CN109126270A - A kind of chemical material solid-liquid separating method - Google Patents
A kind of chemical material solid-liquid separating method Download PDFInfo
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- CN109126270A CN109126270A CN201811279786.XA CN201811279786A CN109126270A CN 109126270 A CN109126270 A CN 109126270A CN 201811279786 A CN201811279786 A CN 201811279786A CN 109126270 A CN109126270 A CN 109126270A
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- 239000007788 liquid Substances 0.000 title claims abstract description 196
- 239000000126 substance Substances 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 27
- 239000000463 material Substances 0.000 title claims abstract description 20
- 239000007787 solid Substances 0.000 claims abstract description 102
- 239000000203 mixture Substances 0.000 claims abstract description 96
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 20
- 238000000926 separation method Methods 0.000 claims abstract description 19
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 77
- 229920004934 Dacron® Polymers 0.000 claims description 75
- 238000001914 filtration Methods 0.000 claims description 75
- 238000003756 stirring Methods 0.000 claims description 53
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 19
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 19
- 238000005192 partition Methods 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 230000005611 electricity Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 description 13
- 239000012535 impurity Substances 0.000 description 10
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- 239000010865 sewage Substances 0.000 description 4
- 229920004933 Terylene® Polymers 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 229920002994 synthetic fiber Polymers 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Filtration Of Liquid (AREA)
- Water Treatment By Sorption (AREA)
Abstract
The invention belongs to solid-liquid separation technique field, specifically a kind of chemical material solid-liquid separating method；It is included in solidliquid mixture to be put into magnetic active carbon, be separated by solid-liquid separation with solid-liquid separating equipment using chemical field and supersonic generator is arranged in chemical field solid-liquid separating equipment；By the present invention in that the rate of separation of solid and liquid can be improved with magnetic active carbon, solidliquid mixture can be kept completely separate by using chemical field with solid-liquid separating equipment.
Description
Technical field
The invention belongs to solid-liquid separation technique field, specifically a kind of chemical material solid-liquid separating method.
Background technique
In the process that Chinese Urbanization scale constantly extends and industrialization degree is continuously improved, it can generate and largely be difficult to
The trade effluent and sanitary sewage of processing, moreover, because the discharge amount of trade effluent is big, water quality is complicated, and toxicity is big, ammonia nitrogen, COD
(COD) comparision contents are high, therefore, how to handle trade effluent, so that it is met the requirement of environmental protection, just seem especially heavy
It wants, so needing the sewage disposal device of complete set just to handle sewage, makes solid matter and liquid in sewage
It can be kept completely separate, to reach the requirement of environmental protection.
Also occur the technical solution of some chemical industry equipment for separating liquid from solid in the prior art, such as application No. is
201710422458 Chinese patent discloses a kind of chemical industry equipment for separating liquid from solid, including cabinet, under the outside of cabinet
Portion is connected with dodge gate, and the lower end of partition is connected with filter vat, and the inside of filter vat is respectively equipped with the first filter plate and second
Filter plate, the first filter plate are located at the top of the second filter plate, and the inner cavity bottom end of cabinet is equipped with two first sliding grooves being parallel to each other, and first
The first matched sliding block is connected in sliding slot, the upper end of the first sliding block is connected with fluid box, and fluid box is located at filter vat
Underface, the equal and external PLC control of the first cylinder, motor, speed changer, the second cylinder, infrared inductor, laser inductor
Device connection.
The technical solution can simply separate solidliquid mixture, but stir in the program solidliquid mixture
It mixes too simple, is not completely separated solidliquid mixture；The solid obtained after filtering does not carry out secondary filter, it cannot be guaranteed that
Liquid component is free of in solid；Liquid is only simply filtered twice, it cannot be guaranteed that in finally obtained liquid not
Containing solid residue；So that the technical solution is restricted.
Summary of the invention
In order to make up for the deficiencies of the prior art, it is not completely separated, separated with solving solidliquid mixture in the prior art
Solid afterwards is still containing liquid component and to the filtering excessively simple question of liquid, and the invention proposes a kind of chemical materials
Solid-liquid separating method.
