CN108967989A - A kind of preparation method of selenium-enriched plant seasoning and selenium-rich salt - Google Patents
A kind of preparation method of selenium-enriched plant seasoning and selenium-rich salt Download PDFInfo
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- CN108967989A CN108967989A CN201810720669.6A CN201810720669A CN108967989A CN 108967989 A CN108967989 A CN 108967989A CN 201810720669 A CN201810720669 A CN 201810720669A CN 108967989 A CN108967989 A CN 108967989A
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- 239000011669 selenium Substances 0.000 title claims abstract description 193
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 title claims abstract description 179
- 229910052711 selenium Inorganic materials 0.000 title claims abstract description 179
- 150000003839 salts Chemical class 0.000 title claims abstract description 83
- 235000011194 food seasoning agent Nutrition 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 37
- 239000002994 raw material Substances 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 28
- 235000002639 sodium chloride Nutrition 0.000 claims description 87
- 239000007788 liquid Substances 0.000 claims description 44
- 238000001914 filtration Methods 0.000 claims description 30
- 238000000605 extraction Methods 0.000 claims description 19
- 239000012530 fluid Substances 0.000 claims description 16
- 230000008569 process Effects 0.000 claims description 14
- 239000000287 crude extract Substances 0.000 claims description 12
- 238000000227 grinding Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 7
- 239000011780 sodium chloride Substances 0.000 claims description 7
- 238000005267 amalgamation Methods 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 45
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 38
- 239000000047 product Substances 0.000 description 20
- 240000001462 Pleurotus ostreatus Species 0.000 description 18
- 235000001603 Pleurotus ostreatus Nutrition 0.000 description 18
- 239000000243 solution Substances 0.000 description 15
- 235000013305 food Nutrition 0.000 description 12
- 206010028980 Neoplasm Diseases 0.000 description 11
- 201000011510 cancer Diseases 0.000 description 10
- 238000001704 evaporation Methods 0.000 description 9
- 230000008020 evaporation Effects 0.000 description 9
- 230000008901 benefit Effects 0.000 description 8
- 239000002002 slurry Substances 0.000 description 8
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 7
- 238000001035 drying Methods 0.000 description 7
- 239000000835 fiber Substances 0.000 description 7
- 229910052740 iodine Inorganic materials 0.000 description 7
- 239000011630 iodine Substances 0.000 description 7
- 238000000108 ultra-filtration Methods 0.000 description 7
- 235000013311 vegetables Nutrition 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000010410 layer Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 235000016709 nutrition Nutrition 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 239000012141 concentrate Substances 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 102000004196 processed proteins & peptides Human genes 0.000 description 5
- 108090000765 processed proteins & peptides Proteins 0.000 description 5
- 150000001413 amino acids Chemical class 0.000 description 4
- 238000000498 ball milling Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 239000011229 interlayer Substances 0.000 description 4
- 230000035764 nutrition Effects 0.000 description 4
- 229920001184 polypeptide Polymers 0.000 description 4
- 241000208671 Campanulaceae Species 0.000 description 3
- 230000001093 anti-cancer Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 235000014106 fortified food Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 238000013517 stratification Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000007738 vacuum evaporation Methods 0.000 description 3
- 240000007440 Agaricus campestris Species 0.000 description 2
- 235000004570 Agaricus campestris Nutrition 0.000 description 2
- 206010039921 Selenium deficiency Diseases 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
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- 150000004676 glycans Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 244000251953 Agaricus brunnescens Species 0.000 description 1
- 244000003416 Asparagus officinalis Species 0.000 description 1
- 235000005340 Asparagus officinalis Nutrition 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 244000000626 Daucus carota Species 0.000 description 1
- 235000002767 Daucus carota Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000006057 Non-nutritive feed additive Substances 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 241000318836 Pleurotus nebrodensis Species 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
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- 239000012535 impurity Substances 0.000 description 1
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- 208000019423 liver disease Diseases 0.000 description 1
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- 230000003716 rejuvenation Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 235000015598 salt intake Nutrition 0.000 description 1
- 238000009288 screen filtration Methods 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/40—Table salts; Dietetic salt substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Seasonings (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses the preparation methods of a kind of selenium-enriched plant seasoning and selenium-rich salt, are related to the preparation method of plant processing technique field and salt processing.The preparation method of selenium-enriched plant seasoning disclosed by the invention, it includes the pulverising step that selenium-enriched plant raw material is ground to 600-2000 mesh, this method passes through the abundant crushing to selenium-enriched plant, keep its dispersibility more preferable, solubility property improves, the precipitation degree for improving selenium element especially organic selenium, is conducive to absorption of human body.
