CN109381498A - The preparation method of sweet wormwood powder - Google Patents
The preparation method of sweet wormwood powder Download PDFInfo
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- CN109381498A CN109381498A CN201710669177.4A CN201710669177A CN109381498A CN 109381498 A CN109381498 A CN 109381498A CN 201710669177 A CN201710669177 A CN 201710669177A CN 109381498 A CN109381498 A CN 109381498A
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- powder
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- sweet wormwood
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- drying
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- 239000000843 powder Substances 0.000 title claims abstract description 58
- 235000001405 Artemisia annua Nutrition 0.000 title claims abstract description 40
- 240000000011 Artemisia annua Species 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 23
- 238000001035 drying Methods 0.000 claims abstract description 16
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 14
- 241001116500 Taxus Species 0.000 claims abstract description 12
- 239000007787 solid Substances 0.000 claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 7
- 229910001380 potassium hypophosphite Inorganic materials 0.000 claims abstract description 7
- CRGPNLUFHHUKCM-UHFFFAOYSA-M potassium phosphinate Chemical compound [K+].[O-]P=O CRGPNLUFHHUKCM-UHFFFAOYSA-M 0.000 claims abstract description 7
- 235000009566 rice Nutrition 0.000 claims abstract description 7
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 7
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims abstract description 6
- 238000000746 purification Methods 0.000 claims abstract description 6
- 239000002893 slag Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 240000007594 Oryza sativa Species 0.000 claims abstract 2
- 238000001816 cooling Methods 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 10
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 5
- 230000000144 pharmacologic effect Effects 0.000 abstract description 5
- 206010037660 Pyrexia Diseases 0.000 description 6
- 241000209094 Oryza Species 0.000 description 5
- 235000019441 ethanol Nutrition 0.000 description 5
- 239000003814 drug Substances 0.000 description 4
- 240000001851 Artemisia dracunculus Species 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000019890 Amylum Nutrition 0.000 description 1
- 241000208838 Asteraceae Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010019345 Heat stroke Diseases 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- 208000031971 Yin Deficiency Diseases 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000005200 bud stage Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 201000004792 malaria Diseases 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 206010029410 night sweats Diseases 0.000 description 1
- 230000036565 night sweats Effects 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000010908 plant waste Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/13—Coniferophyta (gymnosperms)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
- A61K9/143—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
- A61K9/145—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with organic compounds
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Alternative & Traditional Medicine (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of preparation methods of sweet wormwood powder, include the following steps: the Sweet Wormwood Herb of above-mentioned 80~90 parts by weight, the Taxus leaf powder of 6~8 parts by weight and the Radix Glycyrrhizae powder of 1~2 parts by weight are mixed evenly, it is boiled by the weight ratio and water purification cooperation of 1:1.2~1.5, the glutinous rice wrapped up with gauze is put into wherein simultaneously, tanning 3~4 hours, it is filtered to remove slag, sodium sulphate is put into when juice temperature is 80 DEG C or more, it is completely dissolved to it, the potassium hypophosphite of 1~2 parts by weight is added at 45 DEG C or more for juice temperature and the industrial alcohol of 3~5 parts by weight is modulated, the juice modulated is set in a cool and dry place, reaction is cooled down to it, and crystalline solid is precipitated, then crystalline solid taking-up is placed at aeration-drying, powder is placed in after natural extruding obtained by drying in dryer；The present invention can effectively improve the nitrogen content of sweet wormwood powder, enhance its pharmacological property and stability.
Description
Technical field
The present invention relates to a kind of preparation methods of sweet wormwood powder, belong to sweet wormwood powder production technical field.
Background technique
Sweet wormwood is the aerial part of the dry aerial parts of compositae plant Huang wormwood artemisia.Bud stage harvesting, extracts aerial part,
Chopping, is dried.It is used as medicine with heat-clearing, cool blood, moves back steaming, relieving summer-heat, wind-dispelling, antipruritic, only night sweat, anti-heatstroke and other effects, is used as the deficiency of Yin
The antipyretic of hectic fever.It is usually used in warm evil impairment of yin, night fever abating at dawn, fever due to yin deficiency, hectic fever due to yin labor is hot, summer-heat evil fever, and malaria fever and chills are damp and hot
The treatment of the illnesss such as jaundice.There is a product that sweet wormwood is produced into sweet wormwood powder at present, but existing sweet wormwood powder there are nitrogen contents low, medicine
Property it is insufficient, the problems such as being not sufficiently stable.
Summary of the invention
The technical problem to be solved by the present invention is providing a kind of preparation method of sweet wormwood powder, containing for sweet wormwood powder can be improved
Nitrogen quantity enhances its pharmacological property and stability, with overcome the deficiencies in the prior art.