The technical solution adopted by the present invention to solve the technical problems is: a kind of chemical material solid-liquid point of the present invention
From method, method includes the following steps:
S1: it will be put into magnetic active carbon in solidliquid mixture, and stir evenly；It is passed through magnetic active carbon and solidliquid mixture
Mixing, can first by impurity absorption a part of in solidliquid mixture, while also can by quality in solidliquid mixture it is biggish contain magnetic
The impurity absorption of property, improves the efficiency of separation of solid and liquid；
S2: the solidliquid mixture of magnetic active carbon will be mixed in S1 from the feed inlet in chemical field solid-liquid separating equipment
It is passed through, starts chemical field with solid-liquid separating equipment and preliminary Stirring is carried out to solidliquid mixture；It is carried out in solidliquid mixture
When preliminary Stirring, magnetic active carbon is filled with solidliquid mixture together Stirring, magnetic active carbon with solidliquid mixture
Tap touching enables to be adsorbed by magnetic active carbon completely in solidliquid mixture containing magnetic impurity；
S3: supersonic generator is set at secondary filtration unit in chemical field solid-liquid separating equipment；When solid-liquid is mixed
When closing the water in object by secondary filtration unit, supersonic generator work；Supersonic generator transmitting ultrasonic wave makes secondary mistake
Woven dacron on strainer generates vibration, will not be excessive because of solid impurity under the premise of guaranteeing that woven dacron can collect solid impurity
And woven dacron is caused to be blocked, improve the speed of liquid filtering；
Wherein, chemical field solid-liquid separating equipment described in S2, including motor, feed inlet, work box, electrically operated valve
And controller；The controller is for controlling the work of solidliquid mixture separation equipment；The feed inlet is located at the top of work box
Side；The motor is located at the middle part of work box top outer and is vertically arranged with work box, its output end passes through work box
Top simultaneously extends in work box；The output end of the motor and the top of agitating shaft are affixed, and the bottom of agitating shaft is connected with spiral shell
Blender is revolved, spiral agitator is used to be sirred and separated solidliquid mixture row；In the spiral agitator on the side wall of paddle
It is uniformly provided with through-hole, is equipped in through-hole and stirs block, stir block and be rotatablely connected by the side wall of shaft and through-hole, stir block and solid
Liquid mixture is overturn when contacting；The side of the spiral agitator is equipped with discharge port, and electrically operated valve is arranged in discharge port, discharging
The lower section of mouth is connected to solid case, and solid case is for collecting the solid after Stirring；PTFE overlay film is equipped in the solid case,
PTFE overlay film and the side wall of solid case are affixed, and PTFE overlay film was used for liquid remaining in filter solid；The present invention passes through design spiral shell
Blender is revolved, when motor drives spiral agitator rotation, the paddle on spiral agitator can uniformly stir solidliquid mixture
It mixes, realizes the quick separating of solid and liquid in solidliquid mixture, while using spiral agitator Stirring solidliquid mixture
Shi Burong easily causes solidliquid mixture to block, and the side wall of the paddle of spiral agitator is equipped with through-hole, is equipped with and turns in through-hole
Motion block stirs block and is rotatablely connected by the side wall of shaft and through-hole, stirs block and turns over when with solid contact in solidliquid mixture
Turn, improves the stirring rate of spiral agitator, and the solid after Stirring can be collected by solid case, be equipped in fixed case
PTFE overlay film can be filtered liquid remaining in solid, improve the filter effect of separation of solid and liquid.
The solidliquid mixture for being mixed with magnetic active carbon is imported from feed inlet, starts motor, motor rotation drives agitating shaft
Rotation, agitating shaft rotation drive spiral agitator rotation, and solidliquid mixture is rotated together with spiral agitator, in auger
During device rotates, Stirring is carried out to solidliquid mixture, enables the solid and liquid quick separating in solidliquid mixture,
During spiral agitator Stirring, stirs block and ceaselessly overturn because of the reason of being contacted with solidliquid mixture, this
Sample can accelerate spiral agitator to carry out Stirring to solidliquid mixture；When spiral agitator after a period of work, at this time
Solid and liquid in solidliquid mixture are basically separated, and open electrically operated valve, the solid in solidliquid mixture is with auger
Enter in solid case after device rotation from discharge port, is then contacted with PTFE overlay film；PTFE overlay film can be by liquid remaining in solid
Body is filtered, and the solid guaranteed is free of liquid component, further improves the filter effect of solid in solidliquid mixture.
Preferably, the lower section of the spiral agitator is equipped with by-pass filtration unit, and by-pass filtration unit is to solidliquid mixture
In liquid carry out by-pass filtration；The by-pass filtration unit includes partition, rubber bumps and woven dacron；The partition and work
The side wall of case is affixed, and partition is rubber material；The rubber bumps are uniformly arranged in the top of partition, rubber bumps and spiral shell
It revolves blender to completely attach to, and is equipped with honeycomb hole between adjacent rubber bumps, honeycomb hole is uniformly provided in partition；It is described
Woven dacron is coated on the surface that rubber bumps are contacted with spiral agitator, and woven dacron is for collecting the solid not entered in solid case
Residue；The present invention can be carried out by-pass filtration to the liquid flowed down from spiral agitator, be passed through by setting by-pass filtration unit
Solid component remaining in liquid is collected by woven dacron, improves the filter effect of liquid in solidliquid mixture.
Preferably, the honeycomb hole is equipped with chamfering close to the opening of rubber bumps, and chamfering is used cooperatively with rubber bumps；
Spiral agitator, which squeezes rubber bumps in rotation, is collapsible into rubber bumps in honeycomb hole along the direction of chamfering, causes honeycomb
Pneumatics in hole, when spiral agitator stops operating, rubber bumps restore to the original state, and the pressure in honeycomb hole is less than honeycomb hole at this time
Outer pressure, liquid can be inhaled into rapidly in honeycomb hole to achieve the purpose that quickly to filter, and improve the work of this equipment
Efficiency.
