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CN109568175B - Hair wet tissue feed liquid with lasting fragrance retaining function and preparation method thereof - Google Patents

Hair wet tissue feed liquid with lasting fragrance retaining function and preparation method thereof Download PDF

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Publication number
CN109568175B
CN109568175B CN201910030122.8A CN201910030122A CN109568175B CN 109568175 B CN109568175 B CN 109568175B CN 201910030122 A CN201910030122 A CN 201910030122A CN 109568175 B CN109568175 B CN 109568175B
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parts
essence
hair
polymer
feed liquid
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CN109568175A (en
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王文扬
姜春鹏
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Suzhou Greenleaf Daily Commodity Co ltd
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Suzhou Greenleaf Daily Commodity Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0208—Tissues; Wipes; Patches
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/002—Preparations for repairing the hair, e.g. hair cure
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/12—Preparations containing hair conditioners
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Engineering & Computer Science (AREA)
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  • Cosmetics (AREA)

Abstract

The invention relates to the technical field of daily chemical products, in particular to a hair wet tissue feed liquid with a lasting fragrance retaining function and a preparation method thereof. A wet tissue feed liquid with a lasting fragrance-retaining function for hair comprises the following components: solubilizer, polymer, polyethylene glycol-90M, polyquaternium-10, 1, 3-butanediol, essence, preservative, ethanol and deionized water. The hair wet tissue liquid prepared by the invention has lasting fragrance, the fragrance-retaining time can reach 72 hours or more, and when the hair of the product is used and then washed by shampoo, knotting and winding of the hair, especially damaged hair, can be obviously improved, and the effect is more obvious.

