CN110283555A - A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature and preparation method thereof - Google Patents
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature and preparation method thereof Download PDFInfo
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- CN110283555A CN110283555A CN201910583290.XA CN201910583290A CN110283555A CN 110283555 A CN110283555 A CN 110283555A CN 201910583290 A CN201910583290 A CN 201910583290A CN 110283555 A CN110283555 A CN 110283555A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J107/00—Adhesives based on natural rubber
- C09J107/02—Latex
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Abstract
The invention discloses a kind of explosion-proof flame-retardant type tire repair liquids resistant to high temperature and preparation method thereof, raw material including following parts by weight: 20-30 parts of deionized water, 10-15 parts of ethylene glycol, 25-35 parts of natural emulsion, 3-8 parts of polyisoprene, 2-6 parts of polypropylene fibre, 1-5 parts of polystyrene, 10-20 parts of nonylphenol polyoxyethylene ether, 0.5-2.5 parts of polyacrylamide, 0.2-1.5 parts of lauryl sodium sulfate, 10-20 parts of nitrile rubber, 1-5 parts of butanediol laurate, explosion-proof flame-retardant type tire repair liquid resistant to high temperature produced by the present invention, preparation method is simple, raw material is prepared to be easy to get, it is with good economic efficiency, emergency after tyre repairing fluid produced by the present invention can be used for blowing out is inflated, effective speed is fast, it fills and uses, it can be reduced rapidly after use Tyre temperature, use temperature range is wide, can under 60 DEG C of hot environment and subzero 15 DEG C of low temperature environment normal use, prevent tire is secondary from blowing out, it is nonflammable, have flame retardant effect.
Description
Technical field
The present invention relates to tyre technology, specifically a kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature and its preparation
Method.
Background technique
Tyre repairing fluid is when tire is punctured by nail or other tip and hard object matter, for the product of interim tire patching, containing certain
The liquid of the substance of the material or subparticle of kind of short-fibre silk according in certain dosage pre-implant tire, as tire have it is fine
Hole will be blocked；And when tire hole occurs, the air that overflows strongly the liquid with fiber filament or particle together
It releases fiber filament that is squeezed into hole or particle instantaneous time is tightly clogging by its, make tire no longer gas leakage, keep
Enough pressure in tire, enables the vehicle continue to travel, and prevents the accident that may occur.
However existing tyre repairing fluid flame retardant property is poor, and a degree of corrosion can be caused to wheel hub.
Summary of the invention
The purpose of the present invention is to provide a kind of explosion-proof flame-retardant type tire repair liquids resistant to high temperature and preparation method thereof, with solution
Certainly the problems mentioned above in the background art.
To achieve the above object, the invention provides the following technical scheme:
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, the raw material including following parts by weight: deionized water 20-30
Part, 10-15 parts of ethylene glycol, 25-35 parts of natural emulsion, 3-8 parts of polyisoprene, 2-6 parts of polypropylene fibre, polystyrene 1-5
Part, 10-20 parts of nonylphenol polyoxyethylene ether, 0.5-2.5 parts of polyacrylamide, 0.2-1.5 parts of lauryl sodium sulfate, the fine rubber of fourth
10-20 parts of glue, 1-5 parts of butanediol laurate.
As a further solution of the present invention: the raw material including following parts by weight: 22-28 parts of deionized water, ethylene glycol
11-14 parts, 28-32 parts of natural emulsion, 4-6 parts of polyisoprene, 3-5 parts of polypropylene fibre, 2-4 parts of polystyrene, nonyl phenol
12-18 parts of polyoxyethylene ether, 1-2 parts of polyacrylamide, 0.5-1.2 parts of lauryl sodium sulfate, 12-18 parts of nitrile rubber, fourth
2-4 parts of glycol laurate.
