CN109897446A - A kind of special-purpose aqueous colorful ink of paper for daily use and preparation method thereof - Google Patents
A kind of special-purpose aqueous colorful ink of paper for daily use and preparation method thereof Download PDFInfo
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- CN109897446A CN109897446A CN201910167703.6A CN201910167703A CN109897446A CN 109897446 A CN109897446 A CN 109897446A CN 201910167703 A CN201910167703 A CN 201910167703A CN 109897446 A CN109897446 A CN 109897446A
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- 239000001772 cananga odorata hook. f. and thomas. oil Substances 0.000 claims description 2
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- ORAKUVXRZWMARG-WZLJTJAWSA-N lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C ORAKUVXRZWMARG-WZLJTJAWSA-N 0.000 claims description 2
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- KINGXFAMZNIVNL-SXQDSXCISA-N safflor yellow A Natural products OC[C@@H]1O[C@H]2[C@H](OC3=C2C(=O)C(=C(O)C=Cc4ccc(O)cc4)C(=O)[C@]3(O)[C@@H]5O[C@H](CO)[C@@H](O)[C@H](O)[C@H]5O)[C@@H](O)[C@H]1O KINGXFAMZNIVNL-SXQDSXCISA-N 0.000 claims description 2
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- 229940113147 shellac Drugs 0.000 claims description 2
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- HWDGVJUIHRPKFR-UHFFFAOYSA-I copper;trisodium;18-(2-carboxylatoethyl)-20-(carboxylatomethyl)-12-ethenyl-7-ethyl-3,8,13,17-tetramethyl-17,18-dihydroporphyrin-21,23-diide-2-carboxylate Chemical compound [Na+].[Na+].[Na+].[Cu+2].N1=C(C(CC([O-])=O)=C2C(C(C)C(C=C3C(=C(C=C)C(=C4)[N-]3)C)=N2)CCC([O-])=O)C(=C([O-])[O-])C(C)=C1C=C1C(CC)=C(C)C4=N1 HWDGVJUIHRPKFR-UHFFFAOYSA-I 0.000 description 3
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Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicinal Preparation (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses special-purpose aqueous colorful ink of a kind of paper for daily use and preparation method thereof, by following raw material: 5~10.5 parts of binder, 0.4~6 part of edible natural pigment, 1~6 part of powdered activated carbon and 40~100 parts of deionized water are made.The preparation of the special-purpose aqueous colorful ink of paper for daily use is to be uniformly mixed edible natural pigment, binder with deionized water respectively, then obtains the special-purpose aqueous colorful ink of paper for daily use after mixing.The present invention avoids the use of toxic organic solvent using deionized water as solvent, improves the safety of water-based ink；Meet the requirement of environmental protection, safety using edible natural pigment；Product preparation is not difficult, and is suitable for production scene and produces preparation in enormous quantities；This product good penetrability, cohesive force are strong, are not easy to decolourize, applied to the pattern printing of all paper for daily use products, coating, spraying, laminated etc..
Description
Technical field
The invention belongs to paper for daily use manufacture and manufacture field, be related to a kind of special-purpose aqueous colorful ink of paper for daily use and its
Preparation method.
Background technique
The water-based ink technical security of paper for daily use at present, at home there are no enough attention is obtained, life on the market
It applies flexibly paper and largely uses common water borne ink or chemical synthesis pigment, be extremely difficult to the edible correlation of environmental protection, safety
Standard influences the health of people, limits the development of coloured paper for daily use.
Especially novel stamp, embossing paper for daily use, for the personalization of product, surface decoration effect much stronger than tradition
Pure white, true qualities paper for daily use using edible material is fully achieved on novel stamp, embossing paper for daily use be one
A new theory is attempted and a new extremely attractive market opportunity.Edible paper for daily use water-based ink it may be said that
It is a kind of new green environment protection water-based ink, because its ingredient is all made of edible material, printing, coating or spraying can be passed through
Mode is transferred to paper for daily use surface, has more wide application prospect.