Description

Hair wet tissue feed liquid with lasting fragrance retaining function and preparation method thereof
Technical Field
The invention belongs to the technical field of daily chemical products, and particularly relates to a hair wet tissue feed liquid with a lasting fragrance retaining function and a preparation method thereof.
Background
Nowadays, the rhythm of life of people is faster and faster, and simultaneously, also more and more high to the image requirement of self, the product that is applied to hair nursing is more and more. The fragrance can bring good mood to people, especially for hair products, the gusty fragrance emitted from hair between hairs can make people feel physical and mental pleasure, and not only can make people feel comfortable and pleasant, but also can bring comfortable and pleasant experience to people around. In addition, smooth and glossy hair can also greatly improve social goodness. However, the existing hair care products have no obvious or undesirable fragrance retention effect in actual use, and few products specially aiming at the anti-winding and knotting of the hair in washing and washing are available, so that the market has no wet tissue for hair which has lasting fragrance retention or washing anti-winding. Therefore, the invention of a hair wet tissue feed liquid with lasting fragrance and washing and anti-winding functions is urgently needed.
Disclosure of Invention
In order to solve the above problems, a first aspect of the present invention provides a hair wet towel feed liquid with a lasting fragrance-keeping function, comprising the following components: solubilizer, polymer, polyethylene glycol-90M, polyquaternium-10, 1, 3-butanediol, essence, preservative, ethanol and deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 0.2-5 parts of solubilizer, 0.02-0.5 part of polymer, 0.01-0.2 part of polyethylene glycol-90M, 100.05-0.5 part of polyquaternium, 0.5-5 parts of 1, 3-butanediol, 0.1-5 parts of essence, 0.5-1.5 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 1-3 parts of solubilizer, 0.05-0.2 part of polymer, 0.01-0.15 part of polyethylene glycol-90M, 100.1-0.4 part of polyquaternium, 1-3 parts of 1, 3-butanediol, 0.2-1 part of essence, 0.8-1.2 parts of preservative, 1-10 parts of ethanol and 70-80 parts of deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 1.5-2.5 parts of solubilizer, 0.08-0.15 part of polymer, 0.01-0.1 part of polyethylene glycol-90M, 100.1-0.2 part of polyquaternary ammonium salt, 1.5-2.5 parts of 1, 3-butanediol, 0.3-0.8 part of essence, 0.9-1.2 parts of preservative, 1.5-5.0 parts of ethanol and 72-78 parts of deionized water.
As a preferred technical scheme, the solubilizer is selected from one or more of polysorbate-20, polysorbate-80, PEG-40 hydrogenated castor oil and PEG-60 hydrogenated castor oil.
As a preferable technical scheme, the polymer is selected from one or more of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, starch hydroxypropyl trimethyl ammonium chloride, polyquaternium-74 and polyquaternium-47.
As a preferable technical scheme, the weight ratio of the essence to the polymer is 1 (0.1-0.3).
As a preferred technical scheme, the essence is selected from one or more of lavender essence, rose essence, osmanthus flower essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence and juicy peach essence.
As a preferable technical scheme, the preservative is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, poly (aminopropyl) biguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylyl hydroximic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol and p-hydroxyacetophenone.
A preparation method of a hair wet tissue feed liquid with a lasting fragrance-retaining function comprises the following steps:
(1) dispersing the polyethylene glycol-90M and the polyquaternium-10 by using 1, 3-butanediol, adding deionized water, heating to 75-85 ℃, stirring until the mixture is completely dissolved, cooling to 40-50 ℃, adding a polymer, and stirring until the polymer is dissolved to obtain a mixture A;
(2) fully dissolving the solubilizer and the essence and uniformly stirring to obtain a mixture B;
(3) and stirring the mixture A, adding the mixture B, uniformly mixing, adding a preservative, and finally adding ethanol to obtain the hair wet tissue feed liquid with the lasting fragrance keeping function.
Has the advantages that: the hair wet tissue liquid prepared by the invention has lasting fragrance, the fragrance-retaining time can reach 72 hours or more, and when the hair of the product is used and then washed by shampoo, knotting and winding of the hair, especially damaged hair, can be obviously improved, and the effect is more obvious.
Detailed Description
The technical features of the technical solutions provided by the present invention are further clearly and completely described below with reference to the specific embodiments, and the scope of protection is not limited thereto.
The words "preferred", "more preferred", and the like, in the present invention refer to embodiments of the invention that may provide certain benefits, under certain circumstances. However, other embodiments may be preferred, under the same or other circumstances. Furthermore, the recitation of one or more preferred embodiments does not imply that other embodiments are not useful, nor is it intended to exclude other embodiments from the scope of the invention.
When a range of values is disclosed herein, the range is considered to be continuous and includes both the minimum and maximum values of the range, as well as each value between such minimum and maximum values. Further, when a range refers to an integer, each integer between the minimum and maximum values of the range is included. Further, when multiple range-describing features or characteristics are provided, the ranges may be combined. In other words, unless otherwise indicated, all ranges disclosed herein are to be understood to encompass any and all subranges subsumed therein. For example, a stated range from "1 to 10" should be considered to include any and all subranges between the minimum value of 1 and the maximum value of 10. Exemplary subranges of the range 1 to 10 include, but are not limited to, 1 to 6.1, 3.5 to 7.8, 5.5 to 10, and the like.
In order to solve the above problems, a first aspect of the present invention provides a hair wet towel feed liquid with a lasting fragrance-keeping function, comprising the following components: solubilizer, polymer, polyethylene glycol-90M, polyquaternium-10, 1, 3-butanediol, essence, preservative, ethanol and deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 0.2-5 parts of solubilizer, 0.02-0.5 part of polymer, 0.01-0.2 part of polyethylene glycol-90M, 100.05-0.5 part of polyquaternium, 0.5-5 parts of 1, 3-butanediol, 0.1-5 parts of essence, 0.5-1.5 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 1-3 parts of solubilizer, 0.05-0.2 part of polymer, 0.01-0.15 part of polyethylene glycol-90M, 100.1-0.4 part of polyquaternium, 1-3 parts of 1, 3-butanediol, 0.2-1 part of essence, 0.8-1.2 parts of preservative, 1-10 parts of ethanol and 70-80 parts of deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 1.5-2.5 parts of solubilizer, 0.08-0.15 part of polymer, 0.01-0.1 part of polyethylene glycol-90M, 100.1-0.2 part of polyquaternary ammonium salt, 1.5-2.5 parts of 1, 3-butanediol, 0.3-0.8 part of essence, 0.9-1.2 parts of preservative, 1.5-5.0 parts of ethanol and 72-78 parts of deionized water.
Solubilizer
The solubilizer is a surfactant with solubilization capacity, and solubilization refers to a process of increasing solubility of a difficultly soluble medicament in a solvent under the action of the surfactant to form a solution.
In a preferred embodiment, the solubilizing agent of the present invention is selected from one or more of polysorbate-20, polysorbate-80, PEG-40 hydrogenated castor oil, and PEG-60 hydrogenated castor oil.
In a preferred embodiment, the solubilizing agent of the present invention is polysorbate-20, purchased from zheng minggu chemical products limited.
Polymer and method of making same
In a preferred embodiment, the polymer of the present invention is selected from one or more of acrylamidopropyltrimethylammonium chloride/acrylamide copolymers, starch hydroxypropyltrimethylammonium chloride, polyquaternium-74, polyquaternium-47.
In a preferred embodiment, the weight ratio of the perfume of the invention to the polymer is 1 (0.1-0.3).
In a preferred embodiment, the polymer of the present invention is an acrylamidopropyl trimethyl ammonium chloride/acrylamide copolymer available from eosin, Shanghai, Inc.
The inventor adds the polymer into the formula to improve the hair quality, and the inventor finds that the product adopting the formula has excellent washing anti-winding performance for the hair with damaged hair quality, supposes that the surface hydrophilicity of the hair is enhanced after the hair is damaged, the hair is more easily adsorbed on the surface of the hair with negative charge through the synergistic effect of the polysorbate-20 and the polyquaternium-10, the adsorption is firmer, and the anionic surfactant and the cationic polymer form a flocculation in situ on the hair surface during hair washing to reconstruct a hydrophobic layer, thereby not only obviously improving the winding and combing performance between the hair filaments, but also effectively preventing the generation of static electricity and leading the hair to be lighter, graceful and smooth.
Polyethylene glycol
The polyethylene glycol has good water solubility and good intermiscibility with a plurality of organic matter components. They have excellent lubricity, moisture retention, dispersibility, adhesives, antistatic agents, softeners and the like, and are widely applied in the industries of cosmetics, pharmacy, chemical fibers, rubber, plastics, papermaking, paint, electroplating, pesticides, metal processing, food processing and the like.
The polyethylene glycol-90M is used as an adhesive, an emulsion stabilizer and viscosity control in cosmetics, and is purchased from Guangzhou Mei chemical Co.
The inventor of the application finds that the polyethylene glycol added into the formula can play a role in film forming, can smooth hair scales, improve winding and combing properties among hair strands, and synergistically promote the hair to be more bright and natural with other components in the formula.
Polyquaternary ammonium salts
The polyquaterniums of the present invention are cationic conditioning agents for use in personal care products. It is very mild and has good compatibility with anionic, nonionic, cationic and amphoteric surfactant systems. Completely soluble in water, enabling it to be used in transparent systems.
The polyquaternium-10 of the invention is a water-soluble cationic conditioner and is purchased from Wang chemical company Limited in Guangzhou flower.
The inventor of the application finds that the addition of the polymer in the formula can effectively improve the antistatic property and the combing property of the hair, but the single use of the polymer can easily cause the hair to be frizzy and fluffy. The inventors have therefore surprisingly found that the addition of polyquaternium-10 to the formulation not only ameliorates the above-mentioned problems but also provides a longer lasting fragrance to the hair. The inventor conjectures that the possible reasons are that the polyquaternium-10 has lower charge and high water content compared with the polymer, is easier to soften the hair, can interact with the polymer to form a three-dimensional network structure to be adsorbed on the hair, and the essence molecules are embedded in the structure to keep the fragrance for a long time.
Essence
The essence is a raw material for endowing cosmetics with certain fragrance, is one of key raw materials in the manufacturing process, is prepared by blending and mixing various spices, and has certain type of fragrance, namely fragrance type.
In some embodiments, the essence of the present invention is selected from one or more of lavender essence, rose essence, osmanthus essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, and juicy peach essence.
In a preferred embodiment, the fragrance of the present invention is a rose fragrance, purchased from Guangzhou Baoshidi perfumery, Inc.
Preservative
The preservative of the present invention refers to a natural or synthetic chemical ingredient used in foods, medicines, paints, biological specimens, etc. to retard spoilage caused by microbial growth or chemical changes.
In some embodiments, the preservative of the present invention is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, polyallylguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylyl hydroxamic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol, and p-hydroxyacetophenone.
In a preferred embodiment, the preservative of the present invention is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech, Inc.
The second aspect of the invention provides a preparation method of a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the following steps:
(1) dispersing the polyethylene glycol-90M and the polyquaternium-10 by using 1, 3-butanediol, adding deionized water, heating to 75-85 ℃, stirring until the mixture is completely dissolved, cooling to 40-50 ℃, adding a polymer, and stirring until the polymer is dissolved to obtain a mixture A;
(2) fully dissolving the solubilizer and the essence and uniformly stirring to obtain a mixture B;
(3) and stirring the mixture A, adding the mixture B, uniformly mixing, adding a preservative, and finally adding ethanol to obtain the hair wet tissue feed liquid with the lasting fragrance keeping function.