Squeezing rubber bumps when spiral agitator is in rotation makes rubber bumps be collapsible into honeycomb hole along the direction of chamfering
It is interior, cause pneumatics in honeycomb hole；After the solid on spiral agitator in solidliquid mixture is collected by solid case, motor stops turning
Dynamic, rubber bumps restore to the original state when spiral agitator stops operating, and the pressure in honeycomb hole is less than the pressure outside honeycomb hole at this time,
Liquid in solidliquid mixture is inhaled into honeycomb hole after woven dacron filters, and is discharged by honeycomb hole.
Preferably, the lower section of the by-pass filtration unit is equipped with secondary filtration unit, and secondary filtration unit is to from level-one mistake
The liquid for filtering unit outflow carries out secondary filter；The secondary filtration unit include the support plate of inverse Ba type, No.1 raised plate,
No. two raised plates, No. three raised plates, liquid outlet and liquid collecting box；The side wall of the support plate and work box is affixed, and No.1 is convex
Starting board, No. two raised plates and No. three raised plates are uniformly distributed in the top of support plate, and No.1 raised plate, No. two raised plates, three
Number raised plate is affixed with support plate；The No.1 raised plate, No. two raised plates, the number of No. three raised plates are four pieces, and two
Number raised plate is located at the inside of No.1 raised plate, and No. two raised plates are uniformly distributed in the opening of adjacent No.1 raised plate；
No. three raised plates are located at the inside of No. two raised plates, and No. three raised plates are uniformly distributed in opening for No. two adjacent raised plates
At mouthful；The liquid outlet is located at the inside of No. three raised plates, No.1 raised plate, No. two raised plates, No. three raised plates and support plate
Layering is carried out with the use of to liquid；The liquid collecting box is located at the lower section of liquid outlet；The present invention passes through design second level
Filter element can carry out secondary filter to the liquid that flows out from by-pass filtration unit, by No.1 raised plate, No. two raised plates,
No. three raised plates and support plate, which are used cooperatively, carries out layering to liquid, further promotes the filtering of liquid in solidliquid mixture
Effect.
Preferably, the No.1 raised plate, No. two raised plates, No. three raised plates cross sectional shape be arch, and arch
No.1 raised plate, No. two raised plates, No. three raised plates be hollow structure；The No.1 raised plate of hollow structure, No. two protrusions
Plate, No. three raised plates improve liquid flowing under the premise of guaranteeing to carry out layering to the liquid in solidliquid mixture
Rate improves the speed of liquid filtering.
Preferably, the top of the support plate is equipped with one layer of woven dacron according to the shape of support plate, and woven dacron passes through ring
Woven dacron, is adsorbed on the side wall of work box, terylene by the connection of the side wall of shape magnet and work box by the magnetic force of annular magnet
Cloth is for collecting the solid residue not filtered by by-pass filtration unit；The present invention passes through wraps up one layer of woven dacron on the supporting plate,
Can be for re-filtering to the solid residue not filtered by by-pass filtration unit, in the liquid that guarantees without solid at
Point, and the side wall of woven dacron and work box is connected by annular magnet, it, can be by ring when the solid residue on woven dacron is excessive
Shape magnet is removed, and is then cleared up to removing woven dacron, and the cleaning of woven dacron is facilitated using the fixed woven dacron of annular magnet
With replacement, that is, improve the service life of this equipment.
After the liquid in solidliquid mixture is discharged out of honeycomb hole, on the woven dacron in support plate, it is located at liquid out
Woven dacron above mouthful collects the solid residue in liquid, and during collection, supersonic generator work shakes woven dacron
It is dynamic, the solid residue collected blocking woven dacron is prevented, while also accelerating the speed of liquid filtering, liquid is from woven dacron at this time
It drops into liquid outlet vertically；And the liquid for falling into support plate two sides, after woven dacron filters, most of liquid is from adjacent
It is obliquely flowed into the opening of No.1 raised plate at No. two raised plates, a small amount of liquid is after woven dacron filters from No.1
The hollow part of raised plate obliquely flows at No. two raised plates；Most of liquid into No. two raised plate sides passes through two
After the woven dacron filtering of number raised plate side, No. three raised plates are obliquely flowed into from the opening of adjacent No. two raised plates
Place, a small amount of liquid obliquely flow into from No. three raised plates after woven dacron filters from the hollow part of No. two risers, into
Enter most of liquid of No. three raised plate sides after the filtering of the woven dacron of No. three raised plate sides, from adjacent No. three raised plates
Opening obliquely flow into liquid outlet, a small amount of liquid is in from the hollow part of No. three raised plates after woven dacron filters
In skewed inflow liquid outlet, final liquid is flowed out from liquid outlet to be collected by liquid collecting box.