As further scheme of the invention: the raw material including following parts by weight: 25 parts of deionized water, ethylene glycol 12
Part, 30 parts of natural emulsion, 5 parts of polyisoprene, 4 parts of polypropylene fibre, 3 parts of polystyrene, 15 parts of nonylphenol polyoxyethylene ether,
1.5 parts of polyacrylamide, 1 part of lauryl sodium sulfate, 15 parts of nitrile rubber, 3 parts of butanediol laurate.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 5-10min, is mixed
Close liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, heating temperature 110-
130 DEG C, obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by the fine rubber of fourth
Rubber powder end, ethylene glycol, polypropylene fibre are put into ultrasonic vibration instrument, and ultrasonic vibration 5-10min obtains mixed liquor C；(6) it will mix
It closes liquid B, mixed liquor C, polystyrene, butanediol laurate to put into reaction kettle, heated sealed stirring, heating temperature 90-110
DEG C, it is cooling, it is filling to get.
As further scheme of the invention: in step (2), microwave shakes the time for 8min.
As further scheme of the invention: in step (3), heating temperature is 120 DEG C.
As further scheme of the invention: in step (5), the time of ultrasonic vibration is 8min.
As further scheme of the invention: in step (6), heating temperature is 100 DEG C.
Compared with prior art, the beneficial effects of the present invention are: explosion-proof flame-retardant produced by the present invention type tire resistant to high temperature
Tyre repairing fluid, preparation method is simple, prepares raw material and is easy to get, with good economic efficiency, and tyre repairing fluid produced by the present invention can be used for
Emergency inflation after blowing out, effective speed is fast, that is, fills and use, and tyre temperature, use temperature range can be reduced rapidly after use
Extensively, can under 60 DEG C of hot environment and subzero 15 DEG C of low temperature environment normal use, prevent tire is secondary from blowing out, be not easy
Combustion has flame retardant effect, will not corrode wheel hub.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, including following raw material: deionized water 20g, ethylene glycol 10g,
Natural emulsion 25g, polyisoprene 3g, polypropylene fibre 2g, polystyrene 1g, nonylphenol polyoxyethylene ether 10g, polyacrylamide
Amine 0.5g, lauryl sodium sulfate 0.2g, nitrile rubber 10g, butanediol laurate 1g.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 5min, is mixed
Liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, and 110 DEG C of heating temperature,
Obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by nitrile rubber powder,
In ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, ultrasonic vibration 5min obtains mixed liquor C；(6) by mixed liquid B, mixing
Liquid C, polystyrene, butanediol laurate are put into reaction kettle, heated sealed stirring, 90 DEG C of heating temperature, cooling, filling,
To obtain the final product.
Embodiment 2
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, including following raw material: deionized water 30g, ethylene glycol 15g,
Natural emulsion 35g, polyisoprene 8g, polypropylene fibre 6g, polystyrene 5g, nonylphenol polyoxyethylene ether 20g, polyacrylamide
Amine 2.5g, lauryl sodium sulfate 1.5g, nitrile rubber 20g, butanediol laurate 5g.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 10min, is mixed
Liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, and 130 DEG C of heating temperature,
Obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by nitrile rubber powder,
In ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, ultrasonic vibration 10min obtains mixed liquor C；(6) by mixed liquid B, mixing
Liquid C, polystyrene, butanediol laurate are put into reaction kettle, heated sealed stirring, 110 DEG C of heating temperature, cooling, filling,
To obtain the final product.
Embodiment 3
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, including following raw material: deionized water 22g, ethylene glycol 11g,
Natural emulsion 28g, polyisoprene 4g, polypropylene fibre 3g, polystyrene 2g, nonylphenol polyoxyethylene ether 12g, polyacrylamide
Amine 1g, lauryl sodium sulfate 0.5g, nitrile rubber 12g, butanediol laurate 2g.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 6min, is mixed
Liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, and 115 DEG C of heating temperature,
Obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by nitrile rubber powder,
In ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, ultrasonic vibration 6min obtains mixed liquor C；(6) by mixed liquid B, mixing
Liquid C, polystyrene, butanediol laurate are put into reaction kettle, heated sealed stirring, 95 DEG C of heating temperature, cooling, filling,
To obtain the final product.