The present invention will now be described in detail by way of examples, and the starting materials used are commercially available unless otherwise specified.
Examples
Example 1
Embodiment 1 provides a wet tissue feed liquid for hair with a lasting fragrance-retaining function, which comprises the following components: 0.2 part of solubilizer, 0.02 part of polymer, 0.01 part of polyethylene glycol-90M, 100.05 parts of polyquaternium, 0.5 part of 1, 3-butanediol, 0.1 part of essence, 0.5 part of preservative, 0 part of ethanol and 60 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A preparation method of a hair wet tissue feed liquid with a lasting fragrance-retaining function comprises the following steps:
(1) dispersing the polyethylene glycol-90M and the polyquaternium-10 by using 1, 3-butanediol, adding deionized water, heating to 80 ℃, stirring until the mixture is completely dissolved, cooling to 45 ℃, adding a polymer, and stirring until the polymer is dissolved to obtain a mixture A;
(2) fully dissolving the solubilizer and the essence and uniformly stirring to obtain a mixture B;
(3) and stirring the mixture A, adding the mixture B, uniformly mixing, adding a preservative, and finally adding ethanol to obtain the hair wet tissue feed liquid with the lasting fragrance keeping function.
Example 2
Embodiment 2 provides a wet tissue feed liquid for hair with a lasting fragrance-retaining function, which comprises the following components: 5 parts of solubilizer, 0.5 part of polymer, 0.2 part of polyethylene glycol-90M, 100.5 parts of polyquaternium, 5 parts of 1, 3-butanediol, 5 parts of essence, 1.5 parts of preservative, 15 parts of ethanol and 90 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Example 3
Embodiment 3 provides a wet tissue feed liquid for hair with a lasting fragrance-retaining function, which comprises the following components: 1 part of solubilizer, 0.05 part of polymer, 0.01 part of polyethylene glycol-90M, 100.1 parts of polyquaternium, 1 part of 1, 3-butanediol, 0.2 part of essence, 0.8 part of preservative, 1 part of ethanol and 70 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Example 4
Embodiment 4 provides a wet tissue feed liquid for hair with a lasting fragrance function, which comprises the following components: 3 parts of solubilizer, 0.2 part of polymer, 0.15 part of polyethylene glycol-90M, 100.4 parts of polyquaternium, 3 parts of 1, 3-butanediol, 1 part of essence, 1.2 parts of preservative, 10 parts of ethanol and 80 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Example 5
Embodiment 5 provides a wet tissue feed liquid for hair with lasting fragrance function, which comprises the following components: 2 parts of solubilizer, 0.1 part of polymer, 0.01 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 1
Comparative example 1 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 0.01 part of solubilizer, 0.1 part of polymer, 0.01 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 2
Comparative example 2 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 20 parts of solubilizer, 0.1 part of polymer, 0.01 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 3
Comparative example 3 provides a wet wipe feed solution for hair with a lasting fragrance retention function, comprising the following components: 2 parts of solubilizer, 0 part of polymer, 0.01 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 4
Comparative example 4 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 2 parts of solubilizer, 10 parts of polymer, 0.01 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 5
Comparative example 5 provides a hair wipe feed solution with a lasting fragrance retention function, comprising the following components: 2 parts of solubilizer, 0.1 part of polymer, 0.01 part of polyethylene glycol-90M, 100 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 6
Comparative example 6 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 2 parts of solubilizer, 0.1 part of polymer, 0.01 part of polyethylene glycol-90M, 1010 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 7
Comparative example 7 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 2 parts of solubilizer, 0.1 part of polymer, 0 part of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Comparative example 8
Comparative example 8 provides a wet wipe feed solution for hair having a lasting fragrance function, comprising the following components: 2 parts of solubilizer, 0.1 part of polymer, 5 parts of polyethylene glycol-90M, 100.2 parts of polyquaternium, 2 parts of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 1.5 parts of ethanol and 75 parts of deionized water.
The solubilizer is polysorbate-20, purchased from Zhengzhou Mingzui chemical products, Inc.
The polymer was an acrylamidopropyltrimethylammonium chloride/acrylamide copolymer, purchased from eosin, Shanghai, Inc.
The polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou.
The polyquaternium-10 is a water-soluble cationic conditioner, purchased from WANGCHEMICAL CORPORATION OF Guangzhou state flower.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is p-hydroxyacetophenone, purchased from Nanjing Ponno Biotech Co., Ltd.
A method for preparing a hair wet tissue feed liquid with a lasting fragrance-retaining function, which comprises the same steps as example 1.
Evaluation of Performance
1. Fragrance longevity test
The test method comprises the following steps: placing the hair bundle treated with the feed liquid in natural ventilation environment at normal temperature, and smelling the hair bundle with nose after a certain time interval.
2. Hair flexibility test
The test method comprises the following steps: performing sensory evaluation on the hair tresses treated by the feed liquid for flexibility, wherein the evaluation standard adopts 5 grades, and 1 grade represents very poor; 2 denotes the difference; score 3 indicates general; score 4 indicates good.
3. Hair Wet combing test
The test method comprises the following steps: the same batch of 6 tresses of hair was selected and divided into two groups, one for each 3 tresses. One group was blank and one group was sample. Wherein the blank group is directly cleaned by common shampoo sold in the market, the sample group is firstly wiped by wet tissue feed liquid and then cleaned by shampoo sold in the market, and other conditions are ensured to be consistent. An instron hair tester is used for carrying out wet combing test, a hair bundle is pulled from an initial position to an end position at a constant speed, and the total work (energy) of the friction resistance between the hair and the comb teeth in the process represents combing property. The average value of combing work is obtained by testing 3 hair tresses in each group, and the combing work reduction percentage is calculated by comparing with a blank group.
TABLE 1
Figure BDA0001943880900000121
Figure BDA0001943880900000131

