[go: up one dir, main page]

CN108940145B - Mixed pesticide microcapsule mixes preparation facilities - Google Patents

Mixed pesticide microcapsule mixes preparation facilities Download PDF

Info

Publication number
CN108940145B
CN108940145B CN201811099022.2A CN201811099022A CN108940145B CN 108940145 B CN108940145 B CN 108940145B CN 201811099022 A CN201811099022 A CN 201811099022A CN 108940145 B CN108940145 B CN 108940145B
Authority
CN
China
Prior art keywords
pesticide
needle
supply device
liquid supply
shell
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201811099022.2A
Other languages
Chinese (zh)
Other versions
CN108940145A (en
Inventor
司廷
张明
钟风靖
杨超宇
吴强
朱志强
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of Science and Technology of China USTC
Original Assignee
University of Science and Technology of China USTC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Science and Technology of China USTC filed Critical University of Science and Technology of China USTC
Priority to CN201811099022.2A priority Critical patent/CN108940145B/en
Publication of CN108940145A publication Critical patent/CN108940145A/en
Application granted granted Critical
Publication of CN108940145B publication Critical patent/CN108940145B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/26Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
    • A01N25/28Microcapsules or nanocapsules

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Plant Pathology (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a mixed pesticide microcapsule mixing preparation device which comprises a single-shaft needle, a coaxial needle, a shell material liquid supply device and a pesticide liquid supply device, wherein the coaxial needle comprises an inner needle and an outer needle sleeved on the outer side of the inner needle, the pesticide liquid supply device is used for conveying liquid medicine to the single-shaft needle and the inner needle, and the shell material liquid supply device is used for conveying a capsule material to the outer needle. In the mixed pesticide microcapsule mixing preparation device that this application provided, through setting up the pesticide that unipolar syringe needle processing did not contain the shell cyst wall material, the pesticide that contains the cyst wall material through coaxial syringe needle processing for in the pesticide use, the pesticide that does not contain the cyst wall material releases the use preferentially, and the pesticide that contains the cyst wall material is slowly released along with the after-decomposition of cyst wall material and pesticide diffusion pesticide, makes the pesticide can be used fully, and the rate of utilization of pesticide improves.

Description

混合农药微囊混合制备装置Mixed pesticide microcapsule mixing and preparation device

技术领域Technical field

本发明涉及农药制备技术领域,特别涉及一种混合农药微囊混合制备装置。The invention relates to the technical field of pesticide preparation, and in particular to a device for mixing and preparing mixed pesticide microcapsules.

背景技术Background technique

在农业生产中,为了提高产量,通常通过农药施放来达到作物病虫害防治目的,同时喷洒农药进行除草,使得作物具有更大的生存优势,减少劳动者作业量。In agricultural production, in order to increase yields, pesticides are usually used to control crop diseases and insect pests, and pesticides are sprayed for weeding at the same time, so that crops have a greater survival advantage and reduce labor workload.

在农药施放时,农药直接与水形成溶液或悬浊液直接喷洒到田间,虽然会有比较好的即时性,但是会有很大程度的农药浪费,同时会造成相当程度的环境污染,并且环境依赖性强,雨季极易造成农药的无效施放,农药的使用率较低When pesticides are applied, pesticides directly form a solution or suspension with water and are sprayed directly into the field. Although it will be more immediate, it will cause a large amount of pesticide waste and cause a considerable degree of environmental pollution. Strong dependence, the rainy season can easily lead to ineffective application of pesticides, and the use rate of pesticides is low.

因此,如何提高农药的使用率,是本领域技术人员亟待解决的技术问题。Therefore, how to improve the utilization rate of pesticides is an urgent technical problem that needs to be solved by those skilled in the art.

发明内容Contents of the invention

本发明的目的是提供一种混合农药微囊混合制备装置,以提高农药的使用率。The object of the present invention is to provide a device for mixing and preparing mixed pesticide microcapsules to improve the utilization rate of pesticides.

为实现上述目的,本发明提供一种混合农药微囊混合制备装置,包括单轴针头、同轴针头、壳材供液装置及农药供液装置,所述同轴针头包括内针头及套设在所述内针头外侧的外针头,所述农药供液装置用于向所述单轴针头和所述内针头输送药液,所述壳材供液装置用于向所述外针头输送囊材。In order to achieve the above object, the present invention provides a mixed pesticide microcapsule mixing and preparation device, which includes a uniaxial needle, a coaxial needle, a shell liquid supply device and a pesticide liquid supply device. The coaxial needle includes an inner needle and a sheath mounted on There is an outer needle outside the inner needle, the pesticide liquid supply device is used to transport medicinal liquid to the single-axis needle and the inner needle, and the shell material liquid supply device is used to transport capsule material to the outer needle.

优选地,还包括高压电源、连接在所述高压电源正极端部的导电板及连接在所述高压电源负极的电极板,所述单轴针头和所述同轴针头均安装在所述导电板上,所述导电板和所述电极板正对设置,所述单轴针头和所述同轴针头的输出端位于所述导电板和所述电极板之间。Preferably, it also includes a high-voltage power supply, a conductive plate connected to the positive end of the high-voltage power supply, and an electrode plate connected to the negative pole of the high-voltage power supply. Both the uniaxial needle and the coaxial needle are installed on the conductive plate. The conductive plate and the electrode plate are arranged facing each other, and the output ends of the uniaxial needle and the coaxial needle are located between the conductive plate and the electrode plate.

优选地,所述导电板由多个可拆卸连接的阵列模块构成,所述阵列模块上至少安装有一个所述单轴针头和至少一个所述同轴针头。Preferably, the conductive plate is composed of a plurality of detachably connected array modules, and at least one of the uniaxial needles and at least one of the coaxial needles are installed on the array modules.

