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CN109394590A - A kind of soft foundation compositions of crease-resistant silk and preparation method thereof - Google Patents

A kind of soft foundation compositions of crease-resistant silk and preparation method thereof Download PDF

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Publication number
CN109394590A
CN109394590A CN201811654699.8A CN201811654699A CN109394590A CN 109394590 A CN109394590 A CN 109394590A CN 201811654699 A CN201811654699 A CN 201811654699A CN 109394590 A CN109394590 A CN 109394590A
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colorant
composition
dimethyl silicone
silicone polymer
crease
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CN109394590B (en
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苏晋峰
邓伟健
林锦雄
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Guangzhou I & B Biological Technology Co Ltd
Guangzhou Aibei Biological Technology Co Ltd
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Guangzhou I & B Biological Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Dermatology (AREA)
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  • Biotechnology (AREA)
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  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention provides a kind of crease-resistant soft foundation compositions of silk.The crease-resistant soft foundation compositions of silk of the present invention include coconut oil, Quercus suber bark extract, Quercus suber root extract and egg fruit seed oil.The crease-resistant soft foundation compositions of silk of the present invention can remove free radical, promote the synthesis of collagen, have good effect at crease-resistant aspect.The crease-resistant soft foundation compositions of silk of the present invention can not add preservative, eliminate the allergy risk of preservative initiation, can also make it have good skin sense by ring five dimethyl silicone polymer, Permethyl 99A and ethyl alcohol proportion appropriate.The crease-resistant soft foundation compositions preparation process of silk of the present invention is simple, and condition is controllable, easy to produce.

Description

A kind of soft foundation compositions of crease-resistant silk and preparation method thereof
Technical field
The invention belongs to daily chemical product technical field, it is related to a kind of soft foundation compositions of crease-resistant silk and preparation method thereof.
Background technique
Wrinkle refers to that skin is influenced by external environment, forms free free radical, and free radical destroys normal cell membrane tissue Interior collagen, active material, oxidative cell cause dermal layer of the skin collagen content to gradually decrease, mesh support It thickens and is hardened, follows the string, when elasticity and the water conservation degree of skin corium reduce, skin will follow the string and thinning aging forms wrinkle Line.Women is reaching 24, after five years old, light microgroove is just had between the canthus tip of the brow, especially present social economy is at full speed The problems such as development, environmental pollution and life stress, which is on the rise, further induces the generation of interior free yl, leads to facial wrinkle Line increases.Therefore, crease-resistant to have become the target that numerous women pursue now.Foundation cream is first that skin of face is contacted with the external world Barrier, but anti-wrinkle product is concentrated mainly on skin type at present, and foundation cream is very related to less.
Summary of the invention
A kind of soft foundation cream combination of crease-resistant silk is provided it is an object of the invention to overcome the shortcomings of the prior art place Object and preparation method thereof.
To achieve the above object, the technical scheme adopted by the invention is as follows:
A kind of soft foundation compositions of crease-resistant silk, comprising active functional component, the activity functional component includes coconut oil, Europe The mixture and egg fruit seed oil of continent cork oak bark extract and Quercus suber root extract, the coconut oil, Europe The mixture of cork oak bark extract and Quercus suber root extract accounts for the 0.1-5% of the composition quality, the coconut palm The mass ratio of seed oil, Quercus suber bark extract and Quercus suber root extract is 70:25:5, the egg fruit seed oil Account for the 0.5-5% of the composition quality.
The bark and root extract of Quercus suber can inhibit the secretion of inflammatory cytokine TNF-α, have to skin Significant anti-inflammatory and antiallergic effect, in addition, also there is facilitation to the collagen synthesis in skin;Passion fruit, You Mingbai Fragrant fruit, fruit seed oil is mainly by unsaturated fatty acid, Polyphenols, flavone compound, vitamin E, beta carotene, white Pi Shan Alcohol and its derivative composition, wherein Polyphenols, flavone compound, vitamin E, beta carotene can effectively remove lipid certainly By base and superoxide radical, prevent lipid peroxidation, delaying skin is because of aging, piceatannol and its derivative energy caused by aoxidizing Inhibit the generation of dermal melanin and promote the synthesis of collagen, the present invention is by Quercus suber bark extract, European bolt Skin oak root extract and the combination of egg fruit seed oil, it is found that this three has good synergistic function at crease-resistant aspect.In addition, Coconut oil, external application can protect skin by uv damage, can also not lift intercellular tightness, strengthen the contraction energy of pore Power helps to remove the outer layers of dead skin cells, restores damaged skin, make it is more healthy, smooth at the epidermal-dermal junction of skin, from And further improve skin problem.
