CN109181884A - A kind of preparation method of the crease-resistant effervescent detergent of cotton - Google Patents
A kind of preparation method of the crease-resistant effervescent detergent of cotton Download PDFInfo
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- CN109181884A CN109181884A CN201810778361.7A CN201810778361A CN109181884A CN 109181884 A CN109181884 A CN 109181884A CN 201810778361 A CN201810778361 A CN 201810778361A CN 109181884 A CN109181884 A CN 109181884A
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- parts
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- crease
- meshes
- resistant
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- 239000003599 detergent Substances 0.000 title claims abstract description 33
- 229920000742 Cotton Polymers 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000002245 particle Substances 0.000 claims abstract description 24
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000003756 stirring Methods 0.000 claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 14
- 239000000047 product Substances 0.000 claims abstract description 14
- 239000012153 distilled water Substances 0.000 claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 10
- 235000007303 Thymus vulgaris Nutrition 0.000 claims abstract description 9
- 239000001585 thymus vulgaris Substances 0.000 claims abstract description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 8
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 8
- -1 alkyl glycosides Chemical class 0.000 claims abstract description 8
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 8
- 229930182470 glycoside Natural products 0.000 claims abstract description 8
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 8
- 239000011734 sodium Substances 0.000 claims abstract description 8
- 229920001661 Chitosan Polymers 0.000 claims abstract description 6
- 108010010803 Gelatin Proteins 0.000 claims abstract description 6
- 235000003434 Sesamum indicum Nutrition 0.000 claims abstract description 6
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000706 filtrate Substances 0.000 claims abstract description 6
- 229920000159 gelatin Polymers 0.000 claims abstract description 6
- 239000008273 gelatin Substances 0.000 claims abstract description 6
- 235000019322 gelatine Nutrition 0.000 claims abstract description 6
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 6
- 235000012054 meals Nutrition 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims abstract description 6
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims abstract description 3
- 239000012467 final product Substances 0.000 claims abstract description 3
- 244000000231 Sesamum indicum Species 0.000 claims abstract 2
- 235000015165 citric acid Nutrition 0.000 claims description 12
- 241000246358 Thymus Species 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical class [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000284 extract Substances 0.000 claims description 3
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 claims description 2
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 2
- 229920001249 ethyl cellulose Polymers 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 235000015424 sodium Nutrition 0.000 claims description 2
- 238000005406 washing Methods 0.000 abstract description 14
- 238000004140 cleaning Methods 0.000 abstract description 10
- 230000037303 wrinkles Effects 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 5
- 240000002657 Thymus vulgaris Species 0.000 abstract 1
- 238000005903 acid hydrolysis reaction Methods 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000008188 pellet Substances 0.000 abstract 1
- 239000004744 fabric Substances 0.000 description 9
- 241000207961 Sesamum Species 0.000 description 4
- 238000011084 recovery Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 3
- 238000002310 reflectometry Methods 0.000 description 3
- 239000006229 carbon black Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000008399 tap water Substances 0.000 description 2
- 235000020679 tap water Nutrition 0.000 description 2
- 238000012356 Product development Methods 0.000 description 1
- 230000001153 anti-wrinkle effect Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000000271 synthetic detergent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of cotton preparation methods of crease-resistant effervescent detergent, comprising the following steps: is freeze-dried sesame seed meal；It pulverizes and sieves after taking-up, adds ethanol water, sealing mixes, pressurised extraction；Filtering, takes filtrate, is evaporated under reduced pressure, dries to obtain powders A；Dissolution is mixed in gelatin and distilled water；It is down to room temperature, adds distilled water, is shaken up, adding citric acid hydrolysis；Add powders A to stir, is freeze-dried to obtain product B；Product B, alkyl glycosides and citric acid are mixed well, the pelleting of 10 meshes, dry particle C are crossed；Sodium bicarbonate, sodium energy auxiliary agent, Nano chitosan and anhydrous sodium sulfate are mixed, the pelleting of 10 meshes, dry particle D are crossed；Particle C, particle D and thyme essential oil microballoon are mixed, 16 meshes is crossed and makes pellet to obtain the final product.Cotton prepared by this law has good clean effect with crease-resistant effervescent detergent, hand-washes clean rate and the rate of cleaning of machine-washing is all very high, while cleaning later with preferable wrinkle resistance.
