CN109022826A - Reduction refining integration smelting system - Google Patents
Reduction refining integration smelting system Download PDFInfo
- Publication number
- CN109022826A CN109022826A CN201811218687.0A CN201811218687A CN109022826A CN 109022826 A CN109022826 A CN 109022826A CN 201811218687 A CN201811218687 A CN 201811218687A CN 109022826 A CN109022826 A CN 109022826A
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- Prior art keywords
- magnesium
- pipeline
- heater
- reductive jar
- argon gas
- Prior art date
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- 238000007670 refining Methods 0.000 title claims abstract description 34
- 238000003723 Smelting Methods 0.000 title claims abstract description 15
- 230000010354 integration Effects 0.000 title claims abstract description 14
- 239000011777 magnesium Substances 0.000 claims abstract description 116
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 113
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 113
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 60
- 230000002829 reductive effect Effects 0.000 claims abstract description 40
- 239000007789 gas Substances 0.000 claims abstract description 37
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 229910052786 argon Inorganic materials 0.000 claims abstract description 31
- 238000001816 cooling Methods 0.000 claims abstract description 19
- 238000002425 crystallisation Methods 0.000 claims abstract description 14
- 239000011214 refractory ceramic Substances 0.000 claims abstract description 10
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims description 12
- 229920000742 Cotton Polymers 0.000 claims description 8
- 238000004321 preservation Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 230000005674 electromagnetic induction Effects 0.000 claims description 3
- 239000000919 ceramic Substances 0.000 claims description 2
- 239000011094 fiberboard Substances 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 20
- 238000006722 reduction reaction Methods 0.000 description 11
- 238000005266 casting Methods 0.000 description 10
- 239000012535 impurity Substances 0.000 description 9
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 8
- 239000002904 solvent Substances 0.000 description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 239000005864 Sulphur Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000009749 continuous casting Methods 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910000519 Ferrosilicon Inorganic materials 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 2
- 239000003500 flue dust Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 229910052571 earthenware Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000006056 electrooxidation reaction Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 210000004709 eyebrow Anatomy 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 238000007499 fusion processing Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000007770 graphite material Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/20—Obtaining alkaline earth metals or magnesium
- C22B26/22—Obtaining magnesium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The present invention relates to reduction refining integration smelting systems, including reductive jar, vacuum unit, crystallisation by cooling unit, argon gas protection location and magnesium liquid collector unit；Heat insulating block is set in reductive jar top, reductive jar cooling jacket is set outside reductive jar top, the upper opening of reductive jar is sealed by reductive jar upper cover；Reductive jar is connect by magnesium vapor pipeline with crystallisation by cooling unit；Crystallisation by cooling unit includes crystallizer heater upper cover, potassium sodium plate, heater and crystallizer；Vacuum unit includes vacuum line and vacuum pump；Argon gas protection location includes argon gas pipeline and argon gas feed device；Magnesium liquid collector unit includes refractory ceramics valve and magnesium liquid pipeline, and magnesium liquid pipeline is connect with heater, and the outlet of the entrance and magnesium vapor pipeline of magnesium liquid pipeline is arranged in refractory ceramics valve.The present invention solves that prior art magnesium recovery utilization rate is low, seriously polluted, operating environment is dangerous, the low problem of magnesium ingot quality.
Description
Technical field
The invention belongs to magnesium metal smelting technical fields, and in particular to a kind of reduction refining integration smelting system,
Meet refining and the ingot casting that magnesium metal crude magnesium is realized under the premise of energy conservation and environmental protection requires.
Background technique
Pidgeon process (vacuum ferrosilicon process) refines magnesium crude magnesium obtained (Crystalline Magnesium) and contains many metal impurities and nonmetallic miscellaneous
Matter cause crude magnesium (Crystalline Magnesium) volume it is big, it is loose, be not easy keeping, storage, transport, and these metal impurities can with magnesium formed merchant's method
Electrochemical corrosion occurs for Buddhist nun's battery, and magnesium plays anode, and the metal impurities such as iron and nickel play cathodic process, accelerate the corrosion of magnesium.Cause
This crude magnesium, which must refine, can be only achieved the requirement that industry directly uses.
