CN108904329A - A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof - Google Patents
A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof Download PDFInfo
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- CN108904329A CN108904329A CN201810942671.8A CN201810942671A CN108904329A CN 108904329 A CN108904329 A CN 108904329A CN 201810942671 A CN201810942671 A CN 201810942671A CN 108904329 A CN108904329 A CN 108904329A
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- polyacid
- hand cleanser
- environment friendly
- friendly bacteriostatic
- deionized water
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- 230000003385 bacteriostatic effect Effects 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 241000931143 Gleditsia sinensis Species 0.000 claims abstract description 31
- 239000000126 substance Substances 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- 239000008367 deionised water Substances 0.000 claims description 32
- 229910021641 deionized water Inorganic materials 0.000 claims description 32
- 238000003756 stirring Methods 0.000 claims description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 21
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 17
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 16
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 239000003921 oil Substances 0.000 claims description 15
- 235000019198 oils Nutrition 0.000 claims description 15
- 239000004599 antimicrobial Substances 0.000 claims description 14
- 239000000341 volatile oil Substances 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 13
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 11
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 10
- 239000011964 heteropoly acid Substances 0.000 claims description 10
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 claims description 9
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 8
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 8
- 238000001027 hydrothermal synthesis Methods 0.000 claims description 8
- 229940068918 polyethylene glycol 400 Drugs 0.000 claims description 8
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 8
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 8
- 239000011780 sodium chloride Substances 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- 235000011152 sodium sulphate Nutrition 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 150000004665 fatty acids Chemical class 0.000 claims description 7
- 238000007605 air drying Methods 0.000 claims description 6
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 6
- 150000001408 amides Chemical class 0.000 claims description 5
- 235000019864 coconut oil Nutrition 0.000 claims description 5
- 239000003240 coconut oil Substances 0.000 claims description 5
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims description 2
- 125000002252 acyl group Chemical group 0.000 claims description 2
- 150000001412 amines Chemical class 0.000 claims description 2
- 238000002242 deionisation method Methods 0.000 claims description 2
- 210000004209 hair Anatomy 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- DHRLEVQXOMLTIM-UHFFFAOYSA-N phosphoric acid;trioxomolybdenum Chemical compound O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.OP(O)(O)=O DHRLEVQXOMLTIM-UHFFFAOYSA-N 0.000 claims description 2
- IYDGMDWEHDFVQI-UHFFFAOYSA-N phosphoric acid;trioxotungsten Chemical compound O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.OP(O)(O)=O IYDGMDWEHDFVQI-UHFFFAOYSA-N 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- CGFYHILWFSGVJS-UHFFFAOYSA-N silicic acid;trioxotungsten Chemical compound O[Si](O)(O)O.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1 CGFYHILWFSGVJS-UHFFFAOYSA-N 0.000 claims description 2
- 239000003643 water by type Substances 0.000 claims description 2
- 235000015841 Acacia concinna Nutrition 0.000 claims 1
- 244000044167 Acacia concinna Species 0.000 claims 1
- 238000004090 dissolution Methods 0.000 claims 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract description 6
- 229930182490 saponin Natural products 0.000 abstract description 6
- 150000007949 saponins Chemical class 0.000 abstract description 6
- 201000010099 disease Diseases 0.000 abstract description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 5
- 241000894006 Bacteria Species 0.000 abstract description 3
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 abstract description 3
- 210000001508 eye Anatomy 0.000 abstract description 3
- 230000012010 growth Effects 0.000 abstract description 3
- 239000003242 anti bacterial agent Substances 0.000 abstract description 2
- 230000003266 anti-allergic effect Effects 0.000 abstract description 2
- 230000001093 anti-cancer Effects 0.000 abstract description 2
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 2
- 230000000845 anti-microbial effect Effects 0.000 abstract description 2
- 230000000840 anti-viral effect Effects 0.000 abstract description 2