Summary of the invention
Based on current paper for daily use water-based ink there are the problem of, the object of the present invention is to provide a kind of paper for daily use is dedicated
Aqueous colorful ink and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 5~10.5 parts of binder, edible day
Right 0.4~6 part of pigment, 1~6 part of powdered activated carbon, 40~100 parts of deionized water be made；
Further, the binder is medicinal or edible grade shellac, gum arabic, gum tragacanth, water soluble shells are gathered
Sugar, gelatin, bean gum, at least two kinds in water soluble acrylic resin；
Further, the edible natural pigment is pure plant, animal, extracts main coloring agent: leaf in microorganism
It is green element copper sodium, gardenia blue, Gardenia Yellow, algae indigo plant, red yeast rice Huang, turmeric, annatto, alkermes, bata-carotene, chrysanthemum,
At least two kinds in lutein, safflower yellow；
Further, the powdered activated carbon is the active carbon that high-quality timber and shell manufacture；
Further, this special-purpose aqueous colorful ink also includes 0.001~0.01 part of natural essential oil；
Further, the natural essential oil include lemongrass oil, rock attar of rose, sandalwood oil, sage oil, jasmine oil, attar of rose,
At least one of Java Cananga Oil, sandalwood oil and tangerine oil.
A kind of preparation method of the special-purpose aqueous colorful ink of paper for daily use, includes the following steps:
One, the preparation of outer ink
(1) it is added in dissolution kettle in 10~30 parts of deionized waters, stirring is slowly added into 0.2~4 part of edible natural pigment, stirs
It is spare uniformly to obtain pigment solution；
(2) 20~40 parts of deionized waters are added in dissolution kettle, are warming up to 40~50 DEG C, 5~10 parts of binders are added in stirring, stir
It mixes and is uniformly dissolved, filtering removal insoluble impurities obtains binder solution；
(3) the binder solution of step (2) is stirred, is slowly added into the pigment solution of step (1), is uniformly mixed, obtains
Paper for daily use water-based ink A material is spare；
Two, the preparation of interior ink
(1) 0.1~2 part and 10~30 parts of deionized waters stirrings for mixing chitosan aqueous solution or/and gelatin with arbitrary proportion
The mixing package slurry being mixed into is spare；
(2) 0.2~2 part of edible natural pigment is uniformly mixed with 1~6 part of powdered activated carbon spare；Or it is stirring again
Under conditions of be added by spraying 0.001~0.01 part of natural essential oil be uniformly mixed, obtain natural pigment active carbon or/and natural essential oil
Active carbon, then the chitosan aqueous solution or/and gelatin mixed solution of step (1) is added by spraying under stirring conditions, it is given birth to
Apply flexibly paper water-based ink B material；
Three, the preparation of colorful ink
Under stirring conditions by the paper for daily use water-based ink A material of step 1 preparation, it is slowly added into the life of step 2 preparation
Expected with paper water-based ink B, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
The revolving speed of the above stirring is 40~60 turns per minute.
A kind of special-purpose aqueous colorful ink of paper for daily use is applied to the box including bleaching or true qualities and takes out, soft pumping, tissue, defends
Pattern printing, coating, the spraying, laminated of raw paper, paper for kitchen, tissue product.
Compared with prior art, the present invention have it is following the utility model has the advantages that
(1) the special-purpose aqueous colorful ink of paper for daily use of the invention is using deionized water as solvent, avoids toxic organic molten
The use of agent improves the safety of water-based ink；
(2) the special-purpose aqueous colorful ink of paper for daily use of the invention meets environmental protection, safety using edible natural pigment as colouring material
Requirement；
(3) the special-purpose aqueous colorful ink of paper for daily use of the invention is deep can adsorb the active carbon of natural pigment and natural essential oil
The fixed material of color or/and natural essential oil, can make the printed patterns of paper for daily use product constitute colorful pattern, can also slow release it is natural
Essential oil fragrance.
