CN109207258A - A kind of flavouring essence for tobacco modulator approach and its application with medicinal herbs, baking note - Google Patents
A kind of flavouring essence for tobacco modulator approach and its application with medicinal herbs, baking note Download PDFInfo
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- CN109207258A CN109207258A CN201710541007.8A CN201710541007A CN109207258A CN 109207258 A CN109207258 A CN 109207258A CN 201710541007 A CN201710541007 A CN 201710541007A CN 109207258 A CN109207258 A CN 109207258A
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 40
- 235000008216 herbs Nutrition 0.000 title claims abstract description 27
- 241000208125 Nicotiana Species 0.000 title claims description 39
- 239000000284 extract Substances 0.000 claims abstract description 57
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 53
- 235000009754 Vitis X bourquina Nutrition 0.000 claims abstract description 29
- 235000012333 Vitis X labruscana Nutrition 0.000 claims abstract description 29
- 235000014787 Vitis vinifera Nutrition 0.000 claims abstract description 29
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 241000208140 Acer Species 0.000 claims abstract description 12
- RHDGNLCLDBVESU-UHFFFAOYSA-N but-3-en-4-olide Chemical compound O=C1CC=CO1 RHDGNLCLDBVESU-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000001484 Trigonella foenum graecum Nutrition 0.000 claims abstract description 11
- 244000250129 Trigonella foenum graecum Species 0.000 claims abstract description 11
- 235000001019 trigonella foenum-graecum Nutrition 0.000 claims abstract description 11
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940093503 ethyl maltol Drugs 0.000 claims abstract description 9
- 239000013049 sediment Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 239000000376 reactant Substances 0.000 claims abstract 2
- 241000219095 Vitis Species 0.000 claims description 28
- 239000002994 raw material Substances 0.000 claims description 22
- 238000006243 chemical reaction Methods 0.000 claims description 19
- 235000015203 fruit juice Nutrition 0.000 claims description 19
- 238000002360 preparation method Methods 0.000 claims description 14
- 150000002596 lactones Chemical class 0.000 claims description 11
- 239000004567 concrete Substances 0.000 claims description 10
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims description 7
- 229930007850 β-damascenone Natural products 0.000 claims description 7
- 229930006000 Sucrose Natural products 0.000 claims description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 6
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 230000003068 static effect Effects 0.000 claims description 6
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 claims description 5
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 claims description 5
- 239000000919 ceramic Substances 0.000 claims description 5
- 235000019987 cider Nutrition 0.000 claims description 5
- 230000008030 elimination Effects 0.000 claims description 5
- 238000003379 elimination reaction Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 239000012528 membrane Substances 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 239000004474 valine Substances 0.000 claims description 5
- 229940119429 cocoa extract Drugs 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 238000003860 storage Methods 0.000 claims description 3
- 241000219094 Vitaceae Species 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims description 2
- 239000012153 distilled water Substances 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 238000011010 flushing procedure Methods 0.000 claims description 2
- 235000019674 grape juice Nutrition 0.000 claims description 2
- 235000021021 grapes Nutrition 0.000 claims description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 244000299461 Theobroma cacao Species 0.000 claims 1
- 235000009470 Theobroma cacao Nutrition 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- -1 ethyl malt Chemical compound 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 15
- 239000000796 flavoring agent Substances 0.000 abstract description 8
- 235000019634 flavors Nutrition 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 8
- 230000000391 smoking effect Effects 0.000 abstract description 5
- 244000061176 Nicotiana tabacum Species 0.000 abstract 1
- 240000006365 Vitis vinifera Species 0.000 abstract 1
- 235000020765 fenugreek extract Nutrition 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 abstract 1
- 230000000284 resting effect Effects 0.000 abstract 1