Beneficial effects of the present invention are as follows:
1. a kind of chemical material solid-liquid separating method of the present invention, this method, can be with by using magnetic active carbon
The rate of solidliquid mixture separation is improved, while having used supersonic generator, improves the filtering effect of liquid in being separated by solid-liquid separation
Rate.
2. a kind of chemical material solid-liquid separating method of the present invention, chemical field solid-liquid used in this method
Separation equipment realizes the quick separating of solid and liquid in solidliquid mixture by design spiral agitator, while using spiral
When blender Stirring solidliquid mixture do not allow that solidliquid mixture is easily caused to block, and the side wall of the paddle of spiral agitator
It is equipped with through-hole, is equipped in through-hole and stirs block, block is stirred and is rotatablely connected by the side wall of shaft and through-hole, improve auger
The stirring rate of device；And the solid after Stirring can be collected by solid case, and PTFE overlay film is equipped in fixed case, it can be to solid
Remaining liquid is filtered in body, improves the filter effect of separation of solid and liquid.
3. a kind of chemical material solid-liquid separating method of the present invention, chemical field solid-liquid used in this method
Separation equipment can carry out by-pass filtration to the liquid flowed down from spiral agitator, by washing by design by-pass filtration unit
Solid component remaining in liquid is collected by synthetic fibre cloth, improves the filter effect of liquid in solidliquid mixture.
4. a kind of chemical material solid-liquid separating method of the present invention, chemical field solid-liquid used in this method
Separation equipment can carry out secondary filter to the liquid flowed out from by-pass filtration unit, pass through one by design secondary filtration unit
Number raised plate, No. two raised plates, No. three raised plates and support plate, which are used cooperatively, carries out layering to liquid, is further promoted solid
The filter effect of liquid in liquid mixture.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is process flow chart of the invention；
Fig. 2 is main view of the invention；
Fig. 3 is the lower view in Fig. 2 at A；
Fig. 4 is the partial enlarged view in Fig. 2 at B；
Fig. 5 is the lower view in Fig. 2 at C；
Fig. 6 is the direction view in Fig. 5 at D；
Fig. 7 is the not contracted schematic diagram of rubber bumps；
Fig. 8 is schematic diagram when rubber bumps are shunk；
In figure: motor 1, feed inlet 2, work box 3, electrically operated valve 4, agitating shaft 5, spiral agitator 6, through-hole 61 stir block
62, shaft 63, discharge port 7, solid case 8, PTFE overlay film 9, by-pass filtration unit 10, partition 101, rubber bumps 102, woven dacron
103,112, No. two honeycomb hole 104, annular magnet 105, secondary filtration unit 11, support plate 111, No.1 raised plate raised plates
113, No. three raised plates 114, liquid outlet 115, liquid collecting box 116.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 8, a kind of chemical material solid-liquid separating method of the present invention, this method include following step
It is rapid:
S1: it will be put into magnetic active carbon in solidliquid mixture, and stir evenly；It is passed through magnetic active carbon and solidliquid mixture
Mixing, can first by impurity absorption a part of in solidliquid mixture, while also can by quality in solidliquid mixture it is biggish contain magnetic
The impurity absorption of property, improves the efficiency of separation of solid and liquid；
S2: the solidliquid mixture of magnetic active carbon will be mixed in S1 from the feed inlet in chemical field solid-liquid separating equipment
It is passed through, starts chemical field with solid-liquid separating equipment and preliminary Stirring is carried out to solidliquid mixture；It is carried out in solidliquid mixture
When preliminary Stirring, magnetic active carbon is filled with solidliquid mixture together Stirring, magnetic active carbon with solidliquid mixture
Tap touching enables to be adsorbed by magnetic active carbon completely in solidliquid mixture containing magnetic impurity；
S3: supersonic generator is set at secondary filtration unit in chemical field solid-liquid separating equipment；When solid-liquid is mixed
When closing the water in object by secondary filtration unit, supersonic generator work；Supersonic generator transmitting ultrasonic wave makes secondary mistake
Woven dacron on strainer generates vibration, will not be excessive because of solid impurity under the premise of guaranteeing that woven dacron can collect solid impurity
And woven dacron is caused to be blocked, improve the speed of liquid filtering；
Wherein, chemical field solid-liquid separating equipment described in S2, including it is motor 1, feed inlet 2, work box 3, electronic
Valve 4 and controller；The controller is for controlling the work of solidliquid mixture separation equipment；The feed inlet 2 is located at work box 3
The side at top；The motor 1 is located at the middle part of 3 top outer of work box and is vertically arranged with work box 3, its output end passes through
The top of work box 3 simultaneously extends in work box 3；The top of the output end and agitating shaft 5 of the motor 1 is affixed, agitating shaft 5
Bottom is connected with spiral agitator 6, and spiral agitator 6 is used to be sirred and separated solidliquid mixture row；In the spiral agitator 6
It is uniformly provided with through-hole 61 on the side wall of paddle, is equipped in through-hole and stirs block 62, stirs block 62 and passes through shaft 63 and through-hole 61
Side wall rotation connection, stir block 62 and overturning when solidliquid mixture contacts；The side of the spiral agitator 6 is equipped with discharge port
7, electrically operated valve 4 is arranged in discharge port 7, and the lower section of discharge port 7 is connected to solid case 8, and solid case 8 is for after collecting Stirring
Solid；It is equipped with PTFE overlay film 9 in the solid case 8, PTFE overlay film 9 and the side wall of solid case 8 are affixed, and PTFE overlay film 9 is used for
Cross liquid remaining in filter solid；The present invention is by design spiral agitator 6, when motor 1 drives spiral agitator 6 to rotate,
Paddle on spiral agitator 6 can realize the quick of solid and liquid in solidliquid mixture to solidliquid mixture uniform stirring
Separation, while using 6 Stirring solidliquid mixture of spiral agitator when does not allow that solidliquid mixture is easily caused to block, and spiral is stirred
The side wall for mixing the paddle of device 6 is equipped with through-hole, is equipped in through-hole 61 and stirs block 62, stirs block 62 and pass through shaft 63 and through-hole 61
Side wall rotation connection, stir overturning when with solid contact in solidliquid mixture of block 62, improve stirring for spiral agitator 6
Rate is mixed, and the solid after Stirring can be collected by solid case 8, PTFE overlay film 9 is equipped in fixed case 8, it can be in solid
Remaining liquid is filtered, and improves the filter effect of separation of solid and liquid.
