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CN109315394A - Compound type fruit fly slow-release attractant and preparation method thereof - Google Patents

Compound type fruit fly slow-release attractant and preparation method thereof Download PDF

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Publication number
CN109315394A
CN109315394A CN201811162748.6A CN201811162748A CN109315394A CN 109315394 A CN109315394 A CN 109315394A CN 201811162748 A CN201811162748 A CN 201811162748A CN 109315394 A CN109315394 A CN 109315394A
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China
Prior art keywords
lure
cue
carypohyllene
paraffin
methyl eugenol
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Pending
Application number
CN201811162748.6A
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Chinese (zh)
Inventor
吴仲真
林进添
宾淑英
舒本水
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Zhongkai University of Agriculture and Engineering
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Zhongkai University of Agriculture and Engineering
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Priority to CN201811162748.6A priority Critical patent/CN109315394A/en
Publication of CN109315394A publication Critical patent/CN109315394A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08Oxygen or sulfur directly attached to an aromatic ring system
    • A01N31/16Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/34Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N27/00Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof

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  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

本发明公开了一种复合型实蝇缓释引诱剂及其制备方法,所述复合型实蝇缓释引诱剂由甲基丁香酚、诱蝇酮、β‑石竹烯、石蜡载体和醋酸纤维丝束组成,甲基丁香酚、诱蝇酮、β‑石竹烯和石蜡载体混合填充醋酸纤维丝束。本发明提供的复合型实蝇缓释引诱剂具有较宽引诱范围,制备方法简易、成本低、可操作性强,可降低甲基丁香酚、诱蝇酮和β‑石竹烯中的活性成分被氧化和分解的速度,使用量大大减少,并稳定连续释放甲基丁香酚、诱蝇酮和β‑石竹烯至少12周。

The present invention discloses a compound fruit fly slow-release attractant and a preparation method thereof. Tow composition, methyl eugenol, lupus ketone, beta-caryophyllene and paraffin carrier mix filled with acetate tow. The compound fruit fly slow-release attractant provided by the invention has a wide attracting range, a simple preparation method, low cost and strong operability, and can reduce the amount of active ingredients in methyl eugenol, lupus ketone and β-caryophyllene. The rate of oxidation and decomposition, the amount of use is greatly reduced, and the stable continuous release of methyl eugenol, lupus and β-caryophyllene for at least 12 weeks.

