要想对信号光在横向电场(Transverse Electric,TE)/横向磁场(Transverse Magnetic,TM)模式分别混频,目前常用的办法就是借助独立的光学仪器(光纤偏振分束器)分离输入信号光中的两种本征偏振态(EigenstatePolarization,ESOP),并需要分别优化设计对应连接解调不同模式的4×4MMI实现混频,增加了器件设计与工艺复杂程度、器件尺寸庞大、成本高。除此之外,受CMOS工艺加工精度的局限,无论何种偏振分束器都无法将两种本征偏振态完全分离,还进一步增加了相干光通信中混频器的偏振色散,降低混频器精度。At present, in the field of coherent optical communication, in order to separately mix the signal light in the Transverse Electric (TE)/Transverse Magnetic (TM) mode, the commonly used method is to use an independent optical instrument (fiber polarization Beam splitter) separates the two eigenstate polarization states (ESOP) in the input signal light, and needs to optimize the design of 4 × 4 MMIs corresponding to different modes of demodulation to realize frequency mixing, which increases the complexity of device design and process, The device size is large and the cost is high. In addition, due to the limitation of CMOS process processing accuracy, no matter what kind of polarization beam splitter can not completely separate the two intrinsic polarization states, it further increases the polarization dispersion of the mixer in coherent optical communication and reduces the frequency mixing. device accuracy.

发明内容SUMMARY OF THE INVENTION

(一)要解决的技术问题(1) Technical problems to be solved

鉴于目前传统的用于相干光通讯的混频器尺寸大、精度低、成本高、偏振色散严重等缺点,本发明提出的一种磷化铟基光学混频器及其制备方法,以至少部分解决以上所提出的的技术问题。In view of the disadvantages such as large size, low precision, high cost and serious polarization dispersion of the current traditional mixers used for coherent optical communication, an indium phosphide-based optical mixer and a preparation method thereof proposed by the present invention can at least partially Solve the technical problems raised above.

(二)技术方案(2) Technical solutions

为达到上述目的,本发明提供了一种磷化铟基光学混频器,包括:一外延片器件层,形成于一磷化铟衬底之上,用于实现混频;一二氧化硅上包层,形成于所述外延片器件层之上,用于保护外延片器件层,并提高外延片器件层稳定性;以及一金属薄膜,形成于所述二氧化硅上包层之上,用于控制偏振。In order to achieve the above object, the present invention provides an indium phosphide-based optical mixer, comprising: an epitaxial wafer device layer formed on an indium phosphide substrate for realizing frequency mixing; a cladding layer formed on the epitaxial wafer device layer for protecting the epitaxial wafer device layer and improving the stability of the epitaxial wafer device layer; and a metal thin film formed on the silicon dioxide upper cladding layer, using to control polarization.

其中,外延片器件层包括通过直波导依次连接的:一模斑转换器,将带有相位信息的信号光耦合进入所述外延片器件层;一1×2多模干涉耦合器,将由所述模斑转换器耦合进入所述外延片器件层的带有信息的信号光均分成两束功率和相位相等的光;一第一偏振转换器,将由所述1×2多模干涉耦合器均分的两束功率和相位相等的光中其中一束光的偏振态极化旋转90°;一第二偏振转换器,将由所述1×2多模干涉耦合器均分的两束功率和相位相等的光中,经过一段直波导后的其中另一束光的偏振态极化旋转90°;一2×2多模干涉耦合器,将由所述第一偏振转换器和所述第二偏振转换器旋转后的信号光耦合输出TE和TM两种模式信号光;一第三偏振转换器,将由所述2×2多模干涉耦合器输出的TM模式信号光的偏振态极化旋转90°变为TE模式的信号光;一波导型偏振器,对由所述2×2 多模干涉耦合器输出的TE模式信号光以及由所述第三偏振转换器旋转后的TE模式信号光进行TE模式信号光的过滤,以滤除残余TM模式信号光;以及一4×4多模干涉耦合器,将由所述波导型偏振器过滤后的TE模式信号光与TE模式本振光进行多模干涉,完成对TE模式输入信号的混频。其中,1×2多模干涉耦合器的干涉区长度L=3Lπ/8;所述2×2多模干涉耦合器的干涉区长度为L=Lπ/2;所述4×4多模干涉耦合器的干涉区长度为L=3Lπ/4;所述第一偏振转换器与第二偏振转换器之间的距离L满足 L=π/(2(βTETM));其中,Lπ为拍长,βTE为TE模式的传播常数,βTM为TM 模式的传播常数。The epitaxial wafer device layer includes: a mode spot converter, which couples the signal light with phase information into the epitaxial wafer device layer; a 1×2 multi-mode interference coupler, which is connected by the straight waveguide. The signal light with information coupled into the epitaxial wafer device layer by the mode spot converter is equally divided into two beams of light with equal power and phase; a first polarization converter, which will be equally divided by the 1×2 multi-mode interference coupler The polarization state of one of the two beams of light with equal power and phase is rotated by 90°; a second polarization converter, which equalizes the power and phase of the two beams equally divided by the 1×2 multimode interference coupler In the light, the polarization state of the other beam of light after a straight waveguide is rotated by 90°; a 2×2 multi-mode interference coupler, which will be converted by the first polarization converter and the second polarization converter The rotated signal light is coupled to output TE and TM mode signal light; a third polarization converter rotates the polarization state of the TM mode signal light output by the 2×2 multi-mode interference coupler by 90° into a TE mode signal light; a waveguide type polarizer for performing TE mode signal on the TE mode signal light output by the 2×2 multi-mode interference coupler and the TE mode signal light rotated by the third polarization converter Light filtering to filter out residual TM mode signal light; and a 4×4 multi-mode interference coupler to perform multi-mode interference between the TE mode signal light filtered by the waveguide polarizer and the TE mode local oscillator light to complete Mixing of the TE mode input signal. Among them, the length of the interference region of the 1×2 multi-mode interference coupler is L=3L π /8; the length of the interference region of the 2×2 multi-mode interference coupler is L=L π /2; the 4×4 multi-mode interference coupler The length of the interference region of the interference coupler is L=3L π /4; the distance L between the first polarization converter and the second polarization converter satisfies L=π/(2(β TE −β TM )); wherein , L π is the beat length, β TE is the propagation constant of the TE mode, and β TM is the propagation constant of the TM mode.