Description
Technical field
The present invention relates to salt processing technique field, in particular to a kind of selenium-enriched plant seasoning and selenium-rich salt
Preparation method.
Background technique
The World Health Organization just proposes " 3 1/3 " of cancer prevention and control early in the eighties in last century: 1/3 cancer can prevent；
1/3 cancer can early find, early treatment；1/3 cancer can active treatment extending life, improve life quality.World health
It organizes in the cancer prevention mode suggested, selenium-rich dietotherapy prevention is also a kind of means of pre- anti-cancer.
According to " China's tumour registration annual report " that in April, 2014 is issued, China's cancer morbidity is 285.91/10 ten thousand.According to
To 2049, China's cancer morbidity was likely to be breached 4,00/,100,000 level for estimation, and pathogenesis of cancer, the death rate become in obvious rise
Gesture and rejuvenation trend.
Cancer is high-incidence to have some relations with environmental pollution, and further to destroy China relatively barren for environmental pollution
Selenium soil environment keeps this microelement with anti-cancer efficacy more rare, new threat is formed to residents ' health, science is
Verified selenium deficiency can lead to more than the 40 kinds of diseases such as cancer, hepatopathy, cardiovascular disease, diabetes, lead to more than 400 kinds of diseases indirectly, I
Mostly commodity food and other crop bases, the deputy to the National People's Congress appeal that " selenium-supply ", which is included in Health China, builds again in state serious selenium deficiency area
If among planning, approval allows selemium nutrition product to identify the carcinous matter of suppression of selenium as early as possible, have become a kind of common recognition of whole society.
After " the selenium-supply engineering " of whole people's selenium-supply is the microelement of supplement, and China is enriched the iodine by salt at present, again
One key subjects, that is, selenium-supply will become next direction of product salt raising fitness-for-all, and only salt is that daily needs are taken the photograph
Enter, is very simple as selenium source.Especially country is by selenium from " pollutants in food limitation " GB2762-2005
Middle cancellation embodies just to become apparent, and existing preparation selenium-rich salt is by by animal raw materials, vegetable raw material (including mushroom
Class), extractive from fermentative drying pulverize selenium-rich salt be made with salt hybrid process again, but existing problem has:
1, " selenium " contained by product is total Se content, actually only has " organic selenium " to be only " selenium " ingredient beneficial to human body,
Inorganic selenium actually will not generate positive acting to human body, and the content for improving organic selenium is project urgently to be resolved, for food
The detection project that country only eliminates selenium element from " pollutants in food limitation " GB2762-2005 does not determine selenium-enriched food
National standard, it includes: DB6124.01-2010 " rich that each place (province), which then drafts and carried out regulation to selenium-enriched food using provincial standard,
Selenium food Se content classification standard ", many regulations such as DB61/T556-2012 " selenium-enriched food and relevant food content selenium standard ".
2, the dry gound dry powder of selenium-enriched plant baking contains a large amount of non-soluble fiber, exists in salt processing and making process
Following problem: 1, being difficult to be uniformly distributed and be firmly combined, and leads to final selenium-rich salt, and powder is separated with salt, and selenium distribution is equal in product
Evenness is unstable；2, in total selenium of dry powder inorganic selenium account for it is relatively high, with certain fishy smell, with salt decohesion mouthfeel；3, it does
Selenium in powder mixes among the fibers more, and dissolubility is poor, it is difficult to be absorbed by human body rapid digestion, using effect is caused to decline；It needs
The organic selenium that dispersibility is more preferable, and solubility property improves is prepared by a kind of method, solve problem above, but this method is more numerous
It is trivial.
3, salt needs (national food safety standard pressure standard GB2721 according to national standards as a kind of Special food
" edible salt ", GB2760 " food additives use standard ", GB14880 " food enrichment uses standard ", recommendatory mark
Quasi- GB/T5461 " edible salt " etc.) it processes, production technology is stringent.
