CN108968147A - Frangipanis essence capsule and its preparation method and application - Google Patents
Frangipanis essence capsule and its preparation method and application Download PDFInfo
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- CN108968147A CN108968147A CN201810431662.2A CN201810431662A CN108968147A CN 108968147 A CN108968147 A CN 108968147A CN 201810431662 A CN201810431662 A CN 201810431662A CN 108968147 A CN108968147 A CN 108968147A
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- frangipanis
- egg
- extrait
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- 235000013087 Plumeria rubra Nutrition 0.000 title claims abstract description 121
- 239000002775 capsule Substances 0.000 title claims abstract description 90
- 238000002360 preparation method Methods 0.000 title claims abstract description 49
- 244000071969 Plumeria obtusa Species 0.000 title abstract 8
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 50
- 239000011248 coating agent Substances 0.000 claims abstract description 37
- 238000000576 coating method Methods 0.000 claims abstract description 37
- 239000012528 membrane Substances 0.000 claims abstract description 26
- 239000000287 crude extract Substances 0.000 claims abstract description 22
- 238000000605 extraction Methods 0.000 claims abstract description 18
- 238000012545 processing Methods 0.000 claims abstract description 16
- 239000002243 precursor Substances 0.000 claims abstract description 13
- 238000004140 cleaning Methods 0.000 claims abstract description 11
- 239000006210 lotion Substances 0.000 claims abstract description 9
- 238000000465 moulding Methods 0.000 claims abstract description 8
- 238000007711 solidification Methods 0.000 claims abstract description 6
- 230000008023 solidification Effects 0.000 claims abstract description 6
- 244000215777 Plumeria rubra Species 0.000 claims description 113
- 238000000034 method Methods 0.000 claims description 35
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 11
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 235000011187 glycerol Nutrition 0.000 claims description 10
- 239000002304 perfume Substances 0.000 claims description 8
- 108010010803 Gelatin Proteins 0.000 claims description 7
- 239000008273 gelatin Substances 0.000 claims description 7
- 229920000159 gelatin Polymers 0.000 claims description 7
- 235000019322 gelatine Nutrition 0.000 claims description 7
- 235000011852 gelatine desserts Nutrition 0.000 claims description 7
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 7
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 7
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 7
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical group OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 4
- NXMUXTAGFPJGTQ-UHFFFAOYSA-N decanoic acid;octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCCCCC(O)=O NXMUXTAGFPJGTQ-UHFFFAOYSA-N 0.000 claims description 4
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims description 4
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 150000005691 triesters Chemical class 0.000 claims description 4
- 239000011258 core-shell material Substances 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 3
- 239000008157 edible vegetable oil Substances 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000004615 ingredient Substances 0.000 claims description 2
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 21
- 239000012535 impurity Substances 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 7
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 230000014759 maintenance of location Effects 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 39
- 239000000706 filtrate Substances 0.000 description 25
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- 235000019441 ethanol Nutrition 0.000 description 17
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 14
- 239000007788 liquid Substances 0.000 description 13
- 239000000284 extract Substances 0.000 description 10
- 238000001914 filtration Methods 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 9
- 239000006228 supernatant Substances 0.000 description 9
- 239000006187 pill Substances 0.000 description 7
- 239000000523 sample Substances 0.000 description 7
- 238000001514 detection method Methods 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000012496 blank sample Substances 0.000 description 5
- 239000002826 coolant Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000010992 reflux Methods 0.000 description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 238000010298 pulverizing process Methods 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 description 3
- 241000287828 Gallus gallus Species 0.000 description 3
- 239000001055 blue pigment Substances 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000007794 irritation Effects 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000011895 specific detection Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000002137 ultrasound extraction Methods 0.000 description 3
- 241000208327 Apocynaceae Species 0.000 description 2
- 235000007516 Chrysanthemum Nutrition 0.000 description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 210000000991 chicken egg Anatomy 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000002274 desiccant Substances 0.000 description 2
- 210000002969 egg yolk Anatomy 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 235000015092 herbal tea Nutrition 0.000 description 2
- 239000004816 latex Substances 0.000 description 2
- 229920000126 latex Polymers 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- 239000008158 vegetable oil Substances 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 241000282994 Cervidae Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 239000008868 Flower Essence Substances 0.000 description 1
- 244000111489 Gardenia augusta Species 0.000 description 1
- 235000018958 Gardenia augusta Nutrition 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229940008099 dimethicone Drugs 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000012869 ethanol precipitation Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
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- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 230000002572 peristaltic effect Effects 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
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- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of frangipanis essence capsules and its preparation method and application.The preparation method of the frangipanis essence capsule is the following steps are included: carry out extraction processing, acquisition egg extrait for frangipanis crude extract；Lotion molding, solidification, cleaning treatment are successively carried out to the egg extrait, obtain egg extrait ball；Processing is coated to the egg extrait ball using coating membrane precursor, obtains frangipanis essence capsule.The frangipanis essence capsule preparation method greatly reduces the impurity content of egg extrait; by carrying out processing balling-up to egg extrait; and one layer of coating membrane is coated in outer surface; so that egg extrait has the effect of that retention time is long and the fragrance emission time is long, fragrance remaining time is long; and the preparation process of entire frangipanis essence capsule is simple; equipment requirement is low, is suitble to large-scale production, and the frangipanis essence capsule of acquisition can be used in the fields such as cigarette.
