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CN109294739A - The extracting mode of rose extracting solution - Google Patents

The extracting mode of rose extracting solution Download PDF

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Publication number
CN109294739A
CN109294739A CN201710620907.1A CN201710620907A CN109294739A CN 109294739 A CN109294739 A CN 109294739A CN 201710620907 A CN201710620907 A CN 201710620907A CN 109294739 A CN109294739 A CN 109294739A
Authority
CN
China
Prior art keywords
rose
extracting solution
extracting
nanofiltration
mode
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710620907.1A
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Chinese (zh)
Inventor
丘健
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710620907.1A priority Critical patent/CN109294739A/en
Publication of CN109294739A publication Critical patent/CN109294739A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Seasonings (AREA)

Abstract

The invention discloses a kind of extracting modes of rose extracting solution, it is characterized in that, specifically comprising the following steps: that the collecting, sort of supplementary material, fixation/water-removing, low temperature sub-critical extraction, condensation collects and separates and collects, filters, extracting solution store, inspected periodically, nanofiltration degerming, metering is filling, examine, storage is sold;Wherein, it sorting, inspecting periodically, should reject rejected product in nanofiltration degerming and checkout procedure;Filter residue should be carried out during the filtration process to scrap.The present invention chooses polyphyll red rose, and 100% is extracted from the moisture in the fresh petal of rose, any moisture is not added, and do not conform to preservative without any addition in production process, using nanofiltration mode degerming;It is not only hygienic, and preparation process passes through stringent control, removes all security risks, can directly eat, and for making full use of for rose, the economic benefit for improving rose processing enterprise provides a kind of new technology.