The technical scheme is that a kind of preparation method of sweet wormwood powder, includes the following steps:
The sweet wormwood of 80~90 parts by weight is taken to be ground into the powder of 50~70mm；
The Taxus leaf of 6~8 parts by weight is taken to be ground into the powder of 50~70mm；
The Radix Glycyrrhizae of 1~2 parts by weight is taken to crush the powder for being processed into 80~140mm；
Above-mentioned Sweet Wormwood Herb, Taxus leaf powder and Radix Glycyrrhizae powder are mixed evenly, by 1:1.2~1.5 weight ratio with
Water purification cooperation is boiled, while the glutinous rice wrapped up with gauze being put into wherein, is boiled 3~4 hours, is filtered to remove slag,
Juice temperature is put into sodium sulphate when being 80 DEG C or more, is completely dissolved to it, 1~2 weight is added at 45 DEG C or more for juice temperature
The potassium hypophosphite of part and the industrial alcohol of 3~5 parts by weight are modulated, and the juice modulated are set in a cool and dry place, to it
Crystalline solid is precipitated in cooling reaction, and then crystalline solid taking-up is placed at aeration-drying, powder is placed in drying after natural extruding
It is obtained by drying in machine.
Sweet wormwood powder drying machine is dried to moisture lower than 15%.
The beneficial effects of the present invention are: compared with prior art, the present invention can effectively improve the nitrogen content of sweet wormwood powder, enhancing
Its pharmacological property and stability.In the present invention, glutinous rice boils together with Sweet Wormwood Herb, can increase the various effective elements in sweet wormwood
Stability, starch juice are distributed in sweet wormwood ingredient by high temperature, make total nitrogen content up to 15% or more, sweet wormwood effective component reaches
0.4%.Sodium sulphate can enable sweet wormwood juice crystallize as filler.Taxus leaf is a kind of anticancer xylophyta, is added to
Sweet wormwood pharmacological property can be enhanced in juice, and keep the stability of pharmacological property.Industrial alcohol can not only protect the efficacy of a drug, and drug can be made to be not easy
Volatilization, while being also stabilizer and decomposition point agent.Potassium hypophosphite plays anti-corrosion deodorization, disinfection and removing residual in the present invention
The effect of object.Radix Glycyrrhizae can adjust the mouthfeel of juice, while can dispel the poisonous and harmful substance in juice.Sweet wormwood prepared by the present invention
Powder is suitble to the bathing of having one's hair wash in medicinal health-care, toothpaste production, organic fertilizer production, plant amylum extraction and plant waste processing etc.
Aspect application.
Specific embodiment
Invention is described further below with reference to specific embodiment:
Embodiment 1:
A kind of preparation method of sweet wormwood powder includes the following steps: to take 80 parts of sweet wormwood to be ground into the powder of 50~70mm；Take 6 parts
Taxus leaf be ground into the powder of 50~70mm；2 parts of Radix Glycyrrhizae is taken to crush the powder for being processed into 80~140mm；By above-mentioned blueness
Wormwood artemisia powder, Taxus leaf powder and Radix Glycyrrhizae powder are mixed evenly, and are boiled by the weight ratio and water purification cooperation of 1:1.2,
The glutinous rice wrapped up with gauze is put into wherein simultaneously, boils 3~4 hours, is filtered to remove slag, is 80 DEG C or more in juice temperature
When be put into sodium sulphate, be completely dissolved to it, 1 part of potassium hypophosphite and 3 parts of industrial second are added at 45 DEG C or more for juice temperature
Alcohol is modulated, and the juice modulated is set in a cool and dry place, reaction is cooled down to it and crystalline solid is precipitated, then take crystalline solid
It is placed at aeration-drying out, powder is placed in dryer after natural extruding and is dried, sweet wormwood powder drying machine is dried to moisture
Lower than 15%.
Embodiment 2:
A kind of preparation method of sweet wormwood powder includes the following steps: to take 90 parts of sweet wormwood to be ground into the powder of 50~70mm；Take 8 parts
Taxus leaf be ground into the powder of 50~70mm；1 part of Radix Glycyrrhizae is taken to crush the powder for being processed into 80~140mm；By above-mentioned blueness
Wormwood artemisia powder, Taxus leaf powder and Radix Glycyrrhizae powder are mixed evenly, and are boiled by the weight ratio and water purification cooperation of 1:1.5,
The glutinous rice wrapped up with gauze is put into wherein simultaneously, boils 3~4 hours, is filtered to remove slag, is 80 DEG C or more in juice temperature
When be put into sodium sulphate, be completely dissolved to it, 2 parts of potassium hypophosphite and 5 parts of industrial second are added at 45 DEG C or more for juice temperature
Alcohol is modulated, and the juice modulated is set in a cool and dry place, reaction is cooled down to it and crystalline solid is precipitated, then take crystalline solid
It is placed at aeration-drying out, powder is placed in dryer after natural extruding and is dried, sweet wormwood powder drying machine is dried to moisture
Lower than 15%.