Claims (6)

1. The hair wet tissue feed liquid with the lasting fragrance keeping function is characterized by comprising the following components in parts by weight: 0.2-5 parts of solubilizer, 0.02-0.5 part of polymer, 0.01-0.2 part of polyethylene glycol-90M, 100.05-0.5 part of polyquaternary ammonium salt, 0.5-5 parts of 1, 3-butanediol, 0.1-5 parts of essence, 0.5-1.5 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water, wherein the solubilizer is selected from polysorbate-20, the polymer is selected from acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, and the weight ratio of the essence to the polymer is 1 (0.1-0.3).
2. The hair wet wipe feed liquid according to claim 1, which is characterized by comprising the following components in parts by weight: 1-3 parts of solubilizer, 0.05-0.2 part of polymer, 0.01-0.15 part of polyethylene glycol-90M, 100.1-0.4 part of polyquaternium, 1-3 parts of 1, 3-butanediol, 0.2-1 part of essence, 0.8-1.2 parts of preservative, 1-10 parts of ethanol and 70-80 parts of deionized water.
3. The hair wet wipe feed liquid according to claim 2, which is characterized by comprising the following components in parts by weight: 1.5-2.5 parts of solubilizer, 0.08-0.15 part of polymer, 0.01-0.1 part of polyethylene glycol-90M, 100.1-0.2 part of polyquaternary ammonium salt, 1.5-2.5 parts of 1, 3-butanediol, 0.3-0.8 part of essence, 0.9-1.2 parts of preservative, 1.5-5.0 parts of ethanol and 72-78 parts of deionized water.
4. The hair wet wipe feed liquid of claim 1, wherein the essence is selected from one or more of lavender essence, rose essence, osmanthus essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, and juicy peach essence.
5. The wet wipe feed of claim 1 wherein the preservative is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, polyallybiguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylhydroxamic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol, and p-hydroxyacetophenone.
6. The method for preparing the hair wet wipe feed liquid according to claim 1, which is characterized by comprising the following steps:
(1) dispersing the polyethylene glycol-90M and the polyquaternium-10 by using 1, 3-butanediol, adding deionized water, heating to 75-85 ℃, stirring until the mixture is completely dissolved, cooling to 40-50 ℃, adding a polymer, and stirring until the polymer is dissolved to obtain a mixture A;
(2) fully dissolving the solubilizer and the essence and uniformly stirring to obtain a mixture B;
(3) and stirring the mixture A, adding the mixture B, uniformly mixing, adding a preservative, and finally adding ethanol to obtain the hair wet tissue feed liquid with the lasting fragrance keeping function.
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Publication number Priority date Publication date Assignee Title
CN104188827A (en) * 2014-07-14 2014-12-10 广州立白企业集团有限公司 Hair-washing and bathing wet wipe and preparation method thereof
CN104825363A (en) * 2015-05-13 2015-08-12 朱敏 Easy-to-absorb disposable hair mask and preparation method thereof
CN106333878A (en) * 2016-10-26 2017-01-18 澳宝化妆品（惠州）有限公司 Curly hair rewinding composition using novel anionic polymer

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104188827A (en) * 2014-07-14 2014-12-10 广州立白企业集团有限公司 Hair-washing and bathing wet wipe and preparation method thereof
CN104825363A (en) * 2015-05-13 2015-08-12 朱敏 Easy-to-absorb disposable hair mask and preparation method thereof
CN106333878A (en) * 2016-10-26 2017-01-18 澳宝化妆品（惠州）有限公司 Curly hair rewinding composition using novel anionic polymer

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