Description
Technical field
The present invention relates to a kind of cotton preparation methods of crease-resistant effervescent detergent.
Background technique
With the rapid development of detergent industry, various types of synthetic detergents occur in succession, wherein laundry class product
Development is especially rapid, has the variforms such as washing cream, washing powder, liquid detergent so far, wherein washing powder has been that consumer is extensive
Receiving, becomes the preferred product that people wash clothing, concentrated type detergent also becomes developing direction from now on, its density height,
Dosage is few, washability is strong, foam is few, being suitble to the advantages such as machine washing, oneself is approved by consumer.But these detergent again take by presence
With the inconvenient and big disadvantage of dosage, the detergent of effervesce sheet form comes into being.For cotton fabric, after cleaning
It is easy to happen wrinkle.Therefore, research and development are directed to the crease resistance that has of cotton fabric, while the detergent tablet that clean effect is good
People's lives can be significantly facilitated, the quality of clothing is improved.
Summary of the invention
Technical problems to be solved: a kind of preparation method of crease-resistant effervescent detergent of cotton, prepared cotton are provided
With crease-resistant effervescent detergent with good clean effect, hand-washes the rate of cleaning and the rate of cleaning of machine-washing is all very high, while after cleaning
With preferable wrinkle resistance.
Technical solution: a kind of preparation method of the crease-resistant effervescent detergent of cotton, ingredient by weight, including following step
It is rapid:
(1) it is freeze-dried after sesame seed meal being added water；
(2) 40 meshes be crushed after taking out, 50% ethanol water is added, sealing mixes, and pressurize 500-600MPa, extracts
2-3min, wherein solid-to-liquid ratio 1:70-80；
(3) it filters, takes filtrate, be evaporated under reduced pressure, dry to obtain powders A；
(4) 10-15 parts of gelatin and 50-75 parts of distilled water are mixed, is put into thermostat water bath, in 70 DEG C of stirring and dissolving 50-60
min；
(5) it is down to room temperature, 40-60 parts of distilled water are added, shake up, 1.2-2 parts of citric acids are added, hydrolyze 60- at 40 DEG C
70min；
(6) 40-50 parts of powders As are added and stir 10-20min, carry out being freeze-dried to obtain product B；
(7) B, 9-10 parts of alkyl glycosides of 5-10 parts of products and 5-7 parts of citric acids are mixed well, crosses the pelleting of 10 meshes, it is dry
Obtain particle C；
(8) 5-7 parts of sodium bicarbonates, 2-3 parts of sodium energy auxiliary agents, 1-2 parts of Nano chitosans and 3-5 parts of anhydrous sodium sulfates are mixed,
Cross the pelleting of 10 meshes, dry particle D；
(9) D and 1-2 parts of particle C, particle thyme essential oil microballoons are mixed, crosses the pelleting of 16 meshes, obtaining partial size is 1-3 mm's
The crease-resistant effervescent detergent of cotton.
Further, the product B, alkyl glycosides, citric acid, sodium bicarbonate, sodium energy auxiliary agent and anhydrous sodium sulfate exist
Using preceding all by crushing, it is spare to cross 80 meshes.
Further, the preparation method of the thyme essential oil microballoon:
Step 1: taking 2-5 parts of ethyl celluloses, 80% ethyl alcohol of 40-60 part, stirring and dissolving is added；
Step 2: the glycerol of 5-10 parts of thyme essential oils and 2% is added, stir；
Step 3: adding 1wt% talcum powder, stir evenly；
Step 4: being spray-dried to obtain the final product, charging rate 3mL/min, inlet air temperature is 100 DEG C, atomizing pressure 100kPa.
