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CN109612235A - One kind being used for electromagnetic heating stirring and drying device and its furnace drying method - Google Patents

One kind being used for electromagnetic heating stirring and drying device and its furnace drying method Download PDF

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Publication number
CN109612235A
CN109612235A CN201811322335.XA CN201811322335A CN109612235A CN 109612235 A CN109612235 A CN 109612235A CN 201811322335 A CN201811322335 A CN 201811322335A CN 109612235 A CN109612235 A CN 109612235A
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CN
China
Prior art keywords
conical shell
electromagnetic heating
screw rod
drying
discharging
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811322335.XA
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Chinese (zh)
Inventor
施国有
魏春华
任占胜
夏德明
朱云清
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Juhua Equipment Manufacturing Co Ltd
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Zhejiang Juhua Equipment Manufacturing Co Ltd
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Publication date
Application filed by Zhejiang Juhua Equipment Manufacturing Co Ltd filed Critical Zhejiang Juhua Equipment Manufacturing Co Ltd
Priority to CN201811322335.XA priority Critical patent/CN109612235A/en
Publication of CN109612235A publication Critical patent/CN109612235A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/12Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices
    • F26B11/14Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices the stirring device moving in a horizontal or slightly-inclined plane
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B23/00Heating arrangements
    • F26B23/04Heating arrangements using electric heating
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/04Agitating, stirring, or scraping devices

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

The present invention relates to one kind to be used for electromagnetic heating stirring and drying device and its furnace drying method, including the closed conical shell for being carried out for production reaction, driving motor and speed reducer are respectively equipped with above conical shell, output end of reducer is connected with shaft, shaft one end is along extending to after the conical shell outer wall inside conical shell vertically and be connected with cursor, cursor both ends are connected separately with the first fixing seat and the second fixing seat, the first spinning motor and the second spinning motor are respectively equipped in first fixing seat and the second fixing seat, the output end of first spinning motor and the second spinning motor is connected separately with the first screw rod and the second screw rod, spiral uniform winding is equipped with electromagnetic heating coil along longitudinal direction on conical shell outer cone wall, conical shell bottom is connected with the discharging control assembly for heat drying moisture quickly discharging.Good, long service life that the present invention provides a kind of rush reaction effects, highly-safe and discharging are conveniently used for electromagnetic heating stirring and drying device and its furnace drying method.

Description

One kind being used for electromagnetic heating stirring and drying device and its furnace drying method
Technical field
The present invention relates to perfluoroethylene-propylene production technical fields, and in particular to one kind is filled for electromagnetic heating stirring and drying It sets and its furnace drying method.
Background technique
Perfluoroethylene-propylene FEP or F46 are the copolymers of tetrafluoroethene and hexafluoropropene, and the content of hexafluoropropene is about 15% or so, it is the modified material of polytetrafluoroethylene (PTFE).FEP had not only had characteristic similar with polytetrafluoroethylene (PTFE) but also had had thermoplasticity modeling The excellent machinability of material.Thus it compensates for the deficiency of polytetrafluoroethylene (PTFE) processing difficulties, becomes instead of polytetrafluoroethylene (PTFE) Material.FEP has excellent heat resistance, low frictional properties, non-stick and lubricity, chemical corrosion resistance, thermal stability and electricity Insulating properties, in addition melt-processable, so having wide range of applications, being easy to make.FEP is widely used in electrical, electronics, chemical industry boat The departments such as advanced science technologies and national defense industry such as the industrial departments such as sky, machinery and rocket-powered missile, peaceful boat.Suitable for fluoroplastics institute Applicable every field, and can make and be difficult to process, complex-shaped product.Mechanical industry is used as sealing ring, instrument and meter Components etc.;Electrical industry is used as electric wire insulation layer, cable cover(ing) etc.;Chemical industry is used as pump, valve, rectifying column, heat exchange Equipment anticorrosion material and sealing material are made in device and its components, sealing element, atomic energy industry Central Region;Medically it is used as repairing heart Valve and tiny tracheae.FEP can be used in big sun energy collector with light, good weatherability and high big positive energy transfer rate because of it On.FEP has crystalline texture, and crystallinity 30%-55%, different from PIFE, the crystalline texture of FEP is special to condition of molding Be it is less sensitive to cooling velocity, at processing temperatures, can get the square melt that really flows, will not generally be given birth in its cooling At stomata, therefore it makes general pore-free.Perfluoroethylene-propylene (FEP) is by tetrafluoroethene (TFE) and hexafluoropropene (HFP) It is copolymerized.
Copolyreaction control method: the strictly speaking factor of had an impact polymerization reaction such as temperature, pressure, polymerization Medium, initiator type and quantity and mix monomer ratio etc. can be used as control of the means realization to polymerization process System.FEP uses polymerization reaction in process of production, contains moisture and harmful components in the product, it is necessary to try to remove.