Description
Technical field
The invention belongs to flavors and fragrances technical fields, and in particular to a kind of frangipanis essence capsule and preparation method thereof and answer
With.
Background technique
Frangipanis (English name: Plumeria rubra L.cv.Acutifolia) is Apocynaceae
(Apocynaceae) dungarunga of frangipanis category (Plumeriu).Because its petal is pure white, yolk fickle in love, pole is like protein encapsulation
Yolk is thus gained the name.Mexico and Central America area are originated in, is now cultivated extensively in the torrid zone and subtropical zone.Frangipanis is in China
For introducing and planting, there is the history of centuries.Mainly in the southern tropical and subtropical region such as Fujian, Guangdong, Guangxi, Hainan
Cultivation extensively.
Egg flower variety is very diversified, has Cold boiled chicken egg flower, Plumeria rubra, yellow frangipanis etc., wherein planting the most extensively
Be the white heart kind of chrysanthemum (Plumeriu ruhru " Acutifolia "), alias Burma cape jasmine but chrysanthemum and deer horn tree etc..Egg
Colored flowery odour is fresh, simple and elegant, can extract essential oil and medicinal extract, as cosmetic material, food additives.Dried flower is also used as
It is medicinal, there is clearing heat and detoxicating, moistening lung to arrest cough, free radical resisting and antioxidation and other effects.Frangipanis is in many countries and regions
As a kind of Traditional Folk medicinal plant and it is widely used.In Guangdong, frangipanis is one of the primary raw material of a variety of herbal teas.Closely
In the past few years, the fast development of herbal tea industry, it is in full flourish in national market, greatly pull the demand to frangipanis.Egg
Flower flower can also extract essence and be used for manufacture superior cosmetics, perfumed soap and food additives.As frangipanis is drunk in food
Being widely used in material, frangipanis chemical component and its bioactivity research are also becoming one of the research hotspot of the plant.
It is reported in existing literature: rich in organic principles such as volatile oil, iridoids and flavonoids in frangipanis.
Currently, the report that Flos Plumeriae Acutifoliae extract is applied to flavors and fragrances is not rarely seen.But egg in the prior art
Flower extract includes many impurity, and effect can not be perfectly played when using it as additive.In addition, traditional liquid
Perfuming method, fragrance lasting is not lasting, and fragrance is apt to deteriorate and is lost.It is therefore desirable to seek the production of new egg extrait
Technique, to ensure that egg extrait impurity content is few, be easy to save and has longer fragrance remaining time.
Summary of the invention
For current egg extrait impurity content height, it is not easy to the problems such as preservation and fragrance remaining time are short, the present invention mentions
For a kind of frangipanis essence capsule and preparation method thereof.
Further, the present invention also provides the cigarettes comprising above-mentioned frangipanis essence capsule.
For achieving the above object, the technical solution of the embodiment of the present invention is as follows:
A kind of frangipanis essence capsule, the frangipanis essence capsule be core-shell structure, including frangipanis perfume particles with
And it is coated on the coating membrane on frangipanis perfume particles surface.
Correspondingly, the preparation method of the frangipanis essence capsule, at least includes the following steps:
Frangipanis crude extract is carried out extraction processing by step S01., obtains egg extrait；
Step S02. successively carries out lotion molding, solidification, cleaning treatment to the egg extrait, obtains egg extrait
Ball；
Step S03. is coated processing to the egg extrait ball using coating membrane precursor, obtains egg extrait
Capsule.
Correspondingly, a kind of cigarette, the cigarette have filter stick, contain frangipanis essence capsule, the chicken in the filter stick
Egg flower essence capsule is frangipanis essence capsule as described above or the preparation side using frangipanis essence capsule as described above
Method preparation.
