CN110037334A - It is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application - Google Patents

Abstract

The present invention relates to it is a kind of can lifting electrical heating do not burn the rich essence of cigarette flavor and its application, above-mentioned essence is made of following raw material: 8-15 parts of mixed essential oil, 5-8 parts of bergamot oil, 5-8 parts of orange oil, 1-4 parts of mace oil, 30-40 parts of glycerol, 10-40 parts of alcohol, and total weight number is 100 parts.Mixed essential oil, bergamot oil, orange oil, mace oil etc. is selected to be used as raw material in the present invention, so that essence has the characteristics that smell aromatic and nature, to preferably coordinate with cigarette perfume；Mixed essential oil is obtained through subcritical abstraction in the present invention, so that essential oil quality is pure, smell it is fragrant it is abundant, naturally, be applied to electric heating do not burn cigarette when can eliminate conventional extract residual sense in bring oral cavity in suction, so that mouthfeel is pure, comfortable, so as to improve suction impression.

Description

A kind of flavor that can enhance the aroma richness of electric heating non-burning cigarette and its application

technical field

The invention relates to the technical field of tobacco, in particular to an essence that can enhance the aroma richness of electrically heated non-burning cigarettes and its application.

Background technique

Electric heat-not-burn cigarettes are the hottest new tobacco products in the world in recent years. Different from the electronic cigarette's "use electronic devices to heat e-liquid, and inhale after atomization", it is "use electronic devices to heat tobacco raw materials, and inhale after smoking". Heat-not-burn pods still belong to the category of "cigarettes", but they must be smoked with the cooperation of "electronic" smoking equipment.

It is also smoke inhalation. Traditional cigarettes are smoked after igniting tobacco raw materials. The temperature of the cigarette butt varies between 600 °C and 900 °C. Thousands of components in the tobacco raw materials undergo extremely complex physical and chemical reactions, and the temperature is uncontrollable. The products of various oxidation reactions, reduction reactions, and cracking reactions are even more uncontrollable; and electronic heaters that electrically heat non-burning cigarettes can accurately control the temperature at around 300 °C, the composition of the flue gas is relatively controllable, and the harmful substances are relatively Much less.

Because electric heating non-burning cigarettes mainly generate smoke to meet the needs of smokers, but because the smoke components of electric heating non-burning cigarettes are simpler than traditional cigarettes, it will inevitably cause problems such as poor oral comfort, bitterness, and insufficient aroma. Therefore, the role of the added flavor is particularly critical.

SUMMARY OF THE INVENTION

In view of the above-mentioned problems in the development of rolling, an essence that can enhance the aroma richness of electric heating non-burning cigarettes and its application are provided, aiming to effectively increase the aroma of cigarettes, reduce the bitterness of the mouth, and improve the sweetness of the mouth.

The specific technical solutions are as follows:

The first aspect of the present invention is to provide a kind of essence that can enhance the aroma richness of electric heating non-burning cigarettes, which has the characteristics of being composed of the following raw materials in parts by weight: 8-15 parts of mixed essential oils, 5-8 parts of bergamot oil , 5-8 parts of sweet orange oil, 1-4 parts of nutmeg oil, 30-40 parts of glycerin, 10-40 parts of alcohol, and the total parts by weight are 100 parts;

Among them, the mixed essential oil is extracted from chamomile and jasmine.

The above-mentioned essence also has such a feature, and the preparation method of the mixed essential oil is: the dried chamomile flower and the dried flower of jasmine are mixed and pulverized into flower powder, the flower powder is added to water and ultrasonically treated, and then mixed enzyme is added to it, and then ultrasonically treated. Under enzymatic hydrolysis, an extractant is added to the enzymatically hydrolyzed feed liquid to carry out subcritical extraction, and the extracted feed liquid is subjected to vacuum distillation, centrifugal separation and filtration to obtain mixed essential oils.

The above-mentioned essence also has the feature that the dried chamomile flowers and the dried flowers of jasmine are mixed in a mass ratio of 1:1 and then pulverized into flower powder with a particle size of 80 meshes.

The above-mentioned essence also has the feature that the flower powder and water are mixed in a mass-volume ratio of 1:2-3 and ultrasonically treated for 10-15min before adding the mixed enzyme.

The above-mentioned essence also has the characteristics that the mass-volume ratio of mixed enzyme and water is 1:10, and the enzymolysis time is 50-70min.