The solidliquid mixture for being mixed with magnetic active carbon is imported from feed inlet 2, starts motor 1, the rotation of motor 1 drives stirring
Axis 5 rotates, and the rotation of agitating shaft 5 drives spiral agitator 6 to rotate, and solidliquid mixture is rotated together with spiral agitator 6, in spiral shell
It revolves during blender 6 rotates, Stirring is carried out to solidliquid mixture, enables solid in solidliquid mixture and liquid fastly
Speed separation stirs block 62 because the reason of contact with solidliquid mixture ceaselessly during 6 Stirring of spiral agitator
It is overturning, spiral agitator 6 can be accelerated to carry out Stirring to solidliquid mixture in this way；When spiral agitator work 6 makees one section
After time, the solid in solidliquid mixture and liquid are basically separated at this time, open electrically operated valve 4, the solid in solidliquid mixture
Enter in solid case 8 after being rotated with spiral agitator 6 from discharge port 7, is then contacted with PTFE overlay film 9；PTFE overlay film 9 can be with
Liquid remaining in solid is filtered, the solid guaranteed is free of liquid component, further improves solidliquid mixture
The filter effect of middle solid.
As a kind of specific embodiment of the invention, the lower section of the spiral agitator 6 is equipped with by-pass filtration unit 10,
By-pass filtration unit 10 carries out by-pass filtration to the liquid in solidliquid mixture；The by-pass filtration unit 10 include partition 101,
Rubber bumps 102 and woven dacron 103；The side wall of the partition 101 and work box 3 is affixed, and partition 101 is rubber material；Institute
The top that rubber bumps 102 are uniformly arranged in partition 101 is stated, rubber bumps 102 and spiral agitator 6 completely attach to, and phase
Honeycomb hole 104 is equipped between adjacent rubber bumps 102, honeycomb hole 104 is uniformly provided in partition 101；The woven dacron 103
It is coated on the surface that rubber bumps 102 are contacted with spiral agitator 6, woven dacron 103 does not enter consolidating in solid case for collecting
Body residue；The present invention can carry out level-one mistake to the liquid flowed down from spiral agitator 6 by setting by-pass filtration unit 10
Solid component remaining in liquid, is collected by filter by woven dacron 103, improves the filtering effect of liquid in solidliquid mixture
Fruit.
As a kind of specific embodiment of the invention, the honeycomb hole 104 is equipped with close to the opening of rubber bumps 102
Chamfering, chamfering are used cooperatively with rubber bumps 102；Spiral agitator 6, which squeezes rubber bumps 102 in rotation, makes rubber bumps
102 are collapsible into honeycomb hole 104 along the direction of chamfering, cause pneumatics in honeycomb hole 104, when spiral agitator 6 stops operating
When, rubber bumps 102 restore to the original state, and the pressure in honeycomb hole 104 is less than the pressure outside honeycomb hole 104 at this time, and liquid can be fast
Speed is inhaled into honeycomb hole 104 to achieve the purpose that quickly to filter, and improves the working efficiency of this equipment.
Squeezing rubber bumps 102 when spiral agitator 6 is in rotation is collapsible into rubber bumps 102 along the direction of chamfering
In honeycomb hole 104, pneumatics in honeycomb hole 104 is caused；When the solid on spiral agitator 6 in solidliquid mixture is received by solid case 8
After collection, motor 1 stops operating, and rubber bumps 102 restore to the original state when spiral agitator 6 stops operating, at this time in honeycomb hole 104
Pressure is less than the pressure outside honeycomb hole 104, and the liquid in solidliquid mixture is inhaled into honeycomb hole after the filtering of woven dacron 103
In 104, it is discharged by honeycomb hole 104.
As a kind of specific embodiment of the invention, the lower section of the by-pass filtration unit 10 is equipped with secondary filtration unit
11, secondary filtration unit 11 carries out secondary filter to the liquid flowed out from by-pass filtration unit 10；The secondary filtration unit 11
The raised plate 113, three of support plate 111, No.1 raised plate No. 112, two numbers raised plate 114 including inverse Ba type, 115 and of liquid outlet
Liquid collecting box 116；The support plate 111 and the side wall of work box 3 are affixed, 112, No. two 113 and of raised plate of No.1 raised plate
No. three raised plates 114 are uniformly distributed in the top of support plate 111, and the protrusion of raised plate 113, three of No.1 raised plate 112, two
Plate 114 is affixed with support plate 111；The number of the No.1 raised plate 112, No. two raised plates, 113, No. three raised plates 114 is equal
It is four pieces, No. two raised plates 113 are located at the inside of No.1 raised plate 112, and No. two raised plates 113 are uniformly distributed in adjacent one
The opening of number raised plate 112；No. three raised plates 114 are located at the inside of No. two raised plates 113, and No. three raised plates 114
It is uniformly distributed in the opening of No. two adjacent raised plates 113；The liquid outlet 115 is located at the inside of No. three raised plates 114, and one
Number raised plate 114 of raised plate 113, three of raised plate 112, two and support plate 111, which are used cooperatively, carries out layering to liquid；
The liquid collecting box 116 is located at the lower section of liquid outlet 115；The present invention, can be to from level-one by design secondary filtration unit 11
The liquid that filter element 10 flows out carries out secondary filter, passes through the raised plate of raised plate 113, three of No.1 raised plate 112, two
114 are used cooperatively the filtering effect that liquid in solidliquid mixture is further promoted to liquid progress layering with support plate 111
Fruit.
As a kind of specific embodiment of the invention, the protrusion of raised plate 113, three of the No.1 raised plate 112, two
The cross sectional shape of plate 114 is arch, and the raised plate 114 of raised plate 113, three of bowed No.1 raised plate 112, two is
Hollow structure；The raised plate 114 of raised plate 113, three of No.1 raised plate 112, two of hollow structure is guaranteeing to mix solid-liquid
Under the premise of liquid in object carries out layering, the rate of liquid flowing is improved, improves the speed of liquid filtering.
As a kind of specific embodiment of the invention, the top of the support plate 111 is spread according to the shape of support plate 111
Equipped with one layer of woven dacron 103, woven dacron 103 is connect by annular magnet 105 with the side wall of work box 3, passes through annular magnet 105
Magnetic force woven dacron 103 is adsorbed on the side wall of work box 3, woven dacron 103 for collect not by 10 mistake of by-pass filtration unit
The solid residue of filter；The present invention, can be to by by-pass filtration unit 10 by wrapping up one layer of woven dacron 103 in support plate 111
The solid residue of filtering is for re-filtering, and the ingredient of solid, and woven dacron 103 and work box are free of in the liquid guaranteed
1 side wall is connected by annular magnet 105, when the solid residue on woven dacron 103 is excessive, annular magnet 105 can be taken
Under, it then clears up to removing woven dacron 103, woven dacron 103 is facilitated using the fixed woven dacron 103 of annular magnet 105
Cleaning and replacement, that is, improve the service life of this equipment.
After the liquid in solidliquid mixture is discharged out of honeycomb hole 104, on the woven dacron 103 in support plate 111,
Woven dacron 103 above liquid outlet 115 collects the solid residue in liquid, during collection, supersonic generator
Work, shakes woven dacron, prevents the solid residue collected blocking woven dacron 103, while also accelerating the speed of liquid filtering,
Liquid drops into liquid outlet 115 vertically from woven dacron 103 at this time；And the liquid for falling into 111 two sides of support plate, through washing
After synthetic fibre cloth 103 filters, most of liquid obliquely flows into No. two protrusions 113 from the opening of adjacent No.1 raised plate 112
At plate, a small amount of liquid by woven dacron 103 filtering after from the hollow part of No.1 raised plate 112 obliquely flow into No. two it is convex
At starting board 113；Pass through 103 mistake of woven dacron of No. two 113 sides of raised plate into most of liquid of No. two 113 sides of raised plate
It after filter, is obliquely flowed into from No. three raised plates 114 from the opening of adjacent No. two raised plates 113, a small amount of liquid passes through
Woven dacron 103 obliquely flows into from No. three raised plates 114 after filtering from the hollow part of No. two risers 113, convex into No. three
Most of liquid of 114 side of starting board is after the woven dacron 103 of No. three 114 sides of raised plate filters, from adjacent No. three protrusions
The opening of plate 114 obliquely flows into liquid outlet 115, and a small amount of liquid is after the filtering of woven dacron 103 from No. three protrusions
The hollow part of plate 114 obliquely flows into liquid outlet 115, and final liquid is flowed out from liquid outlet 115 to be received by liquid collecting box 116
Collection.