其中,所述二氧化硅上包层厚度为1μm-3μm;所述金属薄膜位于所述第三偏振转换器与4×4多模干涉耦合器之间的连接直波导上方,采用的材料是Ag、Au、Cu或Al,厚度为100nm-200nm。Wherein, the thickness of the silicon dioxide upper cladding layer is 1 μm-3 μm; the metal film is located above the connecting straight waveguide between the third polarization converter and the 4×4 multi-mode interference coupler, and the material used is Ag , Au, Cu or Al, with a thickness of 100nm-200nm.

为达到上述目的,本发明还提供了一种制备磷化铟基光学混频器的方法,包括:In order to achieve the above object, the present invention also provides a method for preparing an indium phosphide-based optical mixer, comprising:

步骤1、制备一外延片器件层,形成于一磷化铟衬底上;Step 1, preparing an epitaxial wafer device layer, which is formed on an indium phosphide substrate;

步骤2:在外延片器件层之上,生长一二氧化硅上包层;Step 2: growing a silicon dioxide upper cladding layer on the epitaxial wafer device layer;

步骤3:在二氧化硅上包层之上,生长一金属薄膜。Step 3: A metal thin film is grown on the silicon dioxide upper cladding layer.

其中,在磷化铟衬底上,通过光刻、刻蚀和腐蚀工艺制备得到一外延片器件层,所述外延片器件层包括由直波导依次连接的模斑转换器、1×2 多模干涉耦合器、第一偏振转换器、第二偏振转换器、2×2多模干涉耦合器、第三偏振转换器和4×4多模干涉耦合器;其中,刻蚀工艺的刻蚀厚度为4μm-5μm。Wherein, on the indium phosphide substrate, an epitaxial wafer device layer is prepared by photolithography, etching and etching processes, and the epitaxial wafer device layer includes a mode spot converter, a 1×2 multi-mode Interference coupler, first polarization converter, second polarization converter, 2×2 multi-mode interference coupler, third polarization converter and 4×4 multi-mode interference coupler; wherein, the etching thickness of the etching process is 4μm-5μm.

所述第一偏振转换器、第二偏振转换器与第三偏振转换器是通过直波导一侧的倾斜侧壁实现的,所述倾斜侧壁通过溴-甲醇溶液湿法腐蚀得到,倾斜侧壁的倾角为50°-60°;所述金属薄膜生长于所述第三偏振转换器与 4×4多模干涉耦合器之间的连接直波导上方的二氧化硅上包层之上,与第三偏振转换器与4×4多模干涉耦合器之间的直波导形成波导型偏振器The first polarization converter, the second polarization converter and the third polarization converter are realized by the inclined sidewall on one side of the straight waveguide, the inclined sidewall is obtained by wet etching with bromine-methanol solution, and the inclined sidewall is obtained. The inclination angle is 50°-60°; the metal film is grown on the silicon dioxide upper cladding layer above the connecting straight waveguide between the third polarization converter and the 4×4 multimode interference coupler, and is connected with the third polarization converter and the 4×4 multimode interference coupler. Straight waveguides between triple polarization converters and 4×4 multimode interference couplers form waveguide polarizers

(三)有益效果(3) Beneficial effects

从上述技术方案可以看出,本发明提供的一种磷化铟基光学混频器及其制备方法,具有以下有益效果:It can be seen from the above technical solutions that an indium phosphide-based optical mixer and a preparation method thereof provided by the present invention have the following beneficial effects:

(1)本发明提出的磷化铟基光学混频器,具有尺寸微米级的特点,极大地减小了光学混频器的空间尺寸,提高了器件结构的紧凑性。所选用的磷化铟衬底便于与后续的相同材料的平衡光电探测器集成可进一步提高集成度和耦合效率,为未来高性能光学相干光探测器的集成化、小型化打下了坚实的基础。(1) The indium phosphide-based optical mixer proposed by the present invention has the characteristics of micron-scale size, which greatly reduces the spatial size of the optical mixer and improves the compactness of the device structure. The selected indium phosphide substrate is easy to integrate with the subsequent balanced photodetectors of the same material, which can further improve the integration degree and coupling efficiency, and lay a solid foundation for the integration and miniaturization of high-performance optical coherent photodetectors in the future.