优选地,至少一个所述阵列模块上所述单轴针头和所述同轴针头的个数比为1:2。Preferably, the number ratio of the single-axis needles and the coaxial needles on at least one of the array modules is 1:2.

优选地,至少一个所述阵列模块上所述单轴针头和所述同轴针头的个数比为2:1。Preferably, the number ratio of the single-axis needles and the coaxial needles on at least one of the array modules is 2:1.

优选地,还包括储气罐和壳材气体减压阀,所述储气罐通过壳材进气管道与所述壳材供液装置连通,所述壳材供液装置的内部腔体为封闭腔体,所述壳材气体减压阀位于所述壳材进气管道上。Preferably, it also includes a gas storage tank and a shell gas pressure reducing valve. The gas storage tank is connected to the shell liquid supply device through a shell air inlet pipe. The internal cavity of the shell liquid supply device is closed. In the cavity, the shell gas pressure reducing valve is located on the shell air inlet pipe.

优选地,所述壳材供液装置上设有第一气压表和第一减压阀,所述壳材供液装置通过壳材输送管向所述外针头输送壳材,所述壳材输送管上设有第一流量控制阀。Preferably, the shell material liquid supply device is provided with a first air pressure gauge and a first pressure reducing valve, and the shell material liquid supply device transports shell material to the outer needle through a shell material delivery pipe, and the shell material delivery device The pipe is provided with a first flow control valve.

优选地,还包括农药液气体减压阀,所述储气罐通过农药进气管道与所述农药供液装置连通,所述农药供液装置的内部腔体为封闭腔体,所述农药液气体减压阀位于所述农药进气管道上。Preferably, it also includes a pesticide liquid gas pressure reducing valve, the gas storage tank is connected to the pesticide liquid supply device through a pesticide air inlet pipe, the internal cavity of the pesticide liquid supply device is a closed cavity, and the pesticide liquid The gas pressure reducing valve is located on the pesticide air inlet pipe.

优选地,所述农药供液装置上设有第二气压表和第二减压阀,所述农药供液装置通过农药输送管向所述内针头和所述单轴针头输送农药液,所述农药输送管上设有第二流量控制阀。Preferably, the pesticide liquid supply device is provided with a second air pressure gauge and a second pressure reducing valve, and the pesticide liquid supply device transports pesticide liquid to the inner needle and the single-axis needle through a pesticide delivery pipe. The pesticide delivery pipe is provided with a second flow control valve.

优选地,还包括用于接收农药的农药接收装置。Preferably, a pesticide receiving device for receiving pesticides is also included.

在上述技术方案中,本发明提供的混合农药微囊混合制备装置包括单轴针头、同轴针头、壳材供液装置及农药供液装置,同轴针头包括内针头及套设在内针头外侧的外针头,农药供液装置用于向单轴针头和内针头输送药液,壳材供液装置用于向外针头输送囊材。In the above technical solution, the mixed pesticide microcapsule mixing and preparation device provided by the present invention includes a uniaxial needle, a coaxial needle, a shell liquid supply device and a pesticide liquid supply device. The coaxial needle includes an inner needle and a sheath set outside the inner needle. The outer needle, the pesticide liquid supply device is used to transport chemical liquid to the single-axis needle and the inner needle, and the shell material liquid supply device is used to transport capsule material to the outer needle.

通过上述描述可知,在本申请提供的混合农药微囊混合制备装置中,通过设置单轴针头加工不包含外壳囊材的农药,通过同轴针头加工包含囊材的农药,使得在农药使用过程中,不包含囊材的农药优先释放使用。包含囊材的农药随着囊材分解和农药扩散后农药缓慢释放,使得农药能够被充分使用,农药的使用率提高。It can be seen from the above description that in the mixed pesticide microcapsule mixing and preparation device provided by the present application, a single-axis needle is provided to process pesticides that do not contain shell capsule materials, and a coaxial needle is used to process pesticides that contain capsule materials, so that during the use of pesticides, , pesticides that do not contain capsule materials are released and used first. The pesticides containing the capsule material are slowly released as the capsule material decomposes and the pesticide diffuses, so that the pesticide can be fully used and the usage rate of the pesticide is increased.

附图说明Description of drawings

为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据提供的附图获得其他的附图。In order to explain the embodiments of the present invention or the technical solutions in the prior art more clearly, the drawings needed to be used in the description of the embodiments or the prior art will be briefly introduced below. Obviously, the drawings in the following description are only These are embodiments of the present invention. For those of ordinary skill in the art, other drawings can be obtained based on the provided drawings without exerting creative efforts.

图1为本发明实施例所提供的混合农药微囊混合制备装置的结构示意图;Figure 1 is a schematic structural diagram of a mixed pesticide microcapsule mixing and preparation device provided by an embodiment of the present invention;

图2为本发明实施例所提供的农药微囊的结构示意图;Figure 2 is a schematic structural diagram of a pesticide microcapsule provided by an embodiment of the present invention;

图3为本发明实施例所提供的农药高分子微球的结构示意图;Figure 3 is a schematic structural diagram of the pesticide polymer microspheres provided by the embodiment of the present invention;

图4为本发明实施例所提供的第一种阵列模块与同轴针头和单轴针头的结构示意图;Figure 4 is a schematic structural diagram of the first array module, coaxial needle and single-axis needle provided by the embodiment of the present invention;

图5为图4的俯视图;Figure 5 is a top view of Figure 4;

图6为本发明实施例所提供的第二种阵列模块与同轴针头和单轴针头的结构示意图;Figure 6 is a schematic structural diagram of the second array module, coaxial needle and single-axis needle provided by the embodiment of the present invention;

图7为图6的俯视图;Figure 7 is a top view of Figure 6;

图8为本发明实施例所提供的第三种阵列模块与同轴针头和单轴针头的结构示意图;Figure 8 is a schematic structural diagram of a third array module, a coaxial needle and a single-axis needle provided by an embodiment of the present invention;

图9为图8的俯视图。FIG. 9 is a top view of FIG. 8 .