In process of production, material placement carries out polymerization reaction to existing FEP in the reaction vessel, and there are polymerization reactions not Can sufficiently complete progress the problem of, expected requirement is not achieved so as to cause the quality of production of FEP, in production equal quality When FEP, consumed raw material quality is larger, and consumption of raw materials is excessively high, high production cost, and the corrosion of the material in reaction process Property it is stronger, reaction vessel is easily corroded and service life is caused to substantially reduce, simultaneously as FEP in process of production using polymerization Reaction contains moisture and harmful components in the product, not high to the discharging control security of its product at present, does not remove adequately Harmful components are gone to cause the discharging of FEP finished product materials inconvenient, discharging low efficiency is inconvenient to control, to the body of operator Injury can be brought, safety is not high.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide, a kind of rush reaction effect is good, service life Long, highly-safe and discharging is conveniently used for electromagnetic heating stirring and drying device and its furnace drying method.
The technical scheme of the present invention is realized as follows: a kind of be used for electromagnetic heating stirring and drying device, it is characterised in that: Including the enclosed conical shell for carrying out for production reaction, the conical shell upper center divides from top to bottom at position Be not provided with driving motor and speed reducer, the output end of the speed reducer is connected with shaft, the shaft far from speed reducer one End is divided along extending to inside conical shell and being connected with cursor, the both ends of the cursor after conical shell outer wall vertically It is not connected with the first fixing seat and the second fixing seat being symmetrically set in left and right, first fixing seat and the second fixing seat On be respectively arranged with the first spinning motor and the second spinning motor, the output end of first spinning motor and the second spinning motor It is connected separately with the first screw rod and the second screw rod, the length and the two that the length of first screw rod is greater than the second screw rod are along taper The central axes of cylinder are symmetrically set in left and right;Spiral uniform winding is provided with electricity along longitudinal direction on the conical shell outer cone wall Magnetic heating coil, the conical shell inner wall top are provided with pressure sensor, are provided with temperature on the conical shell inner sidewall Sensor is spent, the pressure sensor and temperature sensor are electrically connected with electromagnetic heating coil respectively;The conical shell bottom It is connected with the discharging control assembly for heat drying moisture quickly discharging.
By using above-mentioned technical proposal, the container for material polymerization reaction is conical shell, above conical shell Center position is respectively arranged with driving motor and speed reducer, under driving motor normal operating conditions, provides power and drives and subtract The shaft rotation of fast machine output end connection, the one end of shaft far from speed reducer extends to cone after running through conical shell outer wall vertically Shape inner barrel is simultaneously connected with cursor, and cursor is under the drive of shaft, in conical shell inner rotation, and in its rotation Meanwhile the first fixing seat and the second fixing seat being symmetrically set in left and right are connected separately at the both ends of cursor, first The first spinning motor and the second spinning motor are respectively arranged in fixing seat and the second fixing seat, the first spinning motor drives its defeated The first screw rod rotation of outlet connection, the second screw rod rotation that the second spinning motor drives its output end to connect, in polymerization reaction When progress, so that material is generated compound motion inside conical shell, mainly generate four kinds of forms of motion: by driving inside conical shell Motor-driven rotatable shaft drives cursor to revolve along conical shell internal cone wall, so that the first screw rod and the second screw rod be driven to make object Material is circled along cone wall;During revolution, positioned at the first spinning motor of the first fixing seat and the second fixing seat and Second spinning motor respectively drives the first screw rod and the rotation of the second screw rod, to make material from conical shell bottom in spiral It rises;The revolution of spiral and rotation compound motion are driven a part of material to conical shell top while being revolved and rotation Effect, make this partial material thread mixing under the action of the centrifugal force;The material of rising is by under under the action of self gravity Drop.Four kinds of movements generate convection current, shearing, diffusion inside conical shell, rapidly and uniformly mix to reach, the first screw rod Length is greater than the length of the second screw rod and the two is symmetrically set along the central axes of conical shell in left and right, to further mention Height makes anti-the uniform stirring function and effect of conical shell materials inside to improve the quality of production and reaction effect of material It should adequately carry out, reduce production cost, spiral uniform winding is provided with electromagnetic heating along longitudinal direction on conical shell outer cone wall Coil, by being powered to electromagnetic heating coil, heats it quickly to conical shell, reaches when polymerization reaction is carried out To production temperature, production reaction is carried out under lasting heat preservation and heating, it is opposite with existing heating method, using electromagnetic induction heating Mode heats conical shell, and heat conversion is relatively high, control heat in place, meanwhile, it is convenient to the temperature inside conical shell Degree is controlled, after polymerization reaction, under being acted on by the continuous heating of electromagnetic heating coil, to the object inside conical shell Material is dried, and pressure sensor is provided at the top of conical shell inner wall, is provided with temperature sensing on conical shell inner sidewall Device, when detecting that pressure inside conical shell or temperature are more than reaction temperature and pressure value, transmitting electric signal to electromagnetism adds Heat coil reduces heating power to play the role of real-time control reaction temperature and pressure value and guarantees the accurate of polymerization reaction It efficiently carries out, this electromagnetic heating stirring and drying device is by allowing the stirring of material uniform high-efficiency, to reach full and uniform poly- Close reaction, improve reaction environment temperature can accelerate reaction efficiency, electromagnetic heating can be very good control heating temperature and Internal pressure value, and the moisture in conical shell is dried after the completion of reaction, thus allow FER innocuous, conical shell bottom It is connected with the discharging control assembly for heat drying moisture quickly discharging, guarantee discharging safely and fast facilitates control, reduces Injury generated to the body of operator, it is good, long service life that the present invention provides a kind of rushs reaction effects, highly-safe and out Material is conveniently used for electromagnetic heating stirring and drying device.