Embodiment 4
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, including following raw material: deionized water 28g, ethylene glycol 14g,
Natural emulsion 32g, polyisoprene 6g, polypropylene fibre 5g, polystyrene 4g, nonylphenol polyoxyethylene ether 18g, polyacrylamide
Amine 2g, lauryl sodium sulfate 1.2g, nitrile rubber 18g, butanediol laurate 4g.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 8min, is mixed
Liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, and 125 DEG C of heating temperature,
Obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by nitrile rubber powder,
In ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, ultrasonic vibration 9min obtains mixed liquor C；(6) by mixed liquid B, mixing
Liquid C, polystyrene, butanediol laurate are put into reaction kettle, heated sealed stirring, 105 DEG C of heating temperature, cooling, filling,
To obtain the final product.
Embodiment 5
A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, including following raw material: deionized water 25g, ethylene glycol 12g,
Natural emulsion 30g, polyisoprene 5g, polypropylene fibre 4g, polystyrene 3g, nonylphenol polyoxyethylene ether 15g, polyacrylamide
Amine 1.5g, lauryl sodium sulfate 1g, nitrile rubber 15g, butanediol laurate 3g.
A kind of preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, comprising the following steps: (1) weigh each component
Raw material, it is spare；(2) by lauryl sodium sulfate, polyacrylamide investment deionized water, microwave shakes 8min, is mixed
Liquid A；(3) by natural emulsion, polyisoprene, mixed liquor A investment reaction kettle, heated sealed is stirred, and 120 DEG C of heating temperature,
Obtain mixed liquid B；(4) nitrile rubber is put into micronizer, nitrile rubber powder is made；(5) by nitrile rubber powder,
In ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, ultrasonic vibration 8min obtains mixed liquor C；(6) by mixed liquid B, mixing
Liquid C, polystyrene, butanediol laurate are put into reaction kettle, heated sealed stirring, 100 DEG C of heating temperature, cooling, filling,
To obtain the final product.
Embodiment 1-5 and commercial product are subjected to test experiments, the experimental results are shown inthe following table:
Table 1: tyre repairing fluid test result record sheet
| Flame retardant property | To the corrosivity of wheel hub | |
| Embodiment 1 | Significantly | Slight erosion |
| Embodiment 2 | Significantly | Slight erosion |
| Embodiment 3 | Significantly | It is unobvious |
| Embodiment 4 | Significantly | It is unobvious |
| Embodiment 5 | Significantly | It is corrosion-free |
| Commercial product | It is poor | Obvious corrosion |
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
Various changes can be made.
Claims (8)
1. a kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature, which is characterized in that the raw material including following parts by weight: go from
Sub- water 20-30 parts, it is 10-15 parts of ethylene glycol, 25-35 parts of natural emulsion, 3-8 parts of polyisoprene, 2-6 parts of polypropylene fibre, poly-
1-5 parts of styrene, 10-20 parts of nonylphenol polyoxyethylene ether, 0.5-2.5 parts of polyacrylamide, lauryl sodium sulfate 0.2-1.5
Part, 10-20 parts of nitrile rubber, 1-5 parts of butanediol laurate.
2. explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 1, which is characterized in that including following weight
The raw material of number: 22-28 parts of deionized water, 11-14 parts of ethylene glycol, 28-32 parts of natural emulsion, 4-6 parts of polyisoprene, poly- third
3-5 parts of alkene fiber, 2-4 parts of polystyrene, 12-18 parts of nonylphenol polyoxyethylene ether, 1-2 parts of polyacrylamide, dodecyl sulphur
Sour sodium 0.5-1.2 parts, 12-18 parts of nitrile rubber, 2-4 parts of butanediol laurate.
3. explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 1, which is characterized in that including following weight
The raw material of number: 25 parts of deionized water, 12 parts of ethylene glycol, 30 parts of natural emulsion, 5 parts of polyisoprene, 4 parts of polypropylene fibre,
3 parts of polystyrene, 15 parts of nonylphenol polyoxyethylene ether, 1.5 parts of polyacrylamide, 1 part of lauryl sodium sulfate, nitrile rubber 15
Part, 3 parts of butanediol laurate.
4. a kind of preparation method of explosion-proof flame-retardant according to claim 1 to 3 type tire repair liquid resistant to high temperature,
It is characterized in that, comprising the following steps: (1) each component raw material is weighed, it is spare；(2) lauryl sodium sulfate, polyacrylamide are thrown
Enter in deionized water, microwave shakes 5-10min, obtains mixed liquor A；(3) natural emulsion, polyisoprene, mixed liquor A are put into
In reaction kettle, heated sealed stirring, obtains mixed liquid B by 110-130 DEG C of heating temperature；(4) nitrile rubber is put into and is pulverized
In machine, nitrile rubber powder is made；(5) by nitrile rubber powder, ethylene glycol, polypropylene fibre investment ultrasonic vibration instrument, surpass
5-10min is swung in acoustic shock, obtains mixed liquor C；(6) mixed liquid B, mixed liquor C, polystyrene, butanediol laurate are put into anti-
Answer in kettle, heated sealed stirring is 90-110 DEG C of heating temperature, cooling, it is filling to get.
5. the preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 4, which is characterized in that step
Suddenly in (2), microwave shakes the time for 8min.
6. the preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 4, which is characterized in that step
Suddenly in (3), heating temperature is 120 DEG C.
7. the preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 4, which is characterized in that step
Suddenly in (5), the time of ultrasonic vibration is 8min.
8. the preparation method of explosion-proof flame-retardant type tire repair liquid resistant to high temperature according to claim 4, which is characterized in that step
Suddenly in (6), heating temperature is 100 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910583290.XA CN110283555A (en) | 2019-07-01 | 2019-07-01 | A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910583290.XA CN110283555A (en) | 2019-07-01 | 2019-07-01 | A kind of explosion-proof flame-retardant type tire repair liquid resistant to high temperature and preparation method thereof |
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| CN101602932A (en) * | 2009-07-20 | 2009-12-16 | 郑燕梅 | Tire repair filling liquid and preparation method thereof |
| CN102197105A (en) * | 2008-10-24 | 2011-09-21 | 株式会社普利司通 | Puncture-sealing agent manufacturing method |
| CN104364340A (en) * | 2012-06-27 | 2015-02-18 | 住友橡胶工业株式会社 | Puncture sealing agent |
| CN106109259A (en) * | 2016-07-08 | 2016-11-16 | 拉芳家化股份有限公司 | A kind of shampoo bath gel preventing stink with perspiration |
| CN106318283A (en) * | 2016-08-23 | 2017-01-11 | 广东普士通实业有限公司 | Automatic tire repair liquid |
| CN106883790A (en) * | 2017-04-20 | 2017-06-23 | 深圳市爱动科技有限公司 | A kind of emergency repair of tire liquid and preparation method thereof |
| CN108047510A (en) * | 2017-12-29 | 2018-05-18 | 杭州方周科技有限公司 | A kind of car tyre repairing fluid and preparation method thereof |
| CN108531108A (en) * | 2018-03-22 | 2018-09-14 | 杭州方周科技有限公司 | A kind of low ammonia automobile tyre repairing fluid and preparation method thereof |
-
2019
- 2019-07-01 CN CN201910583290.XA patent/CN110283555A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1717465A (en) * | 2002-11-27 | 2006-01-04 | 株式会社普利司通 | Puncture sealing agent |
| CN102197105A (en) * | 2008-10-24 | 2011-09-21 | 株式会社普利司通 | Puncture-sealing agent manufacturing method |
| CN101602932A (en) * | 2009-07-20 | 2009-12-16 | 郑燕梅 | Tire repair filling liquid and preparation method thereof |
| CN104364340A (en) * | 2012-06-27 | 2015-02-18 | 住友橡胶工业株式会社 | Puncture sealing agent |
| CN106109259A (en) * | 2016-07-08 | 2016-11-16 | 拉芳家化股份有限公司 | A kind of shampoo bath gel preventing stink with perspiration |
| CN106318283A (en) * | 2016-08-23 | 2017-01-11 | 广东普士通实业有限公司 | Automatic tire repair liquid |
| CN106883790A (en) * | 2017-04-20 | 2017-06-23 | 深圳市爱动科技有限公司 | A kind of emergency repair of tire liquid and preparation method thereof |
| CN108047510A (en) * | 2017-12-29 | 2018-05-18 | 杭州方周科技有限公司 | A kind of car tyre repairing fluid and preparation method thereof |
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Application publication date: 20190927 |
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