其中图1-9中:1、导电板;2、电极板;3、高压电源;4、储气罐;5、壳材气体减压阀;6、壳材储液器;7、泵;Among them, in Figure 1-9: 1. Conductive plate; 2. Electrode plate; 3. High-voltage power supply; 4. Gas storage tank; 5. Shell gas pressure reducing valve; 6. Shell liquid reservoir; 7. Pump;

8、壳材供液装置;8-1、第一减压阀;8-2、第一气压表;8. Shell liquid supply device; 8-1. First pressure reducing valve; 8-2. First pressure gauge;

9、第一流量控制阀;10、壳材输送管;11、农药输送管;12、内针头原液入口;13、外针头原液入口;14、单轴针头原液入口;15、外针头;16、内针头;17、农药微囊;18、单轴针头;19、农药高分子微球;20、阵列模块;21、农药液气体减压阀;22、农药储液器;9. First flow control valve; 10. Shell material delivery pipe; 11. Pesticide delivery pipe; 12. Inner needle raw solution inlet; 13. Outer needle raw solution inlet; 14. Single-axis needle raw solution inlet; 15. Outer needle; 16. Inner needle; 17. Pesticide microcapsule; 18. Uniaxial needle; 19. Pesticide polymer microspheres; 20. Array module; 21. Pesticide liquid gas pressure reducing valve; 22. Pesticide liquid reservoir;

23、农药供液装置;23-1、第二减压阀;23-2、第二气压表;23. Pesticide liquid supply device; 23-1. Second pressure reducing valve; 23-2. Second air pressure gauge;

24、第二流量控制阀。24. Second flow control valve.

具体实施方式Detailed ways

本发明的核心是提供一种混合农药微囊混合制备装置,以提高农药的使用率。The core of the present invention is to provide a mixing and preparation device for mixed pesticide microcapsules to improve the utilization rate of pesticides.

为了使本领域的技术人员更好地理解本发明的技术方案,下面结合附图和实施方式对本发明作进一步的详细说明。In order to enable those skilled in the art to better understand the technical solutions of the present invention, the present invention will be further described in detail below in conjunction with the drawings and embodiments.

请参考图1至图9,在一种具体实施方式中,本发明具体实施例提供的混合农药微囊混合制备装置包括单轴针头18、同轴针头、壳材供液装置8及农药供液装置23,其中,单轴针头18、同轴针头可以在二维平面上排布阵列。同轴针头包括内针头16及套设在内针头16外侧的外针头15,内针头16和外针头15同轴布置。农药供液装置23用于向单轴针头18和内针头16输送药液,壳材供液装置8用于向外针头15输送囊材。优选,单轴针头18、同轴针头均为多个,且整体呈阵列排布。为了便于收集农药,优选,该混合农药微囊混合制备装置还包括用于接收农药的农药接收装置,具体的,农药接收装置根据实际需要可以为金属板、滚筒、传送带、液体接收池等,以便收集制备的农药微囊17和农药高分子微球19。Please refer to Figures 1 to 9. In a specific implementation, the mixed pesticide microcapsule mixing and preparation device provided by specific embodiments of the present invention includes a single-axis needle 18, a coaxial needle, a shell material liquid supply device 8 and a pesticide liquid supply device. Device 23, in which the uniaxial needles 18 and coaxial needles can be arranged in an array on a two-dimensional plane. The coaxial needle includes an inner needle 16 and an outer needle 15 that is sleeved outside the inner needle 16. The inner needle 16 and the outer needle 15 are coaxially arranged. The pesticide liquid supply device 23 is used to transport the pesticide liquid to the single-axis needle 18 and the inner needle 16 , and the shell material liquid supply device 8 is used to transport the capsule material to the outer needle 15 . Preferably, there are multiple uniaxial needles 18 and coaxial needles, and the whole is arranged in an array. In order to facilitate the collection of pesticides, preferably, the mixed pesticide microcapsule mixing and preparation device also includes a pesticide receiving device for receiving pesticides. Specifically, the pesticide receiving device can be a metal plate, a roller, a conveyor belt, a liquid receiving pool, etc. according to actual needs, so that The prepared pesticide microcapsules 17 and pesticide polymer microspheres 19 are collected.