4, selenium-enriched plant itself contain the nutrition such as many microelements, albumen, polypeptide other than " selenium " element at
Point and aromatic substance, selenium-enriched plant grinding dry powder not can guarantee effective nutrition and can be absorbed by the body, while it is special
Plant scent can not necessarily allow selenium-rich product salt to have pleasant sign smell.
5, the processing enterprise of existing nutrition fortifier and selenium-rich raw material, using a large amount of additive and processing aid, most
The product salt made eventually still has the substance of many natural constituents while selenium-rich, can not judge the battalion to final products
It forms and point whether generates negative role.
In consideration of it, the present invention is specifically proposed.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation method of selenium-enriched plant seasoning, which can be improved organic
Se content effectively absorbs convenient for human body；The smell for correcting selenium-enriched plant, meets the requirement of seasoning, is used for salt processing system
It can be uniformly distributed during work, be firmly combined with salt, improve the quality of selenium-rich salt.
Another object of the present invention is to provide a kind of preparation method of selenium-rich salt, the selenium-rich salt which obtains has
Machine Se content is high, is evenly distributed.
The present invention is implemented as follows:
A kind of preparation method of selenium-enriched plant seasoning comprising: pulverising step；
The pulverising step includes: that selenium-enriched plant raw material system is ground to 600-2000 mesh.
A kind of preparation method of selenium-rich salt comprising:
Selenium-enriched plant seasoning is prepared using the preparation method of selenium-enriched plant seasoning as described above；
The selenium-enriched plant seasoning is mixed with raw material salt.
The invention has the following advantages:
The preparation method of a kind of selenium-enriched plant seasoning provided by the invention comprising selenium-enriched plant raw material is ground to 600-
The pulverising step of 2000 mesh, this method keep fiber dispersion more preferable, solubility property mentions by the abundant crushing to selenium-enriched plant
Height, and then non-solubility fiber content is reduced, organic selenium content can be improved, be used for uniformly dividing in salt processing and making process
Cloth is firmly combined with salt, improves the stability of selenium-rich product salt quality.
On the other hand, the preparation method of selenium-rich salt provided by the invention, will be by the preparation of above-mentioned selenium-enriched plant seasoning
The selenium-enriched plant seasoning that method is prepared is mixed with raw material salt, obtains selenium-rich salt, organic selenium contains in prepared selenium-rich salt
Amount is high, and selenium element is uniformly distributed salt surface, not stratified, not hardened, can be used as the food sources of daily selenium-supply, not only has and relax
Suitable mouthfeel and nutritional ingredient abundant, while there are delicious and pleasant surface characteristics.
Specific embodiment
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, according to normal conditions or manufacturer builds
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
The preparation method of a kind of selenium-enriched plant seasoning of the embodiment of the present invention and selenium-rich salt is carried out specifically below
It is bright.
On the one hand, the embodiment of the invention provides a kind of preparation methods of selenium-enriched plant seasoning comprising following steps:
S1 cleans (optional step)
Selenium-enriched plant is cleaned, impurity is removed.
S2 dices (optional step)
Selenium-enriched plant is subjected to processing of dicing.
If selenium-enriched plant volume is larger, it can pass it through after dicing, enter back into subsequent step；If selenium-enriched plant itself
Small volume does not influence grinding effect, can directly grind it.
S3 is crushed
Selenium-enriched plant raw material after dicing is ground to 600-2000 mesh by grinder.
Selenium-enriched plant raw material, which is ground in the range of 600-2000 mesh, can sufficiently crush the fibre contained in selenium-enriched plant
Dimension element keeps its dispersibility more preferable, and solubility property is improved, and fills other nutrients such as nutriment therein such as selenium
It analyzes, is easily absorbed by the body.It is too low to grind mesh number, the other degree of soluble fraction is not achieved in cellulose, and grinding mesh number is too high,
Need time-consuming too long, increase energy consumption.
Preferably, selenium-enriched plant raw material is ground to 600-1000 mesh perhaps 800-1200 mesh or 1200-1800 mesh,
Or 1700-2000 mesh.
S4 heating
After the grinding steps, add water to mix in plant material powder or slurries to be settled to preset vol, be placed in 60-100 DEG C of item
Under part, 3-6h is heated, selenium-enriched plant crude extract is obtained.
Wherein, preset vol can select according to the actual situation, without limitation.
S5 is filtered for the first time
After the heating stepses, by the selenium-enriched plant seasoning through strainer filtering, initial extraction liquid is obtained.