Frangipanis essence capsule of the present invention has the beneficial effect that
Compared with the existing technology, the frangipanis essence capsule of the above-mentioned offer of the present invention, due in egg extrait surface shape
At one layer of coating membrane, egg extrait is saved for a long time, it is stable and controllable for quality, when there is lasting in use
Between it is long the advantages that.
The preparation method of frangipanis essence capsule of the present invention has the beneficial effect that
The preparation method of frangipanis essence capsule of the present invention, on the one hand by carrying out extraction processing to frangipanis crude extract,
The impurity content of egg extrait is greatly reduced, on the other hand, by carrying out processing balling-up to egg extrait, and outside
Surface coats one layer of coating membrane, so that egg extrait has, retention time is long and the fragrance emission time is long, fragrance remaining time is long
Effect, and the preparation process of entire frangipanis essence capsule is simple, and equipment requirement is low, is suitble to large-scale production.
Cigarette provided by the invention, due to adding above-mentioned frangipanis essence capsule in filter stick, so that cigarette has chicken
Egg flower fragrance of a flower aromatic style, can significantly improve that flue gas fragrance is rich, preferably reduce the irritation of cigarette smoke, improve and rich
Rich cigarette flavor promotes mouthfeel and pleasant impression, and the fragrance for being obviously improved cigarette is rich, the interest of aesthetic quality and suction, and
And effect can continue to cigarette to aspirate to terminate.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention more comprehensible, with reference to embodiments, to the present invention into
Row is further described.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not used to limit
The present invention.
Present example provides a kind of preparation method of frangipanis essence capsule.
Specifically, the preparation method of the frangipanis essence capsule, at least includes the following steps:
Frangipanis crude extract is carried out extraction processing by step S01., obtains egg extrait；
Step S02. successively carries out lotion molding, solidification, cleaning treatment to the egg extrait, obtains egg extrait
Ball；
Step S03. is coated processing to the egg extrait ball using coating membrane precursor, obtains egg extrait
Capsule.
Further details of explanation is done to the preparation method of the frangipanis essence capsule below.
Frangipanis crude extract involved in step S01 of the present invention refers to the drying for selling medicinal material market or medicinal material company
Frangipanis petal is after pulverization process, using (a) soak at room temperature method, (b) heating reflux method, (c) ultrasonic extraction, (d)
The extract that the processing of at least one of supercritical extraction, (e) subcritical abstraction method obtains.In crushing process, by frangipanis
Petal is crushed to 40~100 mesh.Therefore in step S01, can be and directly handle crude extract, be also possible to by
Frangipanis petal extracts to obtain using said extracted mode.
The purpose of the coarse extraction step is sufficiently to extract flavor substance in raw material frangipanis, and as few as possible again
The other impurity of introducing, so that reduce subsequent technique isolates and purifies difficulty.It is carried out when using at least one of above-mentioned mode
When coarse extraction, the specific steps of which are as follows:
(a) soak at room temperature method: frangipanis petal is placed in extracting solution, is impregnated 12~48h at room temperature, is taken filtrate；It repeats
The above process at least 3 times, merge all filtrates.
The extracting solution that soak at room temperature method is related to is at least one of water, acetone soln, methanol solution and ethanol solution.Its
In, the volumn concentration of acetone soln, methanol solution and ethanol solution is 30~80%.Frangipanis petal and extracting solution
The ratio of quality is 1:7~10.It is big can effectively to reduce a large amount of water-soluble amino acids, polysaccharide etc. for the preferred acetone of the extracting solution
Molecule dissolution, is conducive to subsequent process.
(b) heating reflux method: being obtained by filtration filtrate after 1~4h of heating and refluxing extraction in extracting solution for frangipanis petal,
It repeats the above process at least 3 times, merges all filtrates.The extracting solution that heating reflux method uses be acetone soln, methanol solution and
At least one of ethanol solution.The volumn concentration of acetone soln, methanol solution and ethanol solution is 30~80%, chicken
The ratio of the quality of egg flower petal and extracting solution is 1:7~10.
(c) ultrasonic extraction: frangipanis petal is placed in 1~2h of ultrasonic wave extraction in extracting solution, is then obtained by filtration
Filtrate repeats the above process at least 3 times, merges all filtrates.The extracting solution that ultrasonic extraction uses be water, acetone soln,
At least one of methanol solution and ethanol solution.Wherein, the volumn concentration of acetone soln, methanol solution and ethanol solution
It is 30~80%, the ratio of the quality of frangipanis petal and extracting solution is 1:7~10.The frequency of the ultrasonic wave be 40~
60KHz, certainly, the present invention is not limited thereto, can also use other suitable frequency.