为了便于拆装混合农药微囊制备装置,优选,导电板1由多个可拆卸连接的阵列模块20构成,阵列模块20上至少安装有一个单轴针头18和至少一个同轴针头,如图4所示。针头模块上的单轴针头18和同轴针头的数目可以调整,以实现对农药微囊17和农药高分子微球19突释和缓释性能的精确调控,具体的,如图8所示,阵列模块20上单轴针头18和同轴针头的个数比为1:2,具体地导电板上至少一个阵列模块20上单轴针头18和同轴针头的个数比为1:2,其它阵列模块20上单轴针头18和同轴针头的个数可以自由设置。当然,如图6所示,至少阵列模块20上单轴针头18和同轴针头的个数比还可以为2:1,具体地导电板上至少一个阵列模块20上单轴针头18和同轴针头的个数比为2:1,其它阵列模块20上单轴针头18和同轴针头的个数可以自由设置。当然,也可以根据对农药微囊17和农药高分子微球19突释和缓释性能的不同要求,选择其它数量同轴和单轴针头18组成的针头模块。具体的,在针头模块的针头顶部形成稳定的锥-射流结构,并且分别破碎形成农药微囊17和农药高分子微球19。农药微囊17作为外壳为高分子材料,内核由高分子与农药混合形成,其中,农药高分子微球19由高分子和农药混合形成。In order to facilitate the disassembly and assembly of the mixed pesticide microcapsule preparation device, preferably, the conductive plate 1 is composed of a plurality of detachably connected array modules 20. At least one uniaxial needle 18 and at least one coaxial needle are installed on the array module 20, as shown in Figure 4 shown. The number of uniaxial needles 18 and coaxial needles on the needle module can be adjusted to achieve precise control of the burst and sustained release properties of the pesticide microcapsules 17 and pesticide polymer microspheres 19. Specifically, as shown in Figure 8, The number ratio of the uniaxial needles 18 and the coaxial needles on the array module 20 is 1:2. Specifically, the number ratio of the uniaxial needles 18 and the coaxial needles on at least one array module 20 on the conductive plate is 1:2. The number of single-axis needles 18 and coaxial needles on the array module 20 can be set freely. Of course, as shown in FIG. 6 , at least the number ratio of the uniaxial needles 18 and the coaxial needles on the array module 20 can be 2:1. Specifically, the ratio of the uniaxial needles 18 and the coaxial needles on at least one array module 20 on the conductive board can be 2:1. The ratio of the number of needles is 2:1, and the number of single-axis needles 18 and coaxial needles on other array modules 20 can be freely set. Of course, needle modules composed of other numbers of coaxial and uniaxial needles 18 can also be selected according to different requirements for the burst release and sustained release properties of the pesticide microcapsules 17 and the pesticide polymer microspheres 19 . Specifically, a stable cone-jet structure is formed on the top of the needle of the needle module, and is broken down to form pesticide microcapsules 17 and pesticide polymer microspheres 19 respectively. The outer shell of the pesticide microcapsule 17 is a polymer material, and the inner core is made of a mixture of polymer and pesticide. Among them, the pesticide polymer microsphere 19 is made of a mixture of polymer and pesticide.

制备混合农药微囊,时,农药储液器22内的原液,具体可以为高分子和农药的混合溶液,壳材储液器6内的原液,具体可以为高分子溶液,经泵7分别被抽入密闭的农药供液装置23和壳材供液装置8中,农药供液装置23中的原液进入内针头16和单轴针头18,壳材供液装置8中的原液则进入外针头15,具体的,单轴针头18和同轴针头输出端通过设置高压电源的作用下,出料,具体的,通过在导电板1和电极板2之间设置高电压,在电场力形成的剪切力的作用下,形成单个农药颗粒。When preparing mixed pesticide microcapsules, the original solution in the pesticide reservoir 22 can be a mixed solution of polymers and pesticides, and the original solution in the shell material reservoir 6 can be a polymer solution. Pump into the sealed pesticide liquid supply device 23 and shell material liquid supply device 8. The raw liquid in the pesticide liquid supply device 23 enters the inner needle 16 and the single-axis needle 18, and the raw liquid in the shell material liquid supply device 8 enters the outer needle 15. , specifically, the single-axis needle 18 and the coaxial needle output end are discharged under the action of a high-voltage power supply. Specifically, by setting a high voltage between the conductive plate 1 and the electrode plate 2, the shear formed by the electric field force Under the action of force, individual pesticide particles are formed.

通过上述描述可知,在本申请具体实施例所提供的混合农药微囊混合制备装置中,通过设置单轴针头18加工不包含外壳囊材的农药,通过同轴针头加工包含囊材的农药,使得在农药使用过程中,不包含囊材的农药优先释放使用,包含囊材的农药随着囊材分解和农药扩散后农药缓慢释放,使得农药能够被充分使用,农药的使用率提高。It can be seen from the above description that in the mixed pesticide microcapsule mixing and preparation device provided by the specific embodiment of the present application, the pesticides that do not contain the shell capsule material are processed by setting the single-axis needle 18, and the pesticides that contain the capsule material are processed by the coaxial needle, so that During the use of pesticides, pesticides that do not contain capsule materials are released and used first. Pesticides containing capsule materials are slowly released as the capsule materials decompose and the pesticides diffuse, so that the pesticides can be fully used and the pesticide usage rate is increased.

本混合农药微囊混合制备装置可以通过控制模块上的单轴针头18、同轴针头的数量来控制所制备的混合农药微囊的突释和缓释性能,提高农药的使用效率,降低农药的使用成本,减少对环境和人的危害,具有广泛的应用前景以及很高的潜在应用价值。The mixed pesticide microcapsule mixing and preparation device can control the burst release and sustained release properties of the prepared mixed pesticide microcapsules by controlling the number of uniaxial needles 18 and coaxial needles on the module, thereby improving the use efficiency of pesticides and reducing the consumption of pesticides. The cost of use reduces the harm to the environment and people, and it has broad application prospects and high potential application value.

采用集群化的针头阵列进行农药微囊17和农药高分子微球19的制备,提高了农药微囊17和农药高分子微球19的生产效率,并且可以通过控制阵列上的针头组成、壳材原液和农药原液流量、内壳材原液和农药原液成分来控制所制备的混合农药微囊的农药释放性能,实现一步到位地制备混合农药微囊。Using a clustered needle array to prepare pesticide microcapsules 17 and pesticide polymer microspheres 19 improves the production efficiency of pesticide microcapsules 17 and pesticide polymer microspheres 19, and can control the needle composition and shell material on the array. The pesticide release performance of the prepared mixed pesticide microcapsules can be controlled by controlling the flow rate of the original solution and pesticide original solution, the inner shell material original solution, and the composition of the pesticide original solution, thereby achieving one-step preparation of mixed pesticide microcapsules.