Wherein, strainer mesh number can be 400-1000 mesh.
S6 stratification
After the first time filtration step, the initial extraction liquid is subjected to stewing process, makes initial extraction liquid point
Layer, wherein time of repose 60-120min.
Preferably, stewing process is stood in constant temperature (60 DEG C) condition, in a manner of sealing (isolation air), shading.
Second of filtering of S7
Take the supernatant liquid filtering in the initial extraction liquid positioned at upper layer (in some embodiments it is possible to be with super
Filter membrane classified filtering), it collects filtered fluid (if it is classified filtering, then collecting filtered fluids at different levels)；
It takes and is located at the progress centrifugal filtration processing of lower layer's turbid solution in the initial extraction liquid, collect clarified solution, refilter (
In some embodiments, it is also possible to ultrafiltration membrane classified filtering), it collects filtered fluid and (if it is classified filtering, then collects at different levels
Filtered fluid)；
Filtered fluids at different levels are mixed according to default proportion, obtain amalgamation liquid；
Wherein, centrifugal filtration revolving speed is 1000-3500rpm.
Illustrate: classified filtering is to be filtered by difference by the way that aperture is descending, accelerates isolated speed, generally
In the case of, 400 mesh are filtered as initial filter, filtrate using 600 mesh, 800,1000 mesh.Ultrafiltration process is entered if necessary,
Using molecular weight as Filtration Goal, 50000 molecular weight filtrations obtain Thick many candies, and 20000 molecular weight filtration films obtain smart polysaccharide, and 5000
Molecular weight obtains high content of peptides, and 1000 the following are obtain small polypeptide and amino acid；The characteristics of classified filtering is at different levels
The main component of filtered fluid is different.Therefore, filtered fluids at different levels can be mixed according to different ratios according to actual needs.
Filter process is that the continuous filtration process of a classification can accelerate the replacement number that efficiency reduces filter screen, crucial
Point is some available section pregnant solution, such as: someone is greater than the tool of 100,000-100 ten thousand molecular weight in research mushroom polysaccharide
Standby anticancer function, the functional polypeptide of molecular weight 5000-3000,1000 micromolecule polypeptides below.
Supernatant and turbid solution are separately filtered, it is possible to reduce the abrasion to filter plant, and improve the rate of filtration.
S8 is concentrated by evaporation
After second of filtration step, the amalgamation liquid is evaporated concentration and is seasoned to get the selenium-enriched plant of liquid
Material is selenium-enriched plant seasoned liquid.
It should be noted that according to actual needs, being concentrated into preset vol.
Preferably, it is concentrated by evaporation and carries out under vacuum conditions.
It is further preferred that the vacuum degree of vacuum condition is -680~-780mmhg.
(optional step) is lyophilized in S9
Above-mentioned selenium-enriched plant seasoned liquid is freeze-dried to obtain the selenium-enriched plant seasoning of powdery.Conducive to transporting and protect
It deposits.
Preferably, in some embodiments of the present invention, selenium-enriched plant is the one or more of selenium-rich mushroom.
It should be noted that selenium-rich mushroom can be fresh goods either dry product.
It is highly preferred that selenium-rich mushroom includes mushroom with abundant selenium, selenium-enriched agaricus bisporus, Se-rich xianggu, selenium-rich Pleurotus nebrodensis, selenium-rich wood
One of ear is a variety of.
It is highly preferred that rich selenium vegetables include one of the blue flower in selenium-rich west, selenium-rich asparagus, selenium-rich bamboo shoots, selenium-rich carrot or
It is a variety of.
To sum up, the preparation method of selenium-enriched plant seasoning provided in an embodiment of the present invention passes through sufficiently grinding to selenium-enriched plant
Mill, keeps fiber dispersion more preferable, and solubility property improves, and then reduces non-solubility fiber content, and organic selenium content can be improved, will
It is used to be uniformly distributed in salt processing and making process, be firmly combined with salt, improves the stability of selenium-rich product salt quality.
On the other hand, the present invention provides a kind of preparation methods of selenium-rich salt comprising following steps:
Selenium-enriched plant seasoning is prepared using the preparation method of selenium-enriched plant seasoning as described above；
The selenium-enriched plant seasoning is mixed with raw material salt.
Further, in some embodiments of the present invention, it is mixed into 3kg-100kg's in raw material salt described in every 1000kg
The selenium-enriched plant seasoning.