It is a large amount of water-soluble without inciting somebody to action that the above-mentioned extracting method enumerated can efficiently extract frangipanis fragrance matter
Impurity extracts.
Specifically, the extraction filtrate that the above-mentioned extracting method enumerated obtains is concentrated in 40~60 DEG C of environment, preferably
50 DEG C, and by solvent recovery.The process of the concentration can carry out in Rotary Evaporators, obtain frangipanis crude extract as a result,.When
So the present invention is not limited thereto, can also use other suitable instrument.
Preferably, the extraction processing process in step S01, the extractant used are olive oil, Glycerin, mixed triester with caprylic acid capric acid, eat
At least one of oil, laruyl alcohol glyceride, isopropyl palmitate.This several kind of extractants can effectively will be in frangipanis crude extract
Egg extrait separated with other compositions, the egg extrait impurity content of acquisition is few, and frangipanis can be made
Essence capsule.
It is further preferred that the ingredient proportion of the frangipanis crude extract and extractant is 1:1~1.5 according to mass ratio.
Under the ratio, frangipanis crude extract and extractant pass through stirring, stand the separation that egg extrait can be realized, so that frangipanis
Essence retains in the oily liquids of upper layer.Generally, the mixing time of repose of frangipanis crude extract and extractant be 12~for 24 hours,
Extraction and separation can be realized.
In actual process, suitable drying can also be added to containing in egg Rose Absolute shape liquid for acquisition
Egg extrait is dried in agent.Generally, the time of drying process be 12~for 24 hours.
Preferably, the desiccant of addition is at least one of anhydrous sodium sulfate, anhydrous calcium chloride.These types of desiccant,
Other impurities will not be introduced, and facilitate separation.Finally by filtering, collection filtrate, it can be obtained and meet egg extrait glue
The egg extrait of capsule manufacture craft.
In above-mentioned steps S02, the molding of egg extrait lotion, curing process can be carried out using pill dripping machine.Specifically, will
Egg extrait lotion is made in the egg extrait of acquisition, is then added dropwise in reaction solution, make egg extrait lotion with react
Liquid reacts, thus surface cure balling-up.It is then started the cleaning processing using cleaning solution, further reinforces solidification twice, often
It is started the cleaning processing after secondary solidification, can be obtained egg extrait ball.
Preferably, the reaction solution be gelatin, glycerol, deionized water mixture；It is in mass ratio the gelatin: sweet
Oil: deionized water=(4.0~6.0): (2.5~4.0): (1.5~3).
Preferably, cleaning solution is at least one of ethyl alcohol, deionized water.Using ethyl alcohol, deionized water as cleaning solution,
In cleaning process, impurity is not introduced, cleaning effect is good.
In the curing process, it needs for the egg extrait ball of acquisition to be soaked in molding coolant liquid, be solidified into ensureing
It has good uniformity when ball.
Preferably, coolant is formed are as follows: one of silicone oil, vegetable oil, paraffin, olive oil, Glycerin, mixed triester with caprylic acid capric acid are several
Kind is compounded.
More specifically, the preparation of egg extrait ball is carried out using the quick pill dripping machine of DW-50.The quick dripping pill of the DW-50
Machine can size, shape and the state of reaction to drop control, to meet Product Process steady production.Drop-wise is complete
Free gravity falling bodies dripping pill forming technique, equipment is by three reaction containers with magnetic rotation axis, dropper, control system group
At since the equipment belongs to mature equipment, therefore the present invention no longer provides specific structure chart.
It is also magnetic mixing drum in reaction container, four liquid outlets of lower setting and a discharge port, magnetic mixing drum have
Frequency control function.Dropper is the rotation dropper that can maintain liquid level constant in the top of magnetic mixing drum, can
The bore of the drop of dripping uniform particle sizes, water dropper is replaceable, is furnished with 50 water droppers altogether, height of each water dropper away from reaction solution can root
It is adjusted according to actual conditions, while the liquid level of egg extrait lotion can be determined by the height of the overflow hole in chassis, from
And the continual and steady of egg extrait emulsion droplets can be kept.And control system is the control and regulation of whole system.
