CN109537365A - A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper - Google Patents
A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper Download PDFInfo
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- CN109537365A CN109537365A CN201811308376.3A CN201811308376A CN109537365A CN 109537365 A CN109537365 A CN 109537365A CN 201811308376 A CN201811308376 A CN 201811308376A CN 109537365 A CN109537365 A CN 109537365A
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- CN
- China
- Prior art keywords
- siraitia grosvenorii
- preparation
- tipping paper
- chicken flavor
- characteristic chicken
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Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
- A24D1/022—Papers for roll-your-own cigarettes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
Landscapes
- Fats And Perfumes (AREA)
Abstract
本专利公开了一种具有罗汉果特征香味接装纸的制备方法。包括以下步骤：(1)罗汉果精油的制备；(2)罗汉果浸膏的制备；(3)具有罗汉果特征香味香精调配；(4)具有罗汉果特征香味接装纸制备：(5)对接装纸进行压纹、干燥、分切，密封保存。本发明工艺步骤简单，制备的接装纸投入生产后，通过感官评吸，能够明显增加卷烟甜润感，烟气更加柔和细腻，增加卷烟抽吸的舒适度，降低卷烟的刺激性，余味较干净，降低卷烟的枯焦气，降低卷烟的干燥感，能够明显体现罗汉果特征香味，并且罗汉果香味持久。This patent discloses a preparation method of a tipping paper with the characteristic aroma of Luo Han Guo. The method comprises the following steps: (1) preparation of essential oil of Luo Han Guo; (2) preparation of Luo Han Guo extract; (3) preparation of aroma essence with Luo Han Guo characteristic; (4) preparation of tipping paper with characteristic aroma of Luo Han Guo: (5) carrying out butt packing paper Embossed, dried, cut, sealed and stored. The process steps of the invention are simple, and after the prepared tipping paper is put into production, through sensory evaluation, the sweetness of the cigarette can be significantly increased, the smoke is softer and more delicate, the smoking comfort of the cigarette is increased, the irritation of the cigarette is reduced, and the aftertaste is clean. , reduce the scorch gas of cigarettes, reduce the dry feeling of cigarettes, can obviously reflect the characteristic aroma of Luo Han Guo, and the aroma of Luo Han Guo is lasting.
Description
Technical field
The invention belongs to tobacco industry field, a kind of specific preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper.
Background technique
With the increasingly raising of people's quality of life, smoking and health problem be people's growing interest focus and discussion
Hot spot, in this context tobacco business actively develop reduce cigarette harm to the human body work sutdy, in cigarette addition in
Herbal medicine can reduce harm of the cigarette to human body.CN 1931039A discloses a kind of cigarette Chinese herb feed additive, can be effective
Reduce respiratory disease.Bronchitis is because of one of disease the most apparent caused by smoking.Siraitia grosvenorii has relieving cough and reducing sputum, clear
Thermal detoxification, clearing away heat and moistening the bowels and other effects are usually used in treating the diseases such as tracheitis, bronchitis, asthma, sphagitis, add in cigarette
Add Siraitia grosvenorii essential oil, medicinal extract can reduce harm brought by cigarette.
With the raising of the level of consumption, people are more and more to cigarette taste requirements, in order to more be selected to consumer,
Occurs the cigarette of various different tastes in the market, and the addition manner of flavors and fragrances also becomes diversification.CN 105533794
A kind of method for preparing the fragrant cigarette perfume (or spice) line of honey using longan honey is disclosed, cigarette sweet moisture feeling can be increased, improve cigarette person's
Cigarette impression.205474593 N of CN discloses the preparation method of tea flavour tipping paper, provides the cigarette of more tastes for consumer.
The present invention provide Siraitia grosvenorii characteristic chicken flavor tipping paper preparation method, make cigarette have Siraitia grosvenorii feature fragrance and can
Improve cigarette quality.
Summary of the invention
It is an object of the invention to overcome the shortage of prior art, cigarette irritation and miscellaneous gas can reduced by providing one kind,
Mitigating dry sensation, improves pleasant impression, harm of the cigarette to human body can also be reduced while flue gas is fine and smooth soft by improving sweet degree,
And the preparation method of the cigarette tipping paper with Siraitia grosvenorii characteristic chicken flavor.
A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper, includes the following steps:
The preparation of step 1 Siraitia grosvenorii essential oil: Grosvenor Momordica Fruit is set in a round bottom flask, and water is added and is impregnated, then
Under electric jacket heating, is distilled using volatile oil extractor and extract Siraitia grosvenorii volatile oil；Siraitia grosvenorii volatile oil is extracted, will be had
Machine is mutually dry with anhydrous sodium sulfate, then is concentrated under reduced pressure with rotary evaporator and removes solvent, obtains Siraitia grosvenorii essential oil；；
The preparation of step 2 Luo Han Guo Paste In Foods: Grosvenor Momordica Fruit is wrapped with filter paper, is fitted into Soxhlet extraction device, electric heating
Set heating filters extracting solution with ethanol water refluxing extraction, and filtrate removes solvent with Rotary Evaporators, obtains Siraitia grosvenorii leaching
Cream；
Step 3 dissolves in Siraitia grosvenorii essential oil and Luo Han Guo Paste In Foods in ethanol water, arhat fruity liquid is made, wherein arhat
The mass ratio of fruit essential oil, Luo Han Guo Paste In Foods and dense ethanol water is 0.001-0.01:0.01-0.05:0.949-0.98；
Step 4 is prepared with Siraitia grosvenorii characteristic chicken flavor tipping paper: will be on arhat fruity liquid even spread to tipping paper；
Step 5 embosses tipping paper, is dried, is cut, and is sealed.
Further to improve, the mass ratio 1:5-6.25 of Grosvenor Momordica Fruit and water in the step 1 impregnates 12h.
It is further to improve, it is slightly boiled that with electric jacket deionized water is heated in the step 1, is flowed back with volatile oil extractor
Extract 5-7h.
It is further to improve, with a small amount of washed with ether volatile oil extractor in the step 1, pour into Siraitia grosvenorii volatile oil
In.
It is further to improve, Siraitia grosvenorii volatile oil ether is extracted 2 times in the step 1, merges organic phase with anhydrous
Sodium sulphate is dry for 24 hours.
Further to improve, rotary evaporator heating temperature initial value is set as 30 DEG C of concentrations in the step 1, will then add
Hot temperature is raised to 60 DEG C and removes solvent.
It is further to improve, Grosvenor Momordica Fruit and ethanol water solid-liquid ratio=4-6:50g/mL, ethyl alcohol in the step 2
The concentration of aqueous solution is 70-90%, refluxing extraction 3-5h.
Further to improve, rotary evaporator heating temperature initial value is set as 45 DEG C of concentrations in the step 2, will then add
Hot temperature is raised to 65 DEG C and removes solvent.
Further to improve, the mass fraction of ethanol water is 60% in the step 3.
Further to improve, Siraitia grosvenorii essence additive amount on tipping paper is 0.01-1g/m in the step 42。
This patent gain: present invention process step is simple, after the tipping paper of preparation puts into production, passes through sensory evaluating smoking, energy
Cigarette sweet moisture feeling is enough obviously increased, the softer exquisiteness of flue gas increases the comfort level of cigarette smoking, reduces the irritation of cigarette,
Pleasant impression is cleaner, reduces the withered and burnt smell of cigarette, reduces the dry sensation of cigarette, can obviously embody Siraitia grosvenorii characteristic chicken flavor, and
Siraitia grosvenorii lasting fragrance.
Specific embodiment
The present invention is further explained combined with specific embodiments below.Following embodiment is only used for further tool of the invention
Body description.
Embodiment 1
Grosvenor Momordica Fruit 80g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket adds
Heat collects Siraitia grosvenorii essential oil to slightly boiled, with volatile oil extractor, and refluxing extraction 5h after reflux, is waved with a small amount of washed with ether
Hair oil extractor, mixed liquor are collected into 50mL triangular flask, then with 30mL ether extract 2 times, merge collect organic phase in
In 150mL triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature
Degree is 30 DEG C, and in the case where drop under no liquid, temperature is raised to 60 DEG C, is kept in the case where drop under no liquid
15min.) obtain Siraitia grosvenorii essential oil.
It weighs Grosvenor Momordica Fruit 40g to be wrapped with filter paper, is put into Soxhlet extraction device, 500mL is added in round-bottomed flask
Concentration is 70% ethyl alcohol, and electric jacket is heated to slightly boiled, refluxing extraction 3h, is filtered, and filtrate is collected, and is concentrated under reduced pressure and removes solvent (rotation
Turning evaporimeter initial heating temperature is 45 DEG C, in the case where drop under no liquid, temperature is raised to 65 DEG C, under no liquid
15min is kept in the case where drop.) obtain Luo Han Guo Paste In Foods.
The Siraitia grosvenorii essential oil that will be prepared, medicinal extract are deployed into Siraitia grosvenorii essence, Siraitia grosvenorii essential oil, medicinal extract, 60% ethyl alcohol
Mass ratio=0.001:0.05:0.949.
The deployed essence with Siraitia grosvenorii characteristic chicken flavor is applied on tipping paper, additive amount 0.01g/m2
By on deployed essence even spread to tipping paper, tipping paper is embossed, dried, is cut, is put into production
Prepare the cigarette with Siraitia grosvenorii characteristic flavor on basis.
Embodiment 2
Grosvenor Momordica Fruit 90g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket adds
Heat collects Siraitia grosvenorii essential oil to slightly boiled, with volatile oil extractor, and refluxing extraction 6h after reflux, is waved with a small amount of washed with ether
Hair oil extractor, mixed liquor are collected into 50mL triangular flask, then with 30mL ether extract 2 times, merge collect organic phase in
In 150mL triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature
Degree is 30 DEG C, and in the case where drop under no liquid, temperature is raised to 60 DEG C, is kept in the case where drop under no liquid
15min.) obtain Siraitia grosvenorii essential oil.
It weighs Grosvenor Momordica Fruit 50g to be wrapped with filter paper, is put into Soxhlet extraction device, 500mL is added in round-bottomed flask
Concentration is 80% ethyl alcohol, and electric jacket is heated to slightly boiled, refluxing extraction 4h, is filtered, and filtrate is collected, and is concentrated under reduced pressure and removes solvent (rotation
Turning evaporimeter initial heating temperature is 45 DEG C, in the case where drop under no liquid, temperature is raised to 65 DEG C, under no liquid
15min is kept in the case where drop.) obtain Luo Han Guo Paste In Foods.
The Siraitia grosvenorii essential oil that will be prepared, medicinal extract are deployed into Siraitia grosvenorii essence, Siraitia grosvenorii essential oil, medicinal extract, 60% ethyl alcohol
Mass ratio=0.005:0.03:0.965.
There is Siraitia grosvenorii spy to be applied to additive amount on tipping paper to the essence of fragrance is 0.05g/m by deployed2
By on deployed essence even spread to tipping paper, tipping paper is embossed, dried, is cut, is put into production
Prepare the cigarette with Siraitia grosvenorii characteristic flavor on basis.
Embodiment 3
Grosvenor Momordica Fruit 100g is weighed in 1000mL round-bottomed flask, 500mL deionized water is added and impregnates 12h, electric jacket
Be heated to it is slightly boiled, with volatile oil extractor collect Siraitia grosvenorii essential oil, refluxing extraction 7h, after reflux, with a small amount of washed with ether
Volatile oil extractor, mixed liquor are collected into 50mL triangular flask, then with 30mL ether extract 2 times, merge collect organic phase in
In 150mL triangular flask, organic phase is dry for 24 hours with anhydrous sodium sulfate, is concentrated under reduced pressure and removes solvent (Rotary Evaporators initial heating temperature
Degree is 30 DEG C, and in the case where drop under no liquid, temperature is raised to 60 DEG C, is kept in the case where drop under no liquid
15min.) obtain Siraitia grosvenorii essential oil.
It weighs Grosvenor Momordica Fruit 60g to be wrapped with filter paper, is put into Soxhlet extraction device, 500mL is added in round-bottomed flask
Concentration is 90% ethyl alcohol, and electric jacket is heated to slightly boiled, refluxing extraction 5h, is filtered, and filtrate is collected, and is concentrated under reduced pressure and removes solvent (rotation
Turning evaporimeter initial heating temperature is 45 DEG C, in the case where drop under no liquid, temperature is raised to 65 DEG C, under no liquid
15min is kept in the case where drop.) obtain Luo Han Guo Paste In Foods.
The Siraitia grosvenorii essential oil that will be prepared, medicinal extract are deployed into Siraitia grosvenorii essence, Siraitia grosvenorii essential oil, medicinal extract, 60% ethyl alcohol
Mass ratio=0.01:0.01:0.98.