优选的,该混合农药微囊混合制备装置还包括高压电源3、连接在高压电源3正极端部的导电板1及连接在高压电源3负极的电极板2,单轴针头18和同轴针头均安装在导电板1上,导电板1和电极板2正对设置,单轴针头18和同轴针头的输出端位于导电板1和电极板2之间。采用电雾化技术制备混合农药微囊,其制备的微囊具有大小均匀,结构完整,农药包裹率高,便于接收等优点。Preferably, the mixed pesticide microcapsule mixing and preparation device also includes a high-voltage power supply 3, a conductive plate 1 connected to the positive end of the high-voltage power supply 3, and an electrode plate 2 connected to the negative pole of the high-voltage power supply 3. The uniaxial needle 18 and the coaxial needle are both It is installed on the conductive plate 1, the conductive plate 1 and the electrode plate 2 are arranged facing each other, and the output end of the uniaxial needle 18 and the coaxial needle is located between the conductive plate 1 and the electrode plate 2. Mixed pesticide microcapsules are prepared using electroatomization technology. The microcapsules prepared have the advantages of uniform size, complete structure, high pesticide encapsulation rate, and easy reception.

进一步,该混合农药微囊混合制备装置还包括储气罐4和壳材气体减压阀5,储气罐4通过壳材进气管道与壳材供液装置8连通,壳材供液装置8的内部腔体为封闭腔体,壳材气体减压阀5位于壳材进气管道上。优选的,壳材供液装置8上设有第一气压表8-2和第一减压阀8-1,壳材供液装置8通过壳材输送管10向外针头15输送壳材,壳材输送管10上设有第一流量控制阀9。Further, the mixed pesticide microcapsule mixing and preparation device also includes a gas storage tank 4 and a shell material gas pressure reducing valve 5. The gas storage tank 4 is connected to the shell material liquid supply device 8 through the shell material air inlet pipe. The shell material liquid supply device 8 The internal cavity is a closed cavity, and the shell gas pressure reducing valve 5 is located on the shell air inlet pipe. Preferably, the shell material liquid supply device 8 is provided with a first air pressure gauge 8-2 and a first pressure reducing valve 8-1. The shell material liquid supply device 8 transports shell material to the outer needle 15 through the shell material delivery pipe 10. The material transport pipe 10 is provided with a first flow control valve 9 .

更进一步,该混合农药微囊混合制备装置还包括农药液气体减压阀21,储气罐4通过农药进气管道与农药供液装置23连通,农药供液装置23的内部腔体为封闭腔体,农药液气体减压阀21位于农药进气管道上。优选的,农药供液装置23上设有第二气压表23-2和第二减压阀23-1,农药供液装置23通过农药输送管11向内针头16和单轴针头18输送农药液,农药输送管11上设有第二流量控制阀24。Furthermore, the mixed pesticide microcapsule mixing and preparation device also includes a pesticide liquid gas pressure reducing valve 21. The gas storage tank 4 is connected to the pesticide liquid supply device 23 through the pesticide air inlet pipe. The internal cavity of the pesticide liquid supply device 23 is a closed cavity. body, the pesticide liquid gas pressure reducing valve 21 is located on the pesticide air inlet pipe. Preferably, the pesticide liquid supply device 23 is provided with a second air pressure gauge 23-2 and a second pressure reducing valve 23-1. The pesticide liquid supply device 23 delivers pesticide liquid to the inner needle 16 and the single-axis needle 18 through the pesticide delivery pipe 11. , the pesticide delivery pipe 11 is provided with a second flow control valve 24.

工作时,壳材供液装置8和农药供液装置23内均为密闭腔体,壳材原液和农药原液逐渐流入腔体后,液体上方气体逐渐被压缩,气压逐渐增大,使壳材原液和农药原液的流出速度逐步增大,直到壳材供液装置8和农药供液装置23中原液的流入量与流出量一致。During operation, both the shell material liquid supply device 8 and the pesticide liquid supply device 23 are closed cavities. After the shell material raw liquid and the pesticide raw liquid gradually flow into the cavity, the gas above the liquid is gradually compressed, and the air pressure gradually increases, causing the shell material raw liquid to flow into the cavity. and the outflow speed of the pesticide liquid gradually increase until the inflow amount of the original liquid in the shell material liquid supply device 8 and the pesticide liquid supply device 23 is consistent with the outflow amount.

由于实际制备混合农药微囊时,壳材原液和农药原液单位时间内流入壳材供液装置8和农药供液装置23中的体积较少,与腔体内的气体体积相比可忽略不计,壳材供液装置8和农药供液装置23中气体体积可视为不变,即壳材供液装置8和农药供液装置23中气压始终保持稳定不变,使得壳材供液装置8和农药供液装置23输出的壳材原液和农药原液流量保持不变,从而达到稳定壳材原液和农药原液流量的效果。Since when actually preparing mixed pesticide microcapsules, the volume of the shell material stock solution and the pesticide stock solution flowing into the shell material liquid supply device 8 and the pesticide liquid supply device 23 per unit time is small and can be ignored compared with the gas volume in the cavity. The gas volume in the shell material liquid supply device 8 and the pesticide liquid supply device 23 can be regarded as constant, that is, the air pressure in the shell material liquid supply device 8 and the pesticide liquid supply device 23 always remains stable and constant, so that the shell material liquid supply device 8 and the pesticide liquid supply device 23 The flow rate of the shell material raw liquid and the pesticide raw liquid output by the liquid supply device 23 remains unchanged, thereby achieving the effect of stabilizing the flow rates of the shell material raw liquid and the pesticide raw liquid.