The present invention is further arranged to: the discharging control assembly includes the discharging that one end is connect with conical shell bottom Pipe, the discharge nozzle are connected with drying tube far from one end of conical shell, discharging heating chamber, institute are provided in the drying tube It states and axial uniform winding is provided with dry electromagnetic heating coil on the outer wall of drying tube, be provided with control on the discharge nozzle and cut Disconnected component, the drying tube are provided with rotating blanking valve far from one end of discharge nozzle.
By using above-mentioned technical proposal, when carrying out the discharging of FEP finished product materials, control cutting assembly is opened and is released FEP finished product materials part inside conical shell enters in the discharging heating chamber of drying tube, and control cutting assembly is closed simultaneously Stop FEP finished product materials to continue to output, the drying electromagnetic heating coil being arranged in dry pipe outer wall along axial uniform winding is logical Electricity, and heat temperature raising quickly is carried out to drying tube, to quickly be dried to FEP finished product materials within the regular hour Dry, the FEP finished product materials after completing drying expect quickly to discharge under the switch control of valve under rotation, meanwhile, rotating blanking valve Discharging control uniformly and conveniently, while above structure facilitates discharging to control, ensure that dry to the FEP finished product materials of discharging In place, it after adequately removing moisture contained in FEP finished product materials and harmful components, then is quickly and effectively controlled out Material, guarantee is harmless to the body of operator, highly-safe.
The present invention is further arranged to: the control discharge component includes the driving cylinder that discharge nozzle side is arranged in, institute The output end for stating driving cylinder is connected with push rod, and the push rod is connected with far from one end of driving cylinder for cutting off in discharge nozzle The cutting material plate of discharging.
By using above-mentioned technical proposal, after completing polymerization reaction, by the driving cylinder that discharge nozzle side is arranged in Under driving effect, the push rod of output end connection laterally moves and cutting material plate is driven to open, and FEP finished product materials are from out It is entered in expects pipe in discharging heating chamber and discharging is dried, during drying, driving cylinder driving push rod is transversely It drives cutting material plate to close discharge nozzle, guarantees dry efficiency and effect, it is simple and reliable for structure.
The present invention is further arranged to: sealing block is provided on the discharge nozzle inner sidewall, correspondence is set on the sealing block It is equipped with the card slot being caught in for cutting material plate.
By using above-mentioned technical proposal, in order to guarantee to carry out to the FEP finished product materials entered in discharging heating chamber The efficiency of heating, meanwhile, the effect of dry moisture and harmful substance is improved, sealing block is provided on discharge nozzle inner sidewall, it is close It is correspondingly arranged on the card slot being caught in for cutting material plate on envelope block, snaps onto card slot under drive of the cutting material plate with push rod In, make to discharge heating chamber sealing in place.
The present invention is further arranged to: first screw rod and the second screw rod respectively with conical shell inner wall gap setting.
By using above-mentioned technical proposal, cooperate to further increase the first screw rod and the second screw rod to material Mixing effect, by the first screw rod and the second screw rod respectively with conical shell inner wall gap setting, thus in the first spinning motor and Under second spinning motor driving effect, the first screw rod and the second screw rod are respectively along conical shell central axes symmetrically and to material Carry out stirring sufficiently in place.
The present invention is further arranged to: first screw rod extends to conically shaped far from one end inclination of the first spinning motor The half of the first spiro rod length is arranged between 3/4ths in body bottom, the length of second screw rod.
By using above-mentioned technical proposal, in order to improve the mixing effect that the first screw rod and the second screw rod cooperate each other, First screw rod is extended into conical shell bottom far from one end inclination of the first spinning motor, the length setting of the second screw rod is the The half of one spiro rod length is between 3/4ths.
The present invention is further arranged to: the outer wall of the conical shell includes the filling cladding set gradually from inside to outside The material of layer, base and outer layer, the filling cladding layer and base is Hastelloy, and the outer layer is metal material.
By using above-mentioned technical proposal, the outer wall of conical shell mainly uses filling cladding layer and internal material to carry out It contacts with each other, using Hastelloy as raw material and using laser cladding Hastelloy on the surface of base, and in most outsourcing Covering one layer of outer layer enables the corrosion of conical shell hydrogen fluoride resistant using metal material, and under the action of electromagnetic heating coil Quickly heating reaches reaction temperature and material drying, guarantees in carrying out polymerization process, the service life of conical shell, energy It is enough to improve whole corrosion resistance and service life, guarantee being normally carried out for reaction, reduces the cost of production.