(2)在本发明提出的磷化铟基光学混频器,通过借助基于马赫曾德干涉仪、第三偏振转换器和2×2MMI的偏振分束器,实现对TE信号光和 TM信号光两种信号光模式的分离,并分别将信号光中TE模式和TM模式所携带的信号分别进行了提取,进一步提高了光信号的利用率,拓宽了信号带宽,并且器件仅需输入TE模式本振光即可完成对TE模式和TM 模式的混频。(2) In the indium phosphide-based optical mixer proposed in the present invention, by means of a Mach-Zehnder interferometer, a third polarization converter and a polarization beam splitter based on a 2×2 MMI, the TE signal light and the TM signal light can be separated from each other. The two signal optical modes are separated, and the signals carried by the TE mode and the TM mode in the signal light are extracted respectively, which further improves the utilization rate of the optical signal and broadens the signal bandwidth, and the device only needs to input the TE mode. Vibrating light can complete the mixing of TE mode and TM mode.

(3)在本发明提出的磷化铟基光学混频器中,用于混频的两个4×4 MMI无需分别设计为TE模式和TM模式的尺寸,进一步降低了设计和工艺难度。(3) In the indium phosphide-based optical mixer proposed by the present invention, the two 4×4 MMIs used for frequency mixing do not need to be designed to be the size of the TE mode and the TM mode respectively, which further reduces the design and process difficulty.

(4)本发明提出的磷化铟基光学混频器,通过引入含有金属镀层的波导型偏振器,进一步提高了对TE模式中残余TM模式的抑制,极大地降低了混频器中的偏振模式色散,减小了混频器的相位误差,提高了相干光通讯系统的灵敏度。(4) The indium phosphide-based optical mixer proposed by the present invention further improves the suppression of the residual TM mode in the TE mode by introducing a waveguide polarizer containing a metal coating, and greatly reduces the polarization in the mixer Modal dispersion reduces the phase error of the mixer and improves the sensitivity of the coherent optical communication system.

(5)本发明提出的磷化铟基光学混频器,在CMOS工艺的基础上,将模斑转换器、1×2MMI、第一偏振转换器、第二偏振转换器、2×2MMI、第三偏振转换器、波导型偏振器以及4×4MMI集成在同一衬底上,易于制备和集成,降低成本且可大规模生产。(5) The indium phosphide-based optical mixer proposed by the present invention, on the basis of the CMOS process, combines the mode spot converter, 1×2MMI, first polarization converter, second polarization converter, 2×2MMI, The three polarization converters, the waveguide-type polarizer and the 4×4 MMI are integrated on the same substrate, which is easy to fabricate and integrate, reduces the cost and can be mass-produced.

附图说明Description of drawings

图1为本发明提出的磷化铟基光学混频器中外延片器件层的结构示意图;1 is a schematic structural diagram of an epitaxial wafer device layer in an indium phosphide-based optical mixer proposed by the present invention;

图2为本发明提出的磷化铟基光学混频器沿图1中A-A线截开的剖面结构示意图;FIG. 2 is a schematic cross-sectional structure diagram of the indium phosphide-based optical mixer proposed by the present invention taken along the line A-A in FIG. 1;

图3为本发明提出的磷化铟基光学混频器沿图1中B-B线截开的剖面结构示意图;FIG. 3 is a schematic cross-sectional structure diagram of the indium phosphide-based optical mixer proposed by the present invention taken along the line B-B in FIG. 1;

图4为本发明提出的磷化铟基光学混频器的制备工艺流程图;4 is a flow chart of the preparation process of the indium phosphide-based optical mixer proposed by the present invention;

图5为本发明提出的磷化铟基光学混频器中外延片上制得的器件结构的立体示意图。5 is a schematic perspective view of a device structure fabricated on an epitaxial wafer in the indium phosphide-based optical mixer proposed by the present invention.