Preferably, the mixture of the coconut oil, Quercus suber bark extract and Quercus suber root extract accounts for The 0.8% of the composition quality, the egg fruit seed oil account for the 0.9% of the composition quality.With this condition, European bolt The synergistic function of skin robur bark extract, Quercus suber root extract and egg fruit seed oil is stronger, anti-wrinkle effect ratio Preferably.
Preferably, the composition also includes solvent, and the solvent is ethyl alcohol.General foundation cream is using water as solvent, to increase Add the salubrious sense of foundation cream, but water can cause microbial growth, therefore preservative need to be added in foundation cream to inhibit the life of microorganism It is long, but preservative often will lead to skin allergy, and the present invention substitutes water using ethyl alcohol, and ethyl alcohol itself has bacteriostasis efficacy, therefore The use of preservative can be avoided while increase foundation cream is clearly felt.
Preferably, the ethyl alcohol accounts for the 1-10% of the composition quality.When ethanol content is less than 1%, foundation cream is combined The salubrious degree increase of object is unobvious, and when its content is more than 10%, it is bigger to the irritation of skin.
Preferably, the composition also includes emollients, and the emollients include to account for the composition quality 10-50%'s The Permethyl 99A of ring five dimethyl silicone polymer and 5-30%.Ring five dimethyl silicone polymer and Permethyl 99A are high volatile Grease, the collocation of they and appropriate amount of ethanol use, and obtained foundation cream is not sticky when not only smearing, and moisten while have again it is good Good soft and smooth sense.
Preferably, the ethyl alcohol accounts for the 5% of the composition quality, and the ring five dimethyl silicone polymer accounts for the combination The 28.75% of amount of substance, the Permethyl 99A account for the 23% of the composition quality.With this condition, foundation compositions is clear Refreshing degree and soft and smooth sense are relatively good.
Preferably, the composition also includes emulsifier, film forming agent, thickener, skin sense regulator and colorant, the cream Agent is PEG-10 Polydimethylsiloxane, and the film forming agent is ring five dimethyl silicone polymer and trimethyl silicane alkoxy silicic acid The mixture of ester, the thickener are distearyl dimethylammonium hectorite, and the skin sense regulator includes skin sense regulator 1 and skin Feel regulator 2, the skin sense regulator 1 is the crosslinking of vinyldimethicone and polymethyl siloxane silsesquioxane Polymer, the skin sense regulator 2 are polymethylsilsesquioxane, and the colorant includes colorant 1, colorant 2, colorant 3 and colorant 4, the colorant 1 be yellow iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and The mixture of ring five dimethyl silicone polymer, the colorant 2 are red iron oxide, dimethyl silicone polymer, stearoyl paddy ammonia The mixture of acid disodium, aluminium hydroxide and ring five dimethyl silicone polymer, the colorant 3 are black iron oxide, poly dimethyl Siloxanes, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five dimethyl silicone polymer mixture, the colorant 4 be two Titanium oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five dimethyl silicone polymer mixture, The emollients also include dimethyl silicone polymer and phenyl trimethicone.