当壳材原液和农药原液流量很大时,单位时间内流入壳材供液装置8和农药供液装置23的液体体积相较于腔体内气体体积无法被忽略,壳材供液装置8和农药供液装置23内气体体积将被大幅压缩以提供足够的气压,使得壳材供液装置8和农药供液装置23的原液流出量和流入量保持一致。此时壳材供液装置8和农药供液装置23无法起到稳定壳材原液和农药原液流量的作用,需要打开壳材气体减压阀5和农药液气体减压阀21,使储气罐4中的气体进入壳材供液装置8和农药供液装置23,以保证壳材供液装置8和农药供液装置23中气体体积的稳定。第一减压阀8-1和第二减压阀23-1的压力可设置临界值(一般为壳材供液装置8和农药供液装置23工作时的稳定内压或壳材供液装置8和农药供液装置23所能承受的最大内压),当壳材供液装置8和农药供液装置23中的气压大于这一临界值时,第一减压阀8-1和第二减压阀23-1打开,使壳材供液装置8和农药供液装置23中气压降低直至达到临界值为止。第一气压表8-2和第二气压表23-2实时显示壳材供液装置8和农药供液装置23内的气压值,以便于保证壳材供液装置8和农药供液装置23中的气压稳定。由壳材供液装置8和农药供液装置23中流出的壳材原液和农药原液分别经第一流量控制阀9和第二流量控制阀24到达对应出口,经管道分流后分别注入阵列模块20对应位置的相应入口。When the flow rate of the shell material stock solution and the pesticide stock solution is very large, the volume of liquid flowing into the shell material liquid supply device 8 and the pesticide liquid supply device 23 per unit time cannot be ignored compared to the gas volume in the cavity, and the shell material liquid supply device 8 and the pesticide liquid supply device 23 cannot be ignored. The gas volume in the liquid supply device 23 will be greatly compressed to provide sufficient air pressure, so that the outflow and inflow of the raw liquid from the shell material liquid supply device 8 and the pesticide liquid supply device 23 remain consistent. At this time, the shell material liquid supply device 8 and the pesticide liquid supply device 23 cannot play a role in stabilizing the flow rate of the shell material liquid and pesticide liquid. It is necessary to open the shell gas pressure reducing valve 5 and the pesticide liquid gas pressure reducing valve 21 to allow the gas storage tank to The gas in 4 enters the shell liquid supply device 8 and the pesticide liquid supply device 23 to ensure the stability of the gas volume in the shell liquid supply device 8 and the pesticide liquid supply device 23. The pressure of the first pressure reducing valve 8-1 and the second pressure reducing valve 23-1 can be set to a critical value (generally the stable internal pressure of the shell material liquid supply device 8 and the pesticide liquid supply device 23 when working or the shell material liquid supply device 8 and the maximum internal pressure that the pesticide liquid supply device 23 can withstand), when the air pressure in the shell liquid supply device 8 and the pesticide liquid supply device 23 is greater than this critical value, the first pressure reducing valve 8-1 and the second The pressure reducing valve 23-1 is opened to reduce the air pressure in the shell material liquid supply device 8 and the pesticide liquid supply device 23 until it reaches a critical value. The first air pressure gauge 8-2 and the second air pressure gauge 23-2 display the air pressure values in the shell liquid supply device 8 and the pesticide liquid supply device 23 in real time, so as to ensure that the pressure in the shell liquid supply device 8 and the pesticide liquid supply device 23 is The air pressure is stable. The shell material liquid and pesticide liquid flowing out from the shell material liquid supply device 8 and the pesticide liquid supply device 23 reach the corresponding outlets through the first flow control valve 9 and the second flow control valve 24 respectively, and are respectively injected into the array module 20 after being diverted through the pipeline. The corresponding entrance to the corresponding location.

本说明书中各个实施例采用递进的方式描述,每个实施例重点说明的都是与其他实施例的不同之处,各个实施例之间相同相似部分互相参见即可。Each embodiment in this specification is described in a progressive manner. Each embodiment focuses on its differences from other embodiments. The same and similar parts between the various embodiments can be referred to each other.

对所公开的实施例的上述说明,使本领域专业技术人员能够实现或使用本发明。对这些实施例的多种修改对本领域的专业技术人员来说将是显而易见的,本文中所定义的一般原理可以在不脱离本发明的精神或范围的情况下,在其它实施例中实现。因此,本发明将不会被限制于本文所示的这些实施例,而是要符合与本文所公开的原理和新颖特点相一致的最宽的范围。The above description of the disclosed embodiments enables those skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be practiced in other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (7)