【附图标记说明】[Description of reference numerals]

1:磷化铟衬底1: Indium phosphide substrate

2:外延片器件层2: Epitaxial wafer device layer

3:二氧化硅上包层3: Silica upper cladding

4:金属薄膜4: Metal thin film

201:模斑转换器201: Mode Spot Converter

202:直波导202: Straight Waveguide

203:1×2多模干涉耦合器203: 1×2 Multimode Interference Coupler

204:第一偏振转换器204: First Polarization Converter

205:第二偏振转换器205: Second Polarization Converter

206:2×2多模干涉耦合器206: 2×2 Multimode Interferometric Coupler

207:第三偏振转换器207: Third Polarization Converter

208:波导型偏振器208: Waveguide Polarizer

209:4×4多模干涉耦合器209: 4×4 Multimode Interferometric Coupler

具体实施方式Detailed ways

为使本发明的目的、技术方案和优点更加清楚,以下结合具体实例和附图,对本发明进一步详细说明。需要说明的是,在附图或说明书描述中,相同或相似部分使用相同的图号。附图中未显示或描述的实现方式,为该技术领域中普通技术人员所知的形式。另外,虽然本文可提供包含特定值的参数的示范,但应了解,参数无需确切等于相应的值,而是在可接受的误差容限或涉及约束内近似于相应的值。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be described in further detail below with reference to specific examples and accompanying drawings. It should be noted that, in the drawings or descriptions in the specification, the same drawing numbers are used for the same or similar parts. Implementations not shown or described in the drawings are in the form known to those of ordinary skill in the art. Additionally, although examples of parameters including specific values may be provided herein, it should be understood that the parameters need not be exactly equal to the corresponding value, but rather approximate the corresponding value within acceptable error tolerances or constraints involved.

根据本发明的一方面,在本发明的一个示例性实施例中,提供了一种低偏振色散高带宽的磷化铟基光学混频器,请参照图1,该磷化铟基光学混频器包括:According to an aspect of the present invention, in an exemplary embodiment of the present invention, an indium phosphide-based optical mixer with low polarization dispersion and high bandwidth is provided, please refer to FIG. 1 , the indium phosphide-based optical mixer device includes:

外延片器件层2,形成于磷化铟衬底1之上,用于实现混频;The epitaxial wafer device layer 2 is formed on the indium phosphide substrate 1, and is used to realize frequency mixing;

二氧化硅上包层3,形成于所述外延片器件层2之上,用于保护外延片器件层2,并提高外延片器件层稳定性;以及The silicon dioxide upper cladding layer 3 is formed on the epitaxial wafer device layer 2 for protecting the epitaxial wafer device layer 2 and improving the stability of the epitaxial wafer device layer; and

金属薄膜4,形成于所述二氧化硅上包层3之上,用于控制偏振。The metal thin film 4 is formed on the silicon dioxide upper cladding layer 3 for controlling polarization.

其中,外延片器件层2包括通过直波导202依次连接的模斑转换器201、 1×2MMI203、第一偏振转换器204、第二偏振转换器205、2×2MMI 206、第三偏振转换器207、波导型偏振器208和2个4×4MMI 209:The epitaxial wafer device layer 2 includes a mode spot converter 201 , a 1×2 MMI 203 , a first polarization converter 204 , a second polarization converter 205 , a 2×2 MMI 206 , and a third polarization converter 207 , which are connected in sequence through a straight waveguide 202 . , waveguide polarizer 208 and two 4×4MMI 209:

模斑转换器201,将带有相位信息的信号光耦合进入外延片器件层;The mode spot converter 201 couples the signal light with phase information into the epitaxial wafer device layer;

1×2MMI 203,将进入外延片器件层的带有信息的信号光均分成两束功率和相位相等的光;2MMI 203, which divides the signal light with information entering the epitaxial wafer device layer into two beams of equal power and phase;

第一偏振转换器204,将由1×2MMI 203均分的两束功率和相位相等的光中其中一束光的偏振态极化旋转90°;the first polarization converter 204, which rotates the polarization state polarization of one of the two beams of light equally divided by the 1×2 MMI 203 with equal power and phase by 90°;

第二偏振转换器205,将由1×2MMI 203均分的两束功率和相位相等的光中,经过一段直波导后的其中另一束光的偏振态极化旋转90°;The second polarization converter 205 rotates the polarization state polarization of the other beam after passing through a straight waveguide in the two beams of equal power and phase divided by the 1×2 MMI 203 by 90°;

2×2MMI 206,将由第一偏振转换器204和所述第二偏振转换器205 旋转后的信号光耦合输出TE和TM两种模式信号光;2×2 MMI 206, which couples the signal light rotated by the first polarization converter 204 and the second polarization converter 205 to output two modes of signal light, TE and TM;

第三偏振转换器207,将由2×2MMI 206输出的TM模式信号光的偏振态极化旋转90°变为TE模式的信号光;The third polarization converter 207 rotates the polarization state polarization of the TM mode signal light output by the 2×2 MMI 206 by 90° into the TE mode signal light;

波导型偏振器208,对由2×2MMI 206输出的TE模式信号光以及由第三偏振转换器207旋转后的TE模式信号光进行TE模式信号光的过滤;The waveguide polarizer 208 filters the TE mode signal light output by the 2×2 MMI 206 and the TE mode signal light rotated by the third polarization converter 207;

2个4×4MMI 209,将由波导型偏振器208过滤后的TE模式信号光与TE模式本振光进行多模干涉,完成对TE模式输入信号的混频。Two 4×4 MMIs 209 perform multi-mode interference between the TE mode signal light filtered by the waveguide polarizer 208 and the TE mode local oscillator light to complete the frequency mixing of the TE mode input signal.