- 239000002304 perfume Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 230000035943 smell Effects 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 3
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 150000002561 ketenes Chemical class 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000033764 rhythmic process Effects 0.000 description 2
- 206010042772 syncope Diseases 0.000 description 2
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 208000024756 faint Diseases 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 229940043353 maltol Drugs 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000008771 sex reversal Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
本发明提供一种具有药草、烘烤香韵的加料香精及应用。所述香精是先将果汁美拉德反应物、咖啡浸膏、葫芦巴浸膏、枫槭浸膏、麦芽浸膏、烟用葡萄生物提取物依次按照顺序添加到丙二醇中，混合搅拌均匀，配制成A组分；再将呋喃酮、3％葫芦巴内脂、乙基麦芽酚、突厥烯酮按顺序依次添加到95％的酒精中混合搅拌均匀，配制成B组分；最后将A组分和B组分添加到纯净水搅拌均匀，后静止24‑48小时后，过80‑100目筛网滤去沉渣得到。本发明调配的香精具有强烈药草香、烘烤香香韵嗅香，将其应用于卷烟中，烟支嗅香具有明显的药草、烘烤香韵，且卷烟在抽吸过程中有明显的药草、烘烤香，并提高香气丰满度和卷烟的舒适性。The present invention provides an added flavor with medicinal herbs and baking aroma and application thereof. The essence is to firstly add juice Maillard reactant, coffee extract, fenugreek extract, maple maple extract, malt extract, and tobacco grape biological extract to propylene glycol in sequence, mix and stir evenly, and prepare. Component A; then add furanone, 3% fenugreek, ethyl maltol, and tuclenone to 95% alcohol in sequence, mix well, and prepare component B; finally, add component A Add component B and component B to pure water and stir evenly, and after resting for 24-48 hours, filter the sediment through an 80-100 mesh screen to obtain it. The essence prepared by the invention has strong herbal fragrance, roasted fragrance and smelling fragrance. When it is applied to cigarettes, the cigarette smelling fragrance has obvious medicinal herbs and roasted fragrance, and the cigarette has obvious medicinal herbs in the smoking process. , roast aroma, and improve aroma fullness and cigarette comfort.
Description
Technical field
The present invention relates to technical field of cigarette flavors, specifically a kind of cigarette charging with medicinal herbs, baking note
Essence modulator approach and its application.
Background technique
Flavors and fragrances can be played in cigarette improve tobacco physical and chemical performance, adjust cigarette acid-base balance degree,
It assigns the unique taste of cigarette and style effect, improve the aroma quality of cigarette and the effect of perfume quantity, and tobacco can be improved
Fragrance and jealous, the miscellaneous gas of cover, mitigation stimulation, and realize product quality differentiation, stablize cigarette smoking quality, for cigarette
Style and quality responses have a major impact.With State Bureau " blending engineering " implementation, flavors and fragrances is in Chinese-style cigarette core
Heart technology, especially the effect in terms of constructing the unique taste of cigarette and style will be more and more important.With cigarette consumption
Demand gradually from type, enjoying type is met to novel sex reversal, demand to cigarette by the past it is single suck hobby, gradually form
A variety of demands such as healthy, safe and environment-friendly, consumer not only focus on the comfort and pleasant sexual experience of cigarette smoking, and with volume
The raising of cigarette consumption structure, consumer is in the novelty of cigarette, and specific, the demand in terms of otherness further enhances.
Herbal, baking perfume are notes relatively conventional in tobacco, and with its fragrance, plentiful, comfortable taste is by consumer's
Like.It is applied and cigarette, and the fragrance of cigarette can be improved, keep cigarette perfume plentiful strong.Existing flavor deployment mainly utilize herbal,
Baking perfume (or spice) improves cigarette flavor, and protrudes cigarette to smell fragrant essence rare.
Summary of the invention
The present invention is improved for existing flavoring and casing essence technology, provide it is a kind of with herbal, baking it is fragrant plus
Fragrant flavoring essence and application.This method, which is selected, has strong herbal, and the raw material for toasting note deployed, and be aided with burnt odor,
Fragrant and sweet preparing essence.It is applied to cigarette product, and the apparent medicinal herbs of cigarette can be improved, toast and open packet note, improve distinguishing for cigarette
Knowledge and magnanimity, and herbal, the fragrant note of baking can be obviously experienced in aspiration procedure, promote the rich and comfortable of cigarette flavor
Sense.
