CN109044883A - One kind is frivolous persistently to stay color lip glaze and preparation method thereof - Google Patents
One kind is frivolous persistently to stay color lip glaze and preparation method thereof Download PDFInfo
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- CN109044883A CN109044883A CN201811015391.9A CN201811015391A CN109044883A CN 109044883 A CN109044883 A CN 109044883A CN 201811015391 A CN201811015391 A CN 201811015391A CN 109044883 A CN109044883 A CN 109044883A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 125000003118 aryl group Chemical group 0.000 claims abstract description 15
- 239000002904 solvent Substances 0.000 claims abstract description 15
- 239000002562 thickening agent Substances 0.000 claims abstract description 15
- -1 phenyl dimethicones Chemical class 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 10
- CUNWUEBNSZSNRX-RKGWDQTMSA-N (2r,3r,4r,5s)-hexane-1,2,3,4,5,6-hexol;(z)-octadec-9-enoic acid Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO.OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO.CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O CUNWUEBNSZSNRX-RKGWDQTMSA-N 0.000 claims abstract description 9
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 9
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 9
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960005323 phenoxyethanol Drugs 0.000 claims abstract description 9
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 9
- 229920005573 silicon-containing polymer Polymers 0.000 claims abstract description 9
- 229960005078 sorbitan sesquioleate Drugs 0.000 claims abstract description 9
- ZCTXEAQXZGPWFG-UHFFFAOYSA-N imidurea Chemical compound O=C1NC(=O)N(CO)C1NC(=O)NCNC(=O)NC1C(=O)NC(=O)N1CO ZCTXEAQXZGPWFG-UHFFFAOYSA-N 0.000 claims abstract description 8
- CKQVRZJOMJRTOY-UHFFFAOYSA-N octadecanoic acid;propane-1,2,3-triol Chemical compound OCC(O)CO.CCCCCCCCCCCCCCCCCC(O)=O CKQVRZJOMJRTOY-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229950008882 polysorbate Drugs 0.000 claims abstract description 6
- 229920000136 polysorbate Polymers 0.000 claims abstract description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000011265 semifinished product Substances 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 239000005022 packaging material Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 238000000265 homogenisation Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- 238000013019 agitation Methods 0.000 claims description 9
- 238000010583 slow cooling Methods 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- 238000004458 analytical method Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001514 detection method Methods 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 235000009508 confectionery Nutrition 0.000 claims 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 4
- 230000003020 moisturizing effect Effects 0.000 abstract description 4
- 239000002537 cosmetic Substances 0.000 abstract description 3
- 239000003086 colorant Substances 0.000 abstract description 2
- 238000009738 saturating Methods 0.000 abstract description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 7
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 5
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 5
- 238000003556 assay Methods 0.000 description 5
- 238000009775 high-speed stirring Methods 0.000 description 5
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 239000004005 microsphere Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000600 sorbitol Substances 0.000 description 2
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 description 1
- 241001502050 Acis Species 0.000 description 1
- 229920002367 Polyisobutene Polymers 0.000 description 1
- 241000221095 Simmondsia Species 0.000 description 1
- 235000004433 Simmondsia californica Nutrition 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000013475 authorization Methods 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- NPAXBRSUVYCZGM-UHFFFAOYSA-N carbonic acid;propane-1,2-diol Chemical compound OC(O)=O.CC(O)CO NPAXBRSUVYCZGM-UHFFFAOYSA-N 0.000 description 1
- OGQYPPBGSLZBEG-UHFFFAOYSA-N dimethyl(dioctadecyl)azanium Chemical compound CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC OGQYPPBGSLZBEG-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 1
- 229910000271 hectorite Inorganic materials 0.000 description 1
- 125000002632 imidazolidinyl group Chemical group 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to cosmetic technical field, it is specifically a kind of it is frivolous persistently stay color lip glaze, be grouped as by each group of following parts by weight: A phase component: 50.5~62 parts of solvent, 0.5~0.8 part of thickener；B phase component: 18~20 parts of trimethyl silicane alcoxyl phenyl dimethicones, 5~10 parts of tridecanol trimellitate, 4~4.5 parts of ring five dimethyl silicone polymer, 3~5 parts of the smooth stearate of sorb, 1.5~2.5 parts of sorbitan sesquioleate, 1.5~2.5 parts of stearine, 1.5~2 parts of polysorbate -20,0.3~0.7 part of Phenoxyethanol, 0.2~0.4 part of imidazolidinyl urea；C phase component: colorant；D phase component: aromatic；Also disclose preparation method.The present invention has the advantages that lip glaze contains up to 50% moisture, moisturizing effect can effectively be reached, cooperate special producing technique, with light, thin, saturating, staying color persistently to break, previous lip glaze is thick and heavy, greasy, uneven color is even, fades, the adornment effect sense of viscous cup, easily de- adornment in use feeling.
Description
Technical field
It is especially a kind of frivolous persistently to stay color lip glaze and preparation method thereof the present invention relates to cosmetic technical field.
Background technique
Lip glaze belongs to one kind of lip Cosmetics single-item, can achieve the effect that lipstick and lip gloss can not show using lip glaze.
Before lip glaze occurs, color make-up teacher can manufacture bright-coloured bright plump lip adornment effect plus transparent lip gloss on bright red lipstick surface.Lip
The bright texture two-in-one that is full of of the saturation color of lipstick and lip gloss is only needed gently one brush lip glaze, so that it may realize easily by glaze.
The Chinese patent that Authorization Notice No. is CN104644473B, authorized announcement date is on December 05th, 2017 discloses one
The slim and graceful soft and smooth lasting lip glaze of kind comprising following components in percentage by weight: distearyl dimethylammonium hectorite 1.44~
2.16%, propylene glycol carbonate 0.4~0.6%, polyisobutene 31~58%, jojoba seed oil 8~12%, the different different nonyl of tridecanol
Acid esters 5~8%, colorant 6~12%, ring five dimethyl silicone polymer 13.16~19.24%, trimethyl silicane alkoxy esters of silicon acis
4.55~6.5%, poly- propyl silsesquioxane 2.45~3.5%, microsphere 1~5%, the weight percent of the above components it
Be 100%.By the particle properties using microsphere, the sticky sense of lip glaze is improved, to increase the persistence of lip glaze.
Above-mentioned lasting lip glaze has preferably glutinous soapy feeling, relatively frivolous, so that lip glaze makes after being attached to user's lip
It obtains user's lip to be closed and the relatively dry that seems, moisture retention is insufficient.
Summary of the invention
The purpose of the present invention is to overcome the shortcomings of the existing technology, provides and a kind of frivolous persistently stays color lip glaze and its preparation side
Method.
The purpose of the present invention is achieved through the following technical solutions: one kind is frivolous persistently to stay color lip glaze, by following parts by weight
Each group be grouped as:
A phase component: 50.5~62 parts of solvent, 0.5~0.8 part of thickener；
B phase component: 18~20 parts of trimethyl silicane alcoxyl phenyl dimethicones, tridecanol trimellitate 5~
10 parts, 4~4.5 parts of ring five dimethyl silicone polymer, 3~5 parts of the smooth stearate of sorb, sorbitan sesquioleate 1.5~2.5
Part, 1.5~2.5 parts of stearine, 1.5~2 parts of polysorbate -20,0.3~0.7 part of Phenoxyethanol, imidazolidinyl
0.2~0.4 part of urea；
C phase component: 15,850 0.05~0.15 part of CI, 45,410 0.05~0.15 part of CI, CI 77,891 0.06~
0.12 part, 77,499 0.05~0.15 part of CI, 19,140 0.1~0.2 part of CI；
D phase component: 0.05~0.2 part of aromatic.
Further, described one kind is frivolous persistently stays color lip glaze, is grouped as by each group of following parts by weight:
A phase component: 58 parts of solvent, 0.65 part of thickener；
B phase component: 19 parts of trimethyl silicane alcoxyl phenyl dimethicones, 8 parts of tridecanol trimellitate, ring five
4 parts of the smooth stearate of 4.2 parts of dimethyl silicone polymer, sorb, 2 parts of stearine, gathers 2 parts of sorbitan sesquioleate
1.7 parts of sorbitol ester -20,0.5 part of Phenoxyethanol, 0.3 part of imidazolidinyl urea；
C phase component: 15,850 0.1 parts of CI, 45,410 0.1 parts of CI, 77,891 0.09 parts of CI, 77,499 0.1 parts of CI,
19,140 0.15 parts of CI；
D phase component: 0.12 part of aromatic.
Further, the solvent includes 50~60 parts of water, 0.5~2 part of ethyl alcohol.
Further, the thickener is hydroxyethyl cellulose.
Further, the aromatic is essence.
The frivolous preparation method for persistently staying color lip glaze of described one kind, comprising the following steps:
S1, amount weighs each component in proportion, spare；
S2, by A phase component investment high-voltage high-speed stirring homogenizer in homogeneous, homogeneous built-in temperature control 55~65 DEG C it
Between；
S3, after mixing evenly, is poured into normal agitation machine, when slow cooling is to 40~43 DEG C, sequentially adds B phase component, C
Phase component and D phase component, stir evenly, are cooled to room temperature, and standing 20~for 24 hours, discharging；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates, system with pressure mill by S5, the requirement according to client
At semi-finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production carried out to the powder agglomates of semi-finished product, finished product is made, identify,
It is put in storage after the assay was approved.
Further, in step S2, the step of by homogenizer homogeneous are as follows: two sections high-pressure homogeneous, wherein one section of homogeneous pressure
Power is 120~160MPa, homogeneous 1000~1200mL/min of speed, and homogenizing time is 7~8s, two sections of homogenization pressures are 180~
220MPa, homogeneous 800~1000mL/min of speed, homogenizing time are 7~8s.
Further, in step S3, mixing speed is 600~800rpm, stirs 20~30min, and use positive and negative alternate
Paddling process is stirred, and positive and negative alternate time interval is 1~2min.
Further, in step S3, the cooling rate of slow cooling is 1~2 DEG C/min.
The invention has the following advantages that
1, lip glaze of the invention contains up to 50% moisture, can effectively reach moisturizing effect, cooperates special producing technique,
With light, thin, saturating, staying color persistently to break, previous lip glaze is thick and heavy, greasy, uneven color is even, fades, viscous cup, easily de- adornment in use feeling
Adornment imitate sense.
2, lip glaze ductility beautiful in colour of the invention is strong, contains the polishing degree of saturation, and moisturizing ingredient abundant is effectively breathed out
Delicate lip flesh is protected, enables lips water tender bright, the penetrating lip adornment effect of nature is presented in long-acting moisturizing.When makeup, there is ice to feel well refrigerant
Sense, color development is all good, and adornment is imitated persistently up to 12 hours.
Specific embodiment
Below with reference to embodiment, the present invention will be further described, but protection scope of the present invention is not limited to following institute
It states.
[embodiment 1]:
One kind is frivolous persistently to stay color lip glaze, is grouped as by each group of following parts by weight:
A phase component: 50.5 parts of solvent, 0.8 part of thickener；
B phase component: 18 parts of trimethyl silicane alcoxyl phenyl dimethicones, 5 parts of tridecanol trimellitate, ring five
5 parts of the smooth stearate of 4.5 parts of dimethyl silicone polymer, sorb, 1.5 parts of sorbitan sesquioleate, stearine 2.5
Part, 2 parts of polysorbate -20,0.3 part of Phenoxyethanol, 0.4 part of imidazolidinyl urea；
C phase component: 15,850 0.05 parts of CI, 45,410 0.15 parts of CI, 77,891 0.06 parts of CI, CI 77,499 0.15
Part, 19,140 0.1 parts of CI；
D phase component: 0.2 part of aromatic.
Further, the solvent includes 50 parts of water, 0.5 part of ethyl alcohol.
Further, the thickener is hydroxyethyl cellulose.
Further, the aromatic is essence.
The frivolous preparation method for persistently staying color lip glaze of described one kind, comprising the following steps:
S1, amount weighs each component in proportion, spare；
S2, by homogeneous in A phase component investment high-voltage high-speed stirring homogenizer, the step of homogeneous are as follows: two sections high-pressure homogeneous,
In one section of homogenization pressure be 160MPa, homogeneous speed 1000mL/min, homogenizing time 8s, two sections of homogenization pressures are 180MPa,
Homogeneous speed 800mL/min, homogenizing time 7s, the control of homogeneous built-in temperature is at 65 DEG C；
S3, after mixing evenly, is poured into normal agitation machine, mixing speed 800rpm, stirs 20min, and using positive and negative
Alternate agitation method is stirred, and positive and negative alternate time interval is 2min, and when slow cooling is to 43 DEG C, cooling rate is 2 DEG C/min,
B phase component, C phase component and D phase component are sequentially added, stirs evenly, is cooled to room temperature, stands 20h, discharging；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates, system with pressure mill by S5, the requirement according to client
At semi-finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production carried out to the powder agglomates of semi-finished product, finished product is made, identify,
It is put in storage after the assay was approved.
[embodiment 2]:
One kind is frivolous persistently to stay color lip glaze, is grouped as by each group of following parts by weight:
A phase component: 58 parts of solvent, 0.65 part of thickener；
B phase component: 19 parts of trimethyl silicane alcoxyl phenyl dimethicones, 8 parts of tridecanol trimellitate, ring five
4 parts of the smooth stearate of 4.2 parts of dimethyl silicone polymer, sorb, 2 parts of stearine, gathers 2 parts of sorbitan sesquioleate
1.7 parts of sorbitol ester -20,0.5 part of Phenoxyethanol, 0.3 part of imidazolidinyl urea；
C phase component: 15,850 0.1 parts of CI, 45,410 0.1 parts of CI, 77,891 0.09 parts of CI, 77,499 0.1 parts of CI,
19,140 0.15 parts of CI；
D phase component: 0.12 part of aromatic.
Further, the solvent includes 57 parts of water, 1 part of ethyl alcohol.
Further, the thickener is hydroxyethyl cellulose.
Further, the aromatic is essence.
The frivolous preparation method for persistently staying color lip glaze of described one kind, comprising the following steps:
S1, amount weighs each component in proportion, spare；
S2, by homogeneous in A phase component investment high-voltage high-speed stirring homogenizer, the step of homogeneous are as follows: two sections high-pressure homogeneous,
In one section of homogenization pressure be 140MPa, homogeneous speed 1100mL/min, homogenizing time 7.5s, two sections of homogenization pressures are
200MPa, homogeneous speed 900mL/min, homogenizing time 7.5s, the control of homogeneous built-in temperature is at 60 DEG C；
S3, after mixing evenly, pours into normal agitation machine, sequentially adds B phase component, C phase component and D phase component, stirs
Uniformly, mixing speed 700rpm is stirred 25min, and is stirred using positive and negative alternate paddling process, positive and negative alternate time interval
For 1.5min, when slow cooling is to 42 DEG C, cooling rate is 1.5 DEG C/min, is cooled to room temperature, and 22h, discharging are stood；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates, system with pressure mill by S5, the requirement according to client
At semi-finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production carried out to the powder agglomates of semi-finished product, finished product is made, identify,
It is put in storage after the assay was approved.
[embodiment 3]:
One kind is frivolous persistently to stay color lip glaze, is grouped as by each group of following parts by weight:
A phase component: 62 parts of solvent, 0.5 part of thickener；
B phase component: 20 parts of trimethyl silicane alcoxyl phenyl dimethicones, 10 parts of tridecanol trimellitate, ring
Five 4 parts of dimethyl silicone polymers, 3 parts of the smooth stearate of sorb, 2.5 parts of sorbitan sesquioleate, stearine 1.5
Part, 1.5 parts of polysorbate -20,0.7 part of Phenoxyethanol, 0.2 part of imidazolidinyl urea；
C phase component: 15,850 0.15 parts of CI, 45,410 0.05 parts of CI, 77,891 0.12 parts of CI, CI 77,499 0.05
Part, 19,140 0.2 parts of CI；
D phase component: 0.05 part of aromatic.
Further, the solvent includes 60 parts of water, 2 parts of ethyl alcohol.
Further, the thickener is hydroxyethyl cellulose.
Further, the aromatic is essence.
The frivolous preparation method for persistently staying color lip glaze of described one kind, comprising the following steps:
S1, amount weighs each component in proportion, spare；
S2, by homogeneous in A phase component investment high-voltage high-speed stirring homogenizer, the step of homogeneous are as follows: two sections high-pressure homogeneous,
In one section of homogenization pressure be 120MPa, homogeneous speed 1200mL/min, homogenizing time 7s, two sections of homogenization pressures are 220MPa,
Homogeneous speed 1000mL/min, homogenizing time 8s, the control of homogeneous built-in temperature is between 55 DEG C；
S3, after mixing evenly, is poured into normal agitation machine, mixing speed 600rpm, stirs 30min, and using positive and negative
Alternate agitation method is stirred, and positive and negative alternate time interval is 1min, and when slow cooling is to 40 DEG C, cooling rate is 1 DEG C/min,
B phase component, C phase component and D phase component are sequentially added, stirs evenly, is cooled to room temperature, stands discharging for 24 hours；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates, system with pressure mill by S5, the requirement according to client
At semi-finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production carried out to the powder agglomates of semi-finished product, finished product is made, identify,
It is put in storage after the assay was approved.
[embodiment 4]:
One kind is frivolous persistently to stay color lip glaze, is grouped as by each group of following parts by weight:
A phase component: 58 parts of solvent, 0.7 part of thickener；
B phase component: 19 parts of trimethyl silicane alcoxyl phenyl dimethicones, 5 parts of tridecanol trimellitate, ring five
4 parts of the smooth stearate of 4.5 parts of dimethyl silicone polymer, sorb, 1.8 parts of sorbitan sesquioleate, stearine 1.9
Part, 1.6 parts of polysorbate -20,0.6 part of Phenoxyethanol, 0.3 part of imidazolidinyl urea；
C phase component: 15,850 0.08 parts of CI, 45,410 0.07 parts of CI, 77,891 0.1 parts of CI, CI 77,499 0.1
Part, 19,140 0.15 parts of CI；
D phase component: 0.1 part of aromatic.
Further, the solvent includes 56 parts of water, 2 parts of ethyl alcohol.
Further, the thickener is hydroxyethyl cellulose.
Further, the aromatic is essence.
The frivolous preparation method for persistently staying color lip glaze of described one kind, comprising the following steps:
S1, amount weighs each component in proportion, spare；
S2, by homogeneous in A phase component investment high-voltage high-speed stirring homogenizer, the step of homogeneous are as follows: two sections high-pressure homogeneous,
In one section of homogenization pressure be 150MPa, homogeneous speed 1150mL/min, homogenizing time 7.5s, two sections of homogenization pressures are
200MPa, homogeneous speed 990mL/min, homogenizing time 7.5s, the control of homogeneous built-in temperature is at 62 DEG C；
S3, after mixing evenly, is poured into normal agitation machine, mixing speed 800rpm, stirs 30min, and using positive and negative
Alternate agitation method is stirred, and positive and negative alternate time interval is 1min, and when slow cooling is to 41 DEG C, cooling rate is 1 DEG C/min,
B phase component, C phase component and D phase component are sequentially added, stirs evenly, is cooled to room temperature, stands 21h, discharging；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates, system with pressure mill by S5, the requirement according to client
At semi-finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production carried out to the powder agglomates of semi-finished product, finished product is made, identify,
It is put in storage after the assay was approved.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (9)
1. one kind is frivolous persistently to stay color lip glaze, it is characterised in that: be grouped as by each group of following parts by weight:
A phase component: 50.5~62 parts of solvent, 0.5~0.8 part of thickener；
B phase component: 18~20 parts of trimethyl silicane alcoxyl phenyl dimethicones, 5~10 parts of tridecanol trimellitate,
It is 3~5 parts of the smooth stearate of 4~4.5 parts of ring five dimethyl silicone polymer, sorb, 1.5~2.5 parts of sorbitan sesquioleate, sweet
1.5~2.5 parts of oleostearin acid esters, 1.5~2 parts of polysorbate -20,0.3~0.7 part of Phenoxyethanol, imidazolidinyl urea 0.2
~0.4 part；
C phase component: 15,850 0.05~0.15 part of CI, 45,410 0.05~0.15 part of CI, CI 77,891 0.06~0.12
Part, 77,499 0.05~0.15 part of CI, 19,140 0.1~0.2 part of CI；
D phase component: 0.05~0.2 part of aromatic.
2. one kind according to claim 1 is frivolous persistently to stay color lip glaze, it is characterised in that: by each component of following parts by weight
Composition:
A phase component: 58 parts of solvent, 0.65 part of thickener；
B phase component: 19 parts of trimethyl silicane alcoxyl phenyl dimethicones, 8 parts of tridecanol trimellitate, ring five poly- two
4 parts of the smooth stearate of 4.2 parts of methylsiloxane, sorb, 2 parts of sorbitan sesquioleate, 2 parts of stearine, poly- sorb
1.7 parts of alcohol ester -20,0.5 part of Phenoxyethanol, 0.3 part of imidazolidinyl urea；
C phase component: 15,850 0.1 parts of CI, 45,410 0.1 parts of CI, 77,891 0.09 parts of CI, 77,499 0.1 parts of CI, CI
19140 0.15 parts；
D phase component: 0.12 part of aromatic.
3. one kind according to claim 1 is frivolous persistently to stay color lip glaze, it is characterised in that: the solvent includes water 50~60
Part, 0.5~2 part of ethyl alcohol.
4. one kind according to claim 1 is frivolous persistently to stay color lip glaze, it is characterised in that: the thickener is that ethoxy is fine
Dimension element.
5. one kind according to claim 1 is frivolous persistently to stay color lip glaze, it is characterised in that: the aromatic is essence.
6. the frivolous preparation method for persistently staying color lip glaze of one kind described in any one, feature exist according to claim 1~5
In: the following steps are included:
S1, amount weighs each component in proportion, spare；
S2, A phase component investment high-voltage high-speed is stirred into homogeneous in homogenizer, homogeneous built-in temperature controls between 55~65 DEG C；
S3, after mixing evenly, is poured into normal agitation machine, when slow cooling is to 40~43 DEG C, sequentially adds B phase component, C phase group
Part and D phase component, stir evenly, are cooled to room temperature, and standing 20~for 24 hours, discharging；
S4, by step S3 resulting material sample detection, carry out physico-chemical analysis；
Corresponding mold and aluminum dish are carried out the production of semi-finished product powder agglomates with pressure mill, are made half by S5, the requirement according to client
Finished product；
S6, prepare packaging material and outer packaging material in corresponding, packaging production is carried out to the powder agglomates of semi-finished product, finished product is made, identify, through examining
Test warehousing after passing.
7. the frivolous preparation method for persistently staying color lip glaze of one kind according to claim 6, it is characterised in that: in step S2,
The step of by homogenizer homogeneous are as follows: two sections high-pressure homogeneous, wherein one section of homogenization pressure is 120~160MPa, homogeneous speed
1000~1200mL/min, homogenizing time are 7~8s, and two sections of homogenization pressures are 180~220MPa, homogeneous speed 800~
1000mL/min, homogenizing time are 7~8s.
8. the frivolous preparation method for persistently staying color lip glaze of one kind according to claim 6, it is characterised in that: in step S3,
Mixing speed is 600~800rpm, stirs 20~30min, and be stirred using positive and negative alternate paddling process, the positive and negative alternate time
Between be divided into 1~2min.
9. the frivolous preparation method for persistently staying color lip glaze of one kind according to claim 6, it is characterised in that: in step S3,
The cooling rate of slow cooling is 1~2 DEG C/min.
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| CN109431956A (en) * | 2018-12-27 | 2019-03-08 | 唯客乐化妆品(杭州)有限公司 | A kind of dumb light lip glaze and its preparation process |
| CN109875916A (en) * | 2019-03-18 | 2019-06-14 | 广州尚庄化妆品有限公司 | Black lip glaze of the rose at color craftsman dark night and preparation method thereof |
| CN111840109A (en) * | 2019-04-24 | 2020-10-30 | 广州莎莎生物科技有限公司 | Water-sensitive lip glaze and manufacturing process thereof |
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| CN109875916A (en) * | 2019-03-18 | 2019-06-14 | 广州尚庄化妆品有限公司 | Black lip glaze of the rose at color craftsman dark night and preparation method thereof |
| CN111840109A (en) * | 2019-04-24 | 2020-10-30 | 广州莎莎生物科技有限公司 | Water-sensitive lip glaze and manufacturing process thereof |
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Application publication date: 20181221 |