The present invention is further arranged to: being provided with feed pipe at the top of the conical shell, the feed pipe upper end is hinged with Sealing cover.
By using above-mentioned technical proposal, material passes through the feed pipe being arranged at the top of conical shell and is added to conical shell Middle carry out polymerization reaction, and it is hinged with sealing cover in feed pipe upper end, for guaranteeing after material is added in conical shell Sealing to conical shell facilitates operation.
The present invention discloses a kind of furnace drying method for efficiently promoting the good electromagnetic heating stirring and drying device of reaction effect, Its step are as follows:
1), material is put into: opening sealing cover, and polymerization reaction is produced material required for FEP and is added to from feed pipe It is reacted in conical shell, after the completion of addition, rotary seal lid shuts feed pipe;
2) it, temperature reaction: is powered to electromagnetic heating coil, heats it quickly to conical shell, heating power For 120KW, heating-up time control for the first time was heated to 240 degrees Celsius of reaction temperature at 1.5 hours, when lasting heat preservation charging heats up Between 1.3 hours;
3), auger: drive cursor along conical shell internal cone wall by driving motor drive shaft inside conical shell It revolves, so that the first screw rod and the second screw rod be driven to circle material along cone wall, during revolution, is located at The first spinning motor and the second spinning motor of first fixing seat and the second fixing seat respectively drive the first screw rod and the second screw rod Rotation, to make material from conical shell bottom along spiral, the revolution of spiral and rotation compound motion make a part of material It is driven to the effect by revolution and rotation simultaneously of conical shell top, makes this partial material spiral under the action of the centrifugal force Mixing, the material of rising under the action of self gravity by declining;
4), discharge drying: after completing polymerization reaction, by its output end of the driving of driving cylinder of discharge nozzle side is arranged in The push rod of connection laterally moves and cutting material plate is driven to open, and FEP finished product materials enter discharging heating from discharge nozzle After in chamber, driving cylinder driving push rod transversely drives cutting material plate to close discharge nozzle, and the material inside conical shell is held Continuous heat drying is arranged in the drying electromagnetic heating coil in dry pipe outer wall along axial uniform winding and is powered, and quickly right Drying tube carries out heat temperature raising;
5), drying discharging: the FEP finished product materials after completing drying expect quickly to go out under the switch control of valve under rotation Material.
It is preferred that are as follows: the temperature on pressure sensor and conical shell inner sidewall in step (3), at the top of conical shell inner wall Degree sensor is when detecting that pressure inside conical shell or temperature are more than reaction temperature and pressure value, transmitting electric signal to electricity Magnetic heating coil reduces the electrical power being passed into electromagnetic heating coil, reduces the heating temperature to conical shell.
By using above-mentioned technical proposal, this electromagnetic heating stirring and drying device by allowing the stirring of material uniform high-efficiency, To reaching full and uniform polymerization reaction, the temperature for improving reaction environment can accelerate the efficiency of reaction, and electromagnetic heating can be with Control heating temperature and internal pressure value well, and dry the moisture in conical shell after the completion of reaction, to allow FER material Expect harmless, conical shell bottom is connected with the discharging control assembly for heat drying moisture quickly discharging, guarantees the peace of discharging Complete quick and convenient control reduces and generates injury to the body of operator, good, use that the present invention provides a kind of rush reaction effects Service life is long, highly-safe and discharging is conveniently used for electromagnetic heating stirring and drying device and its furnace drying method.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention without any creative labor, may be used also for those of ordinary skill in the art To obtain other drawings based on these drawings.
Fig. 1 is specific embodiment of the invention structural schematic diagram.
Fig. 2 is the portion A partial enlargement structural representation in Fig. 1.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
As Figure 1-Figure 2, the invention discloses one kind to be used for electromagnetic heating stirring and drying device, of the invention specific real It applies in example, including the enclosed conical shell 1 for being carried out for production reaction, at the 1 upper center position of conical shell It is respectively arranged with driving motor 2 and speed reducer 3 from top to bottom, the output end of the speed reducer 3 is connected with shaft 4, the shaft 4 One end far from speed reducer 3 extends to inside conical shell 1 after 1 outer wall of conical shell and is connected with cursor 5 along vertical, The both ends of the cursor 5 are connected separately with the first fixing seat 6 and the second fixing seat 7 being symmetrically set in left and right, described The first spinning motor 8 and the second spinning motor 9 are respectively arranged in first fixing seat 6 and the second fixing seat 7, described first certainly The output end of rotating motor 8 and the second spinning motor 9 is connected separately with the first screw rod 111 and the second screw rod 112, first screw rod 111 length is greater than the length of the second screw rod 112 and the two is symmetrically set along the central axes of conical shell 1 in left and right;Institute State on 1 outer cone wall of conical shell that spiral uniform winding is provided with electromagnetic heating coil 11, the 1 inner wall top of conical shell along longitudinal direction Portion is provided with pressure sensor 12, is provided with temperature sensor 13, the pressure sensor on 1 inner sidewall of conical shell 12 and temperature sensor 13 be electrically connected respectively with electromagnetic heating coil 11;1 bottom of conical shell is connected with dry for heating The discharging control assembly of dry moisture quickly discharging.