(4) the special-purpose aqueous colorful ink preparation of paper for daily use of the invention is not difficult, and is suitable for production scene and produces in enormous quantities
Preparation；
(5) the special-purpose aqueous colorful ink of paper for daily use of the invention can constitute that colorful pattern, good penetrability, cohesive force are strong, are not easy
Decoloration can be applied to the lives such as box pumping, soft pumping, tissue, toilet paper, paper for kitchen, the tissue of market bleach or true qualities use
The production technologies such as the pattern printing of paper product, laminated.
Specific embodiment
The present invention is described in detail combined with specific embodiments below.Following embodiment will be helpful to the technology of this field
Personnel further understand invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill people of this field
For member, without departing from the inventive concept of the premise, various modifications and improvements can be made.These belong to of the invention
Protection scope.
Embodiment 1
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 4 parts of binder gum arabic, water solubility
1 part of chitosan, 1 part of edible natural pigment Gardenia Yellow, 0.3 part of alkermes, 5 parts of powdered activated carbon, 80 parts of deionized water are made；
The preparation method is as follows:
One, the preparation of outer ink
(1) it is added in dissolution kettle in 20 parts of deionized waters, is warming up to 45 DEG C, stirred with 60 turns per minute, be slowly added into Gardenia Yellow 1
Part edible natural pigment, it is spare to be uniformly mixing to obtain pigment solution；
(2) 40 parts of deionized waters are added in dissolution kettle, are warming up to 45 DEG C, gum arabic 4 is added with 60 turns of stirrings per minute
Part binder, stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) the binder solution of step (2) is molten, with temperature 45 C, 60 turns of stirrings per minute, it is slowly added into the color of step (1)
Plain solution, is uniformly mixed, and it is spare to obtain paper for daily use water-based ink A material；
Two, the preparation of interior ink
(1) 1 part of water soluble chitosan is added in dissolution kettle with 20 parts of deionized waters, is warming up to 45 DEG C, is stirred with 60 turns per minute
It is spare to mix the mixing package slurry being mixed into；
(2) 0.3 part of edible natural pigment of alkermes is stirred with 5 parts of powdered activated carbons mixed with temperature 45 C, 60 turns per minute it is mixed
It closes uniformly, obtains natural pigment active carbon, then step (1) is added by spraying under conditions of temperature 45 C, 60 turns of stirrings per minute
Package slurry, obtain paper for daily use water-based ink B material；
Three, the preparation of colorful ink
By step 1 preparation paper for daily use water-based ink A expect under conditions of temperature 45 C, 60 turns of stirrings per minute, slowly plus
The paper for daily use water-based ink B material for entering step 2 preparation, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
Embodiment 2
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 3 parts of binder gum tragacanth, gelatin 1.5
Part, 1 part of water soluble chitosan, 3 parts of edible natural pigment Gardenia Yellow, 1.5 parts of sodium copper chlorophyllin, 4 parts of powdered activated carbon, go from
86 parts of sub- water is made；
The preparation method is as follows:
One, the preparation of outer ink
(1) 30 parts of deionized waters are added in dissolution kettle, with temperature 50 C, 50 turns of stirrings per minute, are slowly added into copper chlorophyll
1.5 parts of edible natural pigments of sodium salt, it is spare to be uniformly mixing to obtain pigment solution；
(2) 40 parts of deionized waters are added in dissolution kettles, are warming up to 50 DEG C, with 50 turns of stirrings per minute addition, 3 parts of gum tragacanth,
1 part of part binder of gelatin, stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) the binder solution of step (2) is mixed with temperature 50 C, 50 turns per minute, the pigment for being slowly added into step (1) is molten
Liquid is uniformly mixed, and it is spare to obtain paper for daily use water-based ink A material；