其中,1×2MMI、2×2MMI、4×4MMI的多模干涉区长度计算是基于 MMI的多模干涉原理和导模传输分析法,其拍长Lπ为Lπ=4nrwe 2/3λ0,式中,nr为多模干涉区对应模式下的有效折射率;we为对应模式下的有效宽度,λ0为器件的工作波长;因此,1×2MMI 203的干涉区长度L=3Lπ/8;2×2 MMI 206的干涉区长度为L=Lπ/2;4×4MMI 209的干涉区长度为L=3Lπ/4。Among them, the multimode interference region length calculation of 1×2MMI, 2×2MMI and 4×4MMI is based on the multimode interference principle of MMI and the guided mode transmission analysis method, and the beat length L π is L π =4n r w e 2 / 3λ 0 , where n r is the effective refractive index in the corresponding mode of the multi-mode interference region; we e is the effective width in the corresponding mode, and λ 0 is the operating wavelength of the device; therefore, the length of the interference region L of 1×2MMI 203 = 3Lπ /8; the length of the interference region of the 2x2 MMI 206 is L= /2; the length of the interference region of the 4x4 MMI 209 is L= 3Lπ /4.

同时,1×2MMI 203、第一偏振转换器204、第二偏振转换器205、2×2 MMI 206四个器件组合实现偏振分束器的作用。为了达到最理想的分束效果,要求两束光相位差满足±π/2,即第一偏振转换器204与第二偏振转换器205的间距必须满足L=π/(2(βTETM)),式中,βTE为TE模式的传播常数;βTM为TM模式的传播常数。At the same time, the combination of four components, 1×2 MMI 203 , first polarization converter 204 , second polarization converter 205 , and 2×2 MMI 206 , realizes the function of polarization beam splitter. In order to achieve the most ideal beam splitting effect, the phase difference between the two beams is required to satisfy ±π/2, that is, the distance between the first polarization converter 204 and the second polarization converter 205 must satisfy L=π/(2(β TE −β TM )), where β TE is the propagation constant of the TE mode; β TM is the propagation constant of the TM mode.

另外,波导型偏振器208是通过金属薄膜4对TE模和TM模的传输损耗差异来实现对某个模式的消除;本发明的一实施例中,通过在直波导表面淀积100nm-200nm厚的Al金属薄膜可实现对TE模式的损耗控制在 0.5dB-1dB,而对TM模式的损耗高达20dB-30dB;这样可以实现对残余的 TM模式进行进一步滤除的效果,降低了混频器的偏振色散,提高了器件精度。In addition, the waveguide polarizer 208 realizes the elimination of a certain mode through the difference of the transmission loss of the metal film 4 to the TE mode and the TM mode; in an embodiment of the present invention, a thickness of 100nm-200nm is deposited on the surface of the straight waveguide The Al metal thin film can realize the loss of TE mode is controlled at 0.5dB-1dB, while the loss of TM mode is as high as 20dB-30dB; this can achieve the effect of further filtering the residual TM mode, reducing the frequency of the mixer. Polarization dispersion improves device accuracy.

并且,由于本发明提供的磷化铟基光学混频器所选用的磷化铟衬底,便于与后续相同材料的平衡光电探测器集成可进一步提高集成度和耦合效率,为未来高性能光学相干光探测器的集成化、小型化打下了坚实的基础。In addition, due to the indium phosphide substrate selected for the indium phosphide-based optical mixer provided by the present invention, it is convenient to integrate with subsequent balanced photodetectors of the same material, which can further improve the integration degree and coupling efficiency, and provide future high-performance optical coherence. The integration and miniaturization of photodetectors have laid a solid foundation.

请参照图2、图3,所述外延片器件层2位于磷化铟衬底1上方,整个外延片借助MOCVD生长。Referring to FIGS. 2 and 3 , the epitaxial wafer device layer 2 is located above the indium phosphide substrate 1 , and the entire epitaxial wafer is grown by MOCVD.

图2为图1所示的磷化铟基光学混频器沿A-A线的剖面结构示意图。所述外延片器件层中的器件结构201-207以及209均通过在外延片上刻蚀形成。FIG. 2 is a schematic cross-sectional structure diagram of the indium phosphide-based optical mixer shown in FIG. 1 along the line A-A. The device structures 201-207 and 209 in the epitaxial wafer device layer are formed by etching on the epitaxial wafer.