- 229940088710 antibiotic agent Drugs 0.000 abstract description 2
- 230000003115 biocidal effect Effects 0.000 abstract description 2
- 230000004071 biological effect Effects 0.000 abstract description 2
- 238000009395 breeding Methods 0.000 abstract description 2
- 230000001488 breeding effect Effects 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 239000002114 nanocomposite Substances 0.000 abstract description 2
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000002736 nonionic surfactant Substances 0.000 abstract 1
- 230000000144 pharmacologic effect Effects 0.000 abstract 1
- 239000004519 grease Substances 0.000 description 9
- 208000015181 infectious disease Diseases 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 238000002156 mixing Methods 0.000 description 5
- 230000005540 biological transmission Effects 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 235000013162 Cocos nucifera Nutrition 0.000 description 3
- 244000060011 Cocos nucifera Species 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 206010022000 influenza Diseases 0.000 description 3
- 230000000644 propagated effect Effects 0.000 description 3
- 229960005486 vaccine Drugs 0.000 description 3
- 208000035473 Communicable disease Diseases 0.000 description 2
- 206010022004 Influenza like illness Diseases 0.000 description 2
- 241000700605 Viruses Species 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000011081 inoculation Methods 0.000 description 2
- 239000006210 lotion Substances 0.000 description 2
- 230000029058 respiratory gaseous exchange Effects 0.000 description 2
- 210000003491 skin Anatomy 0.000 description 2
- 206010041232 sneezing Diseases 0.000 description 2
- 208000024891 symptom Diseases 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 206010000087 Abdominal pain upper Diseases 0.000 description 1
- 206010067484 Adverse reaction Diseases 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 208000017667 Chronic Disease Diseases 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 241000712431 Influenza A virus Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 208000031320 Teratogenesis Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 230000009610 hypersensitivity Effects 0.000 description 1
- 208000037797 influenza A Diseases 0.000 description 1
- 229960003971 influenza vaccine Drugs 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 210000003928 nasal cavity Anatomy 0.000 description 1
- XRRQZKOZJFDXON-UHFFFAOYSA-N nitric acid;silver Chemical compound [Ag].O[N+]([O-])=O XRRQZKOZJFDXON-UHFFFAOYSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 230000035935 pregnancy Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 241000712461 unidentified influenza virus Species 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof, belong to technical field of daily necessities.The present invention, which utilizes, contains a large amount of saponin(e substance in the pod of Chinese honey locust, saponin(e substance has multiple biological activities and pharmacological action, such as anti-inflammatory, antiallergy, it is antiviral, a variety of diseases such as anticancer, saponin(e is very good natural nonionic surfactant again simultaneously, to the skin of majority, eyes are non-stimulated, the characteristics of on ecological environment without influencing, it is supported on the polyacid compound of metallic silver ion doping, prepare the growth that anti-biotic material is killed and inhibits harmful bacteria, breeding, realize the health of the product for civilian use and cleaning for living environment, play the multi-efficiency of silver ion and polyacid nanocomposite Synergistic antimicrobial.
Description
Technical field
The present invention relates to a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof, belong to technical field of daily necessities.
Background technique
As a kind of infectious disease for seriously threatening human health, the infection sources of Flu-A is illness and symptomless infection
Animal and people, route of transmission mainly have 2 kinds, are coughed by patient and symptomless infection person or the droplet of sneezing generation is through breathing
Road is propagated, and passes through the environment of the respiratory secretions of contact patient and symptomless infection person, alimentary canal excreta and pollution
Behind communal facility surface, then contact itself oral cavity, nasal cavity, eyes etc. mucous membrane propagated.Crowd is generally susceptible, generally
Symptoms are mild by people, can get well by short, but some people at highest risk are poor to influenza resistance, after infection, symptom compared with
Weight, is easy to appear multiple complications, can lead to death when serious.People at highest risk mainly includes：Pregnancy women, with breathing system
The crowd of system disease, disease of cardiovascular system chronic diseases, children and the elderly etc..