It is provided by the invention a kind of with the flavouring essence for tobacco for increasing medicinal herbs, toasting note, it is characterised in that be by following heavy
The substance of amount number is formulated: 2~30 parts of fruit juice maillard reaction thing, 1~8 part of coffee medicinal extract, fenugreek concrete 1~10
Part, 0.3~5 part of maple extract, 0.3~5 part of malt extract, 3~18 parts of grape biology extract, 0.03~0.5 part of furanone,
It is 3% 0.2~5 part of faenum graecum lactones, 0.1~3 part of ethylmaltol, 0.01~1 part of Damascenone, 10~50 parts of propylene glycol, pure
3~30 parts of water purification, 95% 3~20 parts of alcohol；The total weight of above-mentioned substance is 100 parts.
Wherein, the fruit juice maillard reaction thing be by coffee-extract, cocoa extract, cider, valine according to
4~7:1 of weight ratio~4:1~3:1~3 ratio is mixed, in the condition that temperature is 120~180 DEG C, pH is 7.5~10
Product after lower reaction, then obtained after carrying out separation, impurity removal with the ceramic membrane that aperture is 40~60nm.
It is provided by the invention a kind of with the preparation method for increasing medicinal herbs, the flavouring essence for tobacco for toasting note, it is characterised in that
Specific preparation process is as follows:
(1) prepare fruit juice maillard reaction thing, by weight for 4~7:1~4:1~3 ratio weigh coffee-extract,
Cocoa extract and cider, and be mixed and be put into three-neck flask after mixing evenly, be then added total weight of the mixture 5~
20% valine, turn on agitator, mixing speed 150r/min, and use concentrated ammonia liquor regulation system pH value for 7.5~10,
It connects reflux condensing tube, opens condensed water, with oil bath heating to 120~180 DEG C, stop heating after constant temperature 2h, by reaction product
It is put into storage tank, natural cooling, finally carries out separation, impurity removal with the ceramic membrane element that aperture is 40~60nm and obtain fruit juice beauty
Maillard reaction object；
(2) raw material of the following weight fraction of preparation: middle 2~30 parts of the fruit juice maillard reaction thing prepared of step (1),
1~8 part of coffee medicinal extract, 1~10 part of fenugreek concrete, 0.3~5 part of maple extract, 0.3~5 part of malt extract, cigarette are raw with grape
3~18 parts of object extract, 0.2~5 part of 3% faenum graecum lactones, 0.1~3 part of ethylmaltol, is dashed forward at 0.03~0.5 part of furanone
It faints 0.01~1 part of ketenes, 10~50 parts of propylene glycol, 3~30 parts of pure water, 3~20 parts of 95% alcohol；
(3) by 2~30 parts of fruit juice maillard reaction things in step (2), 1~8 part of coffee medicinal extract, 1~10 part of faenum graecum
Medicinal extract, 0.3~5 part of maple extract, 0.3~5 part of malt extract, 3~18 parts of grape biology extract for tobacco are successively in sequence
It is added in 10~50 parts of propylene glycol, is mixed 1-2 hours and is uniformly mixed to raw material components, be configured to component A；
(4) by 0.03~0.5 part of furanone, 0.2~5 part of 3% faenum graecum lactones, 0.1~3 part of ethyl in step (2)
Maltol, 0.01~1 part of Damascenone are successively added in order in 3~20 part 95% of alcohol, stir 1-2 hours to raw material
Component is uniformly mixed, and is configured to B component；
(5) pure by 3~30 parts in the B component and step (1) prepared in the component A prepared in step (3), step (4)
Water is mixed evenly 1-3 hours and is uniformly mixed to raw material components, after then 24-48 hour static, cross 80-100 mesh screen and filters
Sediment is gone to obtain with the flavouring essence for tobacco for increasing medicinal herbs, toasting note
The present invention provides preferably technical solution: described a kind of with the system for increasing medicinal herbs, the flavouring essence for tobacco for toasting note
Preparation Method, it is characterised in that the grape biology extract for tobacco is to be prepared according to the following steps to obtain:
(1) it by grape wash clean, and with being dried after distilled water flushing, is fitted into container, is added according to 100 parts by weight grapes
High-quality white sugar is added in the ratio of 32-37 parts by weight white sugar, and makes white sugar uniform fold on the grape smashed to pieces, and container is sealed
It is good；
(2) by be sealed it is common ferment 18-22 days under conditions of room temperature 32-37 degree, and the grape juice that will be fermented
Filtering, collecting filtrate is grape biology extract for tobacco A；
(3) the grape biology extract for tobacco A in step (2) is subjected to air-distillation, the distillate of collection should be cigarette use
The 70% of grape biology extract A volume, the distillate are heretofore described grape biology extract for tobacco.