In above-mentioned steps S03, coating membrane precursor be to be formed coating membrane material and organic solvent formed solution or
Dispersion.Here dispersion can be latex or pseudo- latex.
Specifically, the material of coating membrane is any one of hydroxypropyl methyl cellulose or hydroxypropyl cellulose.It is organic
Solvent is organic solvent, specially 50~70% ethanol solution.
In specific manufacturing process, seed-coating machine can be used, such as the high-efficiency coating machine of model Pilotcoating II.
The working principle of II high-efficiency coating machine of Pilotcoating are as follows: essence moulding capsules are in the clean closed rotation rolling of seed-coating machine first
In cylinder, ceaselessly make complicated track movement, overturning is smooth, and exchange is frequent, the coating material stirred by agitator, by peristaltic pump
Effect, filter from the spray of import spray gun onto essence capsule, while under air draft and suction function, supplied by hot wind cabinet 100,000 grades
Clean hot wind passes through essence capsule, is discharged by bottom screens from air door, makes to be coated medium in capsule surface rapid draing, is formed hard
Solid, fine and close, smooth surface film.Whole process is completed under PLC control.It is of course also possible to use spray coating technique, is adopted
When with spray coating technique, the clothing liquid of ejection is atomized quickly, and forms small drop uniform wet in egg extrait ball table
Face, then diffusion sprawling, ultimately forms the film for being coated on egg extrait ball surface.
Via the frangipanis essence capsule that above-mentioned preparation method obtains, structure is a kind of core-shell structure, including with egg
Extrait particle is as nucleome, using coating membrane as shell.The coating membrane is coated on the surface of the frangipanis perfume particles.
By the effect of coating membrane, egg extrait is existed steadily in the long term, and is able to extend release when discharging fragrance
Time.
Preferably, the partial size of the frangipanis essence capsule of acquisition is 1.0~4.0mm, and partial size is excessive, when in use, can not
Using complete, the waste of egg extrait is caused, and partial size is too small, then it is depleted in advance, it is unfavorable for the hair of egg extrait
It waves.
Since the main component of above-mentioned coating membrane precursor is times in hydroxypropyl methyl cellulose or hydroxypropyl cellulose
One kind, therefore the coating membrane formed is any one of hydroxypropyl methyl cellulose film or hydroxypropyl cellulose film.
On the basis of the frangipanis essence capsule that above-mentioned preparation method obtains, the present invention furthermore provides a perfume (or spice)
Cigarette.The cigarette has filter stick, added with the frangipanis essence capsule prepared using preparation method as above in the filter stick.
More specifically, in the filter stick of every cigarette, frangipanis essence capsule described in addition one.Due to egg
Extrait capsule has apparent frangipanis fragrance of a flower aromatic style, after being added to the filter stick of cigarette, is perfectly combined with cigarette perfume, can
Significantly improve that flue gas fragrance is rich, enhance the satiety of flue gas by with it is rich, promote mouthfeel and pleasant impression, increase cigarette smoking
Organoleptic quality and suction interest.
Certainly, the frangipanis essence capsule obtained using preparation method of the invention, due to improving egg extrait
Fragrance remaining time, be easy to save, not oxidation by air it is rotten, it is ensured that essence quality is steady in a long-term, therefore the egg that the present invention obtains
Extrait capsule is not limited to can also be applied to essence for food, daily chemical essence, flavouring essence for tobacco, essence glue in cigarettes
The fields such as capsule.
More effectively to illustrate technical solution of the present invention, technology of the invention is illustrated below by multiple specific embodiments
Scheme.
Embodiment 1
A kind of preparation method of frangipanis essence capsule, comprising the following steps:
(1) preparation of frangipanis crude extract
Third that 3500g percent by volume is 70% is added to 50 mesh in frangipanis petal pulverizing medicinal materials after taking 500g dry
For 24 hours, first-time filtrate is obtained by filtration in ketone solution, soaking at room temperature；Filter residue is repeated to extraction 2 times under identical condition, obtains the
Secondary filtrate and third time filtrate.Above-mentioned all filtrates are merged, no alcohol taste is concentrated into Rotary Evaporators and obtains chicken for 50 DEG C
Egg flower crude extract.
(2) the above-mentioned frangipanis crude extract of 100g is taken, 100g Glycerin, mixed triester with caprylic acid capric acid is added, is stirred 2h, 12h is stood, takes
Supernatant.The anhydrous sodium sulfate for accounting for supernatant quality 1% is added into the supernatant obtained, stirring stands 12h, filters, and collects
Filtrate is to get the egg extrait for meeting frangipanis essence capsule preparation process.