The emulsifying capacity of PEG-10 Polydimethylsiloxane is stronger, has lower electrolysis qualitative response and higher heat steady It is qualitative, be conducive to the stabilization of formula;Ring five dimethyl silicone polymer, colorless and odorless will not influence the color and smell of foundation cream, and It can produce lubrication and the feeling that silk is slided;Trimethyl silicane alkoxy silicic acid, there is good water-resistance, which does not stick greasy, peace clearly Whole step is high;Distearyl dimethylammonium hectorite is often used together with pigment collocation;Vinyldimethicone and poly- methyl The cross-linked polymer of siloxanes silsesquioxane has excellent flatness, elasticity, can achieve the effect of thickening and dumb light, Have effects that increase moisturizing simultaneously;Foundation cream made of colorant 1-4 not only has good concealing effect, but also the powder made Bottom will not coloured oil float go out;Dimethyl silicone polymer, greasy property is good, can form one layer uniformly with waterproof after applying skin Property protective film, but without any viscosity and greasy feeling, glossiness is good, and the property with good ultra-violet radiation resisting Energy;Phenyl trimethicone can be such that product clearly smears well, not sticky.
Preferably, by mass percentage, the composition include the emulsifier of 0.5-5%, 0.5-10% film forming agent, The thickener of 0.1-6%, the skin sense regulator 1 of 0.5-10%, the skin sense regulator 2 of 0.5-10%, 0.1-2% colorant 1, The colorant 2 of 0.05-1%, the colorant 3 of 0.02-1%, the colorant 4 of 2-20%, 1-20% dimethyl silicone polymer and The phenyl trimethicone of 0.5-10%.With this condition, the composition has good soft and smooth sense, clearly spends, sprawls Property and patch skin.
Preferably, by mass percentage, the composition includes 2.2% emulsifier, 1.5% film forming agent, 1% Thickener, 5% skin sense regulator 1,5% skin sense regulator 2,0.45% colorant 1,0.28% colorant 2, 4,10% dimethyl silicone polymer of colorant and 3% phenyl trimethicone of 0.12% colorant 3,13%. With this condition, the composition not only has extraordinary soft and smooth sense and salubrious degree, also has extraordinary spreadability and patch skin Property, and cost is also relatively low.
The present invention also provides a kind of preparation methods of crease-resistant soft foundation compositions of silk, comprising the following steps:
(1) emollients, emulsifier, film forming agent and thickener are uniformly mixed, then homogeneous under the conditions of 3500-5000rpm During which the solvent for accounting for the composition quality 0.3-0.7% is added dropwise in 1-5min, continue homogeneous 3-8min, and A phase is made;
(2) colorant is uniformly mixed, B phase is made, skin sense regulator, active functional component and A are added in B phase, C phase is made in homogeneous 1-5min under the conditions of 2000-3500rpm again;
(3) residual solvent is added in C phase under the conditions of 4500-6000rpm, after continuing homogeneous 1-3min, is can be prepared by The composition.
The advantages of the present invention are as follows:
1, the crease-resistant soft foundation compositions of silk of the present invention include coconut oil, Quercus suber bark extract, Quercus suber The innate efficacies ingredient such as root extract and egg fruit seed oil can not only remove free radical, promote collagen synthesis, effective against Wrinkle, moreover it is possible to inhibit melanin production, antibacterial and antiallergic.
2, the crease-resistant soft foundation compositions of silk of the present invention can not be aqueous, does not add preservative, eliminates preservative initiation Allergy risk.
3, the crease-resistant soft foundation compositions of silk of the present invention can have good soft and smooth sense, patch skin, spreadability and salubrious degree.
4, the crease-resistant soft foundation compositions preparation method simple process of silk of the present invention, condition is controllable, easy to produce.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention It is described further.
Embodiment 1
A kind of soft foundation compositions of crease-resistant silk, ingredient and its content are shown in Table 1.
Mass percent/% of each ingredient in 1 embodiment 1-8 foundation compositions of table
The preparation methods of the crease-resistant soft foundation compositions of silk the following steps are included:
(1) by the mixture of ring five dimethyl silicone polymer and trimethyl silicane alkoxy esters of silicon acis, five poly dimethyl silicon of ring Oxygen alkane, Permethyl 99A, dimethyl silicone polymer, phenyl trimethicone, PEG-10 Polydimethylsiloxane and distearyl Dimethylammonium hectorite is uniformly mixed, then homogeneous 1min under the conditions of 3500rpm, is during which added dropwise and is accounted for the composition quality 0.3% Solvent, continue homogeneous 3min, be made A phase;
(2) by yellow iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and the poly- diformazan of ring five The mixture of radical siloxane, red iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five are poly- The mixture of dimethyl siloxane, black iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring Mixture and titanium dioxide, dimethyl silicone polymer, the stearoyl-glutamic acid disodium, hydroxide of five dimethyl silicone polymers Aluminium and the mixture of ring five dimethyl silicone polymer are uniformly mixed, and B phase are made, by vinyldimethicone and poly- methyl The cross-linked polymer of siloxanes silsesquioxane, coconut oil, Quercus suber bark extract and Quercus suber root extract Mixture, egg fruit seed oil, polymethylsilsesquioxane and A are added in B phase, then homogeneous 1min under the conditions of 2000rpm, C phase is made;
(3) remaining ethyl alcohol is added in C phase under the conditions of 4500rpm, after continuing homogeneous 1min, can be prepared by the combination Object.
Embodiment 2
A kind of soft foundation compositions of crease-resistant silk, ingredient and its content are shown in Table 1.
The preparation methods of the crease-resistant soft foundation compositions of silk the following steps are included:
(1) by the mixture of ring five dimethyl silicone polymer and trimethyl silicane alkoxy esters of silicon acis, five poly dimethyl silicon of ring Oxygen alkane, Permethyl 99A, dimethyl silicone polymer, phenyl trimethicone, PEG-10 Polydimethylsiloxane and distearyl Dimethylammonium hectorite is uniformly mixed, then homogeneous 5min under the conditions of 5000rpm, is during which added dropwise and is accounted for the composition quality 0.7% Solvent, continue homogeneous 8min, be made A phase;
(2) by yellow iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and the poly- diformazan of ring five The mixture of radical siloxane, red iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five are poly- The mixture of dimethyl siloxane, black iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring Mixture and titanium dioxide, dimethyl silicone polymer, the stearoyl-glutamic acid disodium, hydroxide of five dimethyl silicone polymers Aluminium and the mixture of ring five dimethyl silicone polymer are uniformly mixed, and B phase are made, by vinyldimethicone and poly- methyl The cross-linked polymer of siloxanes silsesquioxane, coconut oil, Quercus suber bark extract and Quercus suber root extract Mixture, egg fruit seed oil, polymethylsilsesquioxane and A are added in B phase, then homogeneous 5min under the conditions of 3500rpm, C phase is made;
(3) remaining ethyl alcohol is added in C phase under the conditions of 6000rpm, after continuing homogeneous 3min, can be prepared by the combination Object.
Embodiment 3
A kind of soft foundation compositions of crease-resistant silk, ingredient and its content are shown in Table 1, and each ingredient origin is the same as embodiment 1.
The preparation methods of the crease-resistant soft foundation compositions of silk the following steps are included:
(1) by the mixture of ring five dimethyl silicone polymer and trimethyl silicane alkoxy esters of silicon acis, five poly dimethyl silicon of ring Oxygen alkane, Permethyl 99A, dimethyl silicone polymer, phenyl trimethicone, PEG-10 Polydimethylsiloxane and distearyl Dimethylammonium hectorite is uniformly mixed, then homogeneous 3min under the conditions of 4000rpm, is during which added dropwise and is accounted for the composition quality 0.5% Solvent, continue homogeneous 5min, be made A phase;
(2) by yellow iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and the poly- diformazan of ring five The mixture of radical siloxane, red iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five are poly- The mixture of dimethyl siloxane, black iron oxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring Mixture and titanium dioxide, dimethyl silicone polymer, the stearoyl-glutamic acid disodium, hydroxide of five dimethyl silicone polymers Aluminium and the mixture of ring five dimethyl silicone polymer are uniformly mixed, and B phase are made, by vinyldimethicone and poly- methyl The cross-linked polymer of siloxanes silsesquioxane, coconut oil, Quercus suber bark extract and Quercus suber root extract Mixture, egg fruit seed oil, polymethylsilsesquioxane and A are added in B phase, then homogeneous 3min under the conditions of 3000rpm, C phase is made;
(3) remaining ethyl alcohol is added in C phase under the conditions of 5000rpm, after continuing homogeneous 2min, can be prepared by the combination Object.
Embodiment 4-8
It is a kind of soft foundation compositions of crease-resistant silk, ingredient and its content are shown in Table 1.The soft powder of the crease-resistant silk of embodiment 4-8 The preparation method of bottom composition is the same as the preparation method in embodiment 2.
Comparative example 1-6
It is a kind of foundation compositions, ingredient and its content are shown in Table 2.
Mass percent/% of each ingredient in 2 comparative example 1-6 foundation compositions of table
With the following method, measure of merit is carried out to the soft foundation compositions of crease-resistant silk of the invention:
1, anti-wrinkle effect is tested
(1) experimental principle
The wrinkle level of skin of face is carried out by " Wrinkles " detection function of 7 face-image analyzer of Visia Measurement, the wrinkle being scanned can be sketched the contours into a rule filament in shooting the picture come and be distributed in entire face, be passed through The cloud database and its algorithm of instrument score, and the lower expression wrinkle that scores is more.
(2) test method
The volunteer of 70 30-45 years old age brackets is chosen as object on probation, is divided into 14 groups, every group is tried out a kind of examination Sample.Subject in face, tries out each sample coating 1 time daily, continuous 30 days on probation.Respectively at the 0th day, the 15th day and the 30th It when with 7 face-image analyzer of Visia wrinkle test is carried out to subject's skin of face, be denoted as D respectively0、D15And D30, need To illustrate that every group of D0、D15And D30Value is the average value of these numerical value of the group, and makes every group of D by grouping appropriate0Value It is close.
(3) test result
Specific anti-wrinkle effect test is shown in Table 3.
3 anti-wrinkle effect test result of table
As can be seen from Table 3, by the wrinkle testing evaluation result of embodiment 1-5 it is found that with coconut oil, Quercus suber The increase of the mixture additive amount of bark extract and Quercus suber root extract, facial wrinkles amount gradually decrease, but work as and add When dosage is more than 0.8%, the reduction amount of wrinkle is unobvious, and anti-wrinkle effect tends to be saturated;By the wrinkle of embodiment 6-8 and embodiment 3 Line testing evaluation result it is found that with egg fruit seed oil additive amount increase, facial wrinkles amount gradually decreases, but when additive amount is super When 0.9%, the reduction amount of wrinkle is unobvious, and anti-wrinkle effect tends to be saturated;The wrinkle test of embodiment 3 and comparative example 1-2 is commented Split-phase is close, this illustrates that coconut oil does not have an influence to the anti-wrinkle effect of the crease-resistant soft foundation compositions of silk of the present invention substantially, in the composition Play anti-wrinkle effect should be Quercus suber bark extract, Quercus suber root extract and egg fruit seed oil;Embodiment 3 Wrinkle testing evaluation than comparative example 3-4 is high, illustrates that the crease-resistant soft foundation compositions of silk of the present invention are mentioned by Quercus suber bark Take object, Quercus suber root extract and egg fruit seed oil synergistic effect and have relatively good anti-wrinkle effect;Comparative example 5 Wrinkle testing evaluation is significantly lower than embodiment 1, this illustrates coconut oil, Quercus suber in the crease-resistant soft foundation compositions of silk of the present invention When the additive amount of bark extract and Quercus suber root extract mixture is not less than 0.1%, just with relatively good crease-resistant Effect;The wrinkle testing evaluation of comparative example 6 is lower than embodiment 6, this illustrates passion fruit in the crease-resistant soft foundation compositions of silk of the present invention When the additive amount of seed oil is not less than 0.5%, just there is relatively good crease-resistant effect.
2, skin sense validation test
(1) tested material: composition, commercially available common w/o type foundation emulsion, commercially available common O/ described in embodiment 1-8 and comparative example 7 W type foundation emulsion and commercially available common full oil type foundation emulsion.
(2) subject: totally 60 people (male 30 people, 30 people of female the age 18-30 years old, meet subject and volunteer inclusion criteria), with Machine is divided into 12 groups, and every group uses a kind of sample.
(3) appraisal procedure: being applied to the back of the hand for the sample of 50uL, smearing of mildly being circled round with another 10 times, then to beat Point mode (0-10 point, score is higher, and it is better to represent the soft and smooth sense of the product, patch skin, spreadability, salubrious degree), successively comment Soft and smooth sense, patch skin, spreadability and the salubrious degree for estimating sample out, then seek the average value of this four indexs again, are denoted as average Scoring.
(4) it assessment result: applies comprehensive subject's scoring after and counts, the results are shown in Table 4.
4 skin of table senses test result
Sample Soft and smooth sense Paste skin Spreadability Salubrious degree Average score
Embodiment 1 9.3 8.2 9.1 8.9 8.88
Embodiment 2 8.9 8.5 9.2 9.0 8.90
Embodiment 3 9.6 8.4 9.3 8.8 9.03
Embodiment 4 9.4 7.8 7.7 8.3 8.30
Embodiment 5 9.5 9.2 8.8 5.5 8.25
Embodiment 6 8.9 7.2 7.5 8.1 7.93
Embodiment 7 8.8 8.3 9.6 8.6 8.83
Embodiment 8 9.6 8.2 9.2 7.4 8.60
Comparative example 7 7.5 6.8 5.4 3.7 5.85
Commercially available common w/o type foundation emulsion 9.3 8.9 7.8 5.9 7.98
Commercially available common O/W type foundation emulsion 7.6 7.1 8.9 9.4 8.25
Commercially available common full oil type foundation emulsion 9.2 8.2 9.0 5.1 7.88
As shown in Table 4, comparative example 7 is compared, the soft and smooth sense of embodiment 1-8 pastes skin, spreadability and salubrious degree more preferably, this Illustrate to add ring five dimethyl silicone polymer and Permethyl 99A, the skin sense of foundation compositions can be made more preferable, and by adjusting ring five The content of dimethyl silicone polymer, Permethyl 99A and ethyl alcohol can further improve the skin sense of composition to ratio appropriate;It is real Apply the flat of a 1-8 and commercially available common w/o type foundation emulsion, commercially available common O/W type foundation emulsion and commercially available common full oil type foundation emulsion It scores close, wherein the four indices score and average score of embodiment 3 are relatively high.
3, antiseptic property is tested
Strain: pseudomonas aeruginosa [ATCC 9027], staphylococcus aureus [ATCC 6538], escherichia coli [ATCC 8739], candida albicans [ATCC 10231] and aspergillus niger [ATCC 16404].
Test method: according to the antimicrobial preservation efficacy test method in United States Pharmacopeia USP 32<51>respectively to embodiment 1-8 carries out antiseptic property test.
Evaluation criterion: bacterium cannot be less than 2.0, and from 14 days to 28 from the bacterial population log reduction initially by 14 days Its total number of bacteria not can increase;Yeast and mold sum meets all of the above item from not can increase to 14 days and 28 days initially Part can be judged as that antiseptic property is good.
Specific antiseptic property test result is shown in Table 5.
5 antiseptic property test result of table
As can be seen from Table 5, the 14th day and the 28th day, the composition of embodiment 1-8 makes the quantity of bacterium and mould Declined, this illustrates that these compositions have certain preservative efficacy, and wherein embodiment 1-3 and the composition of embodiment 6 are anti- It is rotten functional.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention And range.

Claims (10)

1. a kind of soft foundation compositions of crease-resistant silk, it is characterised in that: the composition includes active functional component, the activity function Imitating ingredient includes coconut oil, the mixture of Quercus suber bark extract and Quercus suber root extract and egg fruit seed Oil, the mixture of the coconut oil, Quercus suber bark extract and Quercus suber root extract account for the combination substance The mass ratio of the 0.1-5% of amount, the coconut oil, Quercus suber bark extract and Quercus suber root extract are 70: 25:5, the egg fruit seed oil account for the 0.5-5% of the composition quality.
2. composition according to claim 1, it is characterised in that: the coconut oil, Quercus suber bark extract and The mixture of Quercus suber root extract accounts for the 0.8% of the composition quality, and the egg fruit seed oil accounts for the composition The 0.9% of quality.
3. composition according to claim 1 or 2, it is characterised in that: the composition also includes solvent, and the solvent is Ethyl alcohol.
4. composition according to claim 3, it is characterised in that: the ethyl alcohol accounts for the 1-10% of the composition quality.
5. composition according to claim 4, it is characterised in that: the composition also includes emollients, the emollients Comprising accounting for the ring five dimethyl silicone polymer of the composition quality 10-50% and the Permethyl 99A of 5-30%.
6. composition according to claim 5, it is characterised in that: the ethyl alcohol accounts for the 5% of the composition quality, described Ring five dimethyl silicone polymer accounts for the 28.75% of the composition quality, and the Permethyl 99A accounts for the composition quality 23%.
7. composition according to claim 6, it is characterised in that: the composition also includes emulsifier, film forming agent, thickening Agent, skin sense regulator and colorant, the emulsifier are PEG-10 Polydimethylsiloxane, and the film forming agent is the poly- diformazan of ring five The mixture of radical siloxane and trimethyl silicane alkoxy esters of silicon acis, the thickener is distearyl dimethylammonium hectorite, described Skin sense regulator includes skin sense regulator 1 and skin sense regulator 2, and the skin sense regulator 1 is vinyldimethicone With the cross-linked polymer of polymethyl siloxane silsesquioxane, the skin sense regulator 2 is polymethylsilsesquioxane, described Toner includes colorant 1, colorant 2, colorant 3 and colorant 4, and the colorant 1 is yellow iron oxide, polydimethylsiloxanes Alkane, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five dimethyl silicone polymer mixture, the colorant 2 is red oxygen Change the mixture of iron, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide and ring five dimethyl silicone polymer, institute Stating colorant 3 is black iron oxide, dimethyl silicone polymer, five poly dimethyl of stearoyl-glutamic acid disodium, aluminium hydroxide and ring The mixture of siloxanes, the colorant 4 are titanium dioxide, dimethyl silicone polymer, stearoyl-glutamic acid disodium, aluminium hydroxide With the mixture of ring five dimethyl silicone polymer, the emollients also include dimethyl silicone polymer and the poly- trimethyl silicane oxygen of phenyl Alkane.
8. composition according to claim 7, it is characterised in that: by mass percentage, the composition includes 0.5- 5% emulsifier, the film forming agent of 0.5-10%, the thickener of 0.1-6%, the skin sense regulator 1 of 0.5-10%, 0.5-10% Skin sense regulator 2, the colorant 1 of 0.1-2%, the colorant 2 of 0.05-1%, 0.02-1% colorant 3,2-20% coloring Agent 4, the dimethyl silicone polymer of 1-20% and 0.5-10% phenyl trimethicone.
9. composition according to claim 8, it is characterised in that: by mass percentage, the composition includes 2.2% Emulsifier, 1.5% film forming agent, 1% thickener, 5% skin sense regulator 1,5% skin sense regulator 2,0.45% The dimethyl silicone polymer of the colorant 4,10% of the colorant 3,13% of the colorant 2,0.12% of colorant 1,0.28% and 3% phenyl trimethicone.
10. a kind of preparation method of composition of any of claims 1-9, it is characterised in that: the preparation method The following steps are included:
(1) emollients, emulsifier, film forming agent and thickener are uniformly mixed, then homogeneous 1- under the conditions of 3500-5000rpm During which the solvent for accounting for the composition quality 0.3-0.7% is added dropwise in 5min, continue homogeneous 3-8min, and A phase is made;
(2) colorant is uniformly mixed, B phase is made, skin sense regulator, active functional component and A are added in B phase, then C phase is made in homogeneous 1-5min under the conditions of 2000-3500rpm;
(3) residual solvent is added in C phase under the conditions of 4500-6000rpm, after continuing homogeneous 1-3min, is can be prepared by described Composition.
CN201811654699.8A 2018-12-29 2018-12-29 Anti-wrinkle silky foundation make-up composition and preparation method thereof Active CN109394590B (en)

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