CN109781606B - A core holder for in-situ seepage CT scanning - Google Patents
A core holder for in-situ seepage CT scanning Download PDFInfo
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Abstract
Description
技术领域Technical Field
本发明涉及一种用于原位CT扫描的渗流实验设备,特别是涉及一种用于原位渗流CT扫描的岩心夹持器。The invention relates to a seepage experimental device for in-situ CT scanning, in particular to a core holder for in-situ seepage CT scanning.
背景技术Background Art
原位CT扫描是指在保持实验温度压力条件的情况下对样品进行实时CT扫描。目前现有的渗流实验设备中,多采用轻质铝-碳纤维复合材料夹持器,因轻质铝-碳纤维复合材料允许CT扫描的X射线通过,且不会对CT扫描过程造成很大影响,因此,轻质铝-碳纤维复合材料夹持器可以作为需要进行原位CT扫描的渗流实验中夹持样品的部件。但是这种轻质铝-碳纤维复合材料的夹持器不仅价格昂贵,而且结构复杂,接口多,易发生渗漏,夹持器必须经过改装才能与CT扫描仪配套,无法直接在CT扫描仪内实时进行流体通过岩心样品的渗流实验。In-situ CT scanning refers to real-time CT scanning of samples while maintaining the experimental temperature and pressure conditions. Currently, most of the existing seepage experimental equipment uses lightweight aluminum-carbon fiber composite material clamps, because lightweight aluminum-carbon fiber composite materials allow CT scanning X-rays to pass through and will not have a great impact on the CT scanning process. Therefore, lightweight aluminum-carbon fiber composite material clamps can be used as components for clamping samples in seepage experiments that require in-situ CT scanning. However, this lightweight aluminum-carbon fiber composite material clamp is not only expensive, but also has a complex structure, many interfaces, and is prone to leakage. The clamp must be modified to match the CT scanner, and it is impossible to directly conduct a real-time seepage experiment of fluid passing through the core sample in the CT scanner.
发明内容Summary of the invention
本发明的目的是提供一种结构简单,不易渗漏,并且能够与微米CT扫描仪兼容的,用于原位渗流CT扫描的岩心夹持器。The object of the present invention is to provide a core holder for in-situ seepage CT scanning which has a simple structure, is not prone to leakage, and is compatible with a micrometer CT scanner.
为实现上述目的,本发明提供了如下方案:To achieve the above object, the present invention provides the following solutions:
本发明提供一种用于原位渗流CT扫描的岩心夹持器,包括岩心固定系统、渗流系统、围压加载系统及支撑底座,所述岩心固定系统包括中空堵头体和套筒,所述中空堵头体竖直固定在所述支撑底座上,所述套筒固定在所述中空堵头体的内部顶端,所述套筒用于固定岩心试样,所述套筒的顶端和底端分别设置上堵头和下堵头;所述渗流系统包括渗流液进液流量泵和渗流液出液流量泵,所述渗流液进液流量泵通过渗流液进管与所述下堵头的底端连接,所述渗流液出液流量泵通过渗流液出管与所述上堵头的顶端连接;所述围压加载系统包括围压罩、围压液进液流量泵和围压液出液流量泵,所述围压罩倒扣在所述中空堵头体的外部,且所述围压罩的开口与所述支撑底座的上表面密封连接,所述围压液进液流量泵通过围压液进管与所述围压罩的一侧连接,所述围压液出液流量泵通过围压液出管与所述围压罩的另一侧连接。The present invention provides a core holder for in-situ seepage CT scanning, comprising a core fixing system, a seepage system, a confining pressure loading system and a supporting base, wherein the core fixing system comprises a hollow plug body and a sleeve, wherein the hollow plug body is vertically fixed on the supporting base, wherein the sleeve is fixed on the inner top of the hollow plug body, wherein the sleeve is used to fix the core sample, wherein the top and bottom of the sleeve are respectively provided with an upper plug and a lower plug; wherein the seepage system comprises a seepage liquid inlet flow pump and a seepage liquid outlet flow pump, wherein the seepage liquid inlet flow pump is connected to the supporting base; ... The seepage liquid inlet pipe is connected to the bottom end of the lower plug, and the seepage liquid outlet flow pump is connected to the top end of the upper plug through the seepage liquid outlet pipe; the confining pressure loading system includes a confining pressure cover, a confining pressure liquid inlet flow pump and a confining pressure liquid outlet flow pump, the confining pressure cover is inverted on the outside of the hollow plug body, and the opening of the confining pressure cover is sealed and connected to the upper surface of the supporting base, the confining pressure liquid inlet flow pump is connected to one side of the confining pressure cover through the confining pressure liquid inlet pipe, and the confining pressure liquid outlet flow pump is connected to the other side of the confining pressure cover through the confining pressure liquid outlet pipe.
可选的,所述中空堵头体为氧化铝陶瓷中空堵头体。Optionally, the hollow plug body is an alumina ceramic hollow plug body.
可选的,所述围压罩为氧化铝陶瓷围压罩,所述围压罩的顶端设置有排气口。Optionally, the confining pressure hood is an alumina ceramic confining pressure hood, and an exhaust port is provided at the top of the confining pressure hood.
可选的,所述套筒为胶套或聚醚醚酮树脂(PEEK)套。Optionally, the sleeve is a rubber sleeve or a polyetheretherketone resin (PEEK) sleeve.
可选的,所述支撑底座为二阶凸台型底座,所述中空堵头体与所述二阶凸台型底座的顶端面中心固定连接。Optionally, the support base is a two-step boss-type base, and the hollow plug body is fixedly connected to the center of the top end surface of the two-step boss-type base.
可选的,所述围压罩倒扣在所述二阶凸台型底座的顶端凸台的外部,所述围压罩与所述二阶凸台型底座之间螺纹连接。Optionally, the confining pressure cover is inverted on the outside of the top boss of the second-step boss-type base, and the confining pressure cover is threadedly connected to the second-step boss-type base.
可选的,所述渗流液进液流量泵和所述渗流液出液流量泵对称分布在所述围压罩的外周,所述渗流液进管贯穿所述二阶凸台型底座的内部自所述中空堵头体的底端进入所述中空堵头体内;所述渗流液出管贯穿所述二阶凸台型底座的内部自所述中空堵头体的顶端进入所述中空堵头体内。Optionally, the seepage liquid inlet flow pump and the seepage liquid outlet flow pump are symmetrically distributed on the periphery of the confining pressure hood, and the seepage liquid inlet pipe penetrates the interior of the second-step boss type base and enters the hollow plug body from the bottom end of the hollow plug body; the seepage liquid outlet pipe penetrates the interior of the second-step boss type base and enters the hollow plug body from the top end of the hollow plug body.
可选的,所述围压液进液流量泵和所述围压液出液流量泵对称分布在所述围压罩的外周,所述二阶凸台型底座的顶端面设置有围压液进阀门和围压液出阀门,所述围压液进管贯穿所述二阶凸台型底座的内部与所述围压液进阀门连接;所述渗流液出管贯穿所述二阶凸台型底座的内部与所述围压液出阀门连接。Optionally, the confining pressure liquid inlet flow pump and the confining pressure liquid outlet flow pump are symmetrically distributed on the periphery of the confining pressure cover, and the top surface of the second-step boss type base is provided with a confining pressure liquid inlet valve and a confining pressure liquid outlet valve, the confining pressure liquid inlet pipe passes through the interior of the second-step boss type base and is connected to the confining pressure liquid inlet valve; the seepage liquid outlet pipe passes through the interior of the second-step boss type base and is connected to the confining pressure liquid outlet valve.
可选的,所述渗流液出管上设置有背压阀,所述背压阀用于调节渗流液的流量。Optionally, a back pressure valve is provided on the seepage liquid outlet pipe, and the back pressure valve is used to adjust the flow rate of the seepage liquid.
本发明相对于现有技术取得了以下技术效果:Compared with the prior art, the present invention has achieved the following technical effects:
本发明提出的用于原位渗流CT扫描的岩心夹持器,结构简单紧凑,并且可与多种渗流系统兼容,既可实现在线实时渗流过程的扫描,也可与渗流系统脱离实现离线保压扫描;同时通过设置结构新颖的覆盖式围压加载系统,不仅围压均匀加载,而且可有效减少围压液渗漏,有效减少漏点,泄漏风险低,整个夹持器可置于CT扫描仪内部,能够实现在进行原位CT扫描的同时进行外加围压的渗流实验,达到了流体在通过岩心试样的同时进行原位渗流CT扫描的目的,可操作性强。The core holder for in-situ seepage CT scanning proposed by the present invention has a simple and compact structure and is compatible with a variety of seepage systems. It can realize online real-time scanning of the seepage process and can also be separated from the seepage system to realize offline pressure-maintaining scanning. At the same time, by setting up a novel structured covering confining pressure loading system, not only the confining pressure is evenly loaded, but also the leakage of the confining pressure fluid can be effectively reduced, the leakage points can be effectively reduced, and the leakage risk is low. The entire holder can be placed inside the CT scanner, and a seepage experiment with an external confining pressure can be performed while performing an in-situ CT scan, thereby achieving the purpose of performing in-situ seepage CT scanning while the fluid passes through the core sample, and the operability is strong.
另外,本发明中覆盖式围压罩以及中空堵头体均采用高强度的氧化铝陶瓷制作,氧化铝陶瓷材料不仅对X射线的吸收程度很低,不会对扫描过程造成干扰,而且可大幅降低岩心夹持器的造价成本。此外,本发明的岩心夹持器中,各个阀门、管线以及流量泵均集中设置在支撑底座的上表面,不仅便于操作及更换,而且可减少夹持器在CT扫描内占据空间,实用性强。In addition, the covering confining pressure cover and the hollow plug body in the present invention are made of high-strength alumina ceramics. The alumina ceramic material not only has a low absorption degree of X-rays and does not interfere with the scanning process, but also can greatly reduce the cost of the core clamp. In addition, in the core clamp of the present invention, each valve, pipeline and flow pump are centrally arranged on the upper surface of the support base, which is not only convenient for operation and replacement, but also can reduce the space occupied by the clamp in the CT scan, and has strong practicality.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative labor.