By using above-mentioned technical proposal, the container for material polymerization reaction is conical shell 1, on conical shell 1 Square center position is respectively arranged with driving motor 2 and speed reducer 3, under 2 normal operating conditions of driving motor, provides power and drives The shaft 4 of dynamic 3 output end of speed reducer connection rotates, and the one end of shaft 4 far from speed reducer 3 is along vertically through 1 outer wall of conical shell After extend to the inside of conical shell 1 and be connected with cursor 5, cursor 5 turns inside conical shell 1 under the drive of shaft 4 It is dynamic, and while its rotation, the first fixing seat 6 being symmetrically set in left and right is connected separately at the both ends of cursor 5 With the second fixing seat 7, the first spinning motor 8 and the second rotation electricity are respectively arranged in the first fixing seat 6 and the second fixing seat 7 Machine 9, the first spinning motor 8 drive the first screw rod 111 rotation of its output end connection, and the second spinning motor 9 drives its output end The second screw rod 112 rotation of connection makes material generate compound motion when polymerization reaction carries out inside conical shell 1, main to produce Raw four kinds of forms of motion: drive cursor 5 along 1 internal cone wall of conical shell by 2 drive shaft 4 of driving motor inside conical shell 1 It revolves, so that the first screw rod 111 and the second screw rod 112 be driven to circle material along cone wall;In the process of revolution In, the first spinning motor 8 and the second spinning motor 9 positioned at the first fixing seat 6 and the second fixing seat 7 respectively drive the first spiral shell Bar 111 and the rotation of the second screw rod 112, to make material from 1 bottom of conical shell along spiral;The revolution and rotation of spiral are multiple Resultant motion is driven a part of material to the effect by revolution and rotation simultaneously of 1 top of conical shell, makes this part of object Expect thread mixing under the action of the centrifugal force;The material of rising under the action of self gravity by declining.Four kinds of movements are in conically shaped Convection current, shearing, diffusion are generated inside body 1, is rapidly and uniformly mixed to reach, and the length of the first screw rod 111 is greater than the second spiral shell The length and the two of bar 112 are symmetrically set along the central axes of conical shell 1 in left and right, to further increase to taper The uniform stirring function and effect of 1 materials inside of cylinder react fully to improve the quality of production and reaction effect of material It carrying out, reduces production cost, spiral uniform winding is provided with electromagnetic heating coil 11 along longitudinal direction on 1 outer cone wall of conical shell, When polymerization reaction carries out, by being powered to electromagnetic heating coil 11, heats it quickly to conical shell 1, reach Temperature is produced, carries out production reaction under lasting heat preservation and heating, it is opposite with existing heating method, using electromagnetic induction heating side Formula heats conical shell 1, and heat conversion is relatively high, control heat in place, meanwhile, it is convenient to the temperature inside conical shell 1 Degree is controlled, after polymerization reaction, under being acted on by the continuous heating of electromagnetic heating coil 11, inside conical shell 1 Material dried, pressure sensor 12 is provided at the top of 1 inner wall of conical shell, is provided on 1 inner sidewall of conical shell Temperature sensor 13 transmits telecommunications when detecting that pressure inside conical shell 1 or temperature are more than reaction temperature and pressure value Number to electromagnetic heating coil 11, heating power is reduced, to play the role of real-time control reaction temperature and pressure value, is guaranteed poly- The precise and high efficiency for closing reaction carries out, this electromagnetic heating stirring and drying device is by allowing the stirring of material uniform high-efficiency, to reach Full and uniform polymerization reaction, the temperature for improving reaction environment can accelerate the efficiency of reaction, and electromagnetic heating can be very good to control Heating temperature processed and internal pressure value, and the moisture in conical shell 1 is dried after the completion of reaction, thus allow FER innocuous, 1 bottom of conical shell is connected with the discharging control assembly for heat drying moisture quickly discharging, guarantees discharging safely and fast Facilitate control, reduces and injury, good, service life that the present invention provides a kind of rush reaction effects are generated to the body of operator Long, highly-safe and discharging is conveniently used for electromagnetic heating stirring and drying device.
In the specific embodiment of the invention, it is described discharging control assembly include one end connect with 1 bottom of conical shell out Expects pipe 21, the discharge nozzle 21 are connected with drying tube 22 far from one end of conical shell 1, are provided with discharging in the drying tube 22 Heating chamber 23 is provided with dry electromagnetic heating coil 24 along axial uniform winding on the outer wall of the drying tube 22, it is described go out Control cutting assembly is provided in expects pipe 21, the drying tube 22 is provided with rotating blanking valve 25 far from one end of discharge nozzle 21.