There is Siraitia grosvenorii spy to be applied to additive amount on tipping paper to the essence of fragrance is 0.1g/m by deployed2。
By on deployed essence even spread to tipping paper, tipping paper is embossed, dried, is cut, is put into production
Prepare the cigarette with Siraitia grosvenorii characteristic flavor on basis.
By tipping paper prepared in the above embodiments, put into spicing machine and produced, smoke panel test personnel according to
" GB5606.4-2005 tobacco and tobacco product sensory evaluation method " carries out sensory evaluating smoking, and result details are shown in Table 1.
Table 1: sensory evaluating smoking's result.
1#: conventional cigarette；2#: the cigarette prepared according to embodiment 1；3#: the cigarette prepared according to embodiment 2；4#: according to
Cigarette prepared by embodiment 3.
Sensory results know that tipping paper prepared by the present invention can obviously increase cigarette sweet moisture feeling, and flue gas is softer thin
It is greasy, increase the comfort level of cigarette smoking, reduce the irritation of cigarette, pleasant impression is cleaner, reduces the withered and burnt smell of cigarette, reduces cigarette
Dry sensation, can obviously embody Siraitia grosvenorii characteristic chicken flavor, and Siraitia grosvenorii lasting fragrance.
Claims (10)
1. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper, which comprises the following steps:
The preparation of step 1 Siraitia grosvenorii essential oil: Grosvenor Momordica Fruit is set in a round bottom flask, and water is added and is impregnated, then in electric heating
Under set heating, is distilled using volatile oil extractor and extract Siraitia grosvenorii volatile oil；Siraitia grosvenorii volatile oil is extracted, by organic phase
It is dry with anhydrous sodium sulfate, then be concentrated under reduced pressure with rotary evaporator and remove solvent, obtain Siraitia grosvenorii essential oil；；
The preparation of step 2 Luo Han Guo Paste In Foods: Grosvenor Momordica Fruit is wrapped with filter paper, is fitted into Soxhlet extraction device, electric jacket adds
Heat filters extracting solution with ethanol water refluxing extraction, and filtrate removes solvent with Rotary Evaporators, obtains Luo Han Guo Paste In Foods；
Step 3 dissolves in Siraitia grosvenorii essential oil and Luo Han Guo Paste In Foods in ethanol water, and arhat fruity liquid is made, wherein Siraitia grosvenorii essence
The mass ratio of oil, Luo Han Guo Paste In Foods and dense ethanol water is 0.001-0.01:0.01-0.05:0.949-0.98；
Step 4 is prepared with Siraitia grosvenorii characteristic chicken flavor tipping paper: will be on arhat fruity liquid even spread to tipping paper；
Step 5 embosses tipping paper, is dried, is cut, and is sealed.
2. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
The mass ratio 1:5-6.25 of Grosvenor Momordica Fruit and water in step 1 impregnates 12h.
3. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
It is slightly boiled that with electric jacket deionized water is heated in step 1, with volatile oil extractor refluxing extraction 5-7h.
4. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
With a small amount of washed with ether volatile oil extractor in step 1, pour into Siraitia grosvenorii volatile oil.
5. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
Siraitia grosvenorii volatile oil ether is extracted 2 times in step 1, it is dry for 24 hours with anhydrous sodium sulfate to merge organic phase.
6. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
Rotary evaporator heating temperature initial value is set as 30 DEG C of concentrations in step 1, and heating temperature is then raised to 60 DEG C and removes solvent.
7. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
Grosvenor Momordica Fruit and ethanol water solid-liquid ratio=4-6:50g/mL in step 2, the concentration of ethanol water are 70-90%, are returned
Stream extracts 3-5h.
8. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
Rotary evaporator heating temperature initial value is set as 45 DEG C of concentrations in step 2, and heating temperature is then raised to 65 DEG C and removes solvent.
9. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
The mass fraction of ethanol water is 60% in step 3.
10. a kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper as described in claim 1, it is characterised in that described
Siraitia grosvenorii essence additive amount on tipping paper is 0.01-1g/m in step 42。
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| CN201811308376.3A CN109537365A (en) | 2018-11-05 | 2018-11-05 | A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111764194A (en) * | 2020-07-02 | 2020-10-13 | 广西中烟工业有限责任公司 | A kind of preparation method of Luo Han Guo flavonoids tipping paper for cigarettes |
| CN114747798A (en) * | 2022-03-30 | 2022-07-15 | 湖北中烟工业有限责任公司 | A kind of tobacco flavor and preparation method thereof |
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Application publication date: 20190329 |