Description

A kind of compound trypetid slow release attractant and preparation method thereof
Technical field
The invention belongs to insect attractant technical fields.More particularly, to a kind of compound trypetid slow release attractant and Preparation method.
Background technique
Trypetid belongs to Tephritidae, is plant-feed insect, and larva is potential food, wherein the citrus fruit fly of Tephritidae, melonfly It is that most destructive agricultural pests, the fruit and vegetable seriously endangered all over the world produce and limit in the world with Bactrocera correcta Local fruit and vegetable trade exports, cause serious economic loss every year.And utilize attractant methyl eugenol, cue-lure and β- Carypohyllene carries out male worm trapping and population monitoring has become the effective technology means of control trypetid pest.
But current trypetid attractant Shortcomings have in terms of two: first, most of trypetid attractant dosage form is liquid agent Vulnerable to illumination and the influence of temperature condition isomerization or oxidation occur for type, cannot keep stable rate of release for a long time, and And operability is poor;Second, single attractant can only lure single trypetid, cannot be right simultaneously using same trapping system A variety of trypetid pests are trapped and killed or are monitored.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the defect and deficiency of existing trypetid attractant, provide it is a kind of have compared with Width lures range, steady and continuous release, lasting period long compound trypetid slow release attractant.
Another object of the present invention is to provide the preparation method of above-mentioned compound trypetid slow release attractant.
To achieve the goals above, the present invention is achieved by following scheme:
A kind of compound trypetid slow release attractant, by methyl eugenol, cue-lure, β-carypohyllene, paraffin carrier and acetate fiber Tow composition, methyl eugenol, cue-lure, β-carypohyllene and paraffin carrier mixing filling acetate silk.
Acetate silk has good penetration by liquid and excellent adsorptivity, being capable of abundant, uniform adsorption methyl fourth Fragrant phenol, cue-lure, β-carypohyllene and paraffin carrier mixture, and in implementation process stable and uniform release methyl eugenol, Cue-lure and β-carypohyllene, and the active constituent that can be reduced in methyl eugenol, cue-lure and β-carypohyllene is oxidized and decomposes Speed, usage amount greatly reduces, and steady and continuous discharges attractant at least 12 weeks.
Preferably, methyl eugenol, cue-lure, three kinds of attractants of β-carypohyllene and paraffin carrier are by following Weight percent mixing: methyl eugenol, cue-lure, the summation 20~50% of three kinds of attractants of β-carypohyllene, paraffin carrier 50~ 80%。
If methyl eugenol, cue-lure and β-carypohyllene dosage collocation are suitable, to citrus fruit fly, melonfly and kind stone The attractant effect of pomegranate trypetid is best.Preferably, the methyl eugenol, cue-lure and β-carypohyllene are mixed by following weight percent It closes: methyl eugenol 10~20%, cue-lure 5~20%, β-carypohyllene 5~10%.
Acetate silk of the present invention can be conventional use of shape and specification, it is preferable that the acetate fiber Tow is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.
A kind of preparation method of compound trypetid slow release attractant, the specific steps of the preparation method are as follows:
S1. solid paraffin is put into container, is heated to being completely dissolved, obtains paraffin liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are infiltrated in paraffin liquid, obtains methyl eugenol, cue-lure, β-China pink The blended liquid of alkene and paraffin liquid;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure, β-carypohyllene and paraffin liquid until complete Hypersorption then takes out and is allowed to cool solidification.
Preferably, a kind of preparation method of compound trypetid slow release attractant, the specific steps of the preparation method are as follows:
S1. solid paraffin is put into beaker, is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are infiltrated in paraffin liquid, be heated to 100 DEG C and stirred evenly, obtain first Base eugenol, cue-lure, β-carypohyllene and paraffin liquid blended liquid;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure, β-carypohyllene and paraffin liquid until complete Hypersorption (no bubble is emerged), then takes out and is allowed to cool solidification.
Compared with prior art, the invention has the following advantages:
Compound trypetid slow release attractant provided by the invention lures range with wider, can lure citrus fruit fly, melon real simultaneously The male worm of 3 kinds of trypetids of fly and Bactrocera correcta realizes 3 kinds of trypetid trappings and Insect infestation monitoring.
In addition, the preparation method of the compound trypetid slow release attractant is simple, at low cost, strong operability, first can be reduced The speed that active constituent in base eugenol, cue-lure and β-carypohyllene is oxidized and decomposes, usage amount greatly reduce, and stablize Continuous release methyl eugenol, cue-lure and β-carypohyllene at least 12 weeks.
Detailed description of the invention
Fig. 1 is compound trypetid slow release attractant schematic diagram.
Fig. 2 is the technological process of production of the compound trypetid slow release attractant of the present invention.
Specific embodiment
The present invention is further illustrated below in conjunction with Figure of description and specific embodiment, but embodiment is not to the present invention It limits in any form.Unless stated otherwise, the present invention uses reagent, method and apparatus routinely try for the art Agent, method and apparatus.
Unless stated otherwise, following embodiment agents useful for same and material are commercially available.
Embodiment 1
A kind of compound trypetid slow release attractant, by methyl eugenol, cue-lure, β-carypohyllene, paraffin carrier and acetate fiber Tow composition, methyl eugenol, cue-lure, β-carypohyllene and paraffin carrier mixing filling acetate silk.The methyl fourth Fragrant phenol, cue-lure and β-carypohyllene are mixed by following weight percent: methyl eugenol 15%, cue-lure 15%, β-carypohyllene 10%.Acetate silk is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.Compound reality described above in the embodiment Fly slow release attractant is as shown in Figure 1.
The preparation method of above-mentioned compound trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain methyl eugenol, cue-lure, β-stone The blended liquid of bamboo alkene and paraffin liquid, the weight percent of 4 kinds of substances is 60% paraffin carrier, 15% methyl fourth in the blended liquid Fragrant phenol, 15% cue-lure, 10% β-carypohyllene are placed in baking oven and are heated to 100 DEG C and stir evenly;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure, β-carypohyllene and paraffin liquid until complete Hypersorption (no bubble is emerged), then takes out and is allowed to cool solidification.