By using above-mentioned technical proposal, when carrying out the discharging of FEP finished product materials, control cutting assembly is opened and is released FEP finished product materials part inside conical shell 1 enters in the discharging heating chamber 23 of drying tube 22, controls cutting assembly It closes and stops FEP finished product materials and continue to output, the drying electromagnetism on 22 outer wall of drying tube along axial uniform winding is set and is added Heat coil 24 is powered, and quickly carries out heat temperature raising to drying tube 22, thus quickly to FEP finished product within the regular hour Material is dried, and the FEP finished product materials after completing drying expect quickly to discharge under the switch control of valve 25 under rotation, together When, the discharging control of rotating blanking valve 25 uniformly and conveniently, while above structure facilitates discharging to control, ensure that discharging FEP finished product materials it is dry in place, after adequately removing moisture contained in FEP finished product materials and harmful components, then carry out Quickly and effectively control discharging, guarantee is harmless to the body of operator, highly-safe.
In the specific embodiment of the invention, the control discharge component includes the driving cylinder that 21 side of discharge nozzle is arranged in 31, the output end of the driving cylinder 31 is connected with push rod 32, and one end connection of the push rod 32 far from driving cylinder 31 is useful The cutting material plate 33 to discharge in cutting discharge nozzle 21.
By using above-mentioned technical proposal, after completing polymerization reaction, by the driving cylinder that 21 side of discharge nozzle is arranged in Under 31 driving effect, the push rod 32 of output end connection laterally moves and cutting material plate 33 is driven to open, FEP finished product object Material from entered in discharge nozzle 21 discharging heating chamber 23 in discharging is dried, during drying, driving cylinder 31 drive Dynamic push rod 32 transversely drives cutting material plate 33 to close discharge nozzle 21, guarantees dry efficiency and effect, simple and reliable for structure.
In the specific embodiment of the invention, sealing block 34, the sealing block 34 are provided on 21 inner sidewall of discharge nozzle On be correspondingly arranged on for the card slot 35 that is caught in of cutting material plate 33.
By using above-mentioned technical proposal, in order to guarantee to the FEP finished product materials entered in discharging heating chamber 23 into The efficiency of row heating, meanwhile, the effect of dry moisture and harmful substance is improved, is provided with sealing block on 21 inner sidewall of discharge nozzle 34, the card slot 35 being caught in for cutting material plate 33 is correspondingly arranged on sealing block 34, in cutting material plate 33 with push rod 32 It is snapped under drive in card slot 35, makes to discharge the sealing of heating chamber 23 in place.
In the specific embodiment of the invention, first screw rod 111 and the second screw rod 112 respectively with 1 inner wall of conical shell Gap setting.
By using above-mentioned technical proposal, in order to further increase the first screw rod 111 and the mutual cooperation pair of the second screw rod 112 The mixing effect of material, by the first screw rod 111 and the second screw rod 112 respectively with 1 inner wall gap setting of conical shell, thus Under 9 driving effect of one spinning motor 8 and the second spinning motor, the first screw rod 111 and the second screw rod 112 are respectively along conical shell 1 Central axes symmetrically and to material carry out stirring sufficiently in place.
In the specific embodiment of the invention, first screw rod 111 is extended to far from one end inclination of the first spinning motor 8 The half of 111 length of the first screw rod is arranged in 3/4ths in 1 bottom of conical shell, the length of second screw rod 112 Between.
By using above-mentioned technical proposal, in order to improve the stirring that the first screw rod 111 and the second screw rod 112 cooperate each other First screw rod 111 is extended to 1 bottom of conical shell, the second screw rod 112 far from one end inclination of the first spinning motor 8 by effect Length the half of 111 length of the first screw rod is set between 3/4ths.
In the specific embodiment of the invention, the outer wall of the conical shell 1 includes that the filling set gradually from inside to outside melts The material of coating 41, base 42 and outer layer 43, the filling cladding layer 41 and base 42 is Hastelloy, and the outer layer 43 is gold Belong to material.
By using above-mentioned technical proposal, the outer wall of conical shell 1 mainly uses filling cladding layer 41 and internal material It contacts with each other, using Hastelloy as raw material and using laser cladding Hastelloy on the surface of base 42, and One layer of outer layer 43 of outermost cladding enables the corrosion of 1 hydrogen fluoride resistant of conical shell using metal material, and in electromagnetic heating line Quickly heating reaches reaction temperature and material drying under the action of circle 11, guarantees in carrying out polymerization process, conical shell 1 Service life, can be improved whole corrosion resistance and service life, guarantee reaction be normally carried out, reduce production at This.
In the specific embodiment of the invention, feed pipe 44,44 upper end of feed pipe are provided at the top of the conical shell 1 It is hinged with sealing cover 45.
By using above-mentioned technical proposal, material passes through the feed pipe 44 being arranged at the top of conical shell 1 and is added to taper Polymerization reaction is carried out in cylinder 1, and is hinged with sealing cover 45 in 44 upper end of feed pipe, and material is added to conically shaped for guaranteeing Sealing after in body 1 to conical shell 1, facilitates operation.