(3) preparation of egg extrait ball: being prepared using the quick pill dripping machine of home equipment DW-50, specifically will step
Suddenly (2) obtain egg extrait be placed in drop disk, by water dropper instill reaction solution in, wherein reaction solution by gelatin, glycerol,
Water composition, the quality proportioning of three are 5:3:2.Egg extrait ball and reaction solution are stirred package, form egg extrait
Egg extrait ball is discharged into dimethicone coolant liquid by discharge port and is solidified by ball, then, with deionized water to egg
Extrait ball is cleaned, and a batch egg extrait ball is made.
(4) it the preparation of frangipanis essence capsule: is prepared using II high-efficiency coating machine of home equipment Pilotcoating.
The egg extrait ball that water was cleaned is dry in roller drier, is subsequently placed in seed-coating machine, and by coating membrane precursor
It is sprayed on egg extrait ball surface, obtains a collection of frangipanis essence capsule；Wherein, the group of coating membrane precursor becomes hydroxypropyl
Methylcellulose 10g, brilliant blue pigment 0.04g, 60% ethanol solution 100g.
Be prepared a collection of frangipanis essence capsule 10 of random Example 1, carry out the detection of respective performances, examine
Survey method is to control common detection methods according to common capsule quality.Specific detection project and testing result are as shown in table 1.
Embodiment 2
A kind of preparation method of frangipanis essence capsule, comprising the following steps:
(1) preparation of frangipanis crude extract
The second that 4000g percent by volume is 75% is added to 50 mesh in frangipanis petal pulverizing medicinal materials after taking 500g dry
Alcoholic solution, heating and refluxing extraction 2h, is obtained by filtration first-time filtrate；Filter residue is repeated to extraction 2 times under identical condition, is obtained
Second of filtrate and third time filtrate.Above-mentioned all filtrates are merged, no alcohol taste is concentrated into Rotary Evaporators and obtains for 50 DEG C
Frangipanis crude extract.
(2) the above-mentioned frangipanis crude extract of 100g is taken, 100g edible oil is added, is stirred 2h, 12h is stood, takes supernatant.
The anhydrous sodium sulfate for accounting for supernatant quality 1% is added into the supernatant obtained, stirring stands 12h, and filtering collects filtrate, i.e.,
The egg extrait of frangipanis essence capsule preparation process must be met.
(3) preparation of egg extrait ball: being prepared using the quick pill dripping machine of home equipment DW-50, specifically will step
Suddenly (2) obtain egg extrait be placed in drop disk, by water dropper instill reaction solution in, wherein reaction solution by gelatin, glycerol,
Water composition, the quality proportioning of three are 5:3:2.Egg extrait ball and reaction solution are stirred package, form egg extrait
Egg extrait ball is discharged into olive oil coolant liquid by discharge port and is solidified by ball, then, with deionized water to the egg fragrance of a flower
Smart ball is cleaned, and a batch egg extrait ball is made.
(4) it the preparation of frangipanis essence capsule: is prepared using II high-efficiency coating machine of home equipment Pilotcoating.
The egg extrait ball that water was cleaned is dry in roller drier, is subsequently placed in seed-coating machine, and by coating membrane precursor
It is sprayed on egg extrait ball surface, obtains a collection of frangipanis essence capsule；Wherein, the group of coating membrane precursor becomes hydroxypropyl
Methylcellulose 10g, brilliant blue pigment 0.04g, 60% ethanol solution 100g.
Be prepared a collection of frangipanis essence capsule 10 of random Example 2, carry out the detection of respective performances, examine
Survey method is to control common detection methods according to common capsule quality.Specific detection project and testing result are as shown in table 1.
Embodiment 3
A kind of preparation method of frangipanis essence capsule, comprising the following steps:
(1) preparation of frangipanis crude extract
Frangipanis petal pulverizing medicinal materials after taking 500g dry to 50 mesh, boil and extract 2h by addition 5000g deionized water,
First-time filtrate is obtained by filtration；Filter residue is repeated to extraction 2 times under identical condition, second of filtrate is obtained and third time is filtered
Liquid.Above-mentioned all filtrates are merged, 50 DEG C of concentrations in Rotary Evaporators, by 80% ethanol precipitation of concentrate, filtering removal
Precipitating collects filtrate, filtrate is concentrated, and carries out secondary alcohol precipitation to concentrate with 75% ethyl alcohol, collects filtrate, inspissated juice is without alcohol
Taste obtains frangipanis crude extract.