1.一种混合农药微囊混合制备装置,其特征在于,包括单轴针头(18)、同轴针头、壳材供液装置(8)及农药供液装置(23),所述同轴针头包括内针头(16)及套设在所述内针头(16)外侧的外针头(15),所述农药供液装置(23)用于向所述单轴针头(18)和所述内针头(16)输送药液,所述壳材供液装置(8)用于向所述外针头(15)输送囊材;1. A mixed pesticide microcapsule mixing and preparation device, characterized in that it includes a uniaxial needle (18), a coaxial needle, a shell material liquid supply device (8) and a pesticide liquid supply device (23). The coaxial needle It includes an inner needle (16) and an outer needle (15) set outside the inner needle (16). The pesticide liquid supply device (23) is used to supply the single-axis needle (18) and the inner needle (16) To transport medicinal liquid, the shell material liquid supply device (8) is used to deliver capsule material to the outer needle (15); 还包括高压电源(3)、连接在所述高压电源(3)正极端部的导电板(1)及连接在所述高压电源(3)负极的电极板(2),所述单轴针头(18)和所述同轴针头均安装在所述导电板(1)上,所述导电板(1)和所述电极板(2)正对设置,所述单轴针头(18)和所述同轴针头的输出端位于所述导电板(1)和所述电极板(2)之间;It also includes a high-voltage power supply (3), a conductive plate (1) connected to the positive end of the high-voltage power supply (3), and an electrode plate (2) connected to the negative end of the high-voltage power supply (3). The single-axis needle ( 18) and the coaxial needle are installed on the conductive plate (1), the conductive plate (1) and the electrode plate (2) are arranged facing each other, the uniaxial needle (18) and the The output end of the coaxial needle is located between the conductive plate (1) and the electrode plate (2); 还包括储气罐(4)和壳材气体减压阀(5),所述储气罐(4)通过壳材进气管道与所述壳材供液装置(8)连通,所述壳材供液装置(8)的内部腔体为封闭腔体,所述壳材气体减压阀(5)位于所述壳材进气管道上;It also includes a gas storage tank (4) and a shell gas pressure reducing valve (5). The gas storage tank (4) is connected to the shell liquid supply device (8) through the shell air inlet pipe. The internal cavity of the liquid supply device (8) is a closed cavity, and the shell gas pressure reducing valve (5) is located on the shell air inlet pipe; 还包括农药液气体减压阀(21),所述储气罐(4)通过农药进气管道与所述农药供液装置(23)连通,所述农药供液装置(23)的内部腔体为封闭腔体,所述农药液气体减压阀(21)位于所述农药进气管道上。It also includes a pesticide liquid gas pressure reducing valve (21). The gas storage tank (4) is connected to the pesticide liquid supply device (23) through a pesticide air inlet pipe. The internal cavity of the pesticide liquid supply device (23) In order to seal the cavity, the pesticide liquid gas pressure reducing valve (21) is located on the pesticide air inlet pipe. 2.根据权利要求1所述的混合农药微囊混合制备装置,其特征在于,所述导电板(1)由多个可拆卸连接的阵列模块(20)构成,所述阵列模块(20)上至少安装有一个所述单轴针头(18)和至少一个所述同轴针头。2. The mixed pesticide microcapsule mixing and preparation device according to claim 1, characterized in that the conductive plate (1) is composed of a plurality of detachably connected array modules (20), and the array module (20) At least one said uniaxial needle (18) and at least one said coaxial needle are installed. 3.根据权利要求2所述的混合农药微囊混合制备装置,其特征在于,至少一个所述阵列模块(20)上所述单轴针头(18)和所述同轴针头的个数比为1:2。3. The mixed pesticide microcapsule mixing and preparation device according to claim 2, characterized in that the number ratio of the uniaxial needles (18) and the coaxial needles on at least one of the array modules (20) is 1:2. 4.根据权利要求2所述的混合农药微囊混合制备装置,其特征在于,至少一个所述阵列模块(20)上所述单轴针头(18)和所述同轴针头的个数比为2:1。4. The mixed pesticide microcapsule mixing and preparation device according to claim 2, characterized in that the number ratio of the uniaxial needles (18) and the coaxial needles on at least one of the array modules (20) is 2:1. 5.根据权利要求4所述的混合农药微囊混合制备装置,其特征在于,所述壳材供液装置(8)上设有第一气压表(8-2)和第一减压阀(8-1),所述壳材供液装置(8)通过壳材输送管(10)向所述外针头(15)输送壳材,所述壳材输送管(10)上设有第一流量控制阀(9)。5. The mixed pesticide microcapsule mixing and preparation device according to claim 4, characterized in that the shell liquid supply device (8) is provided with a first air pressure gauge (8-2) and a first pressure reducing valve ( 8-1), the shell material liquid supply device (8) delivers shell material to the outer needle (15) through the shell material delivery pipe (10), and the shell material delivery pipe (10) is provided with a first flow rate Control valve (9). 6.根据权利要求1所述的混合农药微囊混合制备装置,其特征在于,所述农药供液装置(23)上设有第二气压表(23-2)和第二减压阀(23-1),所述农药供液装置(23)通过农药输送管(11)向所述内针头(16)和所述单轴针头(18)输送农药液,所述农药输送管(11)上设有第二流量控制阀(24)。6. The mixed pesticide microcapsule mixing and preparation device according to claim 1, characterized in that the pesticide liquid supply device (23) is provided with a second air pressure gauge (23-2) and a second pressure reducing valve (23). -1), the pesticide liquid supply device (23) delivers pesticide liquid to the inner needle (16) and the single-axis needle (18) through the pesticide delivery pipe (11), and the pesticide delivery pipe (11) A second flow control valve (24) is provided. 7.根据权利要求1-6中任一项所述的混合农药微囊混合制备装置,其特征在于,还包括用于接收农药的农药接收装置。7. The device for mixing and preparing mixed pesticide microcapsules according to any one of claims 1 to 6, further comprising a pesticide receiving device for receiving pesticides.
CN201811099022.2A 2018-09-20 2018-09-20 Mixed pesticide microcapsule mixes preparation facilities Active CN108940145B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811099022.2A CN108940145B (en) 2018-09-20 2018-09-20 Mixed pesticide microcapsule mixes preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811099022.2A CN108940145B (en) 2018-09-20 2018-09-20 Mixed pesticide microcapsule mixes preparation facilities

Publications (2)

Publication Number Publication Date
CN108940145A CN108940145A (en) 2018-12-07
CN108940145B true CN108940145B (en) 2024-02-23