Description

The extracting mode of rose extracting solution
Technical field
The present invention relates to rose technical fields, the more particularly to extracting mode of rose extracting solution.
Background technique
Extracting the most common method of Rosa Damascana at present is steam distillation, is wanted using the Rosa Damascana that this method is extracted It is distilled by high-temperature steam, high temperature can destroy the fragrance component of some thermal sensitivity in Rosa Damascana, while can generate some boilings Peculiar smell reduces essential oil quality.The Rosa Damascana of China's production is just as poor quality and fail to occupy in the international market always One seat.
Therefore, how to provide a kind of has the characteristics that safety and sanitation, aroma of pure, 100% no added rose extracting solution The problem of extracting mode is those skilled in the art's urgent need to resolve.
Summary of the invention
In view of this, having the characteristics that safety and sanitation, aroma of pure, 100% no added rose the present invention provides a kind of The extracting mode of extracting solution.
To achieve the above object, the invention provides the following technical scheme:
The extracting mode of rose extracting solution, which is characterized in that specifically comprise the following steps: collecting, sort, being solid for supplementary material Color/water-removing, low temperature sub-critical extraction, condensation collects and separates and collects, filters, extracting solution is stored, inspected periodically, nanofiltration removes Bacterium, metering is filling, examines, storage sale;Wherein, it sorting, inspecting periodically, should in nanofiltration degerming and checkout procedure Reject rejected product;Filter residue should be carried out during the filtration process to scrap.
Preferably, in a kind of above-mentioned extracting mode of rose extracting solution, the raw material chooses polyphyll red rose, and 100% The moisture being extracted from the fresh petal of rose, does not add any moisture, and is free of preservative without any addition in production process, Using nanofiltration mode degerming.
Preferably, in a kind of above-mentioned extracting mode of rose extracting solution, the pH value of the extracting solution is 5.0-7.0 in weak Acidity, half peak value of the oxygen of hydrone is about 90Hz or less in the extracting solution.
Preferably, in a kind of above-mentioned extracting mode of rose extracting solution, in the extracting solution containing 0.4% or more rose Rare essential oil composition, the Rosa Damascana composition include citronellol, geraniol, methyl eugenol, eugenol, β benzyl carbinol, rose Ether, nerol etc. other.
It can be seen via above technical scheme that compared with prior art, the present disclosure provides a kind of rose extracting solutions Extracting mode, which is characterized in that specifically comprise the following steps: that the collecting, sort of supplementary material, fixation/water-removing, low temperature are subcritical Extract, condensation collect and separate and collect, filter, extracting solution store, is inspected periodically, nanofiltration degerming, metering it is filling, inspection, Storage sale;Wherein, it sorting, inspecting periodically, should reject rejected product in nanofiltration degerming and checkout procedure;In mistake Filter residue should be carried out during filter to scrap.The present invention chooses polyphyll red rose, and 100% is extracted from the moisture in the fresh petal of rose, Any moisture is not added, and preservative is free of, using nanofiltration mode degerming without any addition in production process;Not only defend It is raw, and preparation process passes through stringent control, removes all security risks, can directly eat, and is making full use of for rose, The economic benefit for improving rose processing enterprise provides a kind of new technology.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this The embodiment of invention for those of ordinary skill in the art without creative efforts, can also basis The attached drawing of offer obtains other attached drawings.
Fig. 1 attached drawing is that rose extracting solution of the invention extracts flow chart.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Have the characteristics that safety and sanitation, aroma of pure, 100% no added rose extraction the embodiment of the invention discloses a kind of The extracting mode of liquid.
Attached drawing 1 is please referred to, is a kind of extracting mode of rose extracting solution disclosed by the invention, specifically includes:
Following steps: supplementary material is collected, is sorted, fixation/water-removing, low temperature sub-critical extraction, condensing to collect and separate and receive Collection, filtering, extracting solution is stored, is inspected periodically, nanofiltration degerming, metering is filling, is examined, storage sale;Wherein, sorting, It inspects periodically, should reject rejected product in nanofiltration degerming and checkout procedure;Filter residue report should be carried out during the filtration process It is useless.
The invention discloses a kind of extracting modes of rose extracting solution, which is characterized in that specifically comprises the following steps: former auxiliary Material is collected, is sorted, fixation/water-removing, low temperature sub-critical extraction, condensing and collect and separate and collect, filter, extracting solution storage, determine Phase inspection, nanofiltration degerming, metering is filling, examines, storage sale;Wherein, sort, inspect periodically, nanofiltration degerming With rejected product should be rejected in checkout procedure;Filter residue should be carried out during the filtration process to scrap.The present invention chooses the red rose of polyphyll Rare, 100% is extracted from the moisture in the fresh petal of rose, does not add any moisture, and be free of in production process without any addition Preservative, using nanofiltration mode degerming;It is not only hygienic, and preparation process passes through stringent control, and it is hidden to remove all safety Suffer from, can directly eat, made full use of for rose, improve rose processing enterprise economic benefit provide it is a kind of new Technology.
In order to further optimize the above technical scheme, raw material chooses polyphyll red rose, and 100% is extracted from the fresh petal of rose In moisture, do not add any moisture, and without any addition in production process, be free of preservative, remove using nanofiltration mode Bacterium.
In order to further optimize the above technical scheme, the pH value of extracting solution is that 5.0-7.0 is weakly acidic, in the extracting solution Half peak value of the oxygen of hydrone is about 90Hz or less.
In order to further optimize the above technical scheme, extracting solution can prepare Rosa Damascana, contain 0.4% or more in extracting solution Rosa Damascana composition, the Rosa Damascana composition include citronellol, geraniol, methyl eugenol, eugenol, β benzyl carbinol, Rose oxide, nerol etc. other.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with other The difference of embodiment, the same or similar parts in each embodiment may refer to each other.For device disclosed in embodiment For, since it is corresponded to the methods disclosed in the examples, so being described relatively simple, related place is said referring to method part It is bright.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one The widest scope of cause.

Claims (4)

1. the extracting mode of rose extracting solution, which is characterized in that specifically comprise the following steps: collecting, sort, being solid for supplementary material Color/water-removing, low temperature sub-critical extraction, condensation collects and separates and collects, filters, extracting solution is stored, inspected periodically, nanofiltration removes Bacterium, metering is filling, examines, storage sale;Wherein, it sorting, inspecting periodically, should in nanofiltration degerming and checkout procedure Reject rejected product;Filter residue should be carried out during the filtration process to scrap.
2. the extracting mode of rose extracting solution according to claim 1, which is characterized in that the raw material chooses the red rose of polyphyll Rare, 100% is extracted from the moisture in the fresh petal of rose, does not add any moisture, and be free of in production process without any addition Preservative, using nanofiltration mode degerming.
3. the extracting mode of rose extracting solution according to claim 1, which is characterized in that the pH value of the extracting solution is 5.0-7.0 is weakly acidic, and half peak value of the oxygen of hydrone is about 90Hz or less in the extracting solution.
4. the extracting mode of rose extracting solution according to claim 1, which is characterized in that contain in the extracting solution 0.4% or more Rosa Damascana composition, the Rosa Damascana composition include citronellol, geraniol, methyl eugenol, cloves Phenol, β benzyl carbinol, rose oxide, nerol etc. other.
CN201710620907.1A 2017-07-25 2017-07-25 The extracting mode of rose extracting solution Pending CN109294739A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710620907.1A CN109294739A (en) 2017-07-25 2017-07-25 The extracting mode of rose extracting solution

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Application Number Priority Date Filing Date Title
CN201710620907.1A CN109294739A (en) 2017-07-25 2017-07-25 The extracting mode of rose extracting solution

Publications (1)

Publication Number Publication Date
CN109294739A true CN109294739A (en) 2019-02-01

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110585074A (en) * 2019-10-22 2019-12-20 中国科学院兰州化学物理研究所 Application of rose essential oil balm in cosmetics

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102895152A (en) * 2012-10-29 2013-01-30 广州栋方日化有限公司 Preparation method for rose extract and cosmetic
CN103614240A (en) * 2013-12-09 2014-03-05 山东金硕生物科技股份有限公司 Production method of Abelmoschus manihot essential oil
CN104543658A (en) * 2013-10-18 2015-04-29 上海爱普植物科技有限公司 Method for preparing natural rose syrup
CN105482897A (en) * 2016-01-27 2016-04-13 江苏耐雀生物工程技术有限公司 Microwave-assisted subcritical essential oil extracting method
CN106190554A (en) * 2016-07-22 2016-12-07 许备占 The preparation method of Wild cottonrose hibiscus extract oil
CN106497678A (en) * 2016-11-18 2017-03-15 河南教育学院 A kind of method that molecular sieve extractant extracts Rosa Damascana
CN106916628A (en) * 2017-01-10 2017-07-04 深圳市大百汇技术有限公司 Bitter citrus immature flower essential oil, its preparation method and application

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102895152A (en) * 2012-10-29 2013-01-30 广州栋方日化有限公司 Preparation method for rose extract and cosmetic
CN104543658A (en) * 2013-10-18 2015-04-29 上海爱普植物科技有限公司 Method for preparing natural rose syrup
CN103614240A (en) * 2013-12-09 2014-03-05 山东金硕生物科技股份有限公司 Production method of Abelmoschus manihot essential oil
CN105482897A (en) * 2016-01-27 2016-04-13 江苏耐雀生物工程技术有限公司 Microwave-assisted subcritical essential oil extracting method
CN106190554A (en) * 2016-07-22 2016-12-07 许备占 The preparation method of Wild cottonrose hibiscus extract oil
CN106497678A (en) * 2016-11-18 2017-03-15 河南教育学院 A kind of method that molecular sieve extractant extracts Rosa Damascana
CN106916628A (en) * 2017-01-10 2017-07-04 深圳市大百汇技术有限公司 Bitter citrus immature flower essential oil, its preparation method and application

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
徐怀德,王云阳主编: "《食品杀菌新技术》", 31 July 2005, 科学技术文献出版社 *
王兴涌主编: "《应用化学专业实验》", 30 June 2009, 中国矿业大学出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110585074A (en) * 2019-10-22 2019-12-20 中国科学院兰州化学物理研究所 Application of rose essential oil balm in cosmetics

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Application publication date: 20190201