It is provided by the invention a kind of with application of the flavouring essence for tobacco in cigarette for increasing medicinal herbs, toasting note, feature
Be: the flavouring essence for tobacco pure water for having increase medicinal herbs, toasting note that any one of claims 1 to 3 is obtained is dilute
It is uniformly sprayed on pipe tobacco after releasing, the additive amount of flavouring essence for tobacco is the 0.3%~0.5% of pipe tobacco total weight.
Heretofore described grape biology extract for tobacco can be formed using prior art preparation, specifically be detailed in open award
The Chinese patent of power, Patent No.: 200710053675.2, denomination of invention are as follows: grape biology extract for tobacco and its rolling up
Application in cigarette；The preparation method of grape biology extract for tobacco is specifically disclosed in the patent.Other materials in the present invention
Directly can commercially it obtain.
The present invention selects the apparent fenugreek concrete of herbal rhythm and faenum graecum lactones as basic note raw material, selects baking fragrant
The apparent fruit juice maillard reaction thing of rhythm, coffee medicinal extract, maple extract, malt extract, furanone and ethylmaltol are as body
Perfume material makes it have apparent medicinal herbs, baking note in terms of smelling perfume (or spice)；And it is aided with grape biology extract adjustment fragrance, increase
Add its rich and comfort.
Present invention allotment has strong herbal, toasts the essence that fragrant note smells perfume, assigns the herbal of cigarette characteristic, dries
Roasting note, be clearly felt that cigarette can in opening packet procedures and smells perfume (or spice), improve product identification；And it can be bright in aspiration procedure
It is aobvious to experience herbal, toast fragrant note, promote the rich of cigarette flavor.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below, but embodiment is not to skill of the present invention
The restriction of art scheme.
Fruit juice maillard reaction thing in following embodiment is prepared in accordance with the following methods: weighing coffee-extract respectively
300g, cocoa extract 150g, cider 50g are mixed evenly and are put into three-neck flask, and 50g valine is added, and open
Blender, mixing speed 150r/min use concentrated ammonia liquor regulation system pH value as 8.6, connect reflux condensing tube, open condensation
Water stops heating, reaction product is put into storage tank, natural cooling, is with aperture with oil bath heating to 150 DEG C, constant temperature 2h
The ceramic membrane element of 40nm carries out separation, impurity removal, obtains fruit juice maillard reaction thing.
Embodiment 1, a kind of essence for increasing medicinal herbs, toasting note for perfuming cigarette charging, specific preparation method is such as
Under:
(1) by 11 parts by weight fruit juice maillard reaction things, 2 parts by weight coffee medicinal extract, 1 parts by weight fenugreek concrete, 0.3 weight
Amount part maple extract, 0.3 parts by weight malt extract, 10 parts by weight grape biology extracts add in order to the third of 35 parts by weight
In glycol, it is mixed 1 hour and is configured to component A to raw material components are uniformly mixed；
(2) by 0.06 parts by weight furanone, 1 parts by weight, 3% faenum graecum lactones, 0.5 parts by weight ethylmaltol, 0.01 weight
Amount part Damascenone adds in order in the alcohol of 20 parts by weight 95%, is mixed to be uniformly mixed to raw material components for 1 hour and match
B component is made；
(3) B component obtained component A that step (1) obtains, step (2) and 18.83 parts by weight pure water are mixed
It is uniformly mixed to raw material components within uniform 2 hours, then after static 24 hours, crosses 80-100 mesh screen elimination sediment and obtain essence.
Embodiment 2, a kind of essence for increasing medicinal herbs, toasting note for perfuming cigarette charging, specific preparation method is such as
Under:
(1) by 10 parts by weight fruit juice maillard reaction things, 3 parts by weight coffee medicinal extract, 2 parts by weight fenugreek concretes, 1 weight
Part maple extract, 2 parts by weight malt extracts, 6 parts by weight grape biology extracts add in order in the propylene glycol to 40 parts by weight
In, it is mixed 1 hour and is configured to component A to raw material components are uniformly mixed；
(2) by 0.2 parts by weight furanone, 3 parts by weight, 3% faenum graecum lactones, 0.15 parts by weight ethylmaltol, 0.03 weight
Amount part Damascenone adds in order in the alcohol of 15 parts by weight 95%, is mixed to be uniformly mixed to raw material components for 1 hour and match
B component is made；
(3) B component obtained component A that step (1) obtains, step (2) and 17.62 parts by weight pure water are mixed
It is uniformly mixed to raw material components within uniform 2 hours, then after static 24 hours, crosses 80-100 mesh screen elimination sediment and obtain essence.
Embodiment 3, a kind of essence for increasing medicinal herbs, toasting note for perfuming cigarette charging, specific preparation method is such as
Under:
(1) by 18 parts by weight fruit juice maillard reaction things, 6 parts by weight coffee medicinal extract, 4 parts by weight fenugreek concretes, 2 weight
Part maple extract, 3 parts by weight malt extracts, 5 parts by weight grape biology extracts add in order in the propylene glycol to 25 parts by weight
In, it is mixed 1 hour and is configured to component A to raw material components are uniformly mixed；
(2) by 0.2 parts by weight furanone, 4 parts by weight, 3% faenum graecum lactones, 1 parts by weight ethylmaltol, 0.3 parts by weight
Damascenone adds in order in the alcohol of 15 parts by weight 95%, is mixed 1 hour and is configured to B to raw material components are uniformly mixed
Component；
(3) B component obtained component A that step (1) obtains, step (2) and 16.5 parts by weight pure water are mixed
It is uniformly mixed to raw material components within uniform 2 hours, then after static 24 hours, crosses 80-100 mesh screen elimination sediment and obtain essence.
Embodiment 4, a kind of essence for increasing medicinal herbs, toasting note for perfuming cigarette charging, specific preparation method is such as
Under:
(1) by 26 parts by weight fruit juice maillard reaction things, 1 parts by weight coffee medicinal extract, 6 parts by weight fenugreek concretes, 3 weight
Part maple extract, 0.5 parts by weight malt extract, 3 parts by weight grape biology extracts add in order to the third the two of 25 parts by weight
In alcohol, it is mixed 1 hour and is configured to component A to raw material components are uniformly mixed；
(2) 0.4 parts by weight furanone, 5 parts by weight, 3% faenum graecum lactones, 3 parts by weight ethylmaltols, 1 parts by weight are dashed forward
Ketenes of fainting adds in order in the alcohol of 10 parts by weight 95%, is mixed 1 hour and is configured to B group to raw material components are uniformly mixed
Point；
(3) B component obtained component A that step (1) obtains, step (2) and 16.1 parts by weight pure water are mixed
It is uniformly mixed to raw material components within uniform 2 hours, then after static 24 hours, crosses 80-100 mesh screen elimination sediment and obtain essence.
Application Example 1: by essence made by above-described embodiment 1~4 using pure water dilution after, be uniformly sprayed onto
In shelves pipe tobacco, essence additive amount is the 0.3% of pipe tobacco total weight, and after being sealed with sealed plastic bag, puts 50 DEG C of baking oven and dries 30
After minute, moisture is adjusted, at 22 ± 1 DEG C of temperature, humidity is to balance 24 hours under 60 ± 1% environment, then rolls into cigarette；And
To be not added with the blank pipe tobacco of any fragrance, cigarette cigarette as a comparison is rolled into after handling according to above-mentioned identical method；And
Please 7 people evaluate group and carry out effect applicating evaluating, evaluation result is as follows:
By smoking result show the essence modulated of the present invention to cigarette smell it is fragrant promoted, have increase cigarette medicinal herbs,
The effect of note is toasted, the richness of the rich and fragrance of cigarette note is promoted, keeps cigarette perfume alcohol just natural.And improve cigarette
Comfort.
It is prepared by the present invention as follows with medicinal herbs, its physical index of the essence of baking note:
Application Example 2: use the essence prepared in embodiment 3 use pure water dilute after respectively according to additive amount for
0.01%, 0.05%, 0.3%, 0.5% ratio is added into 100 grams of middle-grade pipe tobaccos；After being sealed with sealed plastic bag, put
After 50 DEG C of baking oven are dried 30 minutes, moisture is adjusted, at 22 ± 1 DEG C of temperature, humidity is to balance 24 hours under 60 ± 1% environment, then
Cigarette is rolled into, control is done to be not added with the blank cigarette of fragrance and smokes panel test.And ask 7 people to evaluate group and carry out effect applicating evaluating,
Evaluation result is as follows:
It can be seen that by above-mentioned smoking result come when additive amount is less than 0.3%, effect is not obvious, and is being added
Amount all has apparent medicinal herbs, baking note when being 0.3-0.5%, suction note is dull, gives off a strong fragrance plentiful, oral cavity is slightly rubbed
Rubbing feeling；Items effect of smokeing panel test is best when wherein additive amount is 0.3%.
Claims (4)
1. a kind of with the flavouring essence for tobacco for increasing medicinal herbs, toasting note, it is characterised in that matched by the substance of following parts by weight
It makes: 2~30 parts of fruit juice maillard reaction thing, 1~8 part of coffee medicinal extract, 1~10 part of fenugreek concrete, maple extract 0.3~
5 parts, 0.3~5 part of malt extract, 3~18 parts of grape biology extract, 0.03~0.5 part of furanone, 3% faenum graecum lactones 0.2
~5 parts, 0.1~3 part of ethylmaltol, 0.01~1 part of Damascenone, 10~50 parts of propylene glycol, 3~30 parts of pure water, 95%
3~20 parts of alcohol；
The fruit juice maillard reaction thing be by coffee-extract, cocoa extract, cider, valine according to weight ratio 4~
7:1~4:1~3:0.5~2 ratio is mixed, after reacting under conditions of temperature is 120~180 DEG C, pH is 7.5~10
Product, then with aperture be 40~60nm ceramic membrane carry out separation, impurity removal after obtain.
2. a kind of with the preparation method for increasing medicinal herbs, the flavouring essence for tobacco for toasting note, it is characterised in that specific preparation step is such as
Under:
(1) fruit juice maillard reaction thing is prepared, weighs coffee-extract, cocoa by weight for 4~7:1~4:1~3 ratio
Extract and cider, and be mixed and be put into three-neck flask after mixing evenly, total weight of the mixture 5~20% is then added
Valine, turn on agitator, mixing speed 150r/min, and concentrated ammonia liquor regulation system pH value is used to connect for 7.5~10
Reflux condensing tube opens condensed water, with oil bath heating to 120~180 DEG C, stops heating after constant temperature 2h, reaction product is put into
In storage tank, natural cooling finally carries out separation, impurity removal with the ceramic membrane element that aperture is 40~60nm and obtains fruit juice Mei Lade
Reactant；
(2) prepare the raw material of following weight fraction: 2~30 parts of the fruit juice maillard reaction thing of preparation, coffee in step (1)
1~8 part of medicinal extract, 1~10 part of fenugreek concrete, 0.3~5 part of maple extract, 0.3~5 part of malt extract, cigarette are mentioned with grape biology
Take 3~18 parts of object, 0.03~0.5 part of furanone, 0.2~5 part of 3% faenum graecum lactones, 0.1~3 part of ethylmaltol, Tujue's alkene
0.01~1 part of ketone, 10~50 parts of propylene glycol, 3~30 parts of pure water, 3~20 parts of 95% alcohol；
(3) by step (2) 2~30 parts of fruit juice maillard reaction things, 1~8 part of coffee medicinal extract, 1~10 part of fenugreek concrete,
0.3~5 part of maple extract, 0.3~5 part of malt extract, 3~18 parts of grape biology extract for tobacco are successively added in sequence
In 10~50 parts of propylene glycol, it is mixed 1-2 hours and is uniformly mixed to raw material components, be configured to component A；
(4) by 0.03~0.5 part of furanone, 0.2~5 part of 3% faenum graecum lactones, 0.1~3 part of ethyl malt in step (2)
Phenol, 0.01~1 part of Damascenone are successively added in order in 3~20 part 95% of alcohol, stir 1-2 hours to raw material components
It is uniformly mixed, is configured to B component；
(5) 3~30 parts of pure water in the B component and step (1) prepared in the component A prepared in step (3), step (4) are mixed
Stirring 1-3 hour to raw material components are closed to be uniformly mixed, after then 24-48 hour static, 80-100 mesh screen elimination sediment obtain
To the flavouring essence for tobacco that there are increase medicinal herbs, toast note.
3. according to claim 2 a kind of with the preparation method for increasing medicinal herbs, the flavouring essence for tobacco for toasting note, feature
It is that the grape biology extract for tobacco is to be prepared according to the following steps to obtain:
(1) it by grape wash clean, and with being dried after distilled water flushing, is fitted into container, 32- is added according to 100 parts by weight grapes
High-quality white sugar is added in the ratio of 37 parts by weight white sugar, and makes white sugar uniform fold on the grape smashed to pieces, and container is sealed；
(2) by be sealed it is common ferment 18-22 days under conditions of room temperature 32-37 degree, and by the grape juice fermented filter,
Collecting filtrate is grape biology extract for tobacco A；
(3) the grape biology extract for tobacco A in step (2) is subjected to air-distillation, the distillate of collection should be cigarette grape
The 70% of bio-extract A volume, the distillate are heretofore described grape biology extract for tobacco.
4. a kind of with application of the flavouring essence for tobacco in cigarette for increasing medicinal herbs, toasting note, it is characterised in that: by claim
Any one of 1 to the 3 obtained flavouring essence for tobacco for having increase medicinal herbs, toasting note is uniformly sprayed onto cigarette after being diluted with pure water
On silk, the additive amount of flavouring essence for tobacco is the 0.3%~0.5% of pipe tobacco total weight.
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| CN111187666A (en) * | 2020-01-13 | 2020-05-22 | 广州科百欣香料有限公司 | Burnt flavor essence for cigarettes and application thereof |
| CN111961530A (en) * | 2020-07-15 | 2020-11-20 | 云南绅博源生物科技有限公司 | Tobacco added essence and preparation method thereof |
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| CN111961530A (en) * | 2020-07-15 | 2020-11-20 | 云南绅博源生物科技有限公司 | Tobacco added essence and preparation method thereof |
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| CN114525176A (en) * | 2022-01-31 | 2022-05-24 | 河南中烟工业有限责任公司 | Cigarette fenugreek solid spice and preparation method and application thereof |
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