Family

ID=64471716

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811099022.2A Active CN108940145B (en) 2018-09-20 2018-09-20 Mixed pesticide microcapsule mixes preparation facilities

Country Status (1)

Country Link
CN (1) CN108940145B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110651783A (en) * 2018-06-28 2020-01-07 江苏龙灯化学有限公司 Preparation method of pesticide liquid composition, pesticide liquid composition prepared based on preparation method and application of pesticide liquid composition
CN113907058B (en) * 2021-09-08 2022-12-13 安徽农业大学 Pesticide spraying device based on flow focusing and operation method thereof

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4251195A (en) * 1975-12-26 1981-02-17 Morishita Jinta Company, Limited Apparatus for making miniature capsules
CN201200887Y (en) * 2007-12-13 2009-03-04 上海理工大学 Constant pressure infusion device
CN101837255A (en) * 2009-03-17 2010-09-22 华东理工大学 Method and device for preparing micro-bubbles
JP2011255319A (en) * 2010-06-09 2011-12-22 Kobe Univ Method for producing vesicles
CN202725148U (en) * 2012-05-24 2013-02-13 上海理工大学 Concentric double-sprayer microcapsule preparation device
JP2014196297A (en) * 2013-03-08 2014-10-16 学校法人慶應義塾 Drug release method using laser
CN203955203U (en) * 2014-05-21 2014-11-26 宁波宝成生物科技发展有限公司 A kind of microcapsules process units that can sterile working
CN104707575A (en) * 2015-03-30 2015-06-17 西南科技大学 Preparation method of magnetic core-shell alginate microsphere adsorbent
CN106622055A (en) * 2016-10-18 2017-05-10 上海理工大学 Preparation device of high-voltage electric field microcapsules
CN107013440A (en) * 2017-05-23 2017-08-04 中国科学技术大学 The microlayer model active preparation facilities and method of embedded piezoelectric stack disturbance
CN208852872U (en) * 2018-09-20 2019-05-14 中国科学技术大学 Mixed pesticide microcapsule mixing preparation device

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080182056A1 (en) * 2007-01-30 2008-07-31 Eric Bakker Hollow Microsphere Particles

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4251195A (en) * 1975-12-26 1981-02-17 Morishita Jinta Company, Limited Apparatus for making miniature capsules
CN201200887Y (en) * 2007-12-13 2009-03-04 上海理工大学 Constant pressure infusion device
CN101837255A (en) * 2009-03-17 2010-09-22 华东理工大学 Method and device for preparing micro-bubbles
JP2011255319A (en) * 2010-06-09 2011-12-22 Kobe Univ Method for producing vesicles
CN202725148U (en) * 2012-05-24 2013-02-13 上海理工大学 Concentric double-sprayer microcapsule preparation device
JP2014196297A (en) * 2013-03-08 2014-10-16 学校法人慶應義塾 Drug release method using laser
CN203955203U (en) * 2014-05-21 2014-11-26 宁波宝成生物科技发展有限公司 A kind of microcapsules process units that can sterile working
CN104707575A (en) * 2015-03-30 2015-06-17 西南科技大学 Preparation method of magnetic core-shell alginate microsphere adsorbent
CN106622055A (en) * 2016-10-18 2017-05-10 上海理工大学 Preparation device of high-voltage electric field microcapsules
CN107013440A (en) * 2017-05-23 2017-08-04 中国科学技术大学 The microlayer model active preparation facilities and method of embedded piezoelectric stack disturbance
CN208852872U (en) * 2018-09-20 2019-05-14 中国科学技术大学 Mixed pesticide microcapsule mixing preparation device

Also Published As

Publication number Publication date
CN108940145A (en) 2018-12-07

Similar Documents

Publication Publication Date Title
CN108940145B (en) Mixed pesticide microcapsule mixes preparation facilities
CN205922020U (en) Fertigation air entrainment agitating unit
CN107487445B (en) Centrifugal medicine sprays many rotor unmanned aerial vehicle
CN204930093U (en) A new type of electric duster for the prevention and control of vegetable diseases and insect pests in facilities
CN205269517U (en) But wettable powder production is with mixing machine
CN208490671U (en) A kind of novel collection spray irrigation integrated device suitable for greenhouse
CN109261048B (en) Pesticide solid-liquid mixing device
CN208852872U (en) Mixed pesticide microcapsule mixing preparation device
CN107950529B (en) Spodoptera nutans trapping and killing composition and preparation method of nano preparation thereof
CN212414452U (en) A special pest killing device for landscaping
CN107996551A (en) A kind of sprayer for being used to prevent harmful organism
CN207639452U (en) A kind of multi-functional administration device
CN208001944U (en) A kind of online mixed medicine pesticide spraying system of real-time Variable Composition
CN207612930U (en) A kind of environmentally-friendly plastic beehive mixing device
CN205906219U (en) Agricultural unmanned aerial vehicle powder releaser
CN205916333U (en) Pre -pressurizing formula sprinkling system that plant protection unmanned aerial vehicle used
CN201197932Y (en) Fluid dynamic ultrasonic nano-calcium carbonate mixer
CN207126398U (en) One kind flies anti-agricultural chemicals pretreatment system
CN210406381U (en) Pesticide spraying system for agricultural greenhouse
CN204395894U (en) There is the pellet blender of volatile oil flusher
CN204273012U (en) A kind of ultrasonic atomizatio micro sprayer
CN107261878A (en) One kind flies anti-agricultural chemicals pretreatment system
TWI682718B (en) Suspended anti-mosquito bait and preparation method thereof
CN206586232U (en) Seeding device
CN205695223U (en) A kind of liquid hand-held disinsector

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant