CN108935496A - Long-acting mould-proof bacteria remover and preparation method thereof - Google Patents
Long-acting mould-proof bacteria remover and preparation method thereof Download PDFInfo
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- CN108935496A CN108935496A CN201810712674.2A CN201810712674A CN108935496A CN 108935496 A CN108935496 A CN 108935496A CN 201810712674 A CN201810712674 A CN 201810712674A CN 108935496 A CN108935496 A CN 108935496A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/24—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients to enhance the sticking of the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
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- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
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Abstract
The present invention relates to a kind of long-acting mould-proof bacteria removers, include the raw material of following weight percent: mould inhibitor 0.1-2%；Thickener 0.2-2%；Fungicide 0.005-5%；Solvent 5-50%；Surfactant 0.1-5%；Auxiliary agent 0-1%；Water 40-90%.The long-acting mould-proof bacteria remover can continue mould proof 90 days or more, and there is height to sprawl adhesion, and it is mould proof to be suitable for household.
Description
Technical field
The present invention relates to daily chemical product fields, more particularly to long-acting mould-proof bacteria remover and preparation method thereof.
Background technique
As the microorganisms such as mould and bacterium, saccharomycete, it is distributed widely in the biosphere of the earth, growth and breeding are very
Rapidly, metabolism is very vigorous, and is easy variation and adapts to environment, so under appropriate conditions will be in various objects
It grows and breeds on product.The growth of mould is that we live common phenomenon at home, especially regional in south China, annual
Plum rain season and " going back to Nan Tian " time, moist environment are even more the breeding ground that mould breeds.Common phenomenon are as follows: wall occurs mould
Become, furniture blackspot etc. occurs in growing between apparent mould, sanitation of bath-room.
Influence of the growth of mould to human health is even more that cannot ignore.The spore of mould with air flowing
And disperse everywhere, the malaise symptoms such as asthma and headache, dizziness, nausea, rhinorrhea, sneezing can be caused, it is serious also to cause
Respiratory system failure and initiation Pulmonary Diseases.There are many method for preventing article from going mouldy, and it is micro- to can control temperature, humidity, oxygen etc.
The environmental condition that biology is depended on for existence, or physical factor and chemical bactericide are used to kill microorganism or inhibit microorganism
Growing environment etc..Chinese patent CN103651449A discloses a kind of long-acting mould-proof deodorant and preparation method thereof, patent
Design use iodopropynyl butyl formate and parachlorometaxylenol for mould inhibitor, using propylene glycol, polypropylene glycol and
Polyethylene glycol is solubilisation aids, prepares liquid spray type long-acting mould-proof deodorant.But iodopropynyl butyl formate
Additive amount is up to 3%-8%, and the long-acting mould-proof deodorant low-temperature stability of preparation is poor.And liquid sprays mold proof product cannot be compared with
The position at good covering household dead angle.In addition it in spraying process, is also easy to that human body is caused to suck, there are security risks；It is Chinese special
Sharp CN 107549185A discloses a kind of leather fungicide and preparation method thereof, from the point of view of the formula of patent disclosure, uses third
Ring azoles, three kinds of active constituents of sodium pyrithione and iodopropynyl butyl carbamate, heterogeneity have antibacterial activity group, phase
It is had obvious synergistic function between mutually, improves the antibacterial spectrality of mould inhibitor.CN105885203A discloses a kind of solid
Film class mold proof product, it is lower in the application value of household wall and furniture surface.
Summary of the invention
Based on this, the present invention provides a kind of long-acting mould-proof bacteria remover and preparation method thereof.
The specific technical proposal is:
A kind of long-acting mould-proof bacteria remover, includes the raw material of following weight percent:
The mould inhibitor is selected from iodopropynyl butyl formate, the chloro- 3,5-dimethylphenol of 2,4- bis- and didecyl
One or more of methyl polyoxyethanyl propionic acid ammonium；
The thickener be selected from acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, hydroxyethyl cellulose,
One or more of carboxymethyl cellulose and modified magnesium aluminium silicate.
The long-acting mould-proof bacteria remover includes the raw material of following weight percent in one of the embodiments:
The thickener is selected from acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters crosslinking in one of the embodiments,
Polymer.
The mould inhibitor is selected from iodopropynyl butyl formate in one of the embodiments,.
The fungicide is selected from dodecyl benzyl dimethyl ammonium chloride, cetyl two in one of the embodiments,
Methylbenzyl ammonium chloride one or more of gathers own methylene hydrochloride and Cetylpyridinium Chloride.
The solvent is selected from ethyl alcohol, propylene glycol, glycerine, propylene glycol monomethyl ether and dipropyl two in one of the embodiments,
One of alcohol methyl ether is a variety of.
The surfactant is selected from fatty alcohol polyoxyethylene ether, rilanit special, poly- mountain in one of the embodiments,
One or more of pear ester and sorbitan fatty acid ester.
The auxiliary agent includes pH adjusting agent in one of the embodiments, and the pH adjusting agent is selected from organic base.
The organic base is selected from triethanolamine or monoethanolamine in one of the embodiments,.
The present invention also provides the preparation methods of above-mentioned long-acting mould-proof bacteria remover, comprising the following steps:
The thickener and surfactant are added in the water, stirring obtains component A to dissolving；
The mould inhibitor is added in the solvent, stirs to being completely dissolved, adds the fungicide, stirs, obtains B group
Point；
The B component is added into the component A, is stirred evenly, be added auxiliary agent, obtain thickened mixt to get.
The pH value of the thickened mixt is 7.5-9.0 in one of the embodiments,.
Compared with prior art, the invention has the following advantages:
For the present invention by joined specific thickener into specific mould-proof bacteria-removing system, the advantage of generation is as follows:
(1) after particular thickener being added, iodopropynyl formic acid fourth can be reduced under the premise of not influencing drug effect
The additive amount of the mould inhibitors such as ester makes to be not easy to be precipitated under its low temperature, the stability of raising mould-proof bacteria-removing system, and sustainable mould proof 90
More than it, achieve the purpose that play drug effect for a long time.
(2) after particular thickener being added, mildewproof bacteria remover is in gel, there is height to sprawl adhesion, in the mould proof mistake of household
Cheng Zhong is preferably attached to household surface, and can easily cover blank area, and mould proof contact is more abundant, solves household dead angle
It is difficult to the problem covered.
(3) present invention using the antibacterial activity group of heterogeneity by being made specific mould inhibitor and bactericide compounded
With, can kill or inhibit fungus growth and kill and inhibit bacterial growth, have apparent synergistic effect, improve it is antibacterial
Spectrality.On the basis of long-acting mould-proof, 99.9% is up to the killing rate of household common bacteria, solves existing mould inhibitor sterilization
Effect technical problem on the weak side.
Specific embodiment
It to facilitate the understanding of the present invention, below will be to invention is more fully described.The present invention can be with many not
With form realize, however it is not limited to embodiment described herein.On the contrary, purpose of providing these embodiments is makes to this
Disclosure of the invention content understanding is more thorough and comprehensive.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein "and/or" includes one or more phases
Any and all combinations of the listed item of pass.
Long-acting mould-proof bacteria remover and preparation method thereof of the invention is made below in conjunction with specific embodiment further details of
Explanation.
Raw material used in following specific embodiments can derive from commercially available unless otherwise noted.
Didecyl methyl polyoxyethanyl propionic acid ammonium CAS No.94667-33-1.
Embodiment 1-3
According to raw material each in table 1 and its content, prepare the long-acting mould-proof bacteria remover of embodiment 1-3, it is specific the preparation method comprises the following steps:
In container A, first acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer is added in soft water,
It stirs evenly, sufficiently dissolves.Rilanit special and essence are added, stirring is allowed to dissolve, and obtains component A.
In another container B, iodopropynyl butyl formate, propylene glycol and ethyl alcohol are stirred evenly, make iodo third
Alkynylamino butyl formate is completely dissolved, and dodecyl benzyl dimethyl ammonium chloride is added, and stirring and dissolving obtains B component.
Solution in container B is added into A, is stirred sufficiently at transparent and homogeneous liquid.Monoethanolamine is added, adjusts pH value
It is 8, thickens mixed system.Sample detection, carried out after the assay was approved it is filling, packaging to get.
The raw material and content of the long-acting mould-proof bacteria remover of 1 embodiment 1-3 of table
Embodiment 4-6
According to raw material each in table 2 and its content, prepare the long-acting mould-proof bacteria remover of embodiment 4-6, it is specific the preparation method comprises the following steps:
In container A, first acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer is added in soft water,
It stirs evenly, sufficiently dissolves.Rilanit special and essence are added, stirring is allowed to dissolve, and obtains component A.