When work, the solidliquid mixture for being mixed with magnetic active carbon is imported first from feed inlet 2, starts motor 1, motor 1
Rotation drives agitating shaft 5 to rotate, and the rotation of agitating shaft 5 drives spiral agitator 6 to rotate, and solidliquid mixture is with spiral agitator 6
It rotates together, during spiral agitator 6 rotates, Stirring is carried out to solidliquid mixture, is made in solidliquid mixture
Solid and liquid energy quick separating stir block 62 because connecing with solidliquid mixture during 6 Stirring of spiral agitator
The reason of touching, is ceaselessly overturning, and spiral agitator 6 can be accelerated to carry out Stirring to solidliquid mixture in this way；When spiral is stirred
It mixes after device work 6 makees a period of time, the solid in solidliquid mixture and liquid are basically separated at this time, open electrically operated valve 4, and solid-liquid is mixed
It closes after the solid in object is rotated with spiral agitator 6 and enters in solid case 8 from discharge port 7, then contacted with PTFE overlay film 9；
Liquid remaining in solid can be filtered by PTFE overlay film 9, and the solid guaranteed is free of liquid component, be further increased
The filter effect of solid in solidliquid mixture；Squeezing rubber bumps 102 when spiral agitator 6 is in rotation makes rubber bumps
102 are collapsible into honeycomb hole 104 along the direction of chamfering, cause pneumatics in honeycomb hole 104；When solid-liquid is mixed on spiral agitator 6
The solid in object is closed by after the collection of solid case 8, motor 1 stops operating, and rubber bumps 102 are extensive when spiral agitator 6 stops operating
Shape is restored, the pressure in honeycomb hole 104 is less than the pressure outside honeycomb hole 104 at this time, and the liquid in solidliquid mixture passes through terylene
Cloth 103 is inhaled into honeycomb hole 104 after filtering, and is discharged by honeycomb hole 104；When the liquid in solidliquid mixture is from honeycomb hole
In 104 after discharge, on the woven dacron 103 in support plate 111, the woven dacron 103 above liquid outlet 115 will be in liquid
Solid residue collect during collection, supersonic generator work shakes woven dacron, prevents the solid residue collected stifled
Woven dacron 103 is filled in, while also accelerating the speed of liquid filtering, liquid drops into liquid outlet from woven dacron 103 vertically at this time
In 115；And the liquid for falling into 111 two sides of support plate, after the filtering of woven dacron 103, most of liquid is convex from adjacent No.1
Obliquely flowed into the opening of starting board 112 at No. two 113 plates of protrusion, a small amount of liquid by woven dacron 103 filtering after from
The hollow part of No.1 raised plate 112 obliquely flows at No. two raised plates 113；Into the big of No. two 113 sides of raised plate
After the woven dacron 103 of No. two 113 sides of raised plate filters, the opening from adjacent No. two raised plates 113 is in partially liq
Skewed to flow at No. three raised plates 114, a small amount of liquid is after the filtering of woven dacron 103 from the hollow of No. two risers 113
Place obliquely flows at No. three raised plates 114, and most of liquid into No. three 114 sides of raised plate passes through No. three protrusions
After the woven dacron 103 of 114 side of plate filters, liquid outlet is obliquely flowed into from the opening of adjacent No. three raised plates 114
115, a small amount of liquid obliquely flows into liquid outlet 115 from the hollow part of No. three raised plates 114 after the filtering of woven dacron 103
Interior, final liquid is flowed out from liquid outlet 115 to be collected by liquid collecting box 116.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the above embodiments and description only describe originals of the invention
Reason, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes and improvements
It all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent circle
It is fixed.
Claims (6)
1. a kind of chemical material solid-liquid separating method, it is characterised in that: method includes the following steps:
S1: it will be put into magnetic active carbon in solidliquid mixture, and stir evenly；
S2: the solidliquid mixture that magnetic active carbon is mixed in S1 is led to from the feed inlet in chemical field solid-liquid separating equipment
Enter, starts chemical field with solid-liquid separating equipment and preliminary Stirring is carried out to solidliquid mixture；
S3: supersonic generator is set at secondary filtration unit in chemical field solid-liquid separating equipment；Work as solidliquid mixture
In water pass through secondary filtration unit when, supersonic generator work；
Wherein, chemical field solid-liquid separating equipment described in S2, including motor (1), feed inlet (2), work box (3), electricity
Movable valve (4) and controller；The controller is for controlling the work of solidliquid mixture separation equipment；The feed inlet (2) is located at
Side at the top of work box (3)；The motor (1) is located at the middle part of work box (3) top outer and vertical with work box (3) sets
It sets, its output end passes through the top of work box (3) and extends in work box (3)；The output end and agitating shaft of the motor (1)
(5) top is affixed, and the bottom of agitating shaft (5) is connected with spiral agitator (6), and spiral agitator (6) is used to mix solid-liquid
Object row is sirred and separated；It is uniformly provided with through-hole (61) on the side wall of paddle in the spiral agitator (6), is equipped with and turns in through-hole
Motion block (62) stirs block (62) and is rotatablely connected by the side wall of shaft (63) and through-hole (61), stirs block (62) and mix with solid-liquid
Object is overturn when contacting；The side of the spiral agitator (6) is equipped with discharge port (7), and electrically operated valve (4) is arranged in discharge port (7)
Interior, the lower section of discharge port (7) is connected to solid case (8), and solid case (8) is for collecting the solid after Stirring；The solid case
(8) PTFE overlay film (9) are equipped in, PTFE overlay film (9) and the side wall of solid case (8) are affixed, and PTFE overlay film (9) was used for filter solid
The liquid of middle remnants.
2. a kind of chemical material solid-liquid separating method according to claim 1, it is characterised in that: the spiral agitator
(6) lower section is equipped with by-pass filtration unit (10), and by-pass filtration unit (10) carries out level-one mistake to the liquid in solidliquid mixture
Filter；The by-pass filtration unit (10) includes partition (101), rubber bumps (102) and woven dacron (103)；The partition (101)
It is affixed with the side wall of work box (3), and partition (101) is rubber material；The rubber bumps (102) are uniformly arranged in partition
(101) top, rubber bumps (102) and spiral agitator (6) completely attach to, and set between adjacent rubber bumps (102)
Have honeycomb hole (104), honeycomb hole (104) is uniformly provided in partition (101)；The woven dacron (103) is coated on rubber convex
The surface that (102) are contacted with spiral agitator (6) is played, woven dacron (103) is for collecting the solid residue not entered in solid case.
3. a kind of chemical material solid-liquid separating method according to claim 2, it is characterised in that: the honeycomb hole (104)
Opening close to rubber bumps (102) is equipped with chamfering, and chamfering is used cooperatively with rubber bumps (102).
4. a kind of chemical material solid-liquid separating method according to claim 2, it is characterised in that: the by-pass filtration unit
(10) lower section is equipped with secondary filtration unit (11), and secondary filtration unit (11) is to the liquid flowed out from by-pass filtration unit (10)
Carry out secondary filter；The secondary filtration unit (11) includes the support plate (111) of inverse Ba type, No.1 raised plate (112), two
Number raised plate (113), No. three raised plates (114), liquid outlet (115) and liquid collecting box (116)；The support plate (111) with
The side wall of work box (3) is affixed, and No.1 raised plate (112), No. two raised plates (113) and No. three raised plates (114) are uniformly distributed
In the top of support plate (111), and No.1 raised plate (112), No. two raised plates (113), No. three raised plates (114) with support
Plate (111) is affixed；The No.1 raised plate (112), No. two raised plates (113), No. three raised plates (114) number be four
Block, No. two raised plates (113) are located at the inside of No.1 raised plate (112), and No. two raised plates (113) be uniformly distributed in it is adjacent
The opening of No.1 raised plate (112)；No. three raised plates (114) are located at the inside of No. two raised plates (113), and No. three convex
Starting board (114) is uniformly distributed in the opening of No. two adjacent raised plates (113)；The liquid outlet (115) is located at No. three protrusions
The inside of plate (114), No.1 raised plate (112), No. two raised plates (113), No. three raised plates (114) are matched with support plate (111)
It closes use and layering is carried out to liquid；The liquid collecting box (116) is located at the lower section of liquid outlet (115).
5. a kind of chemical material solid-liquid separating method according to claim 4, it is characterised in that: the No.1 raised plate
(112), No. two raised plates (113), No. three raised plates (114) cross sectional shape be arch, and bowed No.1 raised plate
(112), No. two raised plates (113), No. three raised plates (114) are hollow structure.
6. a kind of chemical material solid-liquid separating method according to claim 4, it is characterised in that: the support plate (111)
Top be equipped with one layer of woven dacron (103) according to the shape of support plate (111), woven dacron (103) passes through annular magnet (105)
It is connect with the side wall of work box (3), woven dacron (103) is adsorbed in the side of work box (3) by the magnetic force of annular magnet (105)
On wall, woven dacron (103) is used to collect the solid residue not filtered by by-pass filtration unit (10).
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| CN201811279786.XA CN109126270B (en) | 2018-10-30 | 2018-10-30 | Solid-liquid separation method for chemical materials |
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Address after: 12 km north street, Xinqiang Town, Yueyang County, Yueyang City, Hunan Province Patentee after: Fubon Xiangyu (Yueyang) Biotechnology Co.,Ltd. Country or region after: China Address before: 12 km north street, Xinqiang Town, Yueyang County, Yueyang City, Hunan Province Patentee before: Xiangyu Biotechnology (Yueyang) Co.,Ltd. Country or region before: China |