Vacuum breaker (air vacuum breaker) takes out crystallizer after production of magnesium by pidgeonprocess obtains Crystalline Magnesium, by Crystalline Magnesium from crystallizer
Refining plant is sent into abjection.Refining solvent is added in refining process first in crucible, Crystalline Magnesium is reloaded into, in 750 DEG C of temperature
Lower heating and melting is slowly added into Crystalline Magnesium and melting solvent, when the magnesium in crucible reaches the height of crucible dischargeable capacity, makes earthenware
Magnesium liquid temperature is maintained at 710 DEG C in crucible, refining solvent is then added, while being stirred (stirring while adding), mixing time is about
10 minutes, then temperature is risen to 740 DEG C (or 720 DEG C), and stand 5 ~ 10 minutes, protected after being cooled to 710 DEG C to magnesium liquid
Temperature completes the refining of crude magnesium.Magnesium burns in refining process, need to spread the burning that covering flux prevents magnesium, prevent the oxidation of magnesium
Loss.
Continuous casting machine ingot casting is used after refining, and the crucible for filling molten magnesium is hung in into the heat preservation of tipper valve and is two-mand ladle,
Tipper tilts, and in the ingot mould in crucible on magnesium liquid injection mould ingot conveyer, during ingot casting, spreads lower sulphur powder, makes sulphur powder
It burns on magnesium ingot surface and generates sulfur dioxide gas, prevent the oxidation of magnesium, casting process is completed.
Traditional refining furnace refining crude magnesium and casting process have some disadvantages:
1, traditional method of refining using air vacuum breaker and needs first to refine crude magnesium again from crystallizer taking-up, in reduction furnace
Oxygen, nitrogen combustion generate MgO, MgN in magnesium and air during vacuum breaker in crystallizer, reduce Mg yield, produce simultaneously
Raw dust polluting environment；2, the rate of recovery of smart magnesium is generally 94% or so (Zhu Danqing brief talks ferrosilicon process magnesium in conventional refining processes
Refinery practice and content of magnesium in design, light metal 1996(5) 42-48) refining slag are higher, and waste of resource pollutes environment；3, it refines
It needs to pick and place refining copple by driving in the process, operating process is dangerous；4, refining process is discontinuous, and a large amount of Mg are turning
Oxidation loss in fortune and fusion process；5, the refining solvent added in refining process is 2# solvent, can be produced in solvent adding procedure
Raw poisonous and harmful flue dust, and these flue dust cannot be handled effectively in collection, worker operation environment is poor, seriously polluted；6, casting process
Middle Mg is oxidizable, reduces ingot casting quality；Sulphur powder is spread during ingot casting and generates sulfur dioxide gas, pollutes environment；7, solvent essence
The magnesium ingot purity that refining casting obtains is only 99.95%, and quality is lower；8, the crystallizer of conventional shaft reduction tank is built in reductive jar
In cooling jacket, Crystalline Magnesium purity can be caused low with some impurity in magnesium vapor uphill process.
Summary of the invention
The object of the present invention is to provide a kind of metallic magnesium refining and continuous casting systems, solve and magnesium exists in the prior art
Recovery utilization rate is low, seriously polluted, operating environment is dangerous, the low problem of magnesium ingot quality.
In order to achieve the above object, technical scheme is as follows:
A kind of reduction refining integration smelting system, including reductive jar, vacuum unit, crystallisation by cooling unit, argon gas protection location
With magnesium liquid collector unit；Heat insulating block is set in the reductive jar top, reductive jar cooling jacket is set outside reductive jar top, also
The upper opening of former tank is sealed by reductive jar upper cover；The reductive jar is connected by magnesium vapor pipeline and the crystallisation by cooling unit
It connects；Crystallisation by cooling unit includes crystallizer heater upper cover, potassium sodium plate, heater and crystallizer, and the crystallizer setting is adding
In hot device, potassium sodium plate is arranged in crystallizer upper end, and heater upper cover is arranged in the upper opening of heater；The vacuum unit includes vacuum
Pipeline and vacuum pump, heater connect vacuum pump by vacuum line；The argon gas protection location includes argon gas pipeline and argon gas
Feedway, heater argon gas piping connection argon gas feed device；The magnesium liquid collector unit include refractory ceramics valve and
Magnesium liquid pipeline, magnesium liquid pipeline connect with heater, and the entrance and magnesium vapor pipeline of magnesium liquid pipeline is arranged in refractory ceramics valve
Outlet.
Further, the reductive jar setting is multiple, and the magnesium vapor pipeline includes vertical section and horizontal segment, multiple reduction
Tank is connect by pipeline with the vertical section of magnesium vapor pipeline, and the horizontal segment of magnesium vapor pipeline is connect with intermediate frequency furnace.
Further, the crystallizer is made of non electromagnetic induction heating material.
Further, the crystallizer is made of graphite material.
Further, the magnesium liquid protection pipeline, magnesium vapor pipeline include pipeline body, heat-preservation cotton and heating device；
The heat-preservation cotton is wrapped in outside pipeline body, and the heating device compartment heats pipeline body.
Further, the heat insulating block is made of aluminosilicate fiberboard.
Beneficial effects of the present invention:
The present invention uses the structure put and (be placed into other than reductive jar) outside crystallizer, and impurity is passing through magnesium vapor pipeline in magnesium vapor
When, it carries out playing the role of impurity screening, the crude magnesium quality of crystallization is more preferable from settling.Using argon gas vacuum breaker, crude magnesium is prevented
It is contacted with air, avoids the dust and MgO of the production of vacuum breaker process；Crude magnesium on crystallizer directly heats liquid under ar gas environment
Change, do not have to addition refining solvent, do not contacted with air, ensure that the quality of magnesium, contamination-free generates and easy to operate；Insulating tube
Magnesium liquid in road flows into always casting machine under protection of argon gas, and casts under argon gas protection environment, avoids use
Sulphur powder and caused by sulfur dioxide gas body pollution.
Detailed description of the invention
Fig. 1 is reduction refining integration smelting system structural schematic diagram of the present invention；
Fig. 2 is the schematic diagram of magnesium liquid pipeline and magnesium vapor pipeline of the present invention；
In figure, 1- vacuum pump, 2- vacuum line, 3- heater upper cover, 4- potassium sodium plate, 5- heater, 6- crystallizer, 7- high temperature resistant
Ceramic valve, 8- magnesium liquid pipeline, 9- argon gas pipeline, 10- argon gas feed device, 11- reductive jar upper cover, 12- reductive jar cooling jacket,
13- heat insulating block, 14- reductive jar, 15- magnesium vapor pipeline, 16- pipeline body, 17- heat-preservation cotton, 18- heating device.
Specific embodiment
Below by specific embodiment combination attached drawing, invention is further described in detail.Wherein different embodiments
Middle similar component uses associated similar element numbers.In the following embodiments, many datail descriptions be in order to
The application is better understood.However, those skilled in the art can recognize without lifting an eyebrow, part of feature
It is dispensed, or can be substituted by other elements, material, method in varied situations.In some cases, this Shen
Please it is relevant it is some operation there is no in the description show or describe, this is the core in order to avoid the application by mistake
More descriptions are flooded, and to those skilled in the art, these relevant operations, which are described in detail, not to be necessary, they
Relevant operation can be completely understood according to the general technology knowledge of description and this field in specification.
A kind of reduction refining integration smelting system shown in Figure 1, including reductive jar 14, vacuum unit, cooling knot
Brilliant unit, argon gas protection location and magnesium liquid collector unit；Heat insulating block 13 is set in 14 top of reductive jar, outside 14 top of reductive jar
Reductive jar cooling jacket 12 is set, and the upper opening of reductive jar 14 passes through former tank upper cover 11 and seals；Reductive jar 14 passes through magnesium vapor pipe
Road 15 is connect with crystallisation by cooling unit；Crystallisation by cooling unit includes crystallizer heater upper cover 3, potassium sodium plate 4, heater 5 and knot
Brilliant device 6, crystallizer 6 are arranged in heater 5, and potassium sodium plate 4 is arranged in 6 upper end of crystallizer, and heater is arranged in the upper opening of heater 5
Upper cover 3；Vacuum unit includes vacuum line 2 and vacuum pump 1, and heater 5 connects vacuum pump 1 by vacuum line 2；Argon gas protection
Unit includes argon gas pipeline 9 and argon gas feed device 10, and 5 argon gas pipeline 9 of heater connects argon gas feed device 10；Magnesium liquidization is received
Collecting unit includes refractory ceramics valve 7 and magnesium liquid pipeline 8, and magnesium liquid pipeline 8 is connect with heater 5, and the setting of refractory ceramics valve 7 exists
Magnesium liquid pipeline 8 exports.
Reductive jar 14 is arranged two, and magnesium vapor pipeline 15 includes vertical section and horizontal segment, and two reductive jars 14 pass through threeway
Valve is connect with the vertical section of magnesium vapor pipeline 15, and the horizontal segment of magnesium vapor pipeline 15 is connect with heater 5.
Referring to fig. 2, magnesium liquid pipeline 8, magnesium vapor pipeline 15 include pipeline body 16, heat-preservation cotton 17 and heating device 18；
The heat-preservation cotton 17 is wrapped in outside pipeline body 16, and 18 compartment of heating device heats pipeline body 16.
The use process of apparatus of the present invention is described below:
The present invention is using the structure put and (be placed into other than reductive jar) outside crystallizer, when reduction reaction carries out, opens magnesium vapor pipe
The refractory ceramics valve 7 on road, magnesium vapor enter 6 crystallisation by cooling of crystallizer by magnesium vapor pipeline 15.Impurity is passing through in magnesium vapor
When crossing the vertical section of magnesium vapor pipeline 15, carry out playing the role of impurity screening from settling.Reduction reaction terminates, using argon gas
Argon gas vacuum breaker in feedway 10, prevents crude magnesium and contacts with air, the dust and MgO for avoiding vacuum breaker process from producing；It is broken true
Sky terminates, and closes the refractory ceramics valve 7 on magnesium vapor pipeline 15, opens after opening the refractory ceramics valve 7 on magnesium liquid pipeline 8
Heater 5, the crude magnesium on crystallizer directly heat liquefaction under ar gas environment and enter magnesium liquid pipeline 8, the magnesium liquid in magnesium liquid pipeline 8
It flows into continuous casting machine under protection of argon gas always, and casts under argon gas protection environment, avoid using sulphur powder
Sulfur dioxide gas body pollution caused by and.
Present applicant proposes reduction refining integration smelting system to traditional reductive jar and crystal system mainly have with
Lower innovative point: 1, reductive jar water jacket height is reduced, and places aluminosilicate fiber cotton in water jacket bottom, prevents magnesium vapor at water jacket
Crystallization；2, change crystallizer material, crystallizer cannot be placed on by the material of electromagnetic induction heating by reductive jar using graphite etc.
External top makes the impurity in magnesium vapor from settling, play the effect of double purification in the duct, improve the pure of Crystalline Magnesium
Degree；3, magnesium vapor/magnesium liquid pipeline is subjected to INSULATION DESIGN, and compartment/continous way is carried out to pipeline using heating device and is heated,
Guarantee magnesium liquid/magnesium vapor temperature in pipeline, prevents magnesium from crystallizing or solidifying.
Use above specific case is illustrated the present invention, is merely used to help understand the present invention, not to limit
The system present invention.For those skilled in the art, according to the thought of the present invention, can also make several simple
It deduces, deform or replaces.
Claims (6)
1. reduction refining integration smelting system, it is characterised in that: including reductive jar (14), vacuum unit, crystallisation by cooling list
Member, argon gas protection location and magnesium liquid collector unit；Heat insulating block (13) are set in reductive jar (14) top, reductive jar (14)
Reductive jar cooling jacket (12) are set outside top, the upper opening of reductive jar (14) is sealed by reductive jar upper cover (11)；It is described to go back
Former tank (14) is connect by magnesium vapor pipeline (15) with the crystallisation by cooling unit；Crystallisation by cooling unit includes crystallizer heater
Upper cover (3), potassium sodium plate (4), heater (5) and crystallizer (6), crystallizer (6) setting is in heater (5), crystallizer
(6) heater upper cover (3) are arranged in the upper opening of upper end setting potassium sodium plate (4), heater (5)；The vacuum unit includes vacuum
Pipeline (2) and vacuum pump (1), heater (5) pass through vacuum line (2) connection vacuum pump (1)；The argon gas protection location includes
Argon gas pipeline 9 and argon gas feed device (10), heater (5) argon gas pipeline (9) connect argon gas feed device (10)；The magnesium liquid
Changing collector unit includes refractory ceramics valve (7) and magnesium liquid pipeline (8), and magnesium liquid pipeline (8) is connect with heater (5), high temperature resistant
Ceramic valve (7) is arranged in the outlet of the entrance and magnesium vapor pipeline (15) of magnesium liquid pipeline (8).
2. reduction refining integration smelting system according to claim 1, it is characterised in that: reductive jar (14) setting
Multiple, the magnesium vapor pipeline (15) includes vertical section and horizontal segment, and multiple reductive jars (14) pass through pipeline and magnesium vapor pipeline
(15) vertical section connection, the horizontal segment of magnesium vapor pipeline (15) are connect with intermediate frequency furnace (5).
3. reduction refining integration smelting system according to claim 1 or claim 2, it is characterised in that: the crystallizer (6) is adopted
It is made of non electromagnetic induction heating material.
4. reduction refining integration smelting system according to claim 3, it is characterised in that: the crystallizer (6) uses stone
Black material is made.
5. reduction refining integration smelting system according to claim 4, it is characterised in that: the magnesium liquid protects pipeline
(8), magnesium vapor pipeline (15) includes pipeline body (16), heat-preservation cotton (17) and heating device (18)；The heat-preservation cotton (17)
It is wrapped in pipeline body (16) outside, heating device (18) compartment heats pipeline body (6).
6. reduction refining integration smelting system according to claim 5, it is characterised in that: the heat insulating block (13) is by silicon
Sour aluminum fiberboard is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811218687.0A CN109022826B (en) | 2018-10-19 | 2018-10-19 | Reduction and refining integrated smelting system |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811218687.0A CN109022826B (en) | 2018-10-19 | 2018-10-19 | Reduction and refining integrated smelting system |
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| Publication Number | Publication Date |
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| CN109022826B CN109022826B (en) | 2023-11-24 |
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| CN201811218687.0A Active CN109022826B (en) | 2018-10-19 | 2018-10-19 | Reduction and refining integrated smelting system |
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Cited By (5)
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| CN110863118A (en) * | 2019-11-27 | 2020-03-06 | 国科镁业科技(河南)有限公司 | Application of nickel-based filter material in gas-phase magnesium purification and production system comprising same |
| CN111778410A (en) * | 2020-07-07 | 2020-10-16 | 西安银研镁业装备有限公司 | Clean vacuum pyrometallurgical zinc smelting device and zinc smelting method |
| CN113737019A (en) * | 2021-08-25 | 2021-12-03 | 西安交通大学 | Method and device for continuously extracting crystallized magnesium in Pidgeon magnesium smelting process at high temperature |
| CN113774235A (en) * | 2021-08-25 | 2021-12-10 | 西安交通大学 | Method and device for intermittent continuous extraction of crystalline magnesium in Pidgeon magnesium smelting |
| CN114790516A (en) * | 2021-01-25 | 2022-07-26 | 国科镁业科技(河南)有限公司 | A new type of crystallizer |
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| CN110863118A (en) * | 2019-11-27 | 2020-03-06 | 国科镁业科技(河南)有限公司 | Application of nickel-based filter material in gas-phase magnesium purification and production system comprising same |
| CN111778410A (en) * | 2020-07-07 | 2020-10-16 | 西安银研镁业装备有限公司 | Clean vacuum pyrometallurgical zinc smelting device and zinc smelting method |
| CN114790516A (en) * | 2021-01-25 | 2022-07-26 | 国科镁业科技(河南)有限公司 | A new type of crystallizer |
| CN113737019A (en) * | 2021-08-25 | 2021-12-03 | 西安交通大学 | Method and device for continuously extracting crystallized magnesium in Pidgeon magnesium smelting process at high temperature |
| CN113774235A (en) * | 2021-08-25 | 2021-12-10 | 西安交通大学 | Method and device for intermittent continuous extraction of crystalline magnesium in Pidgeon magnesium smelting |
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