CN109425567A - A kind of characterizing method of the permeability based on carbonate reservoir - Google Patents
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- 230000035699 permeability Effects 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 40
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 title claims abstract description 29
- 239000011148 porous material Substances 0.000 claims abstract description 70
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims abstract description 56
- 229910052753 mercury Inorganic materials 0.000 claims abstract description 56
- 238000001179 sorption measurement Methods 0.000 claims abstract description 21
- 238000002347 injection Methods 0.000 claims abstract description 19
- 239000007924 injection Substances 0.000 claims abstract description 19
- 238000012512 characterization method Methods 0.000 claims abstract description 10
- 238000002474 experimental method Methods 0.000 claims abstract description 5
- 239000011435 rock Substances 0.000 claims description 14
- 238000002459 porosimetry Methods 0.000 claims description 9
- 239000011800 void material Substances 0.000 claims description 3
- 238000011158 quantitative evaluation Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000008092 positive effect Effects 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/082—Investigating permeability by forcing a fluid through a sample
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/088—Investigating volume, surface area, size or distribution of pores; Porosimetry
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Abstract
一种基于碳酸盐岩储层的渗透率的表征方法,通过确定吸附法和高压压汞法均能够表征的孔喉半径的孔径界线,将用吸附法测量得到的孔径界线以下的孔隙结构和高压压汞法测量得到的孔径界线以上的孔隙结构拼接,得到碳酸盐岩储层的孔隙结构特征,获得单位压力进汞饱和度以及不同样本的渗透率,建立最大单位压力进汞饱和度与渗透率之间高精度的函数关系。本发明能表征全孔径段的孔隙结构特征,使后期的测试结果更为准确。采用最大单位压力进汞饱和度来准确计算碳酸盐岩储层的渗透率,避免开展其他大量的岩心实验,在保证碳酸盐岩储层渗透率定量评价结果准确性的同时,提供了一种简单实用的新方法,能够有效地节约成本,具有较强的经济实用性。A characterization method based on the permeability of carbonate reservoirs. By determining the pore size boundary of the pore throat radius that can be characterized by adsorption method and high-pressure mercury intrusion method, the pore structure and pore structure below the pore size boundary measured by adsorption method are determined. The pore structure above the pore size boundary measured by the high-pressure mercury intrusion method is spliced to obtain the pore structure characteristics of carbonate reservoirs, the mercury injection saturation per unit pressure and the permeability of different samples, and the relationship between the maximum unit pressure mercury injection saturation and the permeability of different samples is established. High-precision functional relationship between permeability. The invention can characterize the pore structure characteristics of the full aperture section, so that the later test results are more accurate. The maximum unit pressure of mercury injection saturation is used to accurately calculate the permeability of carbonate reservoirs, avoiding the need to carry out a large number of other core experiments. While ensuring the accuracy of the quantitative evaluation results of carbonate reservoir permeability, it provides a The invention is a simple and practical new method, which can effectively save costs and has strong economical practicability.
Description
技术领域technical field
本发明涉及一种储层渗透率的定量表征方法,尤其涉及一种基于碳酸盐岩储层的渗透率的表征方法。The invention relates to a quantitative characterization method of reservoir permeability, in particular to a characterization method based on the permeability of carbonate rock reservoirs.
背景技术Background technique
在碳酸盐岩储层中,岩石孔隙结构的复杂性造成储层的强非均质性,致使孔隙度与渗透率之间不存在高精度的函数关系。通常使用吸附法、高压压汞法测量页岩储层的微-纳米孔隙结构参数,但在测量时存在的主要问题是:不同方法测量的范围不同,吸附法和高压压汞法均不可能全面表征页岩储层微-纳米孔隙的孔隙结构特征。因而采用由孔隙度建立渗透率计算公式去计算复杂碳酸盐岩储层的渗透率并不可行。另外,由于自由流体模型中的经验常数和平均模型中的经验常数均难以准确确定,因而也难以准确计算复杂碳酸盐岩储层的渗透率。为了准确确定碳酸盐岩储层的渗透率,必须建立该参数与渗透率之间高精度的函数关系,从而准确确定复杂碳酸盐岩储层的渗透率。In carbonate reservoirs, the complexity of the rock pore structure results in strong heterogeneity of the reservoir, so that there is no high-precision functional relationship between porosity and permeability. The micro-nano pore structure parameters of shale reservoirs are usually measured by adsorption method and high-pressure mercury intrusion method, but the main problems in the measurement are: the measurement range of different methods is different, and it is impossible for adsorption method and high-pressure mercury intrusion method to comprehensively measure. Characterization of pore structure characteristics of micro-nanopores in shale reservoirs. Therefore, it is not feasible to use the permeability calculation formula based on porosity to calculate the permeability of complex carbonate reservoirs. In addition, since both the empirical constants in the free-fluid model and the empirical constants in the average model are difficult to accurately determine, it is also difficult to accurately calculate the permeability of complex carbonate reservoirs. In order to accurately determine the permeability of carbonate reservoirs, it is necessary to establish a high-precision functional relationship between this parameter and permeability, so as to accurately determine the permeability of complex carbonate reservoirs.
发明内容SUMMARY OF THE INVENTION
本发明针对上述现有技术存在的问题和不足,提供一种基于碳酸盐岩储层的渗透率的表征方法,能够准确确定碳酸盐岩储层的渗透率。Aiming at the above problems and deficiencies in the prior art, the present invention provides a method for characterizing the permeability of carbonate rock reservoirs, which can accurately determine the permeability of carbonate rock reservoirs.
为实现上述目的,本发明采取以下技术方案:一种基于碳酸盐岩储层的渗透率的表征方法,包括以下步骤:To achieve the above object, the present invention adopts the following technical solutions: a method for characterizing the permeability of carbonate reservoirs, comprising the following steps:
1)通过确定吸附法和高压压汞法均能够表征的孔喉半径的孔径界线,将用吸附法测量得到的孔径界线以下的孔隙结构和高压压汞法测量得到的孔径界线以上的孔隙结构拼接,得到碳酸盐岩储层的孔隙结构特征;1) By determining the pore size boundary of the pore throat radius that can be characterized by adsorption method and high pressure mercury porosimetry, the pore structure below the pore size boundary measured by adsorption method and the pore structure above the pore size boundary measured by high pressure mercury porosimetry are spliced. , to obtain the pore structure characteristics of carbonate reservoirs;
2)对不同空隙结构的岩储层样品进行压汞实验,获得单位压力进汞饱和度以及不同样本的渗透率;2) Perform mercury intrusion experiments on rock reservoir samples with different void structures to obtain the mercury saturation per unit pressure and the permeability of different samples;
3)通过比较各样品的最大单位压力进汞饱和度,建立最大单位压力进汞饱和度与渗透率之间高精度的函数关系;3) By comparing the maximum unit pressure mercury saturation of each sample, a high-precision functional relationship between the maximum unit pressure mercury saturation and permeability is established;
4) 基于该高精度的函数关系,建立以最大单位压力进汞饱和度为参数的碳酸盐岩储层渗透率的计算公式。4) Based on the high-precision functional relationship, a formula for calculating the permeability of carbonate reservoirs with the maximum unit pressure mercury saturation as the parameter is established.