The above-mentioned essence also has the feature that the mixed enzyme is formed by mixing protease and cellulase in a mass ratio of 1:1.

The above-mentioned essence also has the feature that the mass-volume ratio of the flower powder and the extractant is 1:6-10.

The above-mentioned essence also has the feature that the extractant is selected from one or more of propane, butane or isobutane.

The above-mentioned essence also has the characteristics that the subcritical extraction temperature is 50-100° C., the extraction pressure is 1-1.5Mpa, and the extraction time is 1-1.5h.

In the present invention, the ultrasonic processing power is 150-200w, and the frequency is 20-400Hz.

The second aspect of the present invention is to provide an application of an essence in cigarettes, which has the characteristics that the essence is added to the cut tobacco in an amount of 0.05-0.10% by weight of the cut tobacco.

The beneficial effects of the above scheme are:

1), select mixed essential oil, bergamot oil, sweet orange oil, nutmeg oil etc. as raw material in the present invention, make the essence have the characteristics of mellow and natural smell, thereby better coordinate with the smoke incense;

2), the mixed essential oil in the present invention is obtained through subcritical extraction, the essential oil in the present invention is of pure quality, rich and natural in smell, and can eliminate the residual feeling in the mouth that conventional extracts bring during smoking when applied to electrically heated non-burning cigarettes , making the taste pure and comfortable, thereby improving the suction experience.

Detailed ways

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.

It should be noted that the embodiments of the present invention and the features of the embodiments may be combined with each other under the condition of no conflict.

The present invention will be further described below in conjunction with specific embodiments, but not as a limitation of the present invention.

Example 1

An essence that can enhance the aroma richness of electric heating non-burning cigarettes, the preparation of which comprises the following steps: weighing 15 parts of mixed essential oils, 5 parts of bergamot oil, 5 parts of sweet orange oil, 1 part of nutmeg oil, 34 parts of glycerin, 40 parts of alcohol, add alcohol and glycerin into the mixing tank in turn and stir for 20min, then add the rest of the components to the mixing tank, stir for 2.5h, let stand for 2d, and then filter out the sediment with a filter membrane with a pore size of 0.8μm. The filtrate obtains an essence that can enhance the aroma richness of electric heating non-burning cigarettes;

Wherein, the preparation method of the mixed essential oil is as follows: the dried flowers of chamomile and the dried flowers of jasmine are mixed in a mass ratio of 1:1 and then pulverized into flower powder, and the flower powder and water are mixed in a mass ratio of 1:2 and ultrasonically treated for 10 minutes. Then add mixed enzyme (mixed enzyme is formed by mixing protease and cellulase in a mass ratio of 1:1, and the mass-volume ratio of mixed enzyme and water is 1:10), and then enzymatically hydrolyzed for 50min under the action of ultrasound, Add extractant (propane, the mass-volume ratio of flower powder and propane is 1:6) to the feed liquid after enzymolysis to carry out subcritical extraction (subcritical extraction temperature is 50°C, extraction pressure is 1Mpa, extraction time is 1h) , the extracted feed liquid is distilled under reduced pressure, centrifuged and filtered to obtain mixed essential oils.

In the present invention, the GC-MS method is used to detect the essence components.

GC conditions: chromatographic column: medium polar elastic quartz capillary column, the stationary phase is (14% cyanopropyl)-methyl polysiloxane, 30m×0.25mm×0.25μm.

MS conditions: ion source: EI source; ion source temperature: 230° C.; electron energy: 70 eV; scan mode: full scan.

The results show that more aroma substances are produced in the essence provided by the invention, and the specific substances and contents that are increased are shown in the following table:

Chemical Name content(%) Fragrance myrcene 0.21 Light balsamic aroma Caryophyllene 0.1 Mild clove-like aroma Linalool 0.31 lily-of-the-valley fragrance Jasmine 0.09 celery seed-like aroma

As can be seen from the above table, the essence provided by the present invention has added a large number of components with very natural fragrance and mellow fragrance, so that the aroma of the essence can be greatly enriched, and the essence has the characteristics of mellow and natural smell.

In the present invention, the essence obtained in the above embodiment is diluted with 70% ethanol and directly sprayed on the cut tobacco made from reconstituted tobacco leaves, placed in a drying oven at 40° C. for 2 hours, and then made into a new type of electric heating non-burning cigarette, wherein, Flavor in cigarettes accounts for 0.05% of the weight of cut tobacco.