The present invention discloses a kind of furnace drying method for efficiently promoting the good electromagnetic heating stirring and drying device of reaction effect, In the specific embodiment of the invention, its step are as follows:
1), material is put into: opening sealing cover 45, and polymerization reaction is produced material required for FEP and is added from feed pipe 44 Enter into conical shell 1 and reacted, after the completion of addition, rotary seal lid 45 shuts feed pipe 44;
2), temperature reaction: being powered to electromagnetic heating coil 11, heat it quickly to conical shell 1, heats function Rate is 120KW, and heating-up time control for the first time was heated to 240 degrees Celsius of reaction temperature at 1.5 hours, lasting heat preservation charging heating Time 1.3 hours;
3), auger: drive cursor 5 along conical shell 1 by 2 drive shaft 4 of driving motor inside conical shell 1 Cone wall revolves, to drive the first screw rod 111 and the second screw rod 112 to circle material along cone wall, in revolution In the process, the first spinning motor 8 and the second spinning motor 9 positioned at the first fixing seat 6 and the second fixing seat 7 respectively drive first Screw rod 111 and the rotation of the second screw rod 112, to make material from 1 bottom of conical shell along spiral, the revolution and rotation of spiral Compound motion is driven a part of material to the effect by revolution and rotation simultaneously of 1 top of conical shell, makes this part Material thread mixing under the action of the centrifugal force, the material of rising under the action of self gravity by declining;
4), discharge drying: after completing polymerization reaction, by the driving of driving cylinder 31 that 21 side of discharge nozzle is arranged in, its is defeated The push rod 32 of outlet connection laterally moves and cutting material plate 33 is driven to open, and FEP finished product materials enter from discharge nozzle 21 After into discharging heating chamber 23, driving 31 driving push rod 32 of cylinder transversely drives cutting material plate 33 to close discharge nozzle 21, Material continuous heating inside conical shell 1 is dry, and the drying electromagnetism on 22 outer wall of drying tube along axial uniform winding is arranged in Heating coil 24 is powered, and quickly carries out heat temperature raising to drying tube 22;
5), drying discharging: the FEP finished product materials after completing drying expect quickly to go out under the switch control of valve 25 under rotation Material.
Pressure sensor 12 and cone in the specific embodiment of the invention, in step (3), at the top of 1 inner wall of conical shell Temperature sensor 13 on 1 inner sidewall of shape cylinder detect pressure inside conical shell 1 or temperature be more than reaction temperature and When pressure value, transmitting electric signal to electromagnetic heating coil 11 reduces the electrical power being passed into electromagnetic heating coil 11, reduction pair The heating temperature of conical shell 1.
By using above-mentioned technical proposal, this electromagnetic heating stirring and drying device by allowing the stirring of material uniform high-efficiency, To reaching full and uniform polymerization reaction, the temperature for improving reaction environment can accelerate the efficiency of reaction, and electromagnetic heating can be with Control heating temperature and internal pressure value well, and dry the moisture in conical shell 1 after the completion of reaction, to allow FER Innocuous, 1 bottom of conical shell are connected with the discharging control assembly for heat drying moisture quickly discharging, guarantee discharging Safely and fast facilitate control, reduce and injury is generated to the body of operator, that the present invention provides a kind of rush reaction effects is good, makes With the service life it is long, it is highly-safe and discharging be conveniently used for electromagnetic heating stirring and drying device.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (10)

1. one kind is used for electromagnetic heating stirring and drying device, it is characterised in that: including enclosed for being carried out for production reaction Conical shell (1), be respectively arranged with driving motor (2) from top to bottom at conical shell (1) the upper center position and subtract The output end of fast machine (3), the speed reducer (3) is connected with shaft (4), and the one end of the shaft (4) far from speed reducer (3) is along perpendicular Conical shell (1) inside is directly extended to after conical shell (1) outer wall and is connected with cursor (5), the cursor (5) Both ends are connected separately with the first fixing seat (6) and the second fixing seat (7) being symmetrically set in left and right, first fixing seat (6) and in the second fixing seat (7) the first spinning motor (8) and the second spinning motor (9), the first rotation electricity are respectively arranged with The output end of machine (8) and the second spinning motor (9) is connected separately with the first screw rod (111) and the second screw rod (112), and described first The length of screw rod (111) is greater than the length of the second screw rod (112) and the two is mutually right in left and right along the central axes of conical shell (1) Claim setting;Spiral uniform winding is provided with electromagnetic heating coil (11), the cone along longitudinal direction on conical shell (1) the outer cone wall It is provided with pressure sensor (12) at the top of shape cylinder (1) inner wall, is provided with temperature sensor on conical shell (1) inner sidewall (13), the pressure sensor (12) and temperature sensor (13) are electrically connected with electromagnetic heating coil (11) respectively;The taper Cylinder (1) bottom is connected with the discharging control assembly for heat drying moisture quickly discharging.
2. according to claim 1 a kind of for electromagnetic heating stirring and drying device, it is characterised in that: the discharging control Component includes the discharge nozzle (21) that one end is connect with conical shell (1) bottom, and the discharge nozzle (21) is far from conical shell (1) One end is connected with drying tube (22), and discharging heating chamber (23) is provided in the drying tube (22), the drying tube (22) It is provided with dry electromagnetic heating coil (24) on outer wall along axial uniform winding, control cutting is provided on the discharge nozzle (21) Component, the drying tube (22) are provided with rotating blanking valve (25) far from the one end of discharge nozzle (21).