Further, in some embodiments of the present invention, using spray mode by the selenium-enriched plant seasoning with
The raw material salt mixing.
Further, in some embodiments of the present invention, by mixed raw material salt by suitable mode by its water
Divide and be evaporated to product salt government standard, and keeps necessary mobility.
Further, in some embodiments of the present invention, the raw material salt is well salt or sea salt.
Further, in some embodiments of the present invention, by the raw material salt be heated to temperature be 70-85 DEG C when,
The selenium-enriched plant seasoning is mixed with the raw material salt, it is 70-85 DEG C with the water therein that volatilizees that raw material salt, which is heated to temperature,
Point.
To sum up, the preparation method of selenium-rich salt provided in an embodiment of the present invention, organic selenium content in prepared selenium-rich salt
Height, selenium element is uniformly distributed salt surface, not stratified, not hardened, can be used as the food sources of daily selenium-supply, not only has comfortably
Mouthfeel and nutritional ingredient abundant, while there are delicious and pleasant surface characteristics.
Feature and performance of the invention are described in further detail with reference to embodiments.
Embodiment 1
Selenium-rich mushroom seasoning provided in this embodiment the preparation method is as follows:
1. cleaning
Take impregnated in salt water after fresh 200kg Agaricus campestris rich in selenium (total selenium 2.0mg/kg) cleaning mushroom it is spare；The dry richness of 150kg
Selenium oyster mushroom (total selenium 175mg/kg) clears up campanulaceae, cleans dirt, impregnates in clear water spare.
2 dice
Mushroom and oyster mushroom are put into dicer respectively to dice.
3 grindings
By the mushroom after dicing and oyster mushroom block respectively with ball milling mechanism paddle is imported, it is ground to 1000 mesh.
4 heating
After detection is qualified respectively, mushroom slurries and dry mushroom with abundant selenium slurry are injected separately into interlayer reaction kettle (band stirs), it is fixed
Hold to preset vol (mushroom 2000L；Oyster mushroom 3000L), mushroom is placed under the conditions of 80 DEG C, heats 3h；Oyster mushroom is in 100 DEG C of conditions
Under, 4h is heated, Agaricus campestris rich in selenium crude extract and mushroom with abundant selenium crude extract are respectively obtained.
5 filter for the first time
Above two crude extract is filtered through 1000 mesh filter screens, respectively obtains mushroom initial extraction liquid and oyster mushroom initial extraction
Liquid.
6 stratification
By initial extraction liquid inject holding vessel constant temperature (60 DEG C) stewing process, sealing, shading, time of repose be 90min with
On.
7 second of filtering
After the layering of mushroom initial extraction liquid, taking the supernatant ultrafiltration membrane classified filtering on upper layer, (molecule interception is respectively
50000 and 5000, first 50000, it is rear 5000), collect filtered fluid respectively；
It takes lower layer's turbid solution to carry out centrifugal treating (3500rpm, 30min), collects clarified solution；
The clarified solution of collection is used ultrafiltration membrance filter (molecule interception 50000) again, collects filtered fluid.
Merge and merge filtered fluid and clarified solution according to designated ratio, obtains mushroom amalgamation liquid, it is spare.
8 are concentrated by evaporation
Aforesaid liquid is subjected to vacuum (- 680mmhg) using economic benefits and social benefits vacuum evaporation apparatus and is evaporated concentration, oyster mushroom respectively
Liquid is concentrated by evaporation to 20 ° of B é of Baume degrees, and mushroom amalgamation liquid is concentrated by evaporation the oyster mushroom concentrate to 30 ° of B é of Baume degrees to get concentration
And mushroom concentrated liquid, two kinds of obtained concentrates are mixed to get selenium-rich mushroom seasoning.It detects its Se content and other refers to
It marks (amino-acid nitrogen), as a result as follows:
9. needs say that in actual production, oyster mushroom concentrate and mushroom concentrated liquid can be adjusted according to Se content demand
Mixed proportion.Which kind of, no matter with ratio mixing, all belong to the scope of protection of the present invention.
Embodiment 2
The fresh vegetable baste of selenium-rich provided in this embodiment the preparation method is as follows:
1. the blue flower liquid in selenium-rich west
After 1.1 take the blue flower 200kg in fresh selenium-rich west, light salt brine cleaning, ball milling slurrying after dicing obtains western blue flower slurries.