Embodiment 3:
A kind of preparation method of sweet wormwood powder includes the following steps: to take 85 parts of sweet wormwood to be ground into the powder of 50~70mm；Take 7 parts
Taxus leaf be ground into the powder of 50~70mm；1.5 parts of Radix Glycyrrhizae is taken to crush the powder for being processed into 80~140mm；It will be above-mentioned
Sweet Wormwood Herb, Taxus leaf powder and Radix Glycyrrhizae powder are mixed evenly, and are endured by the weight ratio and water purification cooperation of 1:1.3
System, while the glutinous rice wrapped up with gauze being put into wherein, it boils 3~4 hours, is filtered to remove slag, be 80 DEG C in juice temperature
It is put into sodium sulphate when above, is completely dissolved to it, 1.5 potassium hypophosphite and 4 parts of work are added at 45 DEG C or more for juice temperature
Industry ethyl alcohol is modulated, and the juice modulated is set in a cool and dry place, reaction is cooled down to it and crystalline solid is precipitated, then will crystallization
Body taking-up is placed at aeration-drying, and powder is placed in dryer after natural extruding and is dried, sweet wormwood powder drying machine is dried to
Moisture is lower than 15%.
Applicant's test effect explanation:
The above content is a further detailed description of the present invention in conjunction with specific preferred embodiments, and it cannot be said that this hair
Bright specific implementation is only limited to these instructions.For those of ordinary skill in the art to which the present invention belongs, it is not taking off
Under the premise of from present inventive concept, a number of simple deductions or replacements can also be made, all shall be regarded as belonging to protection of the invention
Range.
Claims (2)
1. a kind of preparation method of sweet wormwood powder, characterized by the following steps:
The sweet wormwood of 80~90 parts by weight is taken to be ground into the powder of 50~70mm；
The Taxus leaf of 6~8 parts by weight is taken to be ground into the powder of 50~70mm；
The Radix Glycyrrhizae of 1~2 parts by weight is taken to crush the powder for being processed into 80~140mm；
Above-mentioned Sweet Wormwood Herb, Taxus leaf powder and Radix Glycyrrhizae powder are mixed evenly, by 1:1.2~1.5 weight ratio with
Water purification cooperation is boiled, while the glutinous rice wrapped up with gauze being put into wherein, is boiled 3~4 hours, is filtered to remove slag,
Juice temperature is put into sodium sulphate when being 80 DEG C or more, is completely dissolved to it, 1~2 weight is added at 45 DEG C or more for juice temperature
The potassium hypophosphite of part and the industrial alcohol of 3~5 parts by weight are modulated, and the juice modulated are set in a cool and dry place, to it
Crystalline solid is precipitated in cooling reaction, and then crystalline solid taking-up is placed at aeration-drying, powder is placed in drying after natural extruding
It is obtained by drying in machine.
2. the preparation method of sweet wormwood powder according to claim 1, it is characterised in that: sweet wormwood powder drying machine is dried to moisture
Lower than 15%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710669177.4A CN109381498A (en) | 2017-08-08 | 2017-08-08 | The preparation method of sweet wormwood powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710669177.4A CN109381498A (en) | 2017-08-08 | 2017-08-08 | The preparation method of sweet wormwood powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109381498A true CN109381498A (en) | 2019-02-26 |
Family
ID=65413615
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710669177.4A Pending CN109381498A (en) | 2017-08-08 | 2017-08-08 | The preparation method of sweet wormwood powder |
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| Country | Link |
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| CN (1) | CN109381498A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107929132A (en) * | 2017-12-08 | 2018-04-20 | 蒋琴 | The preparation method of sweet wormwood powder |
| CN110916064A (en) * | 2019-10-16 | 2020-03-27 | 贵州国圣堂生物科技有限公司 | Flavored food prepared with sweet wormwood in auxiliary production and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102754734A (en) * | 2012-05-28 | 2012-10-31 | 鲁东大学 | Chinese herbal livestock feed additive and application thereof |
| CN104082496A (en) * | 2014-06-18 | 2014-10-08 | 郎溪县百信精米厂 | Wine-fragrance rice cake capable of clearing away summer heat |
| CN104474007A (en) * | 2014-07-08 | 2015-04-01 | 郑州大学 | Antipyretic artemisia apiacea and licorice particle and soluble pulvis for veterinary use and preparation method thereof |
-
2017
- 2017-08-08 CN CN201710669177.4A patent/CN109381498A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102754734A (en) * | 2012-05-28 | 2012-10-31 | 鲁东大学 | Chinese herbal livestock feed additive and application thereof |
| CN104082496A (en) * | 2014-06-18 | 2014-10-08 | 郎溪县百信精米厂 | Wine-fragrance rice cake capable of clearing away summer heat |
| CN104474007A (en) * | 2014-07-08 | 2015-04-01 | 郑州大学 | Antipyretic artemisia apiacea and licorice particle and soluble pulvis for veterinary use and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107929132A (en) * | 2017-12-08 | 2018-04-20 | 蒋琴 | The preparation method of sweet wormwood powder |
| CN110916064A (en) * | 2019-10-16 | 2020-03-27 | 贵州国圣堂生物科技有限公司 | Flavored food prepared with sweet wormwood in auxiliary production and preparation method thereof |
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Application publication date: 20190226 |
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