3. according to claim 2 a kind of for electromagnetic heating stirring and drying device, it is characterised in that: the control discharging Component includes driving cylinder (31) of the setting in discharge nozzle (21) side, and the output end of driving cylinder (31) is connected with push rod (32), the push rod (32) is connected with far from one end of driving cylinder (31) for cutting off the cutting object to discharge in discharge nozzle (21) Flitch (33).
4. according to claim 3 a kind of for electromagnetic heating stirring and drying device, it is characterised in that: the discharge nozzle (21) it is provided on inner sidewall sealing block (34), is correspondingly arranged on the sealing block (34) and to be caught in for cutting material plate (33) Card slot (35).
5. according to claim 1 a kind of for electromagnetic heating stirring and drying device, it is characterised in that: first screw rod (111) and the second screw rod (112) respectively with conical shell (1) inner wall gap setting.
6. a kind of according to claim 1 or 5 be used for electromagnetic heating stirring and drying device, it is characterised in that: described first Screw rod (111) extends to conical shell (1) bottom, second screw rod (112) far from one end inclination of the first spinning motor (8) Length setting the first screw rod (111) length half between 3/4ths.
7. one kind described according to claim 1 or 2 or 3 or 4 or 5 is used for electromagnetic heating stirring and drying device, it is characterised in that: The outer wall of the conical shell (1) includes the filling cladding layer (41) set gradually from inside to outside, base (42) and outer layer (43), The material of the filling cladding layer (41) and base (42) is Hastelloy, and the outer layer (43) is metal material.
8. according to claim 7 a kind of for electromagnetic heating stirring and drying device, it is characterised in that: the conical shell (1) top is provided with feed pipe (44), and feed pipe (44) upper end is hinged with sealing cover (45).
9. a kind of furnace drying method for fitting above-mentioned electromagnetic heating stirring and drying device, it is characterised in that: steps are as follows:
1), material is put into: opening sealing cover (45), and polymerization reaction is produced material required for FEP and is added from feed pipe (44) Enter in conical shell (1) and reacted, after the completion of addition, rotary seal lid (45) shuts feed pipe (44);
2), temperature reaction: being powered to electromagnetic heating coil (11), heat it quickly to conical shell (1), heats function Rate is 120KW, and heating-up time control for the first time was heated to 240 degrees Celsius of reaction temperature at 1.5 hours, lasting heat preservation charging heating Time 1.3 hours;
3), auger: conical shell (1) is internal to drive cursor (5) along conically shaped by driving motor (2) drive shaft (4) Body (1) internal cone wall revolves, to drive the first screw rod (111) and the second screw rod (112) that material is made to make circumference fortune along cone wall It is dynamic, during revolution, it is located at the first spinning motor (8) and the second rotation of the first fixing seat (6) and the second fixing seat (7) Motor (9) respectively drives the first screw rod (111) and the second screw rod (112) rotation, to make material from conical shell (1) bottom edge Spiral, the revolution of spiral and rotation compound motion make a part of material be driven to conical shell (1) top simultaneously by The effect of revolution and rotation, makes this partial material thread mixing under the action of the centrifugal force, the material of rising is by self gravity Under the action of decline;
4), discharge drying: after completing polymerization reaction, by the driving of driving cylinder (31) that discharge nozzle (21) side is arranged in, its is defeated The push rod (32) of outlet connection laterally moves and cutting material plate (33) is driven to open, and FEP finished product materials are from discharge nozzle (21) In enter discharging heating chamber (23) in after, driving cylinder (31) driving push rod (32) transversely drive cutting material plate (33) It closes discharge nozzle (21), the internal material continuous heating of conical shell (1) is dry, is arranged on drying tube (22) outer wall along axial direction The drying electromagnetic heating coil (24) of uniform winding is powered, and quickly carries out heat temperature raising to drying tube (22);
5), drying discharging: the FEP finished product materials after completing drying expect quickly to go out under the switch controls of valve (25) under rotation Material.
10. a kind of furnace drying method for electromagnetic heating stirring and drying device according to claim 9, it is characterised in that: In step (3), the temperature on the pressure sensor (12) and conical shell (1) inner sidewall at the top of conical shell (1) inner wall is passed Sensor (13) transmits electric signal when detecting that the internal pressure of conical shell (1) or temperature are more than reaction temperature and pressure value To electromagnetic heating coil (11), the electrical power being passed into electromagnetic heating coil (11) is reduced, reduction adds conical shell (1) Hot temperature.
CN201811322335.XA 2018-11-07 2018-11-07 One kind being used for electromagnetic heating stirring and drying device and its furnace drying method Pending CN109612235A (en)

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CN112146424A (en) * 2020-08-24 2020-12-29 上海成界制药设备有限公司 Discharging method and device after material drying
CN113442331A (en) * 2021-07-13 2021-09-28 东莞市顺东新材料有限公司 Masterbatch dewatering device

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Application publication date: 20190412