图1为本发明提出的用于原位渗流CT扫描的岩心夹持器的俯视图;FIG1 is a top view of a core holder for in-situ seepage CT scanning proposed by the present invention;
图2为图1的A-A剖面示意图;Fig. 2 is a schematic cross-sectional view taken along line A-A of Fig. 1;
图3为图1的B-B剖面示意图;Fig. 3 is a schematic cross-sectional view taken along line B-B of Fig. 1;
图4为本发明中空堵头体顶端结构放大图;FIG4 is an enlarged view of the top structure of the hollow plug body of the present invention;
其中,附图标记为:1、支撑底座;2、中空堵头体;3、套筒;4、渗流液进液流量泵;5、渗流液出液流量泵;6、渗流液进管;7、渗流液出管;8、围压罩;9、围压液进液流量泵;10、围压液出液流量泵;11、围压液进管;12、围压液出管;13、排气口;14、X射线源;15、X射线接收器;16、岩心试样;17、围压液;18、上堵头;19、下堵头。Among them, the accompanying drawings are marked as follows: 1. support base; 2. hollow plug body; 3. sleeve; 4. seepage liquid inlet flow pump; 5. seepage liquid outlet flow pump; 6. seepage liquid inlet pipe; 7. seepage liquid outlet pipe; 8. confining pressure cover; 9. confining pressure liquid inlet flow pump; 10. confining pressure liquid outlet flow pump; 11. confining pressure liquid inlet pipe; 12. confining pressure liquid outlet pipe; 13. exhaust port; 14. X-ray source; 15. X-ray receiver; 16. core sample; 17. confining pressure liquid; 18. upper plug; 19. lower plug.
具体实施方式DETAILED DESCRIPTION
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
本发明的目的是提供一种结构简单,不易渗漏,并且能够与微米CT扫描仪兼容的,用于原位渗流CT扫描的岩心夹持器。The object of the present invention is to provide a core holder for in-situ seepage CT scanning which has a simple structure, is not prone to leakage, and is compatible with a micrometer CT scanner.
基于此,本发明提供一种用于原位渗流CT扫描的岩心夹持器,包括岩心固定系统、渗流系统、围压加载系统及支撑底座,岩心固定系统包括中空堵头体和套筒,中空堵头体竖直固定在支撑底座上,套筒固定在中空堵头体的内部顶端,套筒用于固定岩心试样,套筒的顶端和底端分别设置上堵头和下堵头;渗流系统包括渗流液进液流量泵和渗流液出液流量泵,渗流液进液流量泵通过渗流液进管与下堵头的底端连接,渗流液出液流量泵通过渗流液出管与上堵头的顶端连接;围压加载系统包括围压罩、围压液进液流量泵和围压液出液流量泵,围压罩倒扣在中空堵头体的外部,且围压罩的开口与支撑底座的上表面密封连接,围压液进液流量泵通过围压液进管与围压罩的一侧连接,围压液出液流量泵通过围压液出管与围压罩的另一侧连接。Based on this, the present invention provides a core holder for in-situ seepage CT scanning, including a core fixing system, a seepage system, a confining pressure loading system and a support base. The core fixing system includes a hollow plug body and a sleeve. The hollow plug body is vertically fixed on the support base, and the sleeve is fixed to the inner top of the hollow plug body. The sleeve is used to fix the core sample. The top and bottom of the sleeve are respectively provided with an upper plug and a lower plug; the seepage system includes a seepage liquid inlet flow pump and a seepage liquid outlet flow pump. The seepage liquid inlet The liquid flow pump is connected to the bottom end of the lower plug through the seepage liquid inlet pipe, and the seepage liquid outlet flow pump is connected to the top end of the upper plug through the seepage liquid outlet pipe; the confining pressure loading system includes a confining pressure cover, a confining pressure liquid inlet flow pump and a confining pressure liquid outlet flow pump, the confining pressure cover is inverted on the outside of the hollow plug body, and the opening of the confining pressure cover is sealed and connected to the upper surface of the supporting base, the confining pressure liquid inlet flow pump is connected to one side of the confining pressure cover through the confining pressure liquid inlet pipe, and the confining pressure liquid outlet flow pump is connected to the other side of the confining pressure cover through the confining pressure liquid outlet pipe.