本发明实施的一种基于碳酸盐岩储层的渗透率的表征方法的有益效果是:通过确定吸附法和高压压汞法均能够表征的孔喉半径的孔径界线,将用吸附法测量得到的孔径界线以下的孔隙结构和高压压汞法测量得到的孔径界线以上的孔隙结构拼接,能表征全孔径段的孔隙结构特征,表征结果更为准确,对评价碳酸岩储层的气藏储能力有积极作用。The beneficial effect of the method for characterizing the permeability of carbonate rock reservoirs implemented by the present invention is: by determining the pore size boundary of the pore throat radius that can be characterized by both the adsorption method and the high-pressure mercury intrusion method, the pore size boundary of the pore throat radius that can be characterized by the adsorption method will be measured by the adsorption method. The pore structure below the pore size boundary and the pore structure above the pore size boundary measured by the high-pressure mercury intrusion method can be used to characterize the pore structure characteristics of the full pore size section, and the characterization results are more accurate. have a positive effect.
具体实施方式Detailed ways
下面对本发明的步骤作进一步的具体说明。The steps of the present invention are further described in detail below.
一种基于碳酸盐岩储层的渗透率的表征方法,包括以下步骤:A characterization method based on the permeability of a carbonate reservoir, comprising the following steps:
1)通过确定吸附法和高压压汞法均能够表征的孔喉半径的孔径界线,将用吸附法测量得到的孔径界线以下的孔隙结构和高压压汞法测量得到的孔径界线以上的孔隙结构拼接,得到碳酸盐岩储层的孔隙结构特征。1) By determining the pore size boundary of the pore throat radius that can be characterized by adsorption method and high pressure mercury porosimetry, the pore structure below the pore size boundary measured by adsorption method and the pore structure above the pore size boundary measured by high pressure mercury porosimetry are spliced. , to obtain the pore structure characteristics of carbonate reservoirs.
在本步骤中进行高压压汞法测试时,采用四面注汞的方式,将汞加压注入页岩的柱状样品中,按照汞与孔隙表面做功原理,可以建立孔喉半径与孔隙表面张力、润湿接触角及注入压力之间的数学关系,即瓦什伯恩方程。对于砂岩、碳酸盐岩储层,岩石的屈服强度一般较高,其屈服轻度一般在180Mpa以上,而常规压汞测试的测试压力一般都在200Mpa以下,所以,一般情况下不可能产生施加压力高于岩石孔隙壁的屈服强度的情况,也就不存在汞进入孔喉时的“扩喉”作用。而对于富有机质的泥页岩储层来说,由于其屈服强度低,一般在 100Mpa以下,加上泥页岩储层中有机孔的屈服强度更低,在低压状态下,汞被注入大孔径孔隙,由于泥页岩中孔隙壁强度大于注入压力,不可能产生“扩喉”。但当注入压力增高后,注入压力大于泥页岩孔隙壁的屈服强度,就可能产生“扩喉”作用,假如泥页岩屈服强度为60Mpa,换算成对应的孔喉半径约20nm,即对于该样品,注入压力大于60Mpa时,20nm以下的孔喉产生“扩喉”后,汞分子会进入其中。In the high-pressure mercury intrusion test in this step, the mercury is injected into the columnar sample of shale by means of four-sided mercury injection. Mathematical relationship between wet contact angle and injection pressure, the Washburn equation. For sandstone and carbonate reservoirs, the yield strength of rock is generally higher, and its yield is generally above 180Mpa, while the test pressure of conventional mercury intrusion tests is generally below 200Mpa, so it is generally impossible to produce When the pressure is higher than the yield strength of the rock pore wall, there is no "throat expansion" effect when mercury enters the pore throat. For organic-rich shale reservoirs, due to their low yield strength, generally below 100Mpa, and the yield strength of organic pores in shale reservoirs is lower, under low pressure, mercury is injected into large pore sizes Pores, because the pore wall strength in shale is greater than the injection pressure, it is impossible to produce "throat expansion". However, when the injection pressure increases, the injection pressure is greater than the yield strength of the shale pore wall, which may produce a "throat expansion" effect. If the yield strength of shale is 60Mpa, the corresponding pore throat radius is about 20nm, that is, for this For samples, when the injection pressure is greater than 60Mpa, the pore throats below 20nm will be "expanded", and mercury molecules will enter them.
利用吸附法和高压压汞法对同一个样品进行孔径测试分析。在高压压汞法与吸附法测试的孔径重叠段(80nm以下),明显存在高压压汞法测试的孔径大于吸附法测试的孔径,高压压汞法的“扩喉”作用明显。Pore size analysis was performed on the same sample by adsorption method and high pressure mercury intrusion method. In the overlapping section of pore size (below 80 nm) tested by high pressure mercury porosimetry and adsorption method, it is obvious that the pore size tested by high pressure mercury porosimetry is larger than that measured by adsorption method, and the "throat expansion" effect of high pressure mercury porosimetry is obvious.
2)对不同空隙结构的岩储层样品进行压汞实验,获得单位压力进汞饱和度以及不同样本的渗透率。2) Perform mercury intrusion experiments on rock reservoir samples with different void structures to obtain the mercury saturation per unit pressure and the permeability of different samples.
在本步骤中,选取位于不同深度的样品,分别对各块样品进行压汞实验,得到不同深度岩心样品的渗透率K;然后分别在不同深度岩心样品的毛管压力曲线上获取其在不同进汞压力下的单位压力进汞饱和度SHg/Pc,其中,SHg为进汞饱和度,Pc为进汞压力。In this step, samples at different depths are selected, and mercury injection experiments are performed on each sample respectively to obtain the permeability K of core samples at different depths; The unit pressure mercury injection saturation SHg/Pc under pressure, where SHg is the mercury injection saturation, and Pc is the mercury injection pressure.
3)通过比较各样品的最大单位压力进汞饱和度,建立最大单位压力进汞饱和度与渗透率之间高精度的函数关系。3) By comparing the maximum unit pressure mercury saturation of each sample, a high-precision functional relationship between the maximum unit pressure mercury saturation and permeability is established.
最大单位压力进汞饱和度(SHg/Pc)max与渗透率K之间高精度的函数关系如下:The high-precision functional relationship between the maximum unit pressure mercury saturation (SHg/Pc)max and the permeability K is as follows:
K=f((SHg/Pc)max) (1)K=f((SHg/Pc)max) (1)
4) 基于该高精度的函数关系,建立以最大单位压力进汞饱和度(SHg/Pc)max为参数的碳酸盐岩储层渗透率的计算公式。4) Based on the high-precision functional relationship, a formula for calculating the permeability of carbonate reservoirs with the maximum unit pressure mercury saturation (SHg/Pc)max as the parameter is established.
计算公式的主要表现形式为:The main expressions of the calculation formula are:
K=b(SHg/Pc)maxd (2)K=b(SHg/Pc)maxd (2)
式中,b、d均为常数。In the formula, b and d are both constants.
本发明实施的一种基于碳酸盐岩储层的渗透率的表征方法的有益效果是:通过确定吸附法和高压压汞法均能够表征的孔喉半径的孔径界线,将用吸附法测量得到的孔径界线以下的孔隙结构和高压压汞法测量得到的孔径界线以上的孔隙结构拼接,能表征全孔径段的孔隙结构特征,表征结果更为准确,对评价碳酸岩储层的气藏储能力有积极作用。The beneficial effect of the method for characterizing the permeability of carbonate rock reservoirs implemented by the present invention is: by determining the pore size boundary of the pore throat radius that can be characterized by both the adsorption method and the high-pressure mercury intrusion method, the pore size boundary of the pore throat radius that can be characterized by the adsorption method will be measured by the adsorption method. The pore structure below the pore size boundary and the pore structure above the pore size boundary measured by the high-pressure mercury intrusion method can be used to characterize the pore structure characteristics of the full pore size section, and the characterization results are more accurate. have a positive effect.
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CN114184529B (en) * | 2020-09-15 | 2024-05-07 | 中国石油化工股份有限公司 | Method, device, electronic equipment and medium for acquiring irreducible water saturation |
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