其中,直波导结构为深脊InP波导,脊高4μm,宽2.6μm,可以保证 C波段的信号光在直波导中单模传输。除此之外,深脊有利于进一步降低直波导传输损耗,提高器件响应度;Among them, the straight waveguide structure is a deep ridged InP waveguide with a ridge height of 4 μm and a width of 2.6 μm, which can ensure the single-mode transmission of the C-band signal light in the straight waveguide. In addition, the deep ridge is beneficial to further reduce the transmission loss of the straight waveguide and improve the responsivity of the device;

其中,二氧化硅上包层3厚度约为2μm,在1.55μm波长处折射率约为1.44,对芯层器件起关键保护作用。磷化铟芯片作为一种脆弱、易受潮的集成芯片,淀积二氧化硅上包层对器件进行保护至关重要。Among them, the thickness of the silicon dioxide upper cladding layer 3 is about 2 μm, and the refractive index at the wavelength of 1.55 μm is about 1.44, which plays a key role in protecting the core layer device. As indium phosphide chip is a fragile and easily damped integrated chip, it is very important to deposit silicon dioxide upper cladding to protect the device.

图3为图1所示的磷化铟基光学混频器沿B-B线的剖面结构示意图。所述金属Al薄膜4厚度约为100nm,通过电子束蒸发淀积于第三偏振转换器207与4×4MMI 209之间的连接直波导上方。实现对TM模式的进一步滤除。FIG. 3 is a schematic cross-sectional structure diagram of the indium phosphide-based optical mixer shown in FIG. 1 along the line B-B. The metal Al thin film 4 has a thickness of about 100 nm, and is deposited above the straight waveguide connected between the third polarization converter 207 and the 4×4 MMI 209 by electron beam evaporation. Implements further filtering of TM patterns.

基于图1-3所示的磷化光学混频器,本发明还提供了一种制备图1-3 所示的磷化铟光学混频器的方法,该制备方法包括:Based on the phosphide optical mixer shown in Figures 1-3, the present invention also provides a method for preparing the indium phosphide optical mixer shown in Figures 1-3, the preparation method comprising:

步骤1、制备一外延片器件层,形成于一磷化铟衬底上;Step 1, preparing an epitaxial wafer device layer, which is formed on an indium phosphide substrate;

步骤2:在外延片器件层之上,生长一二氧化硅上包层;Step 2: growing a silicon dioxide upper cladding layer on the epitaxial wafer device layer;

步骤3:在二氧化硅上包层之上,生长一金属薄膜。Step 3: A metal thin film is grown on the silicon dioxide upper cladding layer.

本发明的一实施例提供了更为详细的制备步骤,如图4所示,具体包括如下步骤:An embodiment of the present invention provides more detailed preparation steps, as shown in Figure 4, which specifically includes the following steps:

步骤S401:提供一磷化铟衬底;Step S401: providing an indium phosphide substrate;

步骤S402:制备外延片器件层,具体包括:Step S402: preparing an epitaxial wafer device layer, which specifically includes:

步骤S4021:在磷化铟衬底上,外延生长InP-InGaAsP-InP外延片;Step S4021: epitaxially growing an InP-InGaAsP-InP epitaxial wafer on the indium phosphide substrate;

步骤S4022:在InP-InGaAsP-InP外延片上,生长一二氧化硅掩模;Step S4022: growing a silicon dioxide mask on the InP-InGaAsP-InP epitaxial wafer;

步骤S4023:在所述二氧化硅掩模上旋涂光刻胶后,进行曝光并显影;Step S4023: after spin-coating photoresist on the silicon dioxide mask, exposing and developing;

步骤S4024:刻蚀出用于腐蚀的方槽;Step S4024: etching out a square groove for etching;

步骤S4025:去胶,借助腐蚀剂,腐蚀出偏振转换器的倾斜侧壁;Step S4025: removing the glue, and etching out the inclined sidewall of the polarization converter with the aid of an etchant;

步骤S4026:在外延片器件层上生长一顶层二氧化硅;Step S4026: growing a top layer of silicon dioxide on the epitaxial wafer device layer;

步骤S4027:在所述顶层二氧化硅上旋涂光刻胶,进行曝光,并显影、定影;Step S4027: spin-coating photoresist on the top layer silicon dioxide, exposing, developing and fixing;

步骤S4028:以顶层二氧化硅为硬掩模,刻蚀出图形区结构,完成图形从光刻胶到外延片上的转移;Step S4028: using the top layer of silicon dioxide as a hard mask, etching the pattern area structure, and completing the transfer of the pattern from the photoresist to the epitaxial wafer;

步骤S4029:加热、去胶、并清洗后,得到所述模斑转换器、所述1×2多模干涉耦合器、所述第一偏振转换器、所述第二偏振转换器、所述2×2多模干涉耦合器、所述第三偏振转换器、所述4×4多模干涉耦合器;Step S4029: After heating, degumming, and cleaning, the mode spot converter, the 1×2 multi-mode interference coupler, the first polarization converter, the second polarization converter, the 2 ×2 multi-mode interference coupler, the third polarization converter, the 4 × 4 multi-mode interference coupler;

步骤S403:生长二氧化硅上包层;Step S403: growing a silicon dioxide upper cladding layer;

步骤S404:生长金属Al薄膜,形成所述波导型偏振器;Step S404: growing a metal Al thin film to form the waveguide polarizer;

切片,并进行端面研磨抛光,最终完成磷化铟基光学混频器制备。Slice, and grind and polish the end face, and finally complete the preparation of indium phosphide-based optical mixer.