Harm of the influenza A virus to crowd is reduced, takes effective precautionary measures particularly important, that takes at present arranges
Apply including：Control the infection sources, cutting route of transmission and protection healthy population.It is rear two that crowd, which protects the main path of own health,
Kind, it can be realized by some simple methods, for example form good personal hygiene habit, abundance sleep is diligent in tempering body
Body reduces pressure, and sufficient nutrition avoids contact with the respiratory disease patients such as influenza-like symptom or pneumonia, pays attention to personal hygiene,
It washes one's hands commonly using soap and clear water, especially after cough or sneezing, avoids contact with the animal that may propagate influenza, avoid
Go to crowded place etc..In addition inoculation influenza vaccines are also a kind of effective method, but influenza virus is still constantly sending out
It changes different, once generating new antigenicity, currently available vaccines, existing vaccines is by there is no the effect of prevention & protection, and in addition vaccine inoculation may
Cause different degrees of adverse reaction, if injection site is ached, rubescent, influenza-like symptom, Nausea and vomiting, stomachache, diarrhea, head
It is dizzy, cause some mild reactions such as hypersensitivity, serious person will appear carcinogenic, teratogenesis, permanent or significant disability, even result in
It is dead.
Washing one's hands is method that most convenient effectively cuts off transmission approach.Hand can touch diversified in environment
Pathogenic microorganism, hand have a large amount of sebaceous glands and a hair follicle, secrete grease and sweat, conducive to the adherency of bacterial virus, and hand
Temperature humidity is suitble to many bacterial viruses growths and long-term surviving, and contaminated hand is easy when touching other positions of body will be sick
Substance is propagated over together, causes disease.Prevent disease by washing one's hands, not only it is noted that the frequency of use and method of hand cleanser,
Effective hand lotion is more used, in face of constantly attacking for influenza and other communicable diseases, reinforces personal hygiene and likes, use
Effective hand lotion, often washes one's hands, and can effectively cut off route of transmission, is a kind of active and effective method.
Summary of the invention
The technical problems to be solved by the invention：For hand cleanser higher cost in the prior art, product is used for a long time
There is the problem of injury to the skin of people, provides a kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof.
In order to solve the above technical problems, the technical solution adopted by the present invention is that：
A kind of environment friendly bacteriostatic polyacid hand cleanser, the hand cleanser chemical composition and weight percent content are as follows：
10~12% dodecyl polyoxyethylene ether sodium sulphate, 12~15% neopelexes, 1~3% coco-nut oil fatty acid
Diglycollic amide, 0.6~1.2% sodium chloride, 1~2% glycerol, 0.1~0.2% essence, 0.05~0.20% antimicrobial factors, deionization
Water surplus.
The antimicrobial factors be silver nitrate dissolve in deionized water with after heteropoly acid hybrid reaction be added ammonium oxalate, Chinese honey locust
Volatile oil, polyethylene glycol 400 are uniformly mixed and dry obtained after hydro-thermal reaction.
Described weight of material part be 0.5~1.0 part of silver nitrate, 100~150 parts of deionized waters, 1.2~3.2 parts of heteropoly acids,
0.1~0.5 part of ammonium oxalate, 1~2 part of Chinese honey locust volatile oil, 4~8 parts of polyethylene glycol 400s.
The heteropoly acid is one or more of phosphotungstic acid, phosphomolybdic acid, silico-tungstic acid.
The hybrid reaction process is to be heated with stirring to 60~80 DEG C under nitrogen atmosphere and continue 1~4h of stirring.
The hydrothermal temperature is 120~240 DEG C.
The Chinese honey locust volatile oil is to crush to be laid on filter paper after air-drying Chinese honey locust, is placed in 3~5cm above deionized water
On the bracket at place, steam is passed through in condenser pipe by heating deionized water to boiling, and standing takes upper oil, and with anhydrous sulphur
Sour magnesium dehydration is made.