In another container B, didecyl methyl polyoxyethanyl propionic acid ammonium, propylene glycol and ethyl alcohol are stirred evenly, didecyl is made
Ylmethyl polyoxyethanyl propionic acid ammonium is completely dissolved, and addition gathers own methylene hydrochloride, and stirring and dissolving obtains B component.
Solution in container B is added into A, is stirred sufficiently at transparent and homogeneous liquid.Monoethanolamine is added, adjusts pH value
It is 8, thickens mixed system.Sample detection, carried out after the assay was approved it is filling, packaging to get.
The raw material and content of the long-acting mould-proof bacteria remover of 2 embodiment 4-6 of table
Embodiment 7-9
According to raw material each in table 3 and its content, prepare the long-acting mould-proof bacteria remover of embodiment 7-9, it is specific the preparation method comprises the following steps:
It in container A, first adds hydroxyethyl cellulose into soft water, stirs evenly, sufficiently dissolve.Add hydrogenation castor
Sesame oil and essence, stirring are allowed to dissolve, and obtain component A.
In another container B, iodopropynyl butyl formate, propylene glycol and ethyl alcohol are stirred evenly, make iodo third
Alkynylamino butyl formate is completely dissolved, and dodecyl benzyl dimethyl ammonium chloride is added, and stirring and dissolving obtains B component.
Solution in container B is added into A, is stirred to obtain the final product.Sample detection is carried out filling, packaging after the assay was approved,
To obtain the final product.
The raw material and content of the long-acting mould-proof bacteria remover of 3 embodiment 7-9 of table
Embodiment 10-12
According to raw material each in table 4 and its content, the long-acting mould-proof bacteria remover of embodiment 10-12, specific preparation method are prepared
Are as follows:
In container A, first modified magnesium aluminium silicate is added in soft water, is stirred evenly, is sufficiently dissolved.Add hydrogenation castor
Sesame oil and essence, stirring are allowed to dissolve, and obtain component A.
In another container B, iodopropynyl butyl formate, propylene glycol and ethyl alcohol are stirred evenly, make iodo third
Alkynylamino butyl formate is completely dissolved, and dodecyl benzyl dimethyl ammonium chloride is added, and stirring and dissolving obtains B component.
Solution in container B is added into A, is stirred to obtain the final product.Sample detection is carried out filling, packaging after the assay was approved,
To obtain the final product.
The raw material and content of the long-acting mould-proof bacteria remover of 4 embodiment 10-12 of table
Embodiment 13-15
According to raw material each in table 5 and its content, the long-acting mould-proof bacteria remover of embodiment 13-15, specific preparation method are prepared
Are as follows:
In container A, first acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer is added in soft water,
It stirs evenly, sufficiently dissolves.Rilanit special and essence are added, stirring is allowed to dissolve, and obtains component A.
In another container B, iodopropynyl butyl formate, propylene glycol and ethyl alcohol are stirred evenly, make iodo third
Alkynylamino butyl formate is completely dissolved, and Cetylpyridinium Chloride is added, and stirring and dissolving obtains B component.
Solution in container B is added into A, is stirred sufficiently at transparent and homogeneous liquid.Triethanolamine is added, adjusts pH value
It is 8, thickens mixed system.Sample detection, carried out after the assay was approved it is filling, packaging to get.
The raw material and content of the long-acting mould-proof bacteria remover of 5 embodiment 13-15 of table
Comparative example 1-4
According to raw material each in table 6 and its content, prepare the long-acting mould-proof bacteria remover of comparative example 1-4, specific preparation method with
Embodiment 1 is identical.
The raw material and content of the long-acting mould-proof bacteria remover of 6 comparative example 1-4 of table
Effect application test example
The long-acting mould-proof bacteria remover of embodiment 1-15 and comparative example 1-4 are tested for the property.The specific method is as follows:
1, mould proof measuring evaluation method
Using filter paper as carrier, the mould proof spraying anti-mold effect to aspergillus niger is evaluated.
1) mould proof test: carrier and pretreatment mode: carrier is filter paper, is cut into 4 × 4cm size, and 121 DEG C of high pressures are gone out
Bacterium, 50 DEG C of drying.It adds the mould proof feed liquid of 0.5g respectively on filter paper, it is stand-by to be placed in natural air drying in Biohazard Safety Equipment.
2) preparation of microbiological contamination plate: being added 200 μ L (1-9) × 105CFU/mL black-koji mould suspension on SDA plate, applies
Cloth is uniform, for use.
3) it cultivates: filter paper sample being flattened on the SDA plate of microbiological contamination, carrier is allowed to come into full contact with culture medium.It is positive to put
Enter 28 ± 1 DEG C of cultures.
4) determine grade:
The mould proof grade criterion of table 8
2, sterilization is quantitative kills test
The Guantitative bactericidal test of mildewproof bacteria remover is tested referring to the requirement in the Ministry of Public Health " disinfection technology standard ".
Test strain is common bacteria Escherichia coli, staphylococcus aureus.Mildewproof bacteria remover is in following item to the killing rate of bacterium
Test obtains under part: test fluid concentration is stoste, action time 30min.Experimental result is shown in Table 9,10.
The evaluation of 9 anti-mold effect of table
The evaluation of 10 bactericidal effect of table
There is table 9,10 it is found that the long-acting mould-proof bacteria remover of embodiment 1-15 can effectively inhibit the growth of mildew, it is effectively anti-
The mould time can reach 90 days or more, and be up to common bacteria Escherichia coli and the golden yellow staphylococcic killing rate of Soviet Union
99.9%, also there is height to sprawl characteristic, realizes comprehensive protection to household.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
Limitations on the scope of the patent of the present invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Protect range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of long-acting mould-proof bacteria remover, which is characterized in that include the raw material of following weight percent:
The mould inhibitor is selected from iodopropynyl butyl formate, the chloro- 3,5-dimethylphenol of 2,4- bis- and didecyl methyl
One or more of polyoxyethanyl propionic acid ammonium；
The thickener is selected from acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, hydroxyethyl cellulose, carboxylic first
One or more of base cellulose and modified magnesium aluminium silicate.
2. long-acting mould-proof bacteria remover according to claim 1, which is characterized in that include the original of following weight percent
Material:
3. long-acting mould-proof bacteria remover according to claim 1, which is characterized in that the thickener is selected from acrylic acid (ester)
Class/C10-30 alkylol acrylamide acid esters cross-linked polymer.
4. long-acting mould-proof bacteria remover according to claim 1, which is characterized in that the mould inhibitor is selected from iodo propinyl ammonia
Base butyl formate.
5. long-acting mould-proof bacteria remover according to claim 1-4, which is characterized in that the fungicide is selected from 12
Zephiran, cetalkonium chloride gather in own methylene hydrochloride and Cetylpyridinium Chloride
It is one or more of.
6. long-acting mould-proof bacteria remover according to claim 1-4, which is characterized in that the solvent be selected from ethyl alcohol,
One of propylene glycol, glycerine, propylene glycol monomethyl ether and dipropylene glycol methyl ether are a variety of.
7. long-acting mould-proof bacteria remover according to claim 1-4, which is characterized in that the surfactant is selected from
One or more of fatty alcohol polyoxyethylene ether, rilanit special, polysorbate and sorbitan fatty acid ester.
8. long-acting mould-proof bacteria remover according to claim 1-4, which is characterized in that the auxiliary agent includes pH tune
Agent is saved, the pH adjusting agent is selected from organic base.
9. long-acting mould-proof bacteria remover according to claim 8, which is characterized in that the organic base is selected from triethanolamine or list
Ethanol amine.
10. a kind of preparation method of the described in any item long-acting mould-proof bacteria removers of claim 1-9, which is characterized in that including with
Lower step:
The thickener and surfactant are added in the water, stirring obtains component A to dissolving；
The mould inhibitor is added in the solvent, stirs to being completely dissolved, adds the fungicide, stirs, obtains B component；
The B component is added into the component A, is stirred evenly, be added auxiliary agent, obtain thickened mixt to get.
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Cited By (5)
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| CN110024781A (en) * | 2019-05-23 | 2019-07-19 | 昆明野水生物科技有限公司 | A kind of preparation and its application that can kill gemma rapidly at normal temperature |
| CN110037023A (en) * | 2019-04-19 | 2019-07-23 | 广州佳伲斯防霉抗菌科技有限公司 | A kind of antimildew disinfectant and preparation method thereof for container |
| CN110915804A (en) * | 2019-12-20 | 2020-03-27 | 苏州市科渠金属制品有限公司 | Organic dye mildew preventive |
| CN114711242A (en) * | 2022-02-14 | 2022-07-08 | 绍兴崇高新材料科技有限公司 | Novel mildew-proof material and preparation method and application thereof |
| CN115486451A (en) * | 2022-10-22 | 2022-12-20 | 广州市宝绅科技应用有限公司 | Long-acting slow-release antibacterial mildew inhibitor |
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