其中,外延片是通过MOCVD外延生长得到的;Among them, the epitaxial wafer is obtained by MOCVD epitaxy;

其中,倾斜侧壁通过溴-甲醇溶液湿法腐蚀得到,且倾斜侧壁的倾角为50°-60°:Wherein, the inclined sidewall is obtained by wet etching of bromine-methanol solution, and the inclination angle of the inclined sidewall is 50°-60°:

其中,生长金属薄膜的步骤中,具体包括:Wherein, in the step of growing the metal film, it specifically includes:

在所述二氧化硅上包层上旋涂负胶;spin-coating a negative glue on the silica upper cladding;

在所述负胶上、位于第三偏振转换器与4×4多模干涉耦合器之间的连接直波导上方,光刻开孔;On the negative glue, above the connecting straight waveguide between the third polarization converter and the 4×4 multi-mode interference coupler, a hole is lithographically opened;

在所述开孔处,蒸发淀积金属薄膜;At the opening, a metal film is deposited by evaporation;

负胶剥离并清洗,制备得到所需的波导型偏振器。The negative adhesive is peeled off and cleaned to prepare the desired waveguide type polarizer.

特别注意的是,在制备过程中对磷化铟衬底以及外延片器件层进行清洗时,由于无机清洗会对芯片产生腐蚀,因此采用:在丙酮溶液中水浴加热;用乙醇水浴加热去除残余丙酮;用去离子水冲洗残余乙醇;氮气吹干的清洗方法。It should be noted that when cleaning the indium phosphide substrate and the device layer of the epitaxial wafer during the preparation process, since inorganic cleaning will corrode the chip, use: heating in a water bath in an acetone solution; heating with an ethanol water bath to remove residual acetone ; Rinse residual ethanol with deionized water; Cleaning method by nitrogen blowing.

基于图1-3所示的磷化铟基光学混频器,本发明提供的磷化铟基光学混频器对信号光的混频过程如下:Based on the indium phosphide-based optical mixer shown in Figures 1-3, the frequency mixing process of the indium phosphide-based optical mixer provided by the present invention for signal light is as follows:

信号光通过模斑转换器201耦合进入直波导202,通过1×2MMI多模干涉耦合器203分为两束光强、相位均相等的光。然后通过一个类似于马赫曾德干涉仪的直波导结构,其中第一偏振转换器和第二偏振转换器分别位于马赫曾德延时线两条臂的两侧。光在输入第一偏振转换器204之前需经过一固定长度差来实现整个器件的高效偏振分束。MZI两条臂的光分别输入到2×2MMI多模干涉耦合器206中去在其中完成偏振分束,输出的两路光分别为TE和TM模式。TE模式的输出光通过波导型偏振器208进一步滤除残余TM模式然后输入到用于混频TE模式的4×4MMI多模干涉耦合器209与TE模式的本振光完成混频并输出信号光中的TE模式所携带信号。另一路TM模式输出光经过第三偏振转换器207转换为TE模式并通过波导型偏振器208进一步滤除残余TM模式然后输入到用于混频TE 模式的4×4MMI多模干涉耦合器209与TE模式的本振光完成混频并输出信号光中的TE模式所携带信号。The signal light is coupled into the straight waveguide 202 through the mode-spot converter 201 , and is divided into two beams of light with equal intensity and phase through the 1×2 MMI multi-mode interference coupler 203 . Then it passes through a straight waveguide structure similar to a Mach-Zehnder interferometer, in which the first polarization converter and the second polarization converter are located on the two sides of the two arms of the Mach-Zehnder delay line, respectively. The light needs to pass through a fixed length difference before being input to the first polarization converter 204 to achieve efficient polarization beam splitting of the entire device. The light of the two arms of the MZI is respectively input into the 2×2 MMI multi-mode interference coupler 206 to complete the polarization beam splitting therein, and the two output lights are respectively TE and TM modes. The output light of the TE mode is further filtered by the waveguide type polarizer 208 to filter out the residual TM mode and then input to the 4×4 MMI multi-mode interference coupler 209 for mixing the TE mode to complete the frequency mixing with the local oscillator light of the TE mode and output the signal light The signal carried by the TE mode in . The other TM mode output light is converted into TE mode by the third polarization converter 207 and further filtered by the waveguide polarizer 208 to filter the residual TM mode and then input to the 4×4 MMI multi-mode interference coupler 209 for mixing the TE mode with The local oscillator light in the TE mode completes the frequency mixing and outputs the signal carried by the TE mode in the signal light.