A kind of preparation method of the environment friendly bacteriostatic polyacid hand cleanser, the specific steps are：
（1）It crushes and is laid on filter paper after Chinese honey locust is air-dried, is placed on the bracket above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to boiling, and standing takes upper oil, and is dehydrated with anhydrous magnesium sulfate, is obtained Chinese honey locust and is waved
Hair oil；
（2）It takes silver nitrate to be added in deionized water to stir, ammonium oxalate, Chinese honey locust volatilization is added after adding heteropoly acid hybrid reaction
Oil, polyethylene glycol 400 are uniformly mixed and dry after hydro-thermal reaction, obtain antimicrobial factors；
（3）Dodecyl polyoxyethylene ether sodium sulphate, neopelex is taken to be added in deionized water, with 300~400r/
Min is heated with stirring to 50~60 DEG C, 20~30min of insulated and stirred, and coco-nut oil fatty acid diethanol acyl is added after being cooled to room temperature
Amine, sodium chloride, glycerol continue 20~30min of stirring, add essence, antimicrobial factors, add after 30~40min of insulated and stirred and go
Ionized water obtains environment friendly bacteriostatic polyacid hand cleanser to 100g.
The present invention is compared with other methods, and advantageous effects are：
（1）The present invention has multiple biological activities and medicine using a large amount of saponin(e substance, saponin(e substance is contained in the pod of Chinese honey locust
Reason effect, such as anti-inflammatory, antiallergy, antiviral, a variety of diseases of anticancer, while saponin(e are very good natural nonionic table again
Face activating agent, it is non-stimulated to skin, the eyes of majority, on ecological environment without influence the characteristics of, be supported on metallic silver from
On the polyacid compound of son doping, prepares anti-biotic material and kill and inhibit the growth of harmful bacteria, breeding, realize the product for civilian use
Health and living environment clean, and play the multi-efficiency of silver ion and polyacid nanocomposite Synergistic antimicrobial；
（2）Product of the present invention exposure be not in for a long time in air it is mouldy, rotten, spoiled, property stablize, do not need to be added
Antiseptic kind substance, product are not in lamination by freezing heating repeatedly, and property is reliable, and reaches chemical industry hand cleanser and go out
Bacterium effect.
Specific embodiment
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 50~100g Chinese honey locust powder is taken to be laid in filter paper
On, it being placed on the bracket above deionized water at 3~5cm, steam is passed through in condenser pipe by heating deionized water to boiling,
Continuous heating grease into condenser pipe is not further added by, stand 1~2h after take upper oil, into grease be added 20~
30g anhydrous magnesium sulfate stands filtering removal anhydrous magnesium sulfate after 20~30min, obtains Chinese honey locust volatile oil, take 0.5~1.0g nitric acid
Silver is added in 100~150g deionized water, stirs 20~30min under the conditions of being protected from light with 300~400r/min, adds 1.2
~3.2g heteropoly acid, is heated with stirring to 60~80 DEG C under nitrogen atmosphere, and 0.1~0.5g oxalic acid is added after persistently stirring 1~4h
Ammonium, 1~2g Chinese honey locust volatile oil, 4~8g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing, at 120~240 DEG C
4~8h is reacted, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2~3 times is washed with deionized and is placed in drying box, 60
Dry 3~5h, obtains antimicrobial factors, takes 10~12g dodecyl polyoxyethylene ether sodium sulphate, 12~15g dodecane at~80 DEG C
Base benzene sulfonic acid sodium salt is added in 50~60g deionized water, is heated with stirring to 50~60 DEG C with 300~400r/min, insulated and stirred 20
~30min, addition 1~3g cocoanut fatty acid diethanolamide, 0.6~1.2g sodium chloride, 1~2g are sweet after being cooled to room temperature
Oil continues 20~30min of stirring, adds 0.1~0.2g essence, 0.05~0.20g antimicrobial factors, and insulated and stirred 30~