Slurries are injected interlayer reaction kettle by 1.2, are settled to preset vol 3000L, are placed under the conditions of 80 DEG C, after heating 3h,
Obtain crude extract.
1.3 filter for the first time
Crude extract after 1000 mesh filter screen filtrations, keep the temperature 60 DEG C, 1h stand, then through centrifugal treating (3000rpm,
40min) obtain western blue flower initial extraction liquid.
1.4 second of filtering
It is spare to collect filtered fluid through ultrafiltration membrance filter for initial liquid.
2 mushroom with abundant selenium liquid
2.1 take the dry mushroom with abundant selenium of 150kg (total selenium 175mg/kg), clear up campanulaceae, clean dirt, after impregnating 3h in clear water
Dicer is put into, ball milling mechanism paddle is injected after dicing and is ground to 1000 mesh, obtains oyster mushroom slurries.
Oyster mushroom slurries are injected interlayer reaction kettle by 2.2, are settled to preset vol 3000L, are placed under the conditions of 80 DEG C, are heated
3h obtains crude extract.
2.3 filter for the first time
Crude extract is filtered through 1000 mesh of strainer, then through centrifugal treating 3500rpm, 30min, obtains oyster mushroom initial extraction
Liquid.
2.4 second of filtering
It is spare to collect filtered fluid through ultrafiltration membrance filter for oyster mushroom initial extraction liquid.
3 are concentrated by evaporation
It uses economic benefits and social benefits vacuum evaporation apparatus to carry out vacuum (- 680mmhg) respectively above-mentioned 1,2 filtered fluid to be concentrated by evaporation extremely
20 ° of B é of Baume degrees obtain the blue flower liquid, mushroom with abundant selenium liquid in selenium-rich west and obtain the fresh vegetable baste of selenium-rich after mixing the two liquid,
Its Se content and other indexs (amino-acid nitrogen) are detected, as a result as follows:
4 merge solution: the mixed of the blue flower liquid in selenium-rich west and mushroom with abundant selenium liquid can be adjusted according to seasoning solution Se content demand
Composition and division in a proportion example.Which kind of, no matter with ratio mixing, all belong to the scope of protection of the present invention.
Embodiment 3
The preparation method of the selenium-rich mushroom seasoning of the dry powder-shaped present embodiments provided, specific as follows:
1. cleaning
It takes the dry mushroom with abundant selenium of 150kg (total selenium 175ppm, organic selenium content 70%), clears up campanulaceae, dirt is cleaned, in clear water
Middle immersion is spare.
2 dice
Oyster mushroom investment dicer is diced.
3 grindings
Oyster mushroom block after dicing imports ball milling mechanism paddle, is ground to 1000 mesh.
4 heating
After detection is qualified respectively, oyster mushroom slurry is injected separately into interlayer reaction kettle, preset vol 3000L is settled to, is placed in 95
Under the conditions of DEG C, 4h is heated, crude extract is obtained.
5 filter for the first time
Crude extract is filtered through 1000 mesh filter screens, obtains oyster mushroom initial extraction liquid.
6 stratification
Initial extraction liquid is injected into 60 DEG C of constant temperature stewing process of holding vessel, time of repose 90min.
7 second of filtering
After the layering of oyster mushroom initial extraction liquid, take the supernatant on upper layer spare, lower turbid carry out centrifugal treating (3500rpm,
30min), clarified solution is collected, supernatant and two kinds of liquid are merged, the ultrafiltration membrance filter for being 50000 with molecule interception was collected
Filtrate；
8 are concentrated by evaporation
Above-mentioned filtered fluid is carried out vacuum (- 680mmhg) using economic benefits and social benefits vacuum evaporation apparatus to be concentrated by evaporation to 20 ° of Baume degrees
B é obtains mushroom with abundant selenium concentrate, spare.
9 freeze-dryings
Above-mentioned concentrate is obtained into dry powder-shaped selenium-rich mushroom seasoning through frozen drying.
Its Se content and other indexs (amino-acid nitrogen) are detected, is injected in disk after cooling, as follows with freezing result:
| Selenium-rich mushroom seasoning (dry powder-shaped) | |
| Total selenium | 155.07ppm |
| Organic selenium | 154ppm |
Embodiment 4
The preparation method of selenium-rich well salt provided in this embodiment, specific as follows:
The 40kg selenium-rich mushroom seasoning (total Se content 35ppm) that Example 1 is prepared is spare, takes 1000kg pyrogen
Expect well salt, it is spare.
