CN109304133A - A kind of hydrogenation reactor device for hydrogenation reaction - Google Patents
A kind of hydrogenation reactor device for hydrogenation reaction Download PDFInfo
- Publication number
- CN109304133A CN109304133A CN201811387203.5A CN201811387203A CN109304133A CN 109304133 A CN109304133 A CN 109304133A CN 201811387203 A CN201811387203 A CN 201811387203A CN 109304133 A CN109304133 A CN 109304133A
- Authority
- CN
- China
- Prior art keywords
- balls
- porcelain layers
- tower shell
- porcelain
- layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0207—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
- B01J8/0221—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical shaped bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0285—Heating or cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0292—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds with stationary packing material in the bed, e.g. bricks, wire rings, baffles
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Electromagnetism (AREA)
- Fluid Mechanics (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Thermal Sciences (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention is a kind of hydrogenator device for hydrogenation reaction, including tower shell, which is characterized in that the stack shell of the tower shell is in hollow cylinder structure setting, and the bottom of the tower shell is equipped with discharge nozzle.The present invention is according to the difference of working condition, conducive to the intracorporal reaction temperature of tower shell, pressure carries out real-time monitoring, convenient for tower shell interior reaction temperature and pressure are adjusted, hydrogenation reaction is regulated and controled, by the way that air blowing device one is arranged, air blowing device two and upper layer cooling device, effectively reduce reaction temperature, pass through inlet porting diffuser, distributor, porcelain layers of balls one, porcelain layers of balls two, porcelain layers of balls three, porcelain layers of balls four, porcelain layers of balls five, porcelain layers of balls six, porcelain layers of balls seven, porcelain layers of balls eight and redistributor realize uniform feed flow, by the way that lamp irradiation source is arranged, realize photocatalytic reaction, and then increase catalytic conversion efficiency.
Description
Technical field
The present invention relates to a kind of chemical equipment technical field more particularly to a kind of hydrogenator dresses for hydrogenation reaction
It sets.
Background technique
Hydrogenator is a very important equipment, hydrogenation reaction in Organic Chemistry Laboratory and actual production process
Device synthesizes the lower carbon number hydrocarbons with more high added value and high carbon number branch commonly used in the hydrogenation reaction of carbon dioxide and carbon monoxide etc.
Chain hydrocarbon.Hydrogenator serves not only as the container of hydrogenation reaction, and can also be used for liquids and gases needs and be sufficiently mixed
Occasion.As unit scale constantly expands, hydrogenator is also increasingly enlarged, and the update of hydrogenator manufacturing technology is changed
In generation, is just in progress like a raging fire, however, being limited by various conditions, currently used hydrogenator apparatus structure design is not
Rationally, it is not easy to that tower shell interior reaction temperature and pressure is adjusted, not can be carried out uniform feed flow, be unable to satisfy plus hydrogen is anti-
The requirement of device device is answered, does not have safe and efficient reactor assembly universal at present.
Summary of the invention
Present invention seek to address that the deficiencies in the prior art, and a kind of hydrogenator device for hydrogenation reaction is provided.
The present invention to achieve the above object, using following technical scheme:
A kind of hydrogenator device for hydrogenation reaction, including tower shell, which is characterized in that the tower shell
Stack shell be in hollow cylinder structure setting, the bottom of the tower shell is fixed to be equipped with skirt, the bottom surrounding of the skirt
On the ground by foundation bolt installation, the skirt, which is equipped with, checks access hole, and welding installation orifice plate, described on the skirt
Fireprotection layer is laid by installation orifice plate tie wire net in the outer surface of skirt, is equipped with people at the upper cover of the tower housing tip
Kong Yi, the top of the tower shell are equipped with feed pipe, and the feed end of the feed pipe is connected with external world's storage equipment, it is described into
Expects pipe is located at the side setting of the manhole one, and the discharge end of the feed pipe is connected to the inside of the tower shell, described
The discharge end of feed pipe is equipped with inlet diffuser, and the inlet diffuser is located at the inner upper of the tower shell, the tower
The upper section and lower section of device enclosure interior are respectively equipped with catalyst layer and lower catalyst layer, by upper on the side wall of the tower shell
To having several thermometer temperature-measuring ports being in contact with the upper catalyst layer, the lower catalyst layer, urge on described
Manhole two and pressure transmitter mouth are equipped on the side wall of the tower shell between agent layer and the lower catalyst layer, it is described
Manhole two and the pressure transmitter mouth are located at the outer wall two sides of the tower shell, the top of the upper catalyst layer by
Under to being above successively arranged porcelain layers of balls two and porcelain layers of balls one, equipped with level in the tower shell above the porcelain layers of balls one
Installing pipe, the installation inner coaxial tube be equipped with lamp irradiation source, between lamp irradiation source and the inlet diffuser
The inside of the tower shell is equipped with distributor, and upper layer cooling device, the cooling dress in the upper layer are equipped in the upper catalyst layer
The inside for being mounted on the tower shell is set, the bottom of the upper catalyst layer is successively arranged porcelain layers of balls three and porcelain ball from top to bottom
The bottom of layer four, the porcelain layers of balls four is equipped with catalyst support device, and the catalyst support device is mounted on the tower shell
On the inner wall of body and it is located at the top of the manhole two, is in contact on the tower shell with the lower part of the upper catalyst layer
Side wall be equipped with opening overlying catalyst discharge duct diagonally downward, the feed end of the overlying catalyst discharge duct sequentially passes through
The side wall of the tower shell, the porcelain layers of balls three are connected with the upper catalyst layer, and the top of the lower catalyst layer is set
There is porcelain layers of balls five, the top of the porcelain layers of balls five is equipped with redistributor, and the redistributor is mounted on the interior of the tower shell
Portion and the lower section for being located at the catalyst support device, between the catalyst support device and the redistributor
The inner horizontal of the tower shell is equipped with air blowing device one, the side of the tower shell above the air blowing device one
Cold hydrogen mouth is equipped on wall, the cold hydrogen mouth is located at the lower section of the pressure transmitter mouth, and the lower part of the lower catalyst layer is equipped with
Air blowing device two, the air blowing device two are mounted on the inner wall of the tower shell, the air blowing device two and the tower
Porcelain layers of balls six, porcelain layers of balls seven and porcelain layers of balls eight, the bottom of the tower shell are successively arranged between the bottom of shell from top to bottom
Equipped with discharge nozzle, the feed end of the discharge nozzle sequentially passes through the skirt, the bottom interior wall of the tower shell is connected with outlet
Collector two, the exit collector two are located at the intracorporal bottom of tower shell, and the bottom outside of the tower shell is equipped with
Lower catalyst agent discharge duct, the lower catalyst agent discharge duct are located at the side setting of the discharge nozzle, the lower catalyst agent
The feed end of discharge duct sequentially passes through the bottom of the tower shell, the porcelain layers of balls eight, the porcelain layers of balls seven, the porcelain layers of balls
Six are connected with the lower catalyst layer.