In the present invention, the above-mentioned new electric heating non-burning cigarettes and conventional commercially available electric heating non-burning cigarettes without adding the flavor provided by the present invention are evaluated by a group of 9 people. The smoking results show that the electric heating non-burning cigarette provided by the present invention obviously increases the rich floral aroma compared with the conventional electric heating non-combusting cigarette, and slightly reduces the bitterness in the mouth, and the taste is pure and comfortable when smoking.

Example 2

An essence that can enhance the aroma richness of electric heating non-burning cigarettes, the preparation of which comprises the following steps: weighing 11 parts of mixed essential oils, 6 parts of bergamot oil, 8 parts of sweet orange oil, 3 parts of nutmeg oil, 40 parts of glycerin, 32 parts of alcohol, add alcohol and glycerin into the mixing tank in turn and stir for 20min, then add the remaining components to the mixing tank, stir for 2.5h, let stand for 2d, and then filter the sediment with a filter membrane with a pore size of 0.8μm. The filtrate is an essence that can enhance the aroma richness of electric heating non-burning cigarettes;

Wherein, the preparation method of the mixed essential oil is as follows: the dried flowers of chamomile and the dried flowers of jasmine are mixed in a mass ratio of 1:1 and then pulverized into rear flower powder, and the flower powder and water are mixed in a mass volume ratio of 1:2.5 and ultrasonically treated for 13 minutes. Then add mixed enzyme (mixed enzyme is formed by mixing protease and cellulase in a mass ratio of 1:1, and the mass-volume ratio of mixed enzyme and water is 1:10), and then enzymolysis for 60min under the action of ultrasound, to Add extraction agent (propane, the mass volume ratio of flower powder and propane is 1:8) to the feed liquid after enzymolysis, and carry out subcritical extraction (subcritical extraction temperature is 70°C, extraction pressure is 1.2Mpa, extraction time is 1.3 h), the feed liquid after extraction obtains mixed essential oils through vacuum distillation, centrifugal separation, and filtration.

In the present embodiment, with reference to the test method in Example 1, the essence composition is detected, and the results show that more aroma substances have been produced in the essence provided by the invention, and the increased specific substances and contents are shown in the following table:

Chemical Name content(%) Fragrance myrcene 0.01 Light balsamic aroma Caryophyllene 0.05 Mild clove-like aroma Linalool 0.23 lily-of-the-valley fragrance Jasmine 0.19 celery seed-like aroma

As can be seen from the above table, the essence provided by the present invention has added a large number of components with very natural fragrance and mellow fragrance, so that the aroma of the essence can be greatly enriched, and the essence has the characteristics of mellow and natural smell.

In the present invention, the essence obtained in the above-mentioned embodiment is diluted with 70% ethanol and directly sprayed on the cut tobacco made from reconstituted tobacco leaves, placed in a drying oven at 40° C. for 3 hours, and then made into a new type of electric heating non-burning cigarette, wherein, Flavor in cigarettes accounts for 0.08% of the weight of cut tobacco.

In the present invention, the above-mentioned new electric heating non-burning cigarettes and conventional commercially available electric heating non-burning cigarettes without adding the flavor provided by the present invention are evaluated by a group of 9 people. The smoking results show that the electric heating non-burning cigarette provided by the present invention obviously increases the rich floral aroma compared with the conventional electric heating non-combusting cigarette, and slightly reduces the bitterness in the mouth, and the taste is pure and comfortable when smoking.

Example 3

An essence that can enhance the aroma richness of electric heating non-burning cigarettes, the preparation of which comprises the following steps: weighing 8 parts of mixed essential oil, 7 parts of bergamot oil, 8 parts of sweet orange oil, 4 parts of nutmeg oil, 37 parts of glycerin, 36 parts of alcohol, add alcohol and glycerin into the mixing tank in turn and stir for 20min, add the rest of the components to the mixing tank, stir for 2.5h, let stand for 2d, and then filter the sediment with a filter membrane with a pore size of 0.8μm. The filtrate obtains an essence that can enhance the aroma richness of electric heating non-burning cigarettes;