After 40min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 50g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 3cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 1h, and 20g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 20min, obtains Chinese honey locust volatile oil, takes 0.5g silver nitrate, is added in 100g deionized water, is keeping away
20min is stirred with 300r/min under the conditions of light, 1.2g heteropoly acid is added, is heated with stirring to 60 DEG C under nitrogen atmosphere, is continued
0.1g ammonium oxalate, 1g Chinese honey locust volatile oil is added after stirring 1h, 4g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
4h is reacted at 120 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2 times is washed with deionized and is placed in drying box,
Dry 3h, obtains antimicrobial factors, takes 10g dodecyl polyoxyethylene ether sodium sulphate, 12g neopelex adds at 60 DEG C
Enter in 50g deionized water, be heated with stirring to 50 DEG C, insulated and stirred 20min with 300r/min, 1g coconut is added after being cooled to room temperature
Fatty acid oil diglycollic amide, 0.6g sodium chloride, 1g glycerol continue to stir 20min, add 0.1g essence, 0.05g antibacterial because
Son, after insulated and stirred 30min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 80g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 4cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 1h, and 25g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 25min, obtains Chinese honey locust volatile oil, takes 0.8g silver nitrate, is added in 120g deionized water, is keeping away
20min is stirred with 300r/min under the conditions of light, 2g heteropoly acid is added, is heated with stirring to 70 DEG C under nitrogen atmosphere, persistently stirs
0.3g ammonium oxalate, 1g Chinese honey locust volatile oil is added after mixing 3h, 6g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
6h is reacted at 200 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 2 times is washed with deionized and is placed in drying box, 70
Dry 4h, obtains antimicrobial factors at DEG C, takes 10g dodecyl polyoxyethylene ether sodium sulphate, and 15g neopelex is added
In 60g deionized water, 60 DEG C, insulated and stirred 30min are heated with stirring to 400r/min, 3g coconut oil is added after being cooled to room temperature
Fatty diglycollic amide, 0.8g sodium chloride, 2g glycerol continue to stir 25min, add 0.1g essence, 0.1g antimicrobial factors,
After insulated and stirred 30min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
It is crushed being fitted into pulverizer after Chinese honey locust natural air drying, crosses 40 meshes, 100g Chinese honey locust powder is taken to be laid on filter paper, and
It is placed on the bracket above deionized water at 5cm, steam is passed through in condenser pipe, continuous heating by heating deionized water to boiling
Into condenser pipe, grease is not further added by, and takes upper oil after standing 2h, and 30g anhydrous magnesium sulfate is added into grease, quiet
Filtering removes anhydrous magnesium sulfate after setting 30min, obtains Chinese honey locust volatile oil, takes 1.0g silver nitrate, is added in 150g deionized water, is keeping away
30min is stirred with 400r/min under the conditions of light, 3.2g heteropoly acid is added, is heated with stirring to 80 DEG C under nitrogen atmosphere, is continued
0.5g ammonium oxalate, 2g Chinese honey locust volatile oil is added after stirring 4h, 8g polyethylene glycol 400 is fitted into hydrothermal reaction kettle after mixing,
8h is reacted at 240 DEG C, filter residue is filtered to obtain after being cooled to room temperature, filter residue 3 times is washed with deionized and is placed in drying box,
Dry 5h, obtains antimicrobial factors, takes 12g dodecyl polyoxyethylene ether sodium sulphate, 15g neopelex adds at 80 DEG C
Enter in 60g deionized water, be heated with stirring to 60 DEG C, insulated and stirred 30min with 400r/min, 3g coconut is added after being cooled to room temperature
Fatty acid oil diglycollic amide, 1.2g sodium chloride, 2g glycerol continue to stir 30min, add 0.2g essence, 0.20g antibacterial because
Son, after insulated and stirred 40min plus deionized water is to 100g, obtains environment friendly bacteriostatic polyacid hand cleanser.
Reference examples：The environment friendly bacteriostatic polyacid hand cleanser of Shandong company production.
The environment friendly bacteriostatic polyacid hand cleanser that example and reference examples are prepared is detected, specific test result such as table 1.
1 performance characterization contrast table of table
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| pH | 6.5 | 6.3 | 6.1 | 4.2 |
| Sterilizing rate % | 98 | 98 | 99 | 88 |
| Total plate count CFU/g | 10 | 9 | 11 | 50 |
| Excrement colibacillus group CFU/g | 0 | 0 | 0 | 0 |
As shown in Table 1, environment friendly bacteriostatic polyacid hand cleanser prepared by the present invention has good bacteriostasis property.
Claims (8)
1. a kind of environment friendly bacteriostatic polyacid hand cleanser, which is characterized in that the hand cleanser chemical composition and weight percent content are such as
Under：
10~12% dodecyl polyoxyethylene ether sodium sulphate, 12~15% neopelexes, 1~3% coco-nut oil fatty acid
Diglycollic amide, 0.6~1.2% sodium chloride, 1~2% glycerol, 0.1~0.2% essence, 0.05~0.20% antimicrobial factors, deionization
Water surplus.
2. a kind of environment friendly bacteriostatic polyacid hand cleanser as described in claim 1, which is characterized in that the antimicrobial factors are silver nitrate
Dissolution with addition ammonium oxalate, Chinese honey locust volatile oil, polyethylene glycol 400 after heteropoly acid hybrid reaction, is uniformly mixed in deionized water
And it is dry obtained after hydro-thermal reaction.
3. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that described weight of material part is 0.5
~1.0 parts of silver nitrates, 100~150 parts of deionized waters, 1.2~3.2 parts of heteropoly acids, 0.1~0.5 part of ammonium oxalate, 1~2 portion of Chinese honey locust
Volatile oil, 4~8 parts of polyethylene glycol 400s.
4. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the heteropoly acid be phosphotungstic acid,
One or more of phosphomolybdic acid, silico-tungstic acid.
5. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the hybrid reaction process be
It is heated with stirring to 60~80 DEG C under nitrogen atmosphere and continues 1~4h of stirring.
6. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the hydrothermal temperature is
120~240 DEG C.
7. a kind of environment friendly bacteriostatic polyacid hand cleanser as claimed in claim 2, which is characterized in that the Chinese honey locust volatile oil is by soap
Pod crushes after air-drying and is laid on filter paper, is placed on the bracket above deionized water at 3~5cm, heating deionized water to boiling
It rises, steam is passed through in condenser pipe, standing takes upper oil, and is dehydrated and is made with anhydrous magnesium sulfate.
8. a kind of preparation method of environment friendly bacteriostatic polyacid hand cleanser as described in claim 1~7 any one, feature exist
In, the specific steps are：
（1）It crushes and is laid on filter paper after Chinese honey locust is air-dried, is placed on the bracket above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to boiling, and standing takes upper oil, and is dehydrated with anhydrous magnesium sulfate, is obtained Chinese honey locust and is waved
Hair oil；
（2）It takes silver nitrate to be added in deionized water to stir, ammonium oxalate, Chinese honey locust volatilization is added after adding heteropoly acid hybrid reaction
Oil, polyethylene glycol 400 are uniformly mixed and dry after hydro-thermal reaction, obtain antimicrobial factors；
（3）Dodecyl polyoxyethylene ether sodium sulphate, neopelex is taken to be added in deionized water, with 300~400r/
Min is heated with stirring to 50~60 DEG C, 20~30min of insulated and stirred, and coco-nut oil fatty acid diethanol acyl is added after being cooled to room temperature
Amine, sodium chloride, glycerol continue 20~30min of stirring, add essence, antimicrobial factors, add after 30~40min of insulated and stirred and go
Ionized water obtains environment friendly bacteriostatic polyacid hand cleanser to 100g.
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