Two, the preparation of interior ink
(1) 1 part of water soluble chitosan and 0.5 part of gelatin are added in dissolution kettle with 16 parts of deionized waters, with temperature 50 C, every point
50 turns of the clock mixing package slurries being uniformly mixed are spare；
(2) 3 parts of edible natural pigments of Gardenia Yellow and 4 parts of powdered activated carbons are added in dissolution kettle, with temperature 50 C, per minute 50
Turn to be uniformly mixed, obtains natural pigment active carbon, then be added by spraying under conditions of temperature 50 C, 50 turns of stirrings per minute
The package slurry of step (1) obtains paper for daily use water-based ink B material；
Three, the preparation of colorful ink
By step 1 preparation paper for daily use water-based ink A expect under conditions of temperature 50 C, 50 turns of stirrings per minute, slowly plus
The paper for daily use water-based ink B material for entering step 2 preparation, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
Embodiment 3
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 3 parts of binder gum arabic, gelatin 1.5
Part, 1.5 parts of water soluble chitosan, 0.4 part of edible natural pigment turmeric, 1.5 parts of gardenia blue, natural essential oil lemongrass oil 0.005
Part, 5 parts of powdered activated carbon, 80 parts of deionized water are made；
The preparation method is as follows:
One, the preparation of outer ink
(1) 30 parts of deionized waters are added in dissolution kettle, with temperature 60 C, 50 turns of stirrings per minute, are slowly added into gardenia blue 1.5
Part edible natural pigment, it is spare to be uniformly mixing to obtain pigment solution；
(2) 35 parts of deionized waters are added in dissolution kettle, are warming up to 60 DEG C, gum arabic 3 is added with 50 turns of stirrings per minute
1 part of part, gelatin part binder, stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) by the binder solution of step (2) with temperature 60 C, 50 turns of stirrings per minute, the pigment for being slowly added into step (1) is molten
Liquid is uniformly mixed, and it is spare to obtain paper for daily use water-based ink A material；
Two, the preparation of interior ink
(1) 1 part of water soluble chitosan and 0.5 part of gelatin are added in dissolution kettle with 15 parts of deionized waters, with temperature 60 C, every point
50 turns of the clock mixing package slurries being uniformly mixed are spare；
(2) 0.4 part of edible natural pigment of turmeric and 5 parts of powdered activated carbons are added in dissolution kettle, with temperature 60 C, per minute 50
Turn to be uniformly mixed, then natural essential oil lemongrass oil is added by spraying under conditions of temperature 60 C, 50 turns of stirrings per minute
It 0.005 part, is uniformly mixed, the active carbon of natural pigment active carbon and natural essential oil absorption is obtained, finally with temperature 60 C, every point
The package slurry of step (1) is added under conditions of 50 turns of clock stirrings by spraying, obtains paper for daily use water-based ink B material；
Three, the preparation of colorful ink
By step 1 preparation paper for daily use water-based ink A expect under conditions of temperature 60 C, 50 turns of stirrings per minute, slowly plus
The paper for daily use water-based ink B material for entering step 2 preparation, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
Embodiment 4
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 3 parts of binder gum arabic, water solubility
2 parts of chitosan, 0.5 part of edible natural pigment turmeric, 0.5 part of sodium copper chlorophyllin, 1 part of gardenia blue, natural essential oil sandalwood oil
0.003 part, 4 parts of powdered activated carbon, 90 parts of deionized water are made；
The preparation method is as follows:
One, the preparation of outer ink
(1) 20 parts of deionized waters are added in dissolution kettle, with temperature 50 C, 50 turns of stirrings per minute, are slowly added into copper chlorophyll
1 part of 0.5 part of sodium salt, gardenia blue edible natural pigment, it is spare to be uniformly mixing to obtain pigment solution；
(2) 60 parts of deionized waters are added in dissolution kettle, are warming up to 50 DEG C, gum arabic 3 is added with 50 turns of stirrings per minute
1 part of part, water soluble chitosan binder, stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) by the binder solution of step (2) with temperature 50 C, 50 turns of stirrings per minute, the pigment for being slowly added into step (1) is molten
Liquid is uniformly mixed, and it is spare to obtain paper for daily use water-based ink A material；
Two, the preparation of interior ink
(1) 1 part of water soluble chitosan is added in dissolution kettle with 10 parts of deionized waters, with temperature 50 C, 50 turns of stirrings per minute
The mixing package slurry being mixed into is spare；
(2) 0.5 part of edible natural pigment of turmeric and 4 parts of powdered activated carbons are added in dissolution kettle, with temperature 50 C, per minute 50
Turn to be uniformly mixed, then natural essential oil sandalwood oil 0.003 is added by spraying under conditions of temperature 50 C, 50 turns of stirrings per minute
Part, it is uniformly mixed, the active carbon of natural pigment active carbon and natural essential oil absorption is obtained, finally with temperature 50 C, per minute 50
Turn the package slurry that step (1) is added under conditions of stirring by spraying, obtains paper for daily use water-based ink B material；
Three, the preparation of colorful ink
By step 1 preparation paper for daily use water-based ink A expect under conditions of temperature 50 C, 50 turns of stirrings per minute, slowly plus
The paper for daily use water-based ink B material for entering step 2 preparation, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
Embodiment 5
A kind of special-purpose aqueous colorful ink of paper for daily use, by following raw material: 2 parts of binder gum arabic, water solubility
4 parts of chitosan, 1 part of edible natural pigment alkermes, 0.5 part of turmeric, 1.5 parts of sodium copper chlorophyllin, natural essential oil sandalwood oil
0.003 part, 6 parts of powdered activated carbon, 100 parts of deionized water are made；
The preparation method is as follows:
One, the preparation of outer ink
(1) 30 parts of deionized waters are added in dissolution kettle, with temperature 50 C, 50 turns of stirrings per minute, are slowly added into copper chlorophyll
.5 parts of edible natural pigments of sodium salt, it is spare to be uniformly mixing to obtain pigment solution；
(2) 40 parts of deionized waters are added in dissolution kettle, are warming up to 50 DEG C, gum arabic 2 is added with 50 turns of stirrings per minute
2 parts of part, water soluble chitosan binders, stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) by the binder solution of step (2) with temperature 50 C, 50 turns of stirrings per minute, the pigment for being slowly added into step (1) is molten
Liquid is uniformly mixed, and it is spare to obtain paper for daily use water-based ink A material；
Two, the preparation of interior ink
(1) 2 parts of water soluble chitosan are added in dissolution kettle with 30 parts of deionized waters, with temperature 50 C, 50 turns of stirrings per minute
The mixing package slurry being mixed into is spare；
(2) 0.5 part of edible natural pigment of turmeric and 2 parts of powdered activated carbons are added in dissolution kettle, with temperature 50 C, per minute 50
Turn to be uniformly mixed；Separately 1 part of edible natural pigment of alkermes and 2 parts of powdered activated carbons are added in dissolution kettle, with temperature
50 DEG C, 50 turns per minute are uniformly mixed；Day is added by spraying respectively under conditions of temperature 50 C, 50 turns of stirrings per minute again
Right 0.003 part of sandalwood oil of essential oil is uniformly mixed, and obtains the active carbon of natural pigment active carbon and natural essential oil absorption, finally with
The package slurry of step (1) is added under conditions of temperature 50 C, 50 turns of stirrings per minute by spraying respectively, it is aqueous to obtain paper for daily use
Double interior ink B material；
Three, the preparation of colorful ink
By step 1 preparation paper for daily use water-based ink A expect under conditions of temperature 50 C, 50 turns of stirrings per minute, slowly plus
The aqueous double interior ink B material of paper for daily use for entering step 2 preparation, are uniformly mixed, obtain the special-purpose aqueous colorful oil of paper for daily use
Ink.
Claims (7)
1. a kind of special-purpose aqueous colorful ink of paper for daily use, which is characterized in that by following raw material: binder 5~10.5
Part, 0.4~6 part of edible natural pigment, 1~6 part of powdered activated carbon, 40~100 parts of deionized water be made；
The binder is medicinal or edible grade shellac, gum arabic, gum tragacanth, water soluble chitosan, gelatin, beans
At least two kinds in glue, water soluble acrylic resin；
The edible natural pigment is pure plant, animal, extracts main coloring agent: chlorophyll copper sodium in microorganism
Salt, gardenia blue, Gardenia Yellow, algae indigo plant, red yeast rice Huang, turmeric, annatto, alkermes, bata-carotene, chrysanthemum, lutein,
At least two kinds in safflower yellow.
2. the special-purpose aqueous colorful ink of a kind of paper for daily use according to claim 1, which is characterized in that described powdered activated
Charcoal is the active carbon that high-quality timber and shell manufacture.
3. the special-purpose aqueous colorful ink of a kind of paper for daily use according to claim 1, which is characterized in that special-purpose aqueous colorful
Ink also includes 0.001~0.01 part of natural essential oil.
4. the special-purpose aqueous colorful ink of a kind of paper for daily use according to claim 3, which is characterized in that the natural essential oil
Including in lemongrass oil, rock attar of rose, sandalwood oil, sage oil, jasmine oil, attar of rose, Java Cananga Oil, sandalwood oil and tangerine oil
It is at least one.
5. a kind of preparation method of the special-purpose aqueous colorful ink of paper for daily use according to claim 1, which is characterized in that packet
Include following steps:
One, the preparation of outer ink
(1) it is added in dissolution kettle in 10~30 deionized waters, stirring, is slowly added into 0.2~4 part of edible natural pigment, stirring is equal
It is even that obtain pigment solution spare；
(2) 20~40 parts of deionized waters being added in dissolution kettle, is warming up to 40~50 DEG C, 5~10.5 parts of binders are added in stirring,
Stirring and dissolving is uniform, and filtering removal insoluble impurities obtains binder solution；
(3) by the molten stirring of binder solution of step (2), it is slowly added into the pigment solution of step (1), is uniformly mixed, is obtained
Expect to paper for daily use water-based ink A spare；
Two, the preparation of interior ink
(1) 0.1~2 part and 10~30 parts of deionized waters stirrings for mixing chitosan aqueous solution or/and gelatin with arbitrary proportion
The mixing package slurry being mixed into is spare；
(2) 0.2~2 part of edible natural pigment is uniformly mixed with 1~6 part of powdered activated carbon spare；Or it is stirring again
Under conditions of be added by spraying 0.001~0.01 part of natural essential oil be uniformly mixed, obtain natural pigment active carbon or/and natural essential oil
Active carbon, then the chitosan aqueous solution or/and gelatin mixed solution of step (1) is added by spraying under stirring conditions, it is given birth to
Apply flexibly paper water-based ink B material；
Three, the system of colorful ink
Under stirring conditions by the paper for daily use water-based ink A material of step 1 preparation, it is slowly added into the life of step 2 preparation
Expected with paper water-based ink B, is uniformly mixed, obtains the special-purpose aqueous colorful ink of paper for daily use.
6. a kind of preparation method of the special-purpose aqueous colorful ink of paper for daily use according to claim 5, which is characterized in that institute
The revolving speed for stating stirring is 40~60 turns per minute.
7. the special-purpose aqueous colorful ink of a kind of paper for daily use according to claim 1 or 5, which is characterized in that be applied to packet
Include the box pumping of bleaching or true qualities, pattern printing, coating, the spray of soft pumping, tissue, toilet paper, paper for kitchen, tissue product
It applies, laminated.
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Cited By (2)
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| CN113817357A (en) * | 2021-09-27 | 2021-12-21 | 武汉淡雅香生物科技有限公司 | Natural pigment water-based ink for cigarette tipping paper and preparation method thereof |
| WO2022110534A1 (en) * | 2020-11-27 | 2022-06-02 | 江苏唐彩新材料科技股份有限公司 | Tipping paper aqueous ink containing composite antibacterial material and preparation method therefor |
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