Wherein, the preparation method of the mixed essential oil is as follows: the dried flowers of chamomile and the dried flowers of jasmine are mixed in a mass ratio of 1:1 and then pulverized into flower powder, and the flower powder and water are mixed with a mass ratio of 1:2 and ultrasonically treated for 15 minutes. Then add mixed enzyme (mixed enzyme is formed by mixing protease and cellulase in a mass ratio of 1:1, and the mass-volume ratio of mixed enzyme and water is 1:10), and then enzymatically hydrolyzed for 50min under the action of ultrasound, Add extractant (propane, the mass-volume ratio of flower powder and propane is 1:10) to the feed liquid after enzymolysis to carry out subcritical extraction (subcritical extraction temperature is 100°C, extraction pressure is 1.5Mpa, extraction time is 1.5 h), the feed liquid after extraction obtains mixed essential oils through vacuum distillation, centrifugal separation, and filtration.

In the present embodiment, with reference to the test method in Example 1, the essence composition is detected, and the results show that more aroma substances have been produced in the essence provided by the invention, and the increased specific substances and contents are shown in the following table:

As can be seen from the above table, the essence provided by the present invention has added a large number of components with very natural fragrance and mellow fragrance, so that the aroma of the essence can be greatly enriched, and the essence has the characteristics of mellow and natural smell.

In the present invention, the essence obtained in the above-mentioned embodiment is diluted with 70% ethanol and sprayed directly on the cut tobacco made from reconstituted tobacco leaves, placed in a drying oven at 40° C. for 4 hours, and then made into a new type of cigarette that does not burn by electric heating, wherein , the flavor in the cigarette accounts for 0.10% of the weight of the cut tobacco.

In the present invention, the above-mentioned new electric heating non-burning cigarettes and conventional commercially available electric heating non-burning cigarettes without adding the flavor provided by the present invention are evaluated by a group of 9 people. The smoking results show that the electric heat not burn cigarette provided by the present invention obviously increases the strong floral aroma and slightly reduces the bitterness in the mouth compared with the conventional commercial electric heat not burn cigarette.

The above are only preferred embodiments of the present invention, and are not intended to limit the embodiments and protection scope of the present invention. Those skilled in the art should be aware of the equivalent replacements and obvious changes made by using the contents of the description of the present invention. The obtained solutions should all be included in the protection scope of the present invention.

Claims (10)

1. one kind can lifting electrical heating do not burn the rich essence of cigarette flavor, which is characterized in that by following raw material Composition: 8-15 parts of mixed essential oil, 5-8 parts of bergamot oil, 5-8 parts of orange oil, 1-4 parts of mace oil, 30-40 parts of glycerol, alcohol 10-40 parts, total weight number is 100 parts；

Wherein, the mixed essential oil is obtained by chamomile and Jasmine extraction.

2. essence according to claim 1, which is characterized in that the mixed essential oil the preparation method comprises the following steps: chamomile is done It is ground into after the mixing of colored and dry jasmine flower and spends end, end will be spent to be added to the water and mixed enzyme is added thereto again after being ultrasonically treated, It is digested under ultrasonication again, extractant is added into the feed liquid after enzymatic hydrolysis and carries out subcritical abstraction, feed liquid extracted is through subtracting The mixed essential oil is distilled, is centrifugated, filtering and to be obtained to pressure.

3. essence according to claim 2, which is characterized in that by chamomile dried flower and dry jasmine flower be in mass ratio 1: It is ground into after 1 mixing and spends end.

4. essence according to claim 2, which is characterized in that end will be spent to mix simultaneously by mass volume ratio for 1:2-3 with water Mixed enzyme is added thereto again after ultrasonic treatment 10-15min.

5. essence according to claim 3, which is characterized in that the mass volume ratio of mixed enzyme and water is 1:10, when enzymatic hydrolysis Between be 50-70min.

6. essence according to claim 5, which is characterized in that the mixed enzyme by protease and cellulase in mass ratio It is mixed for 1:1.

7. essence according to claim 2, which is characterized in that the mass volume ratio of Hua Moyu extractant is 1:6-10.

8. essence according to claim 7, which is characterized in that extractant is selected from one of propane, butane or iso-butane Or it is several.

9. essence according to claim 2, which is characterized in that subcritical abstraction temperature is 50-100 DEG C, extracting pressure is 1-1.5Mpa, extraction time 1-1.5h.

10. application of the essence described in claim 1 in cigarette, which is characterized in that essence adds in the tobacco, and additive amount is cigarette The 0.05-0.10% of silk weight.