The technological process of production of the compound trypetid slow release attractant of the above is as shown in Figure 2 in the embodiment.
Compound trypetid slow release attractant in the present embodiment effectively steady and continuous can discharge methyl eugenol, lure fly Ketone and β-carypohyllene, and extended release period, being released effectively the period is 14 weeks.
Embodiment 2
A kind of compound trypetid slow release attractant, by methyl eugenol, cue-lure, β-carypohyllene, paraffin carrier and acetate fiber Tow composition, methyl eugenol, cue-lure, β-carypohyllene and paraffin carrier mixing filling acetate silk.The methyl fourth Fragrant phenol, cue-lure and β-carypohyllene are mixed by following weight percent: methyl eugenol 20%, cue-lure 20%, β-carypohyllene 10%.Acetate silk is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.Compound reality described above in the embodiment Fly slow release attractant is as shown in Figure 1.
The preparation method of above-mentioned compound trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain methyl eugenol, cue-lure, β-stone The blended liquid of bamboo alkene and paraffin liquid, the weight percent of 4 kinds of substances is 50% paraffin carrier, 20% methyl fourth in the blended liquid Fragrant phenol, 20% cue-lure, 10% β-carypohyllene are placed in baking oven and are heated to 100 DEG C and stir evenly;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure, β-carypohyllene and paraffin liquid until complete Hypersorption (no bubble is emerged), then takes out and is allowed to cool solidification.
The technological process of production of the compound trypetid slow release attractant of the above is as shown in Figure 2 in the embodiment.
Compound trypetid slow release attractant in the present embodiment effectively steady and continuous can discharge methyl eugenol, lure fly Ketone and β-carypohyllene, and extended release period, being released effectively the period is 13 weeks.
Embodiment 3
A kind of compound trypetid slow release attractant, by methyl eugenol, cue-lure, β-carypohyllene, paraffin carrier and acetate fiber Tow composition, methyl eugenol, cue-lure, β-carypohyllene and paraffin carrier mixing filling acetate silk.The methyl fourth Fragrant phenol, cue-lure and β-carypohyllene are mixed by following weight percent: methyl eugenol 10%, cue-lure 5%, β-carypohyllene 5%. Acetate silk is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.Compound trypetid described above is slow in the embodiment It is as shown in Figure 1 to release attractant.
The preparation method of above-mentioned compound trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain methyl eugenol, cue-lure, β-stone The blended liquid of bamboo alkene and paraffin liquid, the weight percent of 4 kinds of substances is 80% paraffin carrier, 10% methyl fourth in the blended liquid Fragrant phenol, 5% cue-lure, 5% β-carypohyllene are placed in baking oven and are heated to 100 DEG C and stir evenly;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure, β-carypohyllene and paraffin liquid until complete Hypersorption (no bubble is emerged), then takes out and is allowed to cool solidification.
The technological process of production of the compound trypetid slow release attractant of the above is as shown in Figure 2 in the embodiment.
Compound trypetid slow release attractant in the present embodiment effectively steady and continuous can discharge methyl eugenol, lure fly Ketone and β-carypohyllene, and extended release period, being released effectively the period is 12 weeks.
Comparative example 1
A kind of compound trypetid slow release attractant, is made of attractant and paraffin carrier.The attractant is methyl eugenol, lures Fly ketone and β-carypohyllene mixture, the methyl eugenol, cue-lure and β-carypohyllene are mixed by following weight percent: first Base eugenol 15%, cue-lure 15%, β-carypohyllene 10%.
The preparation method of above-mentioned compound trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain the blending of attractant and paraffin liquid Liquid, in the blended liquid weight percent of 4 kinds of substances be 60% paraffin carrier, 15% methyl eugenol, 15% cue-lure, 10% β-carypohyllene is placed in baking oven and is heated to 100 DEG C and stirs evenly.
It is 4 weeks that compound trypetid slow release attractant in this comparative example, which is released effectively the time, and has not been able to continuous and effective Uniformly release.
Comparative example 2
A kind of trypetid slow release attractant is made of attractant, paraffin carrier and acetate silk, and attractant and paraffin carrier are mixed Close filling acetate silk.The attractant is methyl eugenol, cue-lure and β-carypohyllene mixture, the methyl fourth Fragrant phenol, cue-lure and β-carypohyllene are mixed by following weight percent: methyl eugenol 30%, cue-lure 30%, β-carypohyllene 10%.Acetate silk is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.
The preparation method of above-mentioned trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain the blending of attractant and paraffin liquid Liquid, in the blended liquid weight percent of 4 kinds of substances be 30% paraffin carrier, 30% methyl eugenol, 30% cue-lure, 10% β-carypohyllene is placed in baking oven and is heated to 100 DEG C and stirs evenly;
S3. acetate silk is dipped into the blended liquid of attractant and paraffin liquid until fully absorbing that (no bubble emits Out), it then takes out and is allowed to cool solidification.
The time that is released effectively of trypetid slow release attractant in this comparative example is 8 weeks, but increase accordingly attractant at This.
Comparative example 3
A kind of compound trypetid slow release attractant, is made of, attractant and paraffin attractant, paraffin carrier and acetate silk Carrier mixing filling acetate silk.The attractant be methyl eugenol, cue-lure and β-carypohyllene mixture, it is described Methyl eugenol, cue-lure and β-carypohyllene are mixed by following weight percent: methyl eugenol 30%, cue-lure 5%, β-China pink Alkene 5%.Acetate silk is cylindrical type, and specification is 1.5 cm of diameter, high 3.0 cm.
The preparation method of above-mentioned trypetid slow release attractant includes the following steps:
S1. solid paraffin is put into beaker, is placed in baking oven and is heated to 100 DEG C and stirs to be completely dissolved to paraffin, obtains paraffin Liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are blended into paraffin liquid, obtain the blending of attractant and paraffin liquid Liquid, in the blended liquid weight percent of 4 kinds of substances be 60% paraffin carrier, 30% methyl eugenol, 5% cue-lure, 5% β-carypohyllene, be placed in baking oven and be heated to 100 DEG C and stir evenly;
S3. acetate silk is dipped into the blended liquid of attractant and paraffin liquid until fully absorbing that (no bubble emits Out), it then takes out and is allowed to cool solidification.
The time that is released effectively of compound trypetid slow release attractant in this comparative example is 12 weeks, but the scalemic thereof The melonfly and Bactrocera correcta ratio lured are relatively fewer.