The utility model has the advantages that
1. having good clean effect through the crease-resistant effervescent detergent of cotton prepared by the present invention, hand-washing clean rate highest can
Up to 49.32%, machine washing cleans rate up to 43.31%, significantly larger than commercial detergent 1 and 2, while after cleaning, creasy recovery angle
Up to 148 °, there is preferable wrinkle resistance.
2. each step operation is simple, it is suitble to industrialized production.
Specific embodiment
Embodiment 1
A kind of preparation method of the crease-resistant effervescent detergent of cotton, ingredient is by weight, comprising the following steps:
(1) it is freeze-dried after sesame seed meal being added water；
(2) 40 meshes be crushed after taking out, 50% ethanol water is added, sealing mixes, and pressurize 500MPa, 2min is extracted,
Wherein, solid-to-liquid ratio 1:70；
(3) it filters, takes filtrate, be evaporated under reduced pressure, dry to obtain powders A；
(4) 10 parts of gelatin and 50 parts of distilled water are mixed, is put into thermostat water bath, in 70 DEG C of 50 min of stirring and dissolving；
(5) it is down to room temperature, 40 parts of distilled water are added, shake up, 1.2 parts of citric acids are added, hydrolyze 60min at 40 DEG C；
(6) 40 parts of powders As are added and stir 10min, carry out being freeze-dried to obtain product B；
(7) 5 parts of product B, 9 parts of alkyl glycosides and 5 parts of citric acids are mixed well, crosses the pelleting of 10 meshes, dry particle C；
(8) 5 parts of sodium bicarbonates, 2 parts of sodium energy auxiliary agents, 1 part of Nano chitosan and 3 parts of anhydrous sodium sulfates are mixed, crosses 10 meshes
Pelleting, dry particle D；
(9) particle C, particle D and 1 part of thyme essential oil microballoon are mixed, crosses the pelleting of 16 meshes, obtain the cotton that partial size is 1-3 mm
The crease-resistant effervescent detergent of cloth.
Embodiment 2
A kind of preparation method of the crease-resistant effervescent detergent of cotton, ingredient is by weight, comprising the following steps:
(1) it is freeze-dried after sesame seed meal being added water；
(2) 40 meshes be crushed after taking out, 50% ethanol water is added, sealing mixes, and pressurize 550MPa, extracts
2.5min, wherein solid-to-liquid ratio 1:75；
(3) it filters, takes filtrate, be evaporated under reduced pressure, dry to obtain powders A；
(4) 13 parts of gelatin and 63 parts of distilled water are mixed, is put into thermostat water bath, in 70 DEG C of stirring and dissolving 50-60 min；
(5) it is down to room temperature, 50 parts of distilled water are added, shake up, 1.6 parts of citric acids are added, hydrolyze 65min at 40 DEG C；
(6) 45 parts of powders As are added and stir 15min, carry out being freeze-dried to obtain product B；
(7) 8 parts of product B, 9.5 parts of alkyl glycosides and 6 parts of citric acids are mixed well, crosses the pelleting of 10 meshes, dry particle
C；
(8) 6 parts of sodium bicarbonates, 2.5 parts of sodium energy auxiliary agents, 1.5 parts of Nano chitosans and 4 parts of anhydrous sodium sulfates are mixed, crosses 10
Mesh pelleting, dry particle D；
(9) particle C, particle D and 1.5 parts of thyme essential oil microballoons are mixed, crosses the pelleting of 16 meshes, obtaining partial size is 1-3 mm's
The crease-resistant effervescent detergent of cotton.
Embodiment 3
A kind of preparation method of the crease-resistant effervescent detergent of cotton, ingredient is by weight, comprising the following steps:
(1) it is freeze-dried after sesame seed meal being added water；
(2) 40 meshes be crushed after taking out, 50% ethanol water is added, sealing mixes, and pressurize 600MPa, 3min is extracted,
Wherein, solid-to-liquid ratio 1:80；
(3) it filters, takes filtrate, be evaporated under reduced pressure, dry to obtain powders A；
(4) 15 parts of gelatin and 75 parts of distilled water are mixed, is put into thermostat water bath, in 70 DEG C of 60 min of stirring and dissolving；
(5) it is down to room temperature, 60 parts of distilled water are added, shake up, 2 parts of citric acids are added, hydrolyze 70min at 40 DEG C；
(6) 50 parts of powders As are added and stir 20min, carry out being freeze-dried to obtain product B；
(7) 10 parts of product B, 10 parts of alkyl glycosides and 7 parts of citric acids are mixed well, crosses the pelleting of 10 meshes, dry particle
C；
(8) 7 parts of sodium bicarbonates, 3 parts of sodium energy auxiliary agents, 2 parts of Nano chitosans and 5 parts of anhydrous sodium sulfates are mixed, crosses 10 meshes
Pelleting, dry particle D；
(9) particle C, particle D and 2 parts of thyme essential oil microballoons are mixed, crosses the pelleting of 16 meshes, obtain the cotton that partial size is 1-3 mm
The crease-resistant effervescent detergent of cloth.
Hand washing: at normal temperatures and pressures, under natural ph, the hard water (250 mg/ kg) that 200.00m L is added into beaker (is pressed
GB/T 6367 is prepared), JB-01 carbon black oil soiled cotton item (6cm × 6cm) and the detergent of the present invention prepared and commercially available washing is added
Agent 1 and 2 takes out soiled cotton item after stirring impregnates 30min after making it completely dissolved, and wears rubber gloves concentration by the same person and washes by rubbing with the hands
20 min, washing frequency by rubbing with the hands is to wash by rubbing with the hands 70 times per minute, does 3 parallel laboratory tests respectively and is averaged, then rinses 5 min with tap water
After dry, flatten, measure its reflectivity with leucometer.
Simulation machine washing: JB-01 carbon black oil soiled cotton item (6cm × 6cm) immersion is filled into the prepared present invention of 200.00m L
In the beaker of detergent or commercial detergent 1 and 2, by it under the conditions of 25 DEG C 40 min of electric stirring, and 25 DEG C 60.00
Stirring and washing 5min, taking-up are dried in mL tap water, are flattened, are measured its reflectivity with leucometer.
The pollution cloth of measurement test front and back, multiple measure and calculation average value record data.It is calculated with following formula:
In formula: Dr-cleans rate
Rw-pollution cloth cleans back reflection rate, %
Rs-pollution cloth cleans front-reflection rate, %
Ro-original cloth reflectivity, %.
According to the folding of GB/T 3819-1997 " horn cupping is replied in the measurement of textile fabric wrinkle recovery property " measurement cotton
Wrinkle recovery angle.
The decontamination anti-wrinkle effect of 1 high efficiency composition detergent of table
There is good clean effect through the crease-resistant effervescent detergent of cotton prepared by the present invention, hand-wash the rate of cleaning and reach as high as
49.32%, for the rate of cleaning of machine-washing up to 43.31%, significantly larger than commercial detergent 1 and 2, while after cleaning, creasy recovery angle is high
Up to 148 °, there is preferable wrinkle resistance.
Claims (3)
1. a kind of cotton preparation method of crease-resistant effervescent detergent, it is characterised in that: ingredient by weight, including following step
It is rapid:
(1) it is freeze-dried after sesame seed meal being added water；
(2) 40 meshes be crushed after taking out, 50% ethanol water is added, sealing mixes, and pressurize 500-600MPa, extracts
2-3min, wherein solid-to-liquid ratio 1:70-80；
(3) it filters, takes filtrate, be evaporated under reduced pressure, dry to obtain powders A；
(4) 10-15 parts of gelatin and 50-75 parts of distilled water are mixed, is put into thermostat water bath, in 70 DEG C of stirring and dissolving 50-60
min；
(5) it is down to room temperature, 40-60 parts of distilled water are added, shake up, 1.2-2 parts of citric acids are added, hydrolyze 60- at 40 DEG C
70min；
(6) 40-50 parts of powders As are added and stir 10-20min, carry out being freeze-dried to obtain product B；
(7) B, 9-10 parts of alkyl glycosides of 5-10 parts of products and 5-7 parts of citric acids are mixed well, crosses the pelleting of 10 meshes, it is dry
Obtain particle C；
(8) 5-7 parts of sodium bicarbonates, 2-3 parts of sodium energy auxiliary agents, 1-2 parts of Nano chitosans and 3-5 parts of anhydrous sodium sulfates are mixed,
Cross the pelleting of 10 meshes, dry particle D；
(9) D and 1-2 parts of particle C, particle thyme essential oil microballoons are mixed, crosses the pelleting of 16 meshes, obtaining partial size is 1-3 mm's
The crease-resistant effervescent detergent of cotton.
2. a kind of preparation method of the crease-resistant effervescent detergent of cotton according to claim 1, it is characterised in that: the production
Object B, alkyl glycosides, citric acid, sodium bicarbonate, sodium energy auxiliary agent and anhydrous sodium sulfate, all by crushing, are crossing 80 mesh using preceding
It sieves spare.
3. a kind of preparation method of the crease-resistant effervescent detergent of cotton according to claim 1, it is characterised in that: described hundred
In essential oil microballoon preparation method:
Step 1: taking 2-5 parts of ethyl celluloses, 80% ethyl alcohol of 40-60 part, stirring and dissolving is added；
Step 2: the glycerol of 5-10 parts of thyme essential oils and 2% is added, stir；
Step 3: adding 1wt% talcum powder, stir evenly；
Step 4: being spray-dried to obtain the final product, charging rate 3mL/min, inlet air temperature is 100 DEG C, atomizing pressure 100kPa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810778361.7A CN109181884B (en) | 2018-07-16 | 2018-07-16 | Preparation method of anti-wrinkle effervescent detergent for cotton cloth |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810778361.7A CN109181884B (en) | 2018-07-16 | 2018-07-16 | Preparation method of anti-wrinkle effervescent detergent for cotton cloth |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109181884A true CN109181884A (en) | 2019-01-11 |
| CN109181884B CN109181884B (en) | 2022-04-08 |
Family
ID=64936633
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810778361.7A Expired - Fee Related CN109181884B (en) | 2018-07-16 | 2018-07-16 | Preparation method of anti-wrinkle effervescent detergent for cotton cloth |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109181884B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1839871A (en) * | 2006-01-11 | 2006-10-04 | 南京工业大学 | Azithromycin enteric coated microsphere and preparation method thereof |
| CN101914415A (en) * | 2010-08-27 | 2010-12-15 | 郭俊华 | Effervescent detergent and preparation method thereof |
| CN104177370A (en) * | 2014-09-04 | 2014-12-03 | 陕西源邦生物技术有限公司 | Method for preparing high-content sesamin from sesame seed meal |
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2018
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1839871A (en) * | 2006-01-11 | 2006-10-04 | 南京工业大学 | Azithromycin enteric coated microsphere and preparation method thereof |
| CN101914415A (en) * | 2010-08-27 | 2010-12-15 | 郭俊华 | Effervescent detergent and preparation method thereof |
| CN104177370A (en) * | 2014-09-04 | 2014-12-03 | 陕西源邦生物技术有限公司 | Method for preparing high-content sesamin from sesame seed meal |
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| CN109181884B (en) | 2022-04-08 |
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