Preferably, the inspection access hole uses the form of flanges with neck butt welding, face type is ring joint face, pressure
Power grade is 6.3~25.0MPa.
Preferably, the redistributor includes but is not limited to throttle type redistributor.
Preferably, the porcelain layers of balls one, the porcelain layers of balls two, the porcelain layers of balls three, the porcelain layers of balls four, the porcelain ball
Layer five, the porcelain layers of balls six, the porcelain layers of balls seven, the porcelain bulb diameter in the porcelain layers of balls eight are respectively Φ 13mm, Φ 6mm, Φ
3mm、Φ6mm、Φ6mm、Φ3mm、Φ6mm、Φ13mm。
Preferably, the porcelain layers of balls one, the porcelain layers of balls two, the porcelain layers of balls three, the porcelain layers of balls five, the porcelain ball
The thickness of layer six is 150mm, and the thickness of the porcelain layers of balls four and the porcelain layers of balls seven is respectively 1210mm, 1150mm.
Preferably, the air blowing device one and the air blowing device two are all made of quencher.
Preferably, the catalyst support device includes but is not limited to catalyst grid, catalyst supporting plate.
Preferably, the upper layer cooling device includes but is not limited to coil pipe, tubulation cooling.
Preferably, including but is not limited to catalyst filling, catalysis in the upper catalyst layer and the lower catalyst layer
The mixture of agent and porcelain ball.
The beneficial effects of the present invention are: structure of the invention is novel, design rationally, by the side wall of tower shell by upper
To lower several thermometer temperature-measuring ports being in contact with upper catalyst layer, lower catalyst layer of setting, pressure transmitter, according to production item
The difference of part is conducive to carry out real-time monitoring to the intracorporal reaction temperature of tower shell, pressure, convenient for tower shell interior reaction temperature
And pressure is adjusted, and regulates and controls to hydrogenation reaction, by the way that air blowing device one, the cooling dress of air blowing device two and upper layer is arranged
Set, convenient for terminating reaction, recycling heat and product initial gross separation, effectively reduce reaction temperature, by inlet porting diffuser,
Distributor, porcelain layers of balls one, porcelain layers of balls two, porcelain layers of balls three, porcelain layers of balls four, porcelain layers of balls five, porcelain layers of balls six, porcelain layers of balls seven, porcelain layers of balls
Eight and redistributor realize uniform feed flow, by the way that lamp irradiation source is arranged, realizes photocatalytic reaction, and then increase catalysis
Transformation efficiency.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the invention；
Fig. 2 is another structural schematic diagram of the invention；
Fig. 3 is the partial enlarged view of A in Fig. 1 and Fig. 2；
In figure: 1- feed pipe；2- manhole one；3- thermometer temperature-measuring port；4- overlying catalyst discharge duct；The cold hydrogen mouth of 5-；6-
Pressure transmitter mouth；7- manhole two；8- discharge nozzle；9- lower catalyst agent discharge duct；10- checks access hole；The diffusion of 111- entrance
Device；112- exit collector two；12- air blowing device one；13- redistributor；141- porcelain layers of balls one；142- porcelain layers of balls two；143-
Porcelain layers of balls three；144- porcelain layers of balls four；145- porcelain layers of balls five；146- porcelain layers of balls six；147- porcelain layers of balls seven；148- porcelain layers of balls eight；
The upper catalyst layer of 151-；Catalyst layer under 152-；16- catalyst support device；17- installs orifice plate；18- lamp irradiation source；19- skirt
Seat；20- tower shell；21- distributor；The upper layer 22- cooling device；23- air blowing device two；
It is described in detail below with reference to the embodiment of the present invention referring to attached drawing.
Specific embodiment
Below with reference to embodiment, the invention will be further described:
A kind of hydrogenator device for hydrogenation reaction, including tower shell 20, which is characterized in that the tower shell
The stack shell of body 20 is in hollow cylinder structure setting, and the bottom of the tower shell 20 is fixed to be equipped with skirt 19, the skirt 19
Bottom surrounding installed on the ground by foundation bolt, the skirt 19, which is equipped with, checks access hole 10, on the skirt 19
Fireprotection layer, the tower are laid by installation 17 tie wire net of orifice plate in the outer surface of welding installation orifice plate 17, the skirt 19
Manhole 1 is equipped at the upper cover on 20 top of shell, the top of the tower shell 20 is equipped with feed pipe 1, the feed pipe 1
Feed end is connected with extraneous storage equipment, and the feed pipe 1 is located at the side setting of the manhole 1, and the feed pipe 1 goes out
Material end is connected to the inside of the tower shell 20, and the discharge end of the feed pipe 1 is equipped with inlet diffuser 111, the entrance
Diffuser 111 is located at the inner upper of the tower shell 20, and the upper section and lower section inside the tower shell 20 are respectively equipped with
Upper catalyst layer 151 and lower catalyst layer 152, be equipped on the side wall of the tower shell 20 from top to bottom it is several with it is described on urge
The thermometer temperature-measuring port 3 that agent layer 151, the lower catalyst layer 152 are in contact is located at the upper catalyst layer 151 and described
Manhole 27 and pressure transmitter mouth 6, the manhole are equipped on the side wall of the tower shell 20 between lower catalyst layer 152
27 and the pressure transmitter mouth 6 be located at the outer wall two sides of the tower shell 20, the top of the upper catalyst layer 151
End is successively arranged porcelain layers of balls 2 142 and porcelain layers of balls 1 from bottom to top, the tower above the porcelain layers of balls 1
Horizontal installing pipe is equipped in shell 20, the installation inner coaxial tube is equipped with lamp irradiation source 18, be located at lamp irradiation source 18 and
The inside of the tower shell 20 between the inlet diffuser 111 is equipped with distributor 21, sets in the upper catalyst layer 151
There is upper layer cooling device 22, the upper layer cooling device 22 is mounted on the inside of the tower shell 20, the upper catalyst layer
151 bottom is successively arranged porcelain layers of balls 3 143 and porcelain layers of balls 4 144 from top to bottom, and the bottom of the porcelain layers of balls 4 144, which is equipped with, urges
Agent support device 16, the catalyst support device 16 are mounted on the inner wall of the tower shell 20 and are located at the people
The top in hole 27, the side wall being in contact on the tower shell 20 with the lower part of the upper catalyst layer 151 are equipped with opening inclination
Downward overlying catalyst discharge duct 4, the feed end of the overlying catalyst discharge duct 4 sequentially pass through the tower shell 20
Side wall, the porcelain layers of balls 3 143 are connected with the upper catalyst layer 151, and the top of the lower catalyst layer 152 is equipped with porcelain ball
The top of layer 5 145, the porcelain layers of balls 5 145 is equipped with redistributor 13, and the redistributor 13 is mounted on the tower shell
20 inside and the lower section for being located at the catalyst support device 16, divide positioned at the catalyst support device 16 with described again
The inner horizontal of the tower shell 20 between orchestration 13 is equipped with air blowing device 1, is located at one 12 top of air blowing device
The tower shell 20 side wall on be equipped with cold hydrogen mouth 5, the cold hydrogen mouth 5 is located at the lower section of the pressure transmitter mouth 6, institute
The lower part for stating lower catalyst layer 152 is equipped with air blowing device 2 23, and the air blowing device 2 23 is mounted on the tower shell 20
On inner wall, be successively arranged from top to bottom between the air blowing device 2 23 and the bottom of the tower shell 20 porcelain layers of balls 6 146,
The bottom of porcelain layers of balls 7 147 and porcelain layers of balls 8 148, the tower shell 20 is equipped with discharge nozzle 8, the feed end of the discharge nozzle 8
Sequentially pass through the skirt 19, the bottom interior wall of the tower shell 20 is connected with exit collector 2 112, the exit collector
2 112 are located at the bottom in the tower shell 20, and the bottom outside of the tower shell 20 is equipped with lower catalyst agent discharge duct
9, the lower catalyst agent discharge duct 9 is located at the side setting of the discharge nozzle 8, the charging of the lower catalyst agent discharge duct 9
End sequentially passes through bottom, the porcelain layers of balls 8 148, the porcelain layers of balls 7 147, the porcelain layers of balls six of the tower shell 20
146 are connected with the lower catalyst layer 152.
Preferably, the inspection access hole 10 uses the form of flanges with neck butt welding, face type is ring joint face,
Pressure rating is 6.3~25.0MPa.
Preferably, the redistributor 13 includes but is not limited to throttle type redistributor.
Preferably, the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls four
144, the porcelain layers of balls 5 145, the porcelain layers of balls 6 146, the porcelain layers of balls 7 147, the porcelain ball in the porcelain layers of balls 8 148 are straight
Diameter is respectively Φ 13mm, Φ 6mm, Φ 3mm, Φ 6mm, Φ 6mm, Φ 3mm, Φ 6mm, Φ 13mm.
Preferably, the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls five
145, the thickness of the porcelain layers of balls 6 146 is 150mm, the thickness difference of the porcelain layers of balls 4 144 and the porcelain layers of balls 7 147
For 1210mm, 1150mm.
Preferably, the air blowing device 1 and the air blowing device 2 23 are all made of quencher.
Preferably, the catalyst support device 16 includes but is not limited to catalyst grid, catalyst supporting plate.
Preferably, the upper layer cooling device 22 includes but is not limited to that coil pipe or tubulation are cooling.
Preferably, including but is not limited to filling catalysis in the upper catalyst layer 151 and the lower catalyst layer 152
Agent, catalyst and porcelain ball mixture.
The present invention is in use, reaction raw materials are added in tower shell 20 by feed pipe 1, tower is added by cold hydrogen mouth 5 in hydrogen
In device shell 20, lamp irradiation source 18 is opened, photocatalytic reaction is realized, and then increase catalytic conversion efficiency, is urged with closing
Agent layer 151, lower catalyst layer 152, carry out carbon dioxide hydrogenation reaction, by the side wall of tower shell 20 from top to bottom
Several with thermometer temperature-measuring port 3 that is being in contact, pressure transmitter 6 is set, according to the difference of working condition, is conducive to tower shell
Reaction temperature in 20, pressure carry out real-time monitoring, convenient for 20 interior reaction temperature of tower shell and pressure are adjusted, to adding
Hydrogen reaction is regulated and controled, anti-convenient for terminating by the way that air blowing device 1, air blowing device 2 23 and upper layer cooling device 22 is arranged
Answer, recycle heat and product initial gross separation, effectively reduce reaction temperature, by inlet porting diffuser 111, distributor 21,
Porcelain layers of balls 1, porcelain layers of balls 2 142, porcelain layers of balls 3 143, porcelain layers of balls 4 144, porcelain layers of balls 5 145, porcelain layers of balls 6 146, porcelain ball
Layer 7 147, porcelain layers of balls 8 148 and redistributor 13 realize uniform feed flow, and structure of the invention is novel, and design is reasonable.
Embodiment 1
A kind of hydrogenator device for hydrogenation reaction, including tower shell 20, which is characterized in that the tower shell
The stack shell of body 20 is in hollow cylinder structure setting, and the bottom of the tower shell 20 is fixed to be equipped with skirt 19, the skirt 19
Bottom surrounding installed on the ground by foundation bolt, the skirt 19, which is equipped with, checks access hole 10, on the skirt 19
Fireprotection layer, the tower are laid by installation 17 tie wire net of orifice plate in the outer surface of welding installation orifice plate 17, the skirt 19
Manhole 1 is equipped at the upper cover on 20 top of shell, the top of the tower shell 20 is equipped with feed pipe 1, the feed pipe 1
Feed end is connected with extraneous storage equipment, and the feed pipe 1 is located at the side setting of the manhole 1, and the feed pipe 1 goes out
Material end is connected to the inside of the tower shell 20, and the discharge end of the feed pipe 1 is equipped with inlet diffuser 111, the entrance
Diffuser 111 is located at the inner upper of the tower shell 20, and the upper section and lower section inside the tower shell 20 are respectively equipped with
Upper catalyst layer 151 and lower catalyst layer 152, be equipped on the side wall of the tower shell 20 from top to bottom it is several with it is described on urge
The thermometer temperature-measuring port 3 that agent layer 151, the lower catalyst layer 152 are in contact is located at the upper catalyst layer 151 and described
Manhole 27 and pressure transmitter mouth 6, the manhole are equipped on the side wall of the tower shell 20 between lower catalyst layer 152
27 and the pressure transmitter mouth 6 be located at the outer wall two sides of the tower shell 20, the top of the upper catalyst layer 151
End is successively arranged porcelain layers of balls 2 142 and porcelain layers of balls 1 from bottom to top, the tower above the porcelain layers of balls 1
Horizontal installing pipe is equipped in shell 20, the installation inner coaxial tube is equipped with lamp irradiation source 18, be located at lamp irradiation source 18 and
The inside of the tower shell 20 between the inlet diffuser 111 is equipped with distributor 21, sets in the upper catalyst layer 151
There is upper layer cooling device 22, the upper layer cooling device 22 is mounted on the inside of the tower shell 20, the upper catalyst layer
151 bottom is successively arranged porcelain layers of balls 3 143 and porcelain layers of balls 4 144 from top to bottom, and the bottom of the porcelain layers of balls 4 144, which is equipped with, urges
Agent support device 16, the catalyst support device 16 are mounted on the inner wall of the tower shell 20 and are located at the people
The top in hole 27, the side wall being in contact on the tower shell 20 with the lower part of the upper catalyst layer 151 are equipped with opening inclination
Downward overlying catalyst discharge duct 4, the feed end of the overlying catalyst discharge duct 4 sequentially pass through the tower shell 20
Side wall, the porcelain layers of balls 3 143 are connected with the upper catalyst layer 151, and the top of the lower catalyst layer 152 is equipped with porcelain ball
The top of layer 5 145, the porcelain layers of balls 5 145 is equipped with redistributor 13, and the redistributor 13 is mounted on the tower shell
20 inside and the lower section for being located at the catalyst support device 16, divide positioned at the catalyst support device 16 with described again
The inner horizontal of the tower shell 20 between orchestration 13 is equipped with air blowing device 1, is located at one 12 top of air blowing device
The tower shell 20 side wall on be equipped with cold hydrogen mouth 5, the cold hydrogen mouth 5 is located at the lower section of the pressure transmitter mouth 6, institute
The lower part for stating lower catalyst layer 152 is equipped with air blowing device 2 23, and the air blowing device 2 23 is mounted on the tower shell 20
On inner wall, be successively arranged from top to bottom between the air blowing device 2 23 and the bottom of the tower shell 20 porcelain layers of balls 6 146,
The bottom of porcelain layers of balls 7 147 and porcelain layers of balls 8 148, the tower shell 20 is equipped with discharge nozzle 8, the feed end of the discharge nozzle 8
Sequentially pass through the skirt 19, the bottom interior wall of the tower shell 20 is connected with exit collector 2 112, the exit collector
2 112 are located at the bottom in the tower shell 20, and the bottom outside of the tower shell 20 is equipped with lower catalyst agent discharge duct
9, the lower catalyst agent discharge duct 9 is located at the side setting of the discharge nozzle 8, the charging of the lower catalyst agent discharge duct 9
End sequentially passes through bottom, the porcelain layers of balls 8 148, the porcelain layers of balls 7 147, the porcelain layers of balls six of the tower shell 20
146 are connected with the lower catalyst layer 152.
The inspection access hole 10 uses the form of flanges with neck butt welding, and face type is ring joint face, pressure rating
For 6.3MPa.
The redistributor 13 uses throttle type redistributor.
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 4 144, described
Porcelain layers of balls 5 145, the porcelain layers of balls 6 146, the porcelain layers of balls 7 147, the porcelain bulb diameter in the porcelain layers of balls 8 148 are respectively
Φ13mm、Φ6mm、Φ3mm、Φ6mm、Φ6mm、Φ3mm、Φ6mm、Φ13mm。
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 5 145, described
The thickness of porcelain layers of balls 6 146 is 150mm, and the thickness of the porcelain layers of balls 4 144 and the porcelain layers of balls 7 147 is respectively
1210mm、1150mm。
The air blowing device 1 and the air blowing device 2 23 are all made of quencher.
The catalyst support device 16 is catalyst grid.
The upper layer cooling device 22 is cooling using coil pipe.
Catalyst is filled in the upper catalyst layer 151 and the lower catalyst layer 152.
Embodiment 2
A kind of hydrogenator device for hydrogenation reaction, including tower shell 20, which is characterized in that the tower shell
The stack shell of body 20 is in hollow cylinder structure setting, and the bottom of the tower shell 20 is fixed to be equipped with skirt 19, the skirt 19
Bottom surrounding installed on the ground by foundation bolt, the skirt 19, which is equipped with, checks access hole 10, on the skirt 19
Fireprotection layer, the tower are laid by installation 17 tie wire net of orifice plate in the outer surface of welding installation orifice plate 17, the skirt 19
Manhole 1 is equipped at the upper cover on 20 top of shell, the top of the tower shell 20 is equipped with feed pipe 1, the feed pipe 1
Feed end is connected with extraneous storage equipment, and the feed pipe 1 is located at the side setting of the manhole 1, and the feed pipe 1 goes out
Material end is connected to the inside of the tower shell 20, and the discharge end of the feed pipe 1 is equipped with inlet diffuser 111, the entrance
Diffuser 111 is located at the inner upper of the tower shell 20, and the upper section and lower section inside the tower shell 20 are respectively equipped with
Upper catalyst layer 151 and lower catalyst layer 152, be equipped on the side wall of the tower shell 20 from top to bottom it is several with it is described on urge
The thermometer temperature-measuring port 3 that agent layer 151, the lower catalyst layer 152 are in contact is located at the upper catalyst layer 151 and described
Manhole 27 and pressure transmitter mouth 6, the manhole are equipped on the side wall of the tower shell 20 between lower catalyst layer 152
27 and the pressure transmitter mouth 6 be located at the outer wall two sides of the tower shell 20, the top of the upper catalyst layer 151
End is successively arranged porcelain layers of balls 2 142 and porcelain layers of balls 1 from bottom to top, the tower above the porcelain layers of balls 1
Horizontal installing pipe is equipped in shell 20, the installation inner coaxial tube is equipped with lamp irradiation source 18, be located at lamp irradiation source 18 and
The inside of the tower shell 20 between the inlet diffuser 111 is equipped with distributor 21, sets in the upper catalyst layer 151
There is upper layer cooling device 22, the upper layer cooling device 22 is mounted on the inside of the tower shell 20, the upper catalyst layer
151 bottom is successively arranged porcelain layers of balls 3 143 and porcelain layers of balls 4 144 from top to bottom, and the bottom of the porcelain layers of balls 4 144, which is equipped with, urges
Agent support device 16, the catalyst support device 16 are mounted on the inner wall of the tower shell 20 and are located at the people
The top in hole 27, the side wall being in contact on the tower shell 20 with the lower part of the upper catalyst layer 151 are equipped with opening inclination
Downward overlying catalyst discharge duct 4, the feed end of the overlying catalyst discharge duct 4 sequentially pass through the tower shell 20
Side wall, the porcelain layers of balls 3 143 are connected with the upper catalyst layer 151, and the top of the lower catalyst layer 152 is equipped with porcelain ball
The top of layer 5 145, the porcelain layers of balls 5 145 is equipped with redistributor 13, and the redistributor 13 is mounted on the tower shell
20 inside and the lower section for being located at the catalyst support device 16, divide positioned at the catalyst support device 16 with described again
The inner horizontal of the tower shell 20 between orchestration 13 is equipped with air blowing device 1, is located at one 12 top of air blowing device
The tower shell 20 side wall on be equipped with cold hydrogen mouth 5, the cold hydrogen mouth 5 is located at the lower section of the pressure transmitter mouth 6, institute
The lower part for stating lower catalyst layer 152 is equipped with air blowing device 2 23, and the air blowing device 2 23 is mounted on the tower shell 20
On inner wall, be successively arranged from top to bottom between the air blowing device 2 23 and the bottom of the tower shell 20 porcelain layers of balls 6 146,
The bottom of porcelain layers of balls 7 147 and porcelain layers of balls 8 148, the tower shell 20 is equipped with discharge nozzle 8, the feed end of the discharge nozzle 8
Sequentially pass through the skirt 19, the bottom interior wall of the tower shell 20 is connected with exit collector 2 112, the exit collector
2 112 are located at the bottom in the tower shell 20, and the bottom outside of the tower shell 20 is equipped with lower catalyst agent discharge duct
9, the lower catalyst agent discharge duct 9 is located at the side setting of the discharge nozzle 8, the charging of the lower catalyst agent discharge duct 9
End sequentially passes through bottom, the porcelain layers of balls 8 148, the porcelain layers of balls 7 147, the porcelain layers of balls six of the tower shell 20
146 are connected with the lower catalyst layer 152.
The inspection access hole 10 uses the form of flanges with neck butt welding, and face type is ring joint face, pressure rating
For 18.0MPa.
The redistributor 13 uses throttle type redistributor.
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 4 144, described
Porcelain layers of balls 5 145, the porcelain layers of balls 6 146, the porcelain layers of balls 7 147, the porcelain bulb diameter in the porcelain layers of balls 8 148 are respectively
Φ13mm、Φ6mm、Φ3mm、Φ6mm、Φ6mm、Φ3mm、Φ6mm、Φ13mm。
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 5 145, described
The thickness of porcelain layers of balls 6 146 is 150mm, and the thickness of the porcelain layers of balls 4 144 and the porcelain layers of balls 7 147 is respectively
1210mm、1150mm。
The air blowing device 1 and the air blowing device 2 23 are all made of quencher.
The catalyst support device 16 is catalyst supporting plate.
The upper layer cooling device 22 is cooling using tubulation.
The mixture of catalyst and porcelain ball is filled in the upper catalyst layer 151 and the lower catalyst layer 152.
Embodiment 3
A kind of hydrogenator device for hydrogenation reaction, including tower shell 20, which is characterized in that the tower shell
The stack shell of body 20 is in hollow cylinder structure setting, and the bottom of the tower shell 20 is fixed to be equipped with skirt 19, the skirt 19
Bottom surrounding installed on the ground by foundation bolt, the skirt 19, which is equipped with, checks access hole 10, on the skirt 19
Fireprotection layer, the tower are laid by installation 17 tie wire net of orifice plate in the outer surface of welding installation orifice plate 17, the skirt 19
Manhole 1 is equipped at the upper cover on 20 top of shell, the top of the tower shell 20 is equipped with feed pipe 1, the feed pipe 1
Feed end is connected with extraneous storage equipment, and the feed pipe 1 is located at the side setting of the manhole 1, and the feed pipe 1 goes out
Material end is connected to the inside of the tower shell 20, and the discharge end of the feed pipe 1 is equipped with inlet diffuser 111, the entrance
Diffuser 111 is located at the inner upper of the tower shell 20, and the upper section and lower section inside the tower shell 20 are respectively equipped with
Upper catalyst layer 151 and lower catalyst layer 152, be equipped on the side wall of the tower shell 20 from top to bottom it is several with it is described on urge
The thermometer temperature-measuring port 3 that agent layer 151, the lower catalyst layer 152 are in contact is located at the upper catalyst layer 151 and described
Manhole 27 and pressure transmitter mouth 6, the manhole are equipped on the side wall of the tower shell 20 between lower catalyst layer 152
27 and the pressure transmitter mouth 6 be located at the outer wall two sides of the tower shell 20, the top of the upper catalyst layer 151
End is successively arranged porcelain layers of balls 2 142 and porcelain layers of balls 1 from bottom to top, the tower above the porcelain layers of balls 1
Horizontal installing pipe is equipped in shell 20, the installation inner coaxial tube is equipped with lamp irradiation source 18, be located at lamp irradiation source 18 and
The inside of the tower shell 20 between the inlet diffuser 111 is equipped with distributor 21, sets in the upper catalyst layer 151
There is upper layer cooling device 22, the upper layer cooling device 22 is mounted on the inside of the tower shell 20, the upper catalyst layer
151 bottom is successively arranged porcelain layers of balls 3 143 and porcelain layers of balls 4 144 from top to bottom, and the bottom of the porcelain layers of balls 4 144, which is equipped with, urges
Agent support device 16, the catalyst support device 16 are mounted on the inner wall of the tower shell 20 and are located at the people
The top in hole 27, the side wall being in contact on the tower shell 20 with the lower part of the upper catalyst layer 151 are equipped with opening inclination
Downward overlying catalyst discharge duct 4, the feed end of the overlying catalyst discharge duct 4 sequentially pass through the tower shell 20
Side wall, the porcelain layers of balls 3 143 are connected with the upper catalyst layer 151, and the top of the lower catalyst layer 152 is equipped with porcelain ball
The top of layer 5 145, the porcelain layers of balls 5 145 is equipped with redistributor 13, and the redistributor 13 is mounted on the tower shell
20 inside and the lower section for being located at the catalyst support device 16, divide positioned at the catalyst support device 16 with described again
The inner horizontal of the tower shell 20 between orchestration 13 is equipped with air blowing device 1, is located at one 12 top of air blowing device
The tower shell 20 side wall on be equipped with cold hydrogen mouth 5, the cold hydrogen mouth 5 is located at the lower section of the pressure transmitter mouth 6, institute
The lower part for stating lower catalyst layer 152 is equipped with air blowing device 2 23, and the air blowing device 2 23 is mounted on the tower shell 20
On inner wall, be successively arranged from top to bottom between the air blowing device 2 23 and the bottom of the tower shell 20 porcelain layers of balls 6 146,
The bottom of porcelain layers of balls 7 147 and porcelain layers of balls 8 148, the tower shell 20 is equipped with discharge nozzle 8, the feed end of the discharge nozzle 8
Sequentially pass through the skirt 19, the bottom interior wall of the tower shell 20 is connected with exit collector 2 112, the exit collector
2 112 are located at the bottom in the tower shell 20, and the bottom outside of the tower shell 20 is equipped with lower catalyst agent discharge duct
9, the lower catalyst agent discharge duct 9 is located at the side setting of the discharge nozzle 8, the charging of the lower catalyst agent discharge duct 9
End sequentially passes through bottom, the porcelain layers of balls 8 148, the porcelain layers of balls 7 147, the porcelain layers of balls six of the tower shell 20
146 are connected with the lower catalyst layer 152.
The inspection access hole 10 uses the form of flanges with neck butt welding, and face type is ring joint face, pressure rating
For 25.0MPa.
The redistributor 13 uses throttle type redistributor.
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 4 144, described
Porcelain layers of balls 5 145, the porcelain layers of balls 6 146, the porcelain layers of balls 7 147, the porcelain bulb diameter in the porcelain layers of balls 8 148 are respectively
Φ13mm、Φ6mm、Φ3mm、Φ6mm、Φ6mm、Φ3mm、Φ6mm、Φ13mm。
It is the porcelain layers of balls 1, the porcelain layers of balls 2 142, the porcelain layers of balls 3 143, the porcelain layers of balls 5 145, described
The thickness of porcelain layers of balls 6 146 is 150mm, and the thickness of the porcelain layers of balls 4 144 and the porcelain layers of balls 7 147 is respectively
1210mm、1150mm。
The air blowing device 1 and the air blowing device 2 23 are all made of quencher.
The catalyst support device 16 is catalyst grid.
The upper layer cooling device 22 is cooling using coil pipe.
The mixture of catalyst and porcelain ball is filled in the upper catalyst layer 151 and the lower catalyst layer 152.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the various improvement that the inventive concept and technical scheme of the present invention carry out, or not improved directly apply to other fields
It closes, it is within the scope of the present invention.
Claims (9)
1. a kind of hydrogenator device for hydrogenation reaction, including tower shell (20), which is characterized in that the tower shell
The stack shell of body (20) is in hollow cylinder structure setting, and the bottom of the tower shell (20) is fixed to be equipped with skirt (19), described
The bottom surrounding of skirt (19) is installed on the ground by foundation bolt, and the skirt (19), which is equipped with, checks access hole (10),
The outer surface of welding installation orifice plate (17) on the skirt (19), the skirt (19) passes through installation orifice plate (17) tie wire net
Fireprotection layer is laid, is equipped with manhole one (2), the top of the tower shell (20) at the upper cover on tower shell (20) top
Equipped with feed pipe (1), the feed end of the feed pipe (1) is connected with extraneous storage equipment, and the feed pipe (1) is located at the people
The side in hole one (2) is arranged, and the discharge end of the feed pipe (1) is connected to the inside of the tower shell (20), the charging
The discharge end for managing (1) is equipped with inlet diffuser (111), and the inlet diffuser (111) is located at the interior of the tower shell (20)
Above portion, the internal upper section of the tower shell (20) and lower section are respectively equipped with catalyst layer (151) and lower catalyst layer
(152), be equipped with from top to bottom on the side wall of the tower shell (20) it is several with the upper catalyst layer (151), it is described under urge
The thermometer temperature-measuring port (3) that agent layer (152) is in contact is located at the upper catalyst layer (151) and the lower catalyst layer
(152) manhole two (7) and pressure transmitter mouth (6), the manhole two are equipped on the side wall of the tower shell (20) between
(7) and the pressure transmitter mouth (6) is located at the outer wall two sides of the tower shell (20), the upper catalyst layer
(151) top is successively arranged porcelain layers of balls two (142) and porcelain layers of balls one (141) from bottom to top, is located at the porcelain layers of balls one (141)
Horizontal installing pipe is equipped in the tower shell (20) of top, the installation inner coaxial tube is equipped with lamp irradiation source (18), position
The inside of the tower shell (20) between lamp irradiation source (18) and the inlet diffuser (111) is equipped with distributor
(21), upper layer cooling device (22) are equipped in the upper catalyst layer (151), the upper layer cooling device (22) is mounted on described
The bottom of the inside of tower shell (20), the upper catalyst layer (151) is successively arranged porcelain layers of balls three (143) and porcelain from top to bottom
The bottom of layers of balls four (144), the porcelain layers of balls four (144) is equipped with catalyst support device (16), the catalyst support device
(16) it is mounted on the inner wall of the tower shell (20) and is located at the top of the manhole two (7), the tower shell
(20) side wall being in contact on the lower part of the upper catalyst layer (151) is equipped with the overlying catalyst discharging of opening diagonally downward
It manages (4), the feed end of the overlying catalyst discharge duct (4) sequentially passes through the side wall of the tower shell (20), the porcelain ball
Three (143) of layer are connected with the upper catalyst layer (151), and the top of the lower catalyst layer (152) is equipped with porcelain layers of balls five
(145), the top of the porcelain layers of balls five (145) is equipped with redistributor (13), and the redistributor (13) is mounted on the tower
The inside of shell (20) and the lower section for being located at the catalyst support device (16) are located at the catalyst support device (16)
The inner horizontal of the tower shell (20) between the redistributor (13) is equipped with air blowing device one (12), is located at described
Cold hydrogen mouth (5) is equipped on the side wall of the tower shell (20) above air blowing device one (12), the cold hydrogen mouth (5) is located at institute
The lower section of pressure transmitter mouth (6) is stated, the lower part of the lower catalyst layer (152) is equipped with air blowing device two (23), the air-blowing
Device two (23) is mounted on the inner wall of the tower shell (20), the air blowing device two (23) and the tower shell (20)
Bottom between be successively arranged porcelain layers of balls six (146), porcelain layers of balls seven (147) and porcelain layers of balls eight (148), the tower from top to bottom
The bottom of shell (20) is equipped with discharge nozzle (8), and the feed end of the discharge nozzle (8) sequentially passes through the skirt (19), the tower
The bottom interior wall of device shell (20) is connected with exit collector two (112), and the exit collector two (112) is located at the tower shell
The bottom outside of bottom in body (20), the tower shell (20) is equipped with lower catalyst agent discharge duct (9), the lower catalyst
Agent discharge duct (9) is located at the side setting of the discharge nozzle (8), and the feed end of the lower catalyst agent discharge duct (9) successively passes through
Wear bottom, the porcelain layers of balls eight (148), the porcelain layers of balls seven (147), the porcelain layers of balls six of the tower shell (20)
(146) it is connected with the lower catalyst layer (152).
2. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the inspection
Access hole (10) uses the form of flanges with neck butt welding, and face type is ring joint face, and pressure rating is 6.3~25.0MPa.
3. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that described to divide again
Orchestration (13) includes but is not limited to throttle type redistributor.
4. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the porcelain ball
Layer one (141), the porcelain layers of balls two (142), the porcelain layers of balls three (143), the porcelain layers of balls four (144), the porcelain layers of balls five
(145), the porcelain layers of balls six (146), the porcelain layers of balls seven (147), the porcelain bulb diameter in the porcelain layers of balls eight (148) are respectively
Φ13mm、Φ6mm、Φ3mm、Φ6mm、Φ6mm、Φ3mm、Φ6mm、Φ13mm。
5. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the porcelain ball
Layer one (141), the porcelain layers of balls two (142), the porcelain layers of balls three (143), the porcelain layers of balls five (145), the porcelain layers of balls six
(146) thickness is 150mm, the thickness of the porcelain layers of balls four (144) and the porcelain layers of balls seven (147) be respectively 1210mm,
1150mm。
6. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the air-blowing
Device one (12) and the air blowing device two (23) are all made of quencher.
7. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the catalysis
Agent support device (16) includes but is not limited to catalyst grid, catalyst supporting plate.
8. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that the upper layer
Cooling device (22) includes but is not limited to coil pipe, tubulation cooling.
9. a kind of hydrogenator device for hydrogenation reaction according to claim 1, which is characterized in that urged on described
It include but is not limited to the mixing of catalyst filling, catalyst and porcelain ball in agent layer (151) and the lower catalyst layer (152)
Object.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811387203.5A CN109304133B (en) | 2018-11-21 | 2018-11-21 | Hydrogenation reactor device for hydrogenation reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811387203.5A CN109304133B (en) | 2018-11-21 | 2018-11-21 | Hydrogenation reactor device for hydrogenation reaction |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109304133A true CN109304133A (en) | 2019-02-05 |
| CN109304133B CN109304133B (en) | 2024-03-05 |
Family
ID=65222147
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811387203.5A Active CN109304133B (en) | 2018-11-21 | 2018-11-21 | Hydrogenation reactor device for hydrogenation reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109304133B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110586010A (en) * | 2019-10-29 | 2019-12-20 | 中国石油化工股份有限公司 | Temperature detection system and hydrogenation reactor control method |
| CN111253266A (en) * | 2020-03-16 | 2020-06-09 | 安庆市鑫富化工有限责任公司 | Refining process of 3-aminopropanol |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2125484C1 (en) * | 1996-09-10 | 1999-01-27 | Акционерное общество "Ново-Уфимский нефтеперерабатывающий завод" | Reactor for gas-liquid mixtures |
| CN1853767A (en) * | 2001-06-26 | 2006-11-01 | 株式会社日本触媒 | Reactor filled with solid particles and gas phase catalytic oxidation using the same |
| CN205412952U (en) * | 2016-03-18 | 2016-08-03 | 西北大学 | Coal tar hydrogenation ware |
| CN106166469A (en) * | 2016-08-31 | 2016-11-30 | 东营市俊源石油技术开发有限公司 | A kind of environmental protection hydrocarbon solvent low-voltage hydrogenation takes off arylation reaction device and catalyst filling method |
| CN107815331A (en) * | 2017-12-13 | 2018-03-20 | 中冶焦耐(大连)工程技术有限公司 | A kind of organic sulfur removal reactor |
-
2018
- 2018-11-21 CN CN201811387203.5A patent/CN109304133B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2125484C1 (en) * | 1996-09-10 | 1999-01-27 | Акционерное общество "Ново-Уфимский нефтеперерабатывающий завод" | Reactor for gas-liquid mixtures |
| CN1853767A (en) * | 2001-06-26 | 2006-11-01 | 株式会社日本触媒 | Reactor filled with solid particles and gas phase catalytic oxidation using the same |
| CN205412952U (en) * | 2016-03-18 | 2016-08-03 | 西北大学 | Coal tar hydrogenation ware |
| CN106166469A (en) * | 2016-08-31 | 2016-11-30 | 东营市俊源石油技术开发有限公司 | A kind of environmental protection hydrocarbon solvent low-voltage hydrogenation takes off arylation reaction device and catalyst filling method |
| CN107815331A (en) * | 2017-12-13 | 2018-03-20 | 中冶焦耐(大连)工程技术有限公司 | A kind of organic sulfur removal reactor |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110586010A (en) * | 2019-10-29 | 2019-12-20 | 中国石油化工股份有限公司 | Temperature detection system and hydrogenation reactor control method |
| CN111253266A (en) * | 2020-03-16 | 2020-06-09 | 安庆市鑫富化工有限责任公司 | Refining process of 3-aminopropanol |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109304133B (en) | 2024-03-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103030206B (en) | Supercritical water treatment device and method | |
| CN102274706A (en) | Reactor-exchanger with bayonet tubes and fire tubes suspended from the upper vault of the reactor | |
| CN109304133A (en) | A kind of hydrogenation reactor device for hydrogenation reaction | |
| CN109896501A (en) | A kind of reforming hydrogen production device and the method using the device hydrogen manufacturing | |
| CN112452259A (en) | Heat exchange type ammonia decomposition reactor | |
| CN201519571U (en) | Shell and tube reactor for producing chloroethylene by utilizing acetylene method | |
| CN209465003U (en) | A kind of hydrogenator device for carbon dioxide hydrogenation reaction | |
| CN112546975A (en) | Fluidized bed reactor capable of recycling materials and producing hydrophobic white carbon black | |
| CN102658067B (en) | Ring-shaped fluidized bed reactor | |
| CN206935159U (en) | A kind of efficiently acetylene pyrolysis furnace blender | |
| CN214261820U (en) | Fluidized bed reactor for efficiently producing hydrophobic white carbon black | |
| CN214681633U (en) | Fluidized bed reactor capable of recycling materials and producing hydrophobic white carbon black | |
| CN214032684U (en) | Concurrent heating system device | |
| CN201052457Y (en) | Novel inner circulation slurry-bed reactor | |
| CN205761058U (en) | Eddy flow broken streaming cold hydrogen box | |
| CN105749850B (en) | A kind of special purpose reactor of controlled syntheses parachlorotoluene | |
| CN207440031U (en) | A kind of catalyst test apparatus | |
| CN105694981B (en) | A gasifier nozzle and gasifier | |
| CN209848902U (en) | Energy-saving thermal chlorination reaction device for methane chloride | |
| CN209222076U (en) | Hydrogenator | |
| CN206109338U (en) | Coke oven gas methanation device with membrane separator | |
| CN222358472U (en) | A preheating radial methanol synthesis reactor | |
| CN206466974U (en) | A kind of copper powder fluid bed | |
| CN222401400U (en) | Gas distributor and radial fixed bed reactor | |
| CN207347524U (en) | A kind of biomass gasifying furnace water cooling equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20241203 Address after: 408400 Group 3, Dayan Neighborhood Committee, Shuijiang Town, Nanchuan District, Chongqing (Smart Industry Training Center) Patentee after: Chongqing Runyu New Energy Co.,Ltd. Country or region after: China Address before: Room 029, Room 1912, Building A, Creative Center, Binhai Private Economic Growth Demonstration Base, Jinnan District, Tianjin, 300350 Patentee before: ARSD (TIANJIN) ENERGY TECHNOLOGY CO.,LTD. Country or region before: China |
|
| TR01 | Transfer of patent right |