以上所述的具体实施例,对本发明的目的、技术方案和有益效果进行了进一步详细说明。所应理解的是,以上所述仅为本发明的具体实施例而已、并不用于限制本发明、凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The specific embodiments described above further describe the purpose, technical solutions and beneficial effects of the present invention in detail. It should be understood that the above descriptions are only specific embodiments of the present invention, and are not intended to limit the present invention. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be should be included within the protection scope of the present invention.

Claims (8)

1. An indium phosphide-based optical mixer comprising:
an epitaxial wafer device layer formed on an indium phosphide substrate for realizing frequency mixing;
the upper cladding layer of the silicon dioxide is formed on the epitaxial wafer device layer and used for protecting the epitaxial wafer device layer and improving the stability of the epitaxial wafer device layer; and
a metal film formed on the silica upper cladding for controlling polarization;
wherein, epitaxial wafer device layer includes that it connects gradually through straight waveguide:
a spot size converter optically coupling the signal with the phase information into the epitaxial wafer device layer;
a 1 x 2 multimode interference coupler, which divides the signal light with phase information coupled into the epitaxial wafer device layer by the spot size converter into two beams of light with equal power and phase;
a first polarization converter for rotating the polarization state polarization of one of the two light beams equally divided by the 1 × 2 multimode interference coupler with equal power and phase by 90 °;
the second polarization converter rotates the polarization state polarization of the other light beam which passes through the straight waveguide by 90 degrees from the two light beams with equal power and phase which are equally divided by the 1 multiplied by 2 multimode interference coupler;
a 2 x 2 multimode interference coupler, which couples the two beams of signal light rotated by the first polarization converter and the second polarization converter to output two modes of TE and TM signal light;
a third polarization converter for rotating the polarization state of the TM mode signal light output from the 2 × 2 multimode interference coupler by 90 ° to become a TE mode signal light;
a waveguide type polarizer for filtering the TE mode signal light outputted from the 2 × 2 multimode interference coupler and the TE mode signal light rotated by the third polarization converter to filter out residual TM mode signal light; and
and the 4 x 4 multimode interference coupler performs multimode interference on the TE mode signal light filtered by the waveguide type polarizer and the TE mode local oscillator light to complete frequency mixing of the TE mode input signal.
2. The indium phosphide-based optical mixer of claim 1 wherein the 1 x 2 multimode interference coupler has an interference zone length L-3Lπ8; the length of the interference zone of the 2 x 2 multimode interference coupler is L ═ Lπ2; the length of the interference zone of the 4 multiplied by 4 multimode interference coupler is L-3Lπ(ii)/4; wherein L isπIs a beat length, Lπ=4nrwe 2/3λ0In the formula, nrEffective refractive index of the multimode interference region in a corresponding mode; w is aeTo correspond to the effective width in the mode, λ0Is the operating wavelength of the device.
3. The indium phosphide-based optical mixer of claim 1 wherein the distance L between the first polarization converter and the second polarization converter satisfies L ═ pi/(2 (β)TETM) In which beta isTEIs the propagation constant of the TE mode, betaTMIs the propagation constant of the TM mode.
4. The indium phosphide-based optical mixer of claim 1 wherein the silica overclad layer is 1 μm to 3 μm thick.
5. The indium phosphide-based optical mixer of claim 1 wherein the thin metal film is disposed over a straight waveguide between the third polarization converter and the 4 x 4 multimode interference coupler and is made of Ag, Au, Cu or Al with a thickness of 100nm to 200 nm.
6. A method of making the indium phosphide-based optical mixer of any one of claims 1 to 5, comprising:
step 1: preparing an epitaxial wafer device layer on an indium phosphide substrate;
step 2: forming a silicon dioxide upper cladding layer on the epitaxial wafer device layer; and
and step 3: forming a metal film on the silica upper cladding layer; the preparation of the epitaxial wafer device layer on the indium phosphide substrate specifically comprises the following steps:
preparing an epitaxial wafer device layer on an indium phosphide substrate through photoetching, etching and corrosion processes, wherein the epitaxial wafer device layer comprises a spot size converter, a 1 × 2 multi-mode interference coupler, a first polarization converter, a second polarization converter, a 2 × 2 multi-mode interference coupler, a third polarization converter and a 4 × 4 multi-mode interference coupler which are sequentially connected through a straight waveguide; wherein the etching thickness of the etching process is 4-5 μm.
7. The method for preparing the optical waveguide according to claim 6, wherein the first polarization converter, the second polarization converter and the third polarization converter are realized by inclined sidewalls on one side of the straight waveguide, the inclined sidewalls are obtained by bromine-methanol solution wet etching, and the inclination angle of the inclined sidewalls is 50 ° to 60 °.
8. The method of claim 6, wherein in step 3, the metal film is grown on top of a silica upper cladding over a straight waveguide between the third polarization transformer and the 4 x 4 multimode interference coupler, forming a waveguide-type polarizer with the straight waveguide between the third polarization transformer and the 4 x 4 multimode interference coupler.
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