Claims (5)

1. a kind of compound trypetid slow release attractant, which is characterized in that carried by methyl eugenol, cue-lure, β-carypohyllene, paraffin Body and acetate silk composition, methyl eugenol, cue-lure, β-carypohyllene and paraffin carrier mixing filling acetate fibres Beam.
2. compound trypetid slow release attractant according to claim 1, which is characterized in that methyl eugenol, cue-lure, β- Three kinds of attractants of carypohyllene are mixed with paraffin carrier by following weight percent: methyl eugenol, cue-lure, three kinds of β-carypohyllene The summation 20~50% of attractant, paraffin carrier 50~80%.
3. compound trypetid slow release attractant according to claim 2, which is characterized in that the methyl eugenol lures fly Ketone and β-carypohyllene are mixed by following weight percent: methyl eugenol 10~20%, cue-lure 5~20%, β-carypohyllene 5~ 10%。
4. compound trypetid slow release attractant according to claim 1, which is characterized in that the acetate silk is Cylindrical type, specification are 1.5 cm of diameter, high 3.0 cm.
5. a kind of preparation method of compound trypetid slow release attractant, which is characterized in that the specific steps of the preparation method are as follows:
S1. solid paraffin is put into container, is heated to being completely dissolved, obtains paraffin liquid;
S2. methyl eugenol, cue-lure and β-carypohyllene are infiltrated in paraffin liquid, obtains methyl eugenol, cue-lure, β-China pink The blended liquid of alkene and paraffin liquid;
S3. acetate silk is dipped into the blended liquid of methyl eugenol, cue-lure and β-carypohyllene and paraffin liquid until It fully absorbs, then takes out and be allowed to cool solidification.
CN201811162748.6A 2018-09-30 2018-09-30 Compound type fruit fly slow-release attractant and preparation method thereof Pending CN109315394A (en)

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CN109526959A (en) * 2018-09-30 2019-03-29 仲恺农业工程学院 Fruit fly slow-release attractant and preparation method thereof
CN111903676A (en) * 2020-06-27 2020-11-10 内蒙古大学 Attractant for pollinating insects, method for improving plant maturing rate and application thereof
CN111903675A (en) * 2020-06-22 2020-11-10 内蒙古大学 An attractant for pollinating insects and its application for improving plant seed setting rate
CN113180041A (en) * 2021-04-27 2021-07-30 乌鲁木齐海关技术中心 Efficient drosophila ziziphus attractant

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109526959A (en) * 2018-09-30 2019-03-29 仲恺农业工程学院 Fruit fly slow-release attractant and preparation method thereof
CN111903675A (en) * 2020-06-22 2020-11-10 内蒙古大学 An attractant for pollinating insects and its application for improving plant seed setting rate
CN111903676A (en) * 2020-06-27 2020-11-10 内蒙古大学 Attractant for pollinating insects, method for improving plant maturing rate and application thereof
CN111903676B (en) * 2020-06-27 2023-03-28 内蒙古大学 Attractant for pollinating insects, method for improving plant maturing rate and application thereof
CN113180041A (en) * 2021-04-27 2021-07-30 乌鲁木齐海关技术中心 Efficient drosophila ziziphus attractant

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Application publication date: 20190212