本发明提出的用于原位渗流CT扫描的岩心夹持器,结构简单紧凑,并且可与多种渗流系统兼容,既可实现在线实时渗流过程的扫描,也可与渗流系统脱离实现离线保压扫描;同时通过设置结构新颖的覆盖式围压加载系统,不仅围压均匀加载,而且可有效减少围压液渗漏,有效减少漏点,泄漏风险低,整个夹持器可置于CT扫描仪内部,能够实现在进行原位CT扫描的同时进行外加围压的渗流实验,达到了流体在通过岩心试样的同时进行原位渗流CT扫描的目的,可操作性强。The core holder for in-situ seepage CT scanning proposed by the present invention has a simple and compact structure and is compatible with a variety of seepage systems. It can realize online real-time scanning of the seepage process and can also be separated from the seepage system to realize offline pressure-maintaining scanning. At the same time, by setting up a novel structured covering confining pressure loading system, not only the confining pressure is evenly loaded, but also the leakage of the confining pressure fluid can be effectively reduced, the leakage points can be effectively reduced, and the leakage risk is low. The entire holder can be placed inside the CT scanner, and a seepage experiment with an external confining pressure can be performed while performing an in-situ CT scan, thereby achieving the purpose of performing in-situ seepage CT scanning while the fluid passes through the core sample, and the operability is strong.
为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图和具体实施方式对本发明作进一步详细的说明。In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, the present invention is further described in detail below with reference to the accompanying drawings and specific embodiments.
实施例一:Embodiment 1:
如图1~4所示,本实施例提供一种用于原位渗流CT扫描的岩心夹持器,包括岩心固定系统、渗流系统、围压加载系统及支撑底座1,岩心固定系统包括中空堵头体2和套筒3,中空堵头体2竖直固定在支撑底座1的顶端面,套筒3固定在中空堵头体2的内部顶端,套筒3用于固定岩心试样16,如图4所示,套筒3的顶端和底端分别设置上堵头18和下堵头19,以将岩心试样16固封在套筒3内,其中上堵头18和下堵头19均优选为起密封作用的胶垫结构,密封性好,而且便于拆装;渗流系统包括渗流液进液流量泵4和渗流液出液流量泵5,渗流液进液流量泵4一端通过渗流液进管6与下堵头19的底端中心连接,另一端与渗流液源连接,以便将渗流液泵入套筒3内,相应的,渗流液出液流量泵5的一端通过渗流液出管7与上堵头18的顶端连接,另一端与渗流液收集装置连接,以便将渗流液从套筒3内泵至渗流液收集装置内,其中,渗流液源和渗流液收集装置可为同一装置也可为不同的装置;如图2~3所示,围压加载系统包括围压罩8、围压液进液流量泵9和围压液出液流量泵10,围压罩8倒扣在中空堵头体2的外部,且围压罩8的开口与支撑底座1的上表面密封连接,从而形成覆盖式围压加载系统,围压液进液流量泵9的一端通过围压液进管11与围压罩8的一侧连接,另一端连接围压液源,相应的,围压液出液流量泵10的一端通过围压液出管12与围压罩8的另一侧连接,另一端可与一围压液收集装置连接,其中,围压液源和围压液收集装置可为同一装置也可为不同的装置。试验时,首先打开渗流液进液流量泵4向套筒3内包裹的岩心试样16内泵入渗流液,直至套筒3内达到试验所需孔压,之后打开围压液进液流量泵9向围压罩8内打入围压液17,直至系统中达到试验所需围压,本实施例中,围压液17优选为油或水。As shown in FIGS. 1 to 4 , this embodiment provides a core holder for in-situ seepage CT scanning, including a core fixing system, a seepage system, a confining pressure loading system and a support base 1. The core fixing system includes a hollow plug body 2 and a sleeve 3. The hollow plug body 2 is vertically fixed to the top surface of the support base 1, and the sleeve 3 is fixed to the inner top of the hollow plug body 2. The sleeve 3 is used to fix the core sample 16. As shown in FIG. 4 , the top and bottom ends of the sleeve 3 are respectively provided with upper plugs 18 The upper plug 18 and the lower plug 19 are used to seal the core sample 16 in the sleeve 3, wherein the upper plug 18 and the lower plug 19 are preferably a rubber pad structure with a sealing effect, which has good sealing performance and is easy to disassemble and assemble; the seepage system includes a seepage liquid inlet flow pump 4 and a seepage liquid outlet flow pump 5, one end of the seepage liquid inlet flow pump 4 is connected to the bottom center of the lower plug 19 through the seepage liquid inlet pipe 6, and the other end is connected to the seepage liquid source, so as to pump the seepage liquid into the sleeve 3, and accordingly, the seepage liquid outlet flow pump 5 is connected to the seepage liquid source. One end of the pump 5 is connected to the top of the upper plug 18 through the seepage liquid outlet pipe 7, and the other end is connected to the seepage liquid collecting device, so as to pump the seepage liquid from the sleeve 3 to the seepage liquid collecting device, wherein the seepage liquid source and the seepage liquid collecting device can be the same device or different devices; as shown in Figures 2 and 3, the confining pressure loading system includes a confining pressure cover 8, a confining pressure liquid inlet flow pump 9 and a confining pressure liquid outlet flow pump 10, and the confining pressure cover 8 is inverted on the outside of the hollow plug body 2, and the confining pressure cover 8 The opening is sealed and connected to the upper surface of the support base 1, thereby forming a covered confining pressure loading system. One end of the confining pressure liquid inlet flow pump 9 is connected to one side of the confining pressure cover 8 through the confining pressure liquid inlet pipe 11, and the other end is connected to the confining pressure liquid source. Correspondingly, one end of the confining pressure liquid outlet flow pump 10 is connected to the other side of the confining pressure cover 8 through the confining pressure liquid outlet pipe 12, and the other end can be connected to a confining pressure liquid collecting device, wherein the confining pressure liquid source and the confining pressure liquid collecting device can be the same device or different devices. During the test, the seepage liquid inlet flow pump 4 is first opened to pump the seepage liquid into the core sample 16 wrapped in the sleeve 3 until the pore pressure required for the test is reached in the sleeve 3, and then the confining pressure liquid inlet flow pump 9 is opened to pump the confining pressure liquid 17 into the confining pressure cover 8 until the system reaches the confining pressure required for the test. In this embodiment, the confining pressure liquid 17 is preferably oil or water.
进一步地,本实施例中,中空堵头体2优选为氧化铝陶瓷中空堵头体,氧化铝陶瓷材料不仅对X射线的吸收程度很低,不会对扫描过程造成干扰,而且相比采用轻质铝-碳纤维复合材料,可大幅降低岩心夹持器的造价成本。同时,围压罩8也优选采用氧化铝陶瓷制作,氧化铝陶瓷围压罩不仅对X射线的吸收程度很低,不会对扫描过程造成干扰,而且造价成本低,同时氧化铝陶瓷围压罩可有效减少围压液渗漏,有效减少漏点,泄漏风险低,使整个夹持器可置于CT扫描仪内部,能够实现在进行原位CT扫描的同时进行外加围压的渗流实验,达到了流体在通过岩心试样的同时进行原位渗流CT扫描的目的。如图2~3所示,本实施例优选围压罩8的顶端面与侧壁之间采用圆角过渡设置,可降低压力对围压罩的荷载,有效减少围压液渗漏的风险。Further, in this embodiment, the hollow plug body 2 is preferably an alumina ceramic hollow plug body. The alumina ceramic material not only has a very low absorption degree of X-rays and does not interfere with the scanning process, but also can greatly reduce the cost of the core clamp compared to the use of lightweight aluminum-carbon fiber composite materials. At the same time, the confining pressure cover 8 is also preferably made of alumina ceramics. The alumina ceramic confining pressure cover not only has a very low absorption degree of X-rays and does not interfere with the scanning process, but also has a low cost. At the same time, the alumina ceramic confining pressure cover can effectively reduce the leakage of the confining pressure liquid, effectively reduce the leakage point, and have a low risk of leakage, so that the entire clamp can be placed inside the CT scanner, and can realize the seepage experiment of the external confining pressure while performing the in-situ CT scanning, so as to achieve the purpose of performing in-situ seepage CT scanning while the fluid passes through the core sample. As shown in Figures 2 to 3, in this embodiment, the top surface and side wall of the preferred confining pressure cover 8 are set with a rounded transition, which can reduce the pressure load on the confining pressure cover and effectively reduce the risk of leakage of the confining pressure liquid.
进一步地,如图2~3所示,围压罩8的顶端设置有排气口13。Furthermore, as shown in FIGS. 2-3 , an exhaust port 13 is provided at the top end of the confining pressure cover 8 .
进一步地,本实施例中套筒3优选为弹性佳、呈圆柱状的胶套或聚醚醚酮树脂(PEEK)套。岩心试样16用于插入该套筒3中,再在套筒3的上下两端分别密封安装上堵头18和下堵头19即可实现岩心试样16的固定。其中,上堵头18和下堵头19均优选为起密封作用的胶垫结构,渗流液进管6和渗流液出管7均优选贯穿胶垫结构中部与套筒3的内部连通,而且上堵头18和下堵头19分别与渗流液出管7和渗流液进管6密封连接,以防止渗流液泄露。Furthermore, in this embodiment, the sleeve 3 is preferably a rubber sleeve or polyetheretherketone (PEEK) sleeve with good elasticity and cylindrical shape. The core sample 16 is used to be inserted into the sleeve 3, and then the upper plug 18 and the lower plug 19 are respectively installed at the upper and lower ends of the sleeve 3 to fix the core sample 16. Among them, the upper plug 18 and the lower plug 19 are preferably rubber pad structures with sealing effects, and the seepage liquid inlet pipe 6 and the seepage liquid outlet pipe 7 are preferably connected to the inside of the sleeve 3 through the middle of the rubber pad structure, and the upper plug 18 and the lower plug 19 are respectively sealed and connected to the seepage liquid outlet pipe 7 and the seepage liquid inlet pipe 6 to prevent leakage of the seepage liquid.
进一步地,如图2~3所示,支撑底座1优选设置为二阶凸台型底座,即二阶凸台型底座包括上层凸起和下层底座,上层凸起固定在下层底座的中心,且上层凸起的面积小于下层底座的面积,本实施例中,如图1所示,优选上层凸起和下层底座为同轴不同径的圆柱形结构,这种二阶凸台型底座为现有技术中心常见的一种凸台结构,在此不再赘述。其中,中空堵头体2与二阶凸台型底座的顶端面中心固定连接,本实施例可优选中空堵头体2与二阶凸台型底座一体设置。Further, as shown in Figures 2 and 3, the support base 1 is preferably configured as a two-step boss type base, that is, the two-step boss type base includes an upper boss and a lower base, the upper boss is fixed at the center of the lower base, and the area of the upper boss is smaller than the area of the lower base. In this embodiment, as shown in Figure 1, the upper boss and the lower base are preferably coaxial cylindrical structures with different diameters. This two-step boss type base is a common boss structure in the prior art center, and will not be described in detail here. Among them, the hollow plug body 2 is fixedly connected to the center of the top surface of the two-step boss type base. In this embodiment, the hollow plug body 2 and the two-step boss type base can be preferably set as a whole.
进一步地,如图2~3所示,围压罩8倒扣在二阶凸台型底座的顶端凸台的外部,优选围压罩8倒扣在上述的上层凸台的外部,且优选围压罩8与二阶凸台型底座的上层凸台的外侧壁之间螺纹连接,既便于拆装,又能确保围压罩8内的密封性。Furthermore, as shown in Figures 2 and 3, the confining pressure cover 8 is inverted on the outside of the top boss of the two-step boss type base. Preferably, the confining pressure cover 8 is inverted on the outside of the above-mentioned upper boss, and preferably, the confining pressure cover 8 is threadedly connected to the outer side wall of the upper boss of the two-step boss type base, which is convenient for disassembly and assembly and can ensure the sealing inside the confining pressure cover 8.
进一步地,如图1~2所示,渗流液进液流量泵4和渗流液出液流量泵5对称分布在围压罩8的外周,渗流液进管6贯穿二阶凸台型底座的内部自中空堵头体2的底端进入中空堵头体2内;渗流液出管7贯穿二阶凸台型底座的内部自中空堵头体2的顶端进入中空堵头体2内。相应的,围压液进液流量泵9和围压液出液流量泵10对称分布在围压罩8的外周,二阶凸台型底座的顶端面设置有围压液进阀门和围压液出阀门,围压液进管11贯穿二阶凸台型底座的内部与围压液进阀门连接;渗流液出管12贯穿二阶凸台型底座的内部与围压液出阀门连接。于本实施例中,如图1所示,渗流液进液流量泵4、渗流液出液流量泵5、围压液进液流量泵9和围压液出液流量泵10优选间隔交叉设置在二阶凸台型底座的下层底座上表面,同时渗流液进管6、渗流液出管7、围压液进管11以及渗流液出管12采用贯穿二阶凸台型底座内部的方式与上方的渗流系统和/或围压加载系统连接,各流量泵以及各管路全部设置于夹持器的下部,区别于传统夹持器阀门分布在夹持器上下两端的设计,不仅便于操作及更换,而且可减少夹持器在CT扫描内占据空间,也有利于对各管路的保护,实用性极强。Further, as shown in Figs. 1 and 2, the seepage liquid inlet flow pump 4 and the seepage liquid outlet flow pump 5 are symmetrically distributed on the outer periphery of the confining pressure cover 8, the seepage liquid inlet pipe 6 penetrates the interior of the second-step boss-type base and enters the hollow plug body 2 from the bottom end of the hollow plug body 2; the seepage liquid outlet pipe 7 penetrates the interior of the second-step boss-type base and enters the hollow plug body 2 from the top end of the hollow plug body 2. Correspondingly, the confining pressure liquid inlet flow pump 9 and the confining pressure liquid outlet flow pump 10 are symmetrically distributed on the outer periphery of the confining pressure cover 8, the top surface of the second-step boss-type base is provided with a confining pressure liquid inlet valve and a confining pressure liquid outlet valve, the confining pressure liquid inlet pipe 11 penetrates the interior of the second-step boss-type base and is connected to the confining pressure liquid inlet valve; the seepage liquid outlet pipe 12 penetrates the interior of the second-step boss-type base and is connected to the confining pressure liquid outlet valve. In this embodiment, as shown in Figure 1, the seepage liquid inlet flow pump 4, the seepage liquid outlet flow pump 5, the confining pressure liquid inlet flow pump 9 and the confining pressure liquid outlet flow pump 10 are preferably arranged at intervals and cross-arranged on the upper surface of the lower base of the two-step boss type base. At the same time, the seepage liquid inlet pipe 6, the seepage liquid outlet pipe 7, the confining pressure liquid inlet pipe 11 and the seepage liquid outlet pipe 12 are connected to the upper seepage system and/or the confining pressure loading system in a manner of penetrating the interior of the two-step boss type base. All flow pumps and pipelines are arranged at the bottom of the clamp, which is different from the design of the traditional clamp valves distributed at the upper and lower ends of the clamp. It is not only easy to operate and replace, but also can reduce the space occupied by the clamp in the CT scan, and is also beneficial to the protection of each pipeline, and is extremely practical.
进一步地,渗流液出管7上设置有背压阀,背压阀用于调节渗流液出管7内渗流液流出端的压力,进而调节渗流液的流量。Furthermore, a back pressure valve is provided on the seepage liquid outlet pipe 7, and the back pressure valve is used to adjust the pressure at the seepage liquid outflow end in the seepage liquid outlet pipe 7, thereby adjusting the flow rate of the seepage liquid.
下面以本实施例用于原位渗流CT扫描的岩心夹持器与蔡司Xradia 410型微米CT扫描仪配套使用为例,对本实施例作具体使用说明。The following uses the core holder for in-situ seepage CT scanning of this embodiment in conjunction with a Zeiss Xradia 410 micrometer CT scanner as an example to specifically explain the use of this embodiment.
首先,加载样品时,将岩心试样16插入套筒3内,再在套筒3的上下两端分别密封设置上堵头18和下堵头19,之后将围压罩8倒扣在二阶凸台型底座上,并与二阶凸台型底座的上层凸起螺纹密封连接,如图1~4所示,此时中空堵头体2、套筒3、上堵头18和下堵头19均位于围压罩8的内部。First, when loading the sample, the core sample 16 is inserted into the sleeve 3, and then the upper plug 18 and the lower plug 19 are sealed at the upper and lower ends of the sleeve 3 respectively, and then the confining pressure cover 8 is turned upside down on the second-order boss type base, and is sealed and connected with the upper raised thread of the second-order boss type base, as shown in Figures 1 to 4. At this time, the hollow plug body 2, the sleeve 3, the upper plug 18 and the lower plug 19 are all located inside the confining pressure cover 8.
之后进行渗流试验:首先将整个夹持器固定在蔡司Xradia 410型微米CT扫描仪的样品托盘上,此时如图2所示,夹持器位于X射线源14和X射线接收器15之间。首先,开启围压液进液流量泵9向围压罩8内打入围压液17,直至系统中相关测压部件检测到围压罩8内达到试验所需围压,其中围压液进液流量泵9本身具备检测并显示围压的功能,围压液进液流量泵9为常规的流量泵结构,其具体结构和工作原理在此不再赘述。之后,开启渗流液进液流量泵4,使渗流液从系统左下方流入套筒3包裹的岩心试样16内,直至相关测压部件检测到套筒3内达到试验所需的孔压;此处的孔压采用渗流液进液流量泵4测量,渗流液进液流量泵4本身具备检测并显示孔压的功能,其中渗流液进液流量泵4为常规的流量泵结构,其具体结构和工作原理在此不再赘述。上述的围压值和孔压值均由具体实验要求而确定,一般最大孔压为30MPa,最大围压为35MPa。Then, the seepage test is carried out: first, the entire clamp is fixed on the sample tray of the Zeiss Xradia 410 micrometer CT scanner. At this time, as shown in FIG2 , the clamp is located between the X-ray source 14 and the X-ray receiver 15. First, the confining pressure liquid inlet flow pump 9 is turned on to pump the confining pressure liquid 17 into the confining pressure cover 8 until the relevant pressure measuring components in the system detect that the confining pressure in the confining pressure cover 8 reaches the confining pressure required for the test. The confining pressure liquid inlet flow pump 9 itself has the function of detecting and displaying the confining pressure. The confining pressure liquid inlet flow pump 9 is a conventional flow pump structure, and its specific structure and working principle are not repeated here. After that, the seepage fluid inlet flow pump 4 is turned on to allow the seepage fluid to flow from the lower left of the system into the core sample 16 wrapped in the sleeve 3 until the relevant pressure measuring component detects that the pore pressure required for the test is reached in the sleeve 3; the pore pressure here is measured by the seepage fluid inlet flow pump 4, which itself has the function of detecting and displaying the pore pressure, wherein the seepage fluid inlet flow pump 4 is a conventional flow pump structure, and its specific structure and working principle are not repeated here. The above-mentioned confining pressure value and pore pressure value are determined by the specific experimental requirements, generally the maximum pore pressure is 30MPa, and the maximum confining pressure is 35MPa.