1, mixing for the first time, drying
Above-mentioned selenium-rich mushroom seasoning 20kg is uniformly drenched into (temperature in 1000kg hot charge well salt in mixed on low speed slot
At 85 DEG C or so), 20min is uniformly mixed, (period or spray iodine solution, salt compounded of iodine is made) after being sufficiently mixed, uses fluidized bed drying
Product salt after checking that mobility reaches requirement, takes out standing and is cooled to room temperature, obtain initial product salt.
2, second of mixing, drying
The above-mentioned remaining 20kg of selenium-rich mushroom seasoning is uniformly drenched again in mixed on low speed slot and is produced into above-mentioned initial salt
In product (temperature is at 75 DEG C or so), mix 30min, it is to be mixed uniformly after, anticaking agent is added, using fluidized bed drying product salt,
It checks mobility and detects after moisture content reaches requirement, take out to stand and be cooled to room temperature, obtain selenium-rich well salt.
Gained selenium-rich well salt product: having the mushroom appearance of relatively strong fragrance, and aromatic delicate flavour theoretically contains in every 1000g salt
There is the Se content of 1400 μ g, and organic selenium is calculated according to daily salt intake amount 10g, the selenium intake of 14 μ g can be obtained, according to
The standard of 50 μ g of national health people selenium-supply deducts the amount 24-36 μ g taken in normal food, can substantially meet human body
The requirement of selenium-supply.
Embodiment 5
The preparation method of selenium-rich sea salt provided in this embodiment, specific as follows:
The fresh vegetable seasoning 25kg (Se content 40ppm) of the selenium-rich that Example 2 is prepared is spare, takes 3 dry powder-shaped of example
Selenium-rich mushroom seasoning 3kg (Se content 155ppm) it is spare, take the particle sea salt of 1000kg, 14-20 mesh as raw material for standby.
1, it mixes for the first time
It is put into 1000kg room temperature raw material sea salt in mixed on low speed slot, is heated to 70 DEG C, then be uniformly added into the richness of dry powder-shaped
Selenium mushroom seasoning (period or spray iodine solution, salt compounded of iodine is made), mixes 20min, is uniformly mixed, then uniformly drench into the fresh vegetable tune of selenium-rich
Taste substance 25kg after being sufficiently mixed, using fluidized bed drying product salt, checks mobility and detects after moisture content reaches requirement, take
It stands and is cooled to room temperature out, obtain selenium-rich sea salt.
Certainly it should be noted that can not be mixed into iodine solution without salt compounded of iodine product, sea salt raw material product salt can be added without anticaking agent.
Products obtained therefrom: the appearance with stronger vegetables fragrance has stronger delicate flavour, taste is almost not added in gastronomical process
Essence, the selenium amount containing 1400 μ g in per kilogram salt reach 10g according to daily intake and calculate, and available 14 μ g take the photograph daily
Enter amount.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of preparation method of selenium-enriched plant seasoning, characterized in that it comprises:
Pulverising step；
The pulverising step includes: that selenium-enriched plant raw material is ground to 600-2000 mesh.
2. the preparation method of selenium-enriched plant seasoning according to claim 1, which is characterized in that in the pulverising step
Afterwards, the method also includes heating stepses；
The heating stepses include: to mix the plant material after grinding with water to be settled to preset vol, are placed in 60-100 DEG C of item
Under part, 3-6h is heated, selenium-enriched plant crude extract is obtained.
3. the preparation method of selenium-enriched plant seasoning according to claim 2, which is characterized in that in the heating stepses
Afterwards, the method also includes first time filtration steps；
The first time filtration step are as follows: by the selenium-enriched plant crude extract through strainer filtering, obtain initial extraction liquid.
4. the preparation method of selenium-enriched plant seasoning according to claim 3, which is characterized in that filtered in the first time
After step, the method also includes: stewing process
The stewing process step are as follows: the initial extraction liquid is subjected to stewing process, time of repose 60-120min.
5. the preparation method of selenium-enriched plant seasoning according to claim 4, which is characterized in that the stewing process it
Afterwards, the method also includes second filtration steps；
Second of filtration step are as follows:
The supernatant liquid filtering for being located at upper layer in the initial extraction liquid is taken, filtered fluid is collected；
It takes and is located at the progress centrifugal filtration processing of lower layer's turbid solution in the initial extraction liquid, collect clarified solution, refilter, collected
Filtrate；
Each filtered fluid is mixed, amalgamation liquid is obtained.
6. the preparation method of selenium-enriched plant seasoning according to claim 5, which is characterized in that filtered at described second
After step, the method also includes: concentration step or step of freeze drying；
Concentration step is that the amalgamation liquid is evaporated concentration, obtains the selenium-enriched plant seasoning of liquid；
Step of freeze drying is to be freeze-dried the selenium-enriched plant seasoning of the liquid, obtains the selenium-enriched plant seasoning of powdery
Material.
7. a kind of preparation method of selenium-rich salt, characterized in that it comprises:
Selenium-enriched plant seasoning is prepared using the preparation method of selenium-enriched plant seasoning of any of claims 1-6
Material；
The selenium-enriched plant seasoning is mixed with raw material salt.
8. the preparation method of selenium-rich salt according to claim 7, which is characterized in that be mixed into raw material salt described in every 1000kg
Selenium-enriched plant seasoning described in 3-100kg.
9. the preparation method of selenium-rich salt according to claim 7 or 8, which is characterized in that
The selenium-enriched plant seasoning is mixed with the raw material salt using spray mode.
10. the preparation method of selenium-rich salt according to claim 9, which is characterized in that the raw material salt is heated to temperature
When being 70-85 DEG C, the selenium-enriched plant seasoning is mixed with the raw material salt；
Preferably, the raw material salt is well salt or sea salt.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115363198A (en) * | 2021-05-17 | 2022-11-22 | 盐创(上海)科技有限公司 | Preparation method of selenium-rich edible salt |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101584454A (en) * | 2009-04-17 | 2009-11-25 | 佛山市海天调味食品有限公司 | Selenium-rich soy preparation method |
| CN103719833A (en) * | 2014-01-10 | 2014-04-16 | 申洁 | Selenium-enriched sparassis crispa powder as well as food preparation method and preparation |
| CN105077163A (en) * | 2015-07-19 | 2015-11-25 | 中盐榆林盐化有限公司 | Selenium-enriched salt and preparation method thereof |
| CN106136198A (en) * | 2016-07-15 | 2016-11-23 | 重庆市盐业（集团）有限公司 | Selenium salt and its preparation method and application |
| CN106579297A (en) * | 2016-11-30 | 2017-04-26 | 苏州硒谷科技有限公司 | Organic selenium-enriched plant salt and preparation method thereof |
| CN106901372A (en) * | 2016-12-28 | 2017-06-30 | 陕西天宝大豆食品技术研究所 | Full spirulina peptide nutrient food and preparation method thereof |
-
2018
- 2018-07-03 CN CN201810720669.6A patent/CN108967989A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101584454A (en) * | 2009-04-17 | 2009-11-25 | 佛山市海天调味食品有限公司 | Selenium-rich soy preparation method |
| CN103719833A (en) * | 2014-01-10 | 2014-04-16 | 申洁 | Selenium-enriched sparassis crispa powder as well as food preparation method and preparation |
| CN105077163A (en) * | 2015-07-19 | 2015-11-25 | 中盐榆林盐化有限公司 | Selenium-enriched salt and preparation method thereof |
| CN106136198A (en) * | 2016-07-15 | 2016-11-23 | 重庆市盐业（集团）有限公司 | Selenium salt and its preparation method and application |
| CN106579297A (en) * | 2016-11-30 | 2017-04-26 | 苏州硒谷科技有限公司 | Organic selenium-enriched plant salt and preparation method thereof |
| CN106901372A (en) * | 2016-12-28 | 2017-06-30 | 陕西天宝大豆食品技术研究所 | Full spirulina peptide nutrient food and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王彩云: "香菇调味汁的研究", 《中国调味品》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115363198A (en) * | 2021-05-17 | 2022-11-22 | 盐创(上海)科技有限公司 | Preparation method of selenium-rich edible salt |
| CN115363198B (en) * | 2021-05-17 | 2024-02-13 | 盐创(上海)科技有限公司 | Preparation method of selenium-enriched edible salt |
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