(2) the above-mentioned frangipanis crude extract of 100g is taken, 100g edible oil is added, is stirred 2h, 12h is stood, takes supernatant.
The anhydrous sodium sulfate for accounting for supernatant quality 1% is added into the supernatant obtained, stirring stands 12h, and filtering collects filtrate, i.e.,
The egg extrait of frangipanis essence capsule preparation process must be met.
(3) preparation of egg extrait ball: being prepared using the quick pill dripping machine of home equipment DW-50, specifically will step
Suddenly (2) obtain egg extrait be placed in drop disk, by water dropper instill reaction solution in, wherein reaction solution by gelatin, glycerol,
Water composition, the quality proportioning of three are 5:3:2.Egg extrait ball and reaction solution are stirred package, form egg extrait
Egg extrait ball is discharged into vegetable oil coolant liquid by discharge port and is solidified by ball, then, with deionized water to the egg fragrance of a flower
Smart ball is cleaned, and a batch egg extrait ball is made.
(4) it the preparation of frangipanis essence capsule: is prepared using II high-efficiency coating machine of home equipment Pilotcoating.
The egg extrait ball that water was cleaned is dry in roller drier, is subsequently placed in seed-coating machine, and by coating membrane precursor
It is sprayed on egg extrait ball surface, obtains a collection of frangipanis essence capsule；Wherein, the group of coating membrane precursor becomes hydroxypropyl
Methylcellulose 10g, brilliant blue pigment 0.04g, 60% ethanol solution 100g.
Be prepared a collection of frangipanis essence capsule 10 of random Example 3, carry out the detection of respective performances, examine
Survey method is to control common detection methods according to common capsule quality.Specific detection project and testing result are as shown in table 1.
1 frangipanis essence capsule product parameters of table
The frangipanis essence capsule that Examples 1 to 3 is prepared is used in the preparation of cigarette below, specific as follows:
Application Example 1
The preparation of cigarette: press existing filter stick production technology, the egg extrait for embodiment 1 being obtained by filter-stick forming device
It after capsule is placed in filter stick center, makes an addition in regular-size cigarette filter stick, every cigarette adds a capsule, and after cigarette cigarette sample
As frangipanis essence capsule cigarette.
Application Example 2
The preparation of cigarette: press existing filter stick production technology, the egg extrait for embodiment 2 being obtained by filter-stick forming device
It after capsule is placed in filter stick center, makes an addition in regular-size cigarette filter stick, every cigarette adds a capsule, and after cigarette cigarette sample
As frangipanis essence capsule cigarette.
Application Example 3
The preparation of cigarette: press existing filter stick production technology, the egg extrait for embodiment 3 being obtained by filter-stick forming device
It after capsule is placed in filter stick center, makes an addition in regular-size cigarette filter stick, every cigarette adds a capsule, and after cigarette cigarette sample
As frangipanis essence capsule cigarette.
Blank sample
The preparation of cigarette: existing filter stick production technology is pressed, does not add frangipanis essence capsule in filter tip, makes cigarette.
It is real that application is adjusted according to national standard " GB/T16447-2004 tobacco and tobacco product adjusts and the atmospheric environment of test "
The moisture content of the cigarette sample of example 1~3 and blank sample is applied, by " GB5606.4-2005 cigarette sense organ technical requirements " by Guangdong Province
The smoke panel test aesthetic quality of cigarette sample that group carries out Application Example 1~3 and blank sample of grade cigarette smokes panel test, and each sample is commented
Inhale 3, shown in specific smoking result table 2.
The smoking result of the aesthetic quality of 2 Application Example 1~3 of table and blank sample cigarette
| Sample | Gloss | Fragrance | Harmony | Miscellaneous gas | Irritation | Pleasant impression | It is total |
| Application Example 1 | 4 | 32 | 6 | 12 | 16 | 20 | 90 |
| Application Example 2 | 4 | 32 | 6 | 11 | 16 | 20 | 89 |
| Application Example 3 | 4 | 31 | 6 | 11 | 15 | 20 | 87 |
| Blank sample | 4 | 27 | 5 | 10 | 14 | 18 | 78 |
It can be seen that from above-mentioned comparison smoking result after frangipanis essence capsule is added in cigarettes, cigarette can be made
Aroma quality is promoted, harmony cigarette perfume, enriches cigarette perfume, significantly reduces irritation, and flue gas is full, soft, pleasant impression and miscellaneous gas score mention
Height promotes cigarette sucking quality and sense organ comfort level, and has and significantly return sweet tea sense.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc. within mind and principle should all include within protection scope of the present invention.
Claims (10)
1. a kind of preparation method of frangipanis essence capsule, which is characterized in that at least include the following steps:
Frangipanis crude extract is carried out extraction processing by step S01., obtains egg extrait；
Step S02. successively carries out lotion molding, solidification, cleaning treatment to the egg extrait, obtains egg extrait ball；
Step S03. is coated processing to the egg extrait ball using coating membrane precursor, obtains egg extrait glue
Capsule.
2. the preparation method of frangipanis essence capsule as described in claim 1, it is characterised in that: the extraction of the extraction processing
Agent is at least one of olive oil, Glycerin, mixed triester with caprylic acid capric acid, edible oil, laruyl alcohol glyceride, isopropyl palmitate.
3. such as the preparation method of the described in any item frangipanis essence capsules of claim 1~2, it is characterised in that: in mass ratio,
The ingredient proportion of the frangipanis crude extract and the extractant is 1:1~1.5.
4. such as the preparation method of the described in any item frangipanis essence capsules of claim 1~2, it is characterised in that: the lotion
Molding, curing process are that the egg extrait and reaction solution are carried out mixing treatment, obtain the frangipanis of surface cure balling-up
Essence ball.
5. the preparation method of frangipanis essence capsule as claimed in claim 4, it is characterised in that: the reaction solution be gelatin,
The mixture of glycerol, deionized water；In mass ratio it is the gelatin: glycerol: deionized water=(4.0~6.0): (2.5~
4.0): (1.5~3).
6. the preparation method of frangipanis essence capsule as described in claim 1, it is characterised in that: the coating membrane precursor is
The solution or dispersion that the material and organic solvent for forming coating membrane are formed.
7. a kind of frangipanis essence capsule obtained using preparation method as described in any one of claims 1 to 6, feature are existed
It is core-shell structure in, the frangipanis essence capsule, including frangipanis perfume particles and is coated on the egg extrait
The coating membrane on grain surface.
8. frangipanis essence capsule as claimed in claim 7, which is characterized in that the partial size of the frangipanis essence capsule is
1.0~4.0mm.
9. frangipanis essence capsule as claimed in claim 7, which is characterized in that the coating membrane is hydroxypropyl methyl cellulose
Any one of film or hydroxypropyl cellulose film.
10. a kind of cigarette, the cigarette has filter stick, it is characterised in that: contain frangipanis essence capsule in the filter stick, it is described
Frangipanis essence capsule is the described in any item frangipanis essence capsules of claim 7~9.
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| CN101044918A (en) * | 2007-04-30 | 2007-10-03 | 温纯青 | Frangipani shaped Cigarette with egg extraction for reducing |
| US20110232656A1 (en) * | 2010-03-26 | 2011-09-29 | Philip Morris Usa Inc. | Method for making particle of a hydrophobic additive and a polysaccharide coating and tobacco products containing particle of a hydrophobic additive and a polysaccharide coating |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| CN104687242A (en) * | 2014-10-28 | 2015-06-10 | 深圳市大百汇技术有限公司 | Method for extracting (R)-3-carboxyl-alpha-hydroxyphenyl propionic acid from frangipane, application and cigarette |
| CN105919152A (en) * | 2016-04-20 | 2016-09-07 | 贵州中烟工业有限责任公司 | Preparation method of tobacco substrate realizing non combustion after being heated and containing microcapsule |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1569529A2 (en) * | 2002-12-11 | 2005-09-07 | British American Tobacco (Investments) Limited | Improvements relating to smoking articles |
| CN101044918A (en) * | 2007-04-30 | 2007-10-03 | 温纯青 | Frangipani shaped Cigarette with egg extraction for reducing |
| US20110232656A1 (en) * | 2010-03-26 | 2011-09-29 | Philip Morris Usa Inc. | Method for making particle of a hydrophobic additive and a polysaccharide coating and tobacco products containing particle of a hydrophobic additive and a polysaccharide coating |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| CN104687242A (en) * | 2014-10-28 | 2015-06-10 | 深圳市大百汇技术有限公司 | Method for extracting (R)-3-carboxyl-alpha-hydroxyphenyl propionic acid from frangipane, application and cigarette |
| CN105919152A (en) * | 2016-04-20 | 2016-09-07 | 贵州中烟工业有限责任公司 | Preparation method of tobacco substrate realizing non combustion after being heated and containing microcapsule |
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