再之后,可通过渗流液出管7上的背压阀调节系统右下方,即渗流液出管7内渗流液流出端的压力,进行流体流量的调节,当渗流液流量稳定后,即可开启蔡司Xradia410型微米CT扫描仪的电源进行微米CT扫描。蔡司Xradia410型微米CT扫描仪的X射线源14正对着夹持器,通过X射线接收器15接收穿过岩心试样16的X射线,并通过扫描仪的信号分析系统对X射线信号衰减程度进行分析,从而在外加围压的试验条件下实现对岩心试样16内部结构的三维可视化。需要注意的是,上述有关蔡司Xradia 410型微米CT扫描仪中,X射线源14的X射线发射原理、X射线接收器15的结构原理以及系统对X射线信号衰减程度的分析原理均为本领域公知,该扫描仪中各部件的具体结构以及工作原理在此不再赘述。After that, the back pressure valve on the seepage outlet pipe 7 can be used to adjust the pressure at the lower right side of the system, that is, the pressure at the seepage outlet end of the seepage outlet pipe 7, to adjust the fluid flow. When the seepage flow is stable, the power supply of the Zeiss Xradia 410 micrometer CT scanner can be turned on to perform micrometer CT scanning. The X-ray source 14 of the Zeiss Xradia 410 micrometer CT scanner faces the clamp, receives the X-rays passing through the core sample 16 through the X-ray receiver 15, and analyzes the attenuation degree of the X-ray signal through the signal analysis system of the scanner, thereby realizing the three-dimensional visualization of the internal structure of the core sample 16 under the test condition of the external confining pressure. It should be noted that the X-ray emission principle of the X-ray source 14, the structural principle of the X-ray receiver 15, and the analysis principle of the system for the attenuation degree of the X-ray signal in the above-mentioned Zeiss Xradia 410 micrometer CT scanner are all well known in the art, and the specific structure and working principle of each component in the scanner will not be repeated here.
由此可见,本发明提出的用于原位渗流CT扫描的岩心夹持器,结构简单紧凑,并且可与多种渗流系统兼容,既可实现在线实时渗流过程的扫描,也可与渗流系统脱离实现离线保压扫描;同时通过设置结构新颖的覆盖式围压加载系统,不仅围压均匀加载,而且可有效减少围压液渗漏,有效减少漏点,泄漏风险低,整个夹持器可置于CT扫描仪内部,能够实现在进行原位CT扫描的同时进行外加围压的渗流实验,达到了流体在通过岩心试样的同时进行原位渗流CT扫描的目的,可操作性强。It can be seen that the core holder for in-situ seepage CT scanning proposed by the present invention has a simple and compact structure and is compatible with a variety of seepage systems. It can realize online real-time scanning of the seepage process and can also be separated from the seepage system to realize offline pressure-maintaining scanning; at the same time, by setting up a novel covering confining pressure loading system, not only the confining pressure is loaded evenly, but also the leakage of the confining pressure fluid can be effectively reduced, the leakage points can be effectively reduced, and the leakage risk is low. The entire holder can be placed inside the CT scanner, and it is possible to perform a seepage experiment with an external confining pressure while performing an in-situ CT scan, thereby achieving the purpose of performing in-situ seepage CT scanning while the fluid passes through the core sample, and the operability is strong.
另外,本发明中覆盖式围压罩以及中空堵头体均采用高强度的氧化铝陶瓷制作,氧化铝陶瓷材料不仅对X射线的吸收程度很低,不会对扫描过程造成干扰,而且可大幅降低岩心夹持器的造价成本。此外,本发明的岩心夹持器中,各个流量泵集中设置在支撑底座的上表面,不仅便于操作及更换,而且可减少夹持器在CT扫描内占据空间,实用性强。In addition, the covering confining pressure cover and the hollow plug body in the present invention are made of high-strength alumina ceramics. The alumina ceramic material not only has a low absorption degree of X-rays and does not interfere with the scanning process, but also can greatly reduce the cost of the core holder. In addition, in the core holder of the present invention, each flow pump is centrally arranged on the upper surface of the support base, which is not only convenient for operation and replacement, but also can reduce the space occupied by the holder in the CT scan, and has strong practicality.
需要说明的是,对于本领域技术人员而言,显然本发明不限于上述示范性实施例的细节,而且在不背离本发明的精神或基本特征的情况下,能够以其他的具体形式实现本发明。因此,无论从哪一点来看,均应将实施例看作是示范性的,而且是非限制性的,本发明的范围由所附权利要求而不是上述说明限定,因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内,不应将权利要求中的任何附图标记视为限制所涉及的权利要求。It should be noted that it is obvious to those skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and that the present invention can be implemented in other specific forms without departing from the spirit or essential features of the present invention. Therefore, no matter from which point of view, the embodiments should be regarded as exemplary and non-restrictive, and the scope of the present invention is defined by the appended claims rather than the above description, and it is intended that all changes falling within the meaning and scope of the equivalent elements of the claims are included in the present invention, and any figure mark in the claims should not be regarded as limiting the claims involved.
本发明中应用了具体个例对本发明的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处。综上所述,本说明书内容不应理解为对本发明的限制。The present invention uses specific examples to illustrate the principles and implementation methods of the present invention. The above examples are only used to help understand the method and core ideas of the present invention. At the same time, for those skilled in the art, according to the ideas of the present invention, there will be changes in the specific implementation methods and application scope. In summary, the content